SDMS Document Harding Lawson Associates January 3, 1995 Ms. Sherrel Henry United States Environmental Protection Agency Section II Emergency and Remedial Response Division 26 Federal Plaza, Room 747 Nevif York, New York 10278 115535 Non-CLP Results of Potable Water Sampling Island Chemical Company St. Croix, U.S. Virgin Islands Dear Ms. Henry: Due to a laboratory error, the non-CLP portion of the potable water results was not included in the data package originally delivered. The non-CLP data consist of pyridine results and raw data from the pyridine analyses. Enclosed please find one (1] copy of the non-CLP portion of the results. The purpose and origin of the samples were discussed in the cover letter (dated December 22, 1994] submitted with the CLP portion of the data package. Please call me if you have any questions. Yours very truly, HARDING LAWSON ASSOCIATES 300001 4sr Engineering and Environmental Services 131 North Third Street, Philadelphia, PA 19106-1903 215/627-450"5~ Fax 215/627-4250 A Subsidiary of Harding Associates • Offices Nationwide I N C O R P O R A T E D ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS Analytical Results - Semivolatile Organics by Method 8270 Harding Lawson Associates Client ID: PT-1/110494 Description: NA Sample ID: UNS-001 Matrix: Water Wet/Dry Basis: NA Collected: 11/04/94 Received: 11/05/94 Prepared: 11/11/94 Analyzed: 11/16/94 Percent Moisture: NA CAS No. 110-86-1 P a r a m e t e r Pyridine Concentration, ug/l (ppb) Sample ND Blank ND Detection Limit 10.0 ND-Not Detected at or above the detection limit stated. 300002 161 James Drive West, Suite 100 St. Rose, LA 70087 TEL: 504-469-0333 FAX: 504-469-0555 An Equal Opportunity Employer 201 ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS Analytical Results - Semivolatile Organics by Method 8270 Harding Lawson Associates Client ID: PT-2/110494 Description: NA Sample ID: UNS-002 Matrix: Water Wet/Dry Basis: NA Collected: 11/04/94 Received: 11/05/94 Prepared: 11/11/94 Analyzed: 11/16/94 Percent Moisture: NA CAS No. P a r a m e t e r Concentration, ug/l (ppb) Sample Blank Detection Limit 110-86-1 Pyridine ND ND 10.0 ND-Not Detected at or above the detection limit stated. 300003 161 James Drive West, Suite 100 St. Rose, LA 70087 TEL: 504-469-0333 FAX: 504-469-0555 An Equal Opportunity Employer 202 I N C O R P O R A T E D ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS Analytical Results - Semivolatile Organics by Method 8270 Harding Lawson Associates Client ID: PT-102/110494 Description: NA Sample ID: UNS-003 Matrix: Water Wet/Dry Basis: NA Collected: 11/04/94 Received: 11/05/94 Prepared: 11/11/94 Analyzed: 11/16/94 Percent Moisture: NA CAS No. 110-86-1 P a r a m e t e r P y r i d i n e Concentration, ug/l (ppb) Sample ND Blank ND Detection Limit 10.0 ND-Not Detected at or above the detection limit stated. 300004 161 James Drive West, Suite 100 St. Rose, LA 70087 TEL: 504-469-0333 FAX: 504-469-0555 An Equal Opportunity Employer 203 ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS Analytical Results - Semivolatile Organics by Method 8270 Harding Lawson Associates Client ID: MS/110494 Description: MATRIX SPIKE Sample ID: UNS-005 Matrix: Water Wet/Dry Basis: NA Collected: 11/04/94 Received: 11/05/94 Prepared: 11/23/94 Analyzed: 11/29/94 Percent Moisture: NA CAS No. P a r a m e t e r Concentration, ug/l (ppb) (*) MATRIX SPIKE Sample Blank Detection Limit 110-86-1 Pyridine ND ND 10.0 ND-Not Detected at or above the detection limit stated. (*) See Narrative 300005 161 James Drive West, Suite 100 St. Rose, LA 70087 TEL: 504-469-0333 FAX: 504-469-0555 An Equal Opportunity Employer 204 ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS Analytical Results - Semivolatile Organics by Method 8270 Harding Lawson Associates Client ID: MS/110494 Description: MATRIX SPIKE DUPLICATE Sample ID: UNS-006 Matrix: Water Wet/Dry Basis: NA Collected: 11/04/94 Received: 11/05/94 Prepared: 11/23/94 Analyzed: 11/29/94 Percent Moisture: NA CAS No. 110-86-1 P a r a m e t e r P y r i d i n e Concentration, ug/l (ppb) (*) MATRIX SPIKE DUPLICATE Detection Sample Blank Limit ND ND 10.0 ND-Not Detected at or above the detection limit stated. (*) See Narrative 300006 161 James Drive West. Suite 100 St. Rose, LA 70087 TEL: 504-469-0333 FAX: 504-469-0555 An Equal Opportunity Employer 205 ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS QA/QC SUMMARY SEMIVOLATILE ORGANICS BATCH #11271 Semivolatile Blank Parameter Phenol 2-Chlorophenol 1,4-Dichlorobenzene N-Nitroso-di-n-propylamine 1,2,4-Trichlorobenzene 4-Chloro-3-methylphenol Acenaphthene 4-Nitrophenol 2,4-Dinitrotoluene Pentachlorophenol Pyrene Spike Level 75.0 75.0 50.0 50.0 50.0 75.0 50.0 75.0 50.0 75.0 50.0 and Matrix Spike - Units ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l Results Recovery (%) Blank Spike 55 75 61 61 70 92 83 87* 77 25 86 MS 61 81 63 63 71 90 86 91* 78 46 84 MSD 49 66 49 59 58 86 81 89* 79 51 85 EPA/CLP QC Limits 12-110 27-123 36- 97 41-116 39- 98 23- 97 46-118 10- 80 24- 96 9-103 26-127 Semivolatile Surrogate Recovery Sample No. Blank 1 Blank Spike MS/110494 (UNS-005) MS/110494 (UNS-006) Blank 2 PT-1/110494 FT-2/110494 PT-102/110494 Nitro- benzene-d5 81 78 86 71 64 75 78 69 2-Fluoro- bipheny1 86 77 78 77 59 76 78 68 Terphenyl-dl4 76 63 71 66 78 79 85 80 Phenol-d5 65 69 70 58 72 83 89 79 2-Fluoro- phenol 81 74 73 58 67 76 83 65 2,4,6-Tri- bromophenol 78 85 85 83 80 89 95 76 QC Limits (35-114) (43-116) (33-141) (10-94) (21-100) (10-123) * Value outside QC limits 300007 161 JamesDrive West, Suite 100 St. Rose, LA 70087 TEL: 504-469-0333 FAX: 504-469-0555 An Equal Opportunity Employer Mass L i s t 11/09/94 9 : 2 6 : 0 0 + 8:33 Sample: DFTPP 244-92-PERF Conds. : RTX-5 O. 25riM X 30M Data: Cali: BP110994A BP110994A 513 1 l.OUM 45/4-325(220 #512 to #514 averaged - #505 XI. 00 Base RIC: m/2 198 14672. INST B 39 443 Mass 39? 50? 51? 52? 57? 69 74 75 76 77 78 79 80 81 93 98 99 101 107 110 1 111 117 127 128 129 141 167 175 179 ISO 186 187 196 198 199 204 205 206 207 217 221 224 225 227 ^ 244 f 255 256 274 275 276 S s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s 0. 00 7. RA 3. 19 7. 10 31. 73 1. 05 3. 55 41. 09 2. 94 5. 48 1. 17 41.61 2. 86 2. 26 1. 17 3. 47 3. 31 2. 78 2. 42 1. 13 9. 88 22. 38 3. 59 4. 68 45. 56 3. 55 14. 40 2. 14 5. OS 1. 41 2. 54 1. 13 9. 44 1. 53 3. 71 100. 00 6. 41 2. 62 4. 35 19. 44 2. 66 4. 48 6. 81 9. 27 1. 53 3. 23 7. 58 37. 30 5. 24 2. 14 21. 17 1. 94 0. Inten. 79. 176. 787. 26. 88. 1019. 73. 136. 29. 1032. 71. 56. 29. 86. 82. 69. 60. 28. 245. 555. 89. 116. 1130. 88. 357. 53. 126. 35. 63. 28. 234. 38. 92. 2480. 159. 65. 108. 482. 66. 111. 169. 230. 38. 80. 188. 925. 130. 53. 525. 43. Minima Maxima Mass 296 365 423 441 442 443 . \ Min # s S S S S S Inten: 0 y. RA 3. 79 1. 33 1. 98 5. 32 44. 76 8. 19 0 Inten 94 33 49 132 1110 203 300008 GC/MS Tuning and Mass Calibration DECAFLUOROTRIPHENYLPHOSPHINE Case Number: Laboratory: GULF Contract: Inst ID: B Sens Date: 11/09/94 Sens Time: 9:26:00 Lab ID: BP110994A Cali Date: 10/02/91 Analyst: JAM Data release authorized by: M/E Ion Abundance Criteria Spec # 512 51 30 to 60y. of mass 198 31.73 68 less than 2'/. of mass 69 0.00 ( 0.00) 1 69 mass 69 relative abundance 41.09 70 less than 27. of mass 69 0.00 < 0.00) 1 127 40 TO 607. of mass 198 45. 56 197 less than 17. of mass 198 0.00 198 base peak. 1007. relative abundance 100.00 199 5 TO 97. of mass 198 6. 41 275 10 TO 307. of mass 198 21. 17 365 greater than 17. of mass 198 1. 33 441 less than mass 443 5.32 442 greater than 407. of mass 198 44. 76 443 17 TO 237. of mass 442 8. 19 (18.29) 2 1 - value in parenthesis is 7. of mass 69 2 - value in parenthesis is 7. of mass 442 300009 DATA FROM FILE: BS110994A SCANS 353 TO 1163 ACQUIRED: 11/99/94 ^:4S:QQ CALI: BS110994A #1 SAMPLE: SSTD050 290-02-SU25 CONDS.: RTX-5 .0.25MM K 30M 1.0UM 45/4-325(520 INST B o o o o 400 4 6:40 •J 100.07 ( G1888.) CS50 2-FLUOROPHENOL 0.6 (SS-5> 500 . 8:20 600 _ 10:00 700 11:40 800 . 13:20 --1.—•flBawmiiuii] umaiiw 300 . 15:00 -L=. 16:40 mt ^^Ssf^-miiMOPHBioL-oi %rg^cii-7, -01QQ D1-1.4 DICHLOROBENZENE (IS-1> CS75 1.. 2-CL2BENZENE-D4 0.4 (SS-8) ^ ^ m D5-NI TROBENZENE 0.2 (SS-1) ^^TTT;?>^TBRUMOPHENC.L -«40 DS-NAPHTHALENE (IS-2) CS25 2-FLLiOROB I PHENYL 0.7 (SS-2) •Qi^Q D10-ACENAPHTHENE — O a S U - W 0-PHENANTHRENE (IS-4) CS30 D14-P-TERPHENYL 0.5 CI75 D12-PERYLENE (I S-6.) Quantitation Report File: BS110994A Data: BS110994A. TI 11/09/94 9:48:00 iample: SSTD050 290-02-SV25 Fonds. : RTX-5 0. 25MM X 30M l.OUM 45/4-325(220 Formula: X X X Instrument: B Submitted by: Analyst: JAM INST B height: Acct. No. 1. 001 AMOUNT=AREA * REF AMNT/ R a t i o RRT(L) R a t i o m 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 •=>7 ^8 9 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 8:23 10: 20 12: 59 15: 12 19: 36 24:31 6:25 7: 56 9: 17 11: 56 14: 10 17: 33 8: 07 8: 41 7: 57 8: 02 8: 08 8:20 8:25 7: 58 3:31 3: 31 8: 39 8: 42 8: 50 8: 51 9:03 9: 04 9: 10 9: 19 9: 39 9: 47 9: 50 10:01 9: 58 10: 09 10: 16 10: 22 10: 28 10: 36 11: 10 11: 23 11: 42 11: 51 11: 55 12: 07 12: £0 12: 35 12: 46 12: 57 1. 00 1. 00 1. 00 1. 00 00 00 00 00 00 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 00 00 00 oo 1. 00 00 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 765 0. 946 0. 898 0. 919 1. 091 0. 895 0. 968 1. 036 0. 948 0. 958 O. 970 0. 994 1. 004 O. 950 0. 419 0. 419 1. 032 1. 038 1. 054 1. 056 1. 080 1. 082 1. 093 O. 902 0. 934 O. 947 O. 952 O. 969 O. 965 0. 982 0. 994 1. 003 1. 013 1. 026 1. 081 1. 102 O. 901 0. 913 0. 918 0. 933 0. 950 0. 969 0. 983 O. 997 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 00 00 00 00 00 00 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 00 00 00 00 00 00 1. 00 1. 00 1. 00 1. 00 Amnt 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25, 00 25, 00 25. 00 25. 00 25. 00 25, 00 25. 00 25. 00 25. 00 Amntt^ 300014 Quantitation Report File: BS110994A Data: BS110994A. TI 11/09/94 9:48:00 ample: SSTD050 290-02-SV25 onds. : RTX-5 0. 25MM X 30M l.OUM 45/4-325©20 Formula: X X X Instrument: B Submitted by: Analyst: JAM INST B Weight: Acct. No. 1. 001 AMOUNT=AREA * REF AMNT/(REF AREA * RESP FACT) Resp. fac. from Library Entry No 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 |b7 "68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 No 51 52 53 54 ^ 5 | 6 57 58 Name C550 C321 C555 C560 C565 C570 C543 C580 C585 C590 C595 C610 C615 C625 C630 C635 C640 C645 C650 C655 D200 C647 C715 C720 C725 C730 C740 C735 C760 C765 C770 C775 C780 C785 C790 m/z 153 232 184 109 168 165 165 149 •ACENAPHTHENE 0. 8 2, 3. A, 6-TETRACHLOROPHENOL tc2. 4DINITR0PHEN0L 8<4N ITROPHENOL DIBENZOFURAN 2.4DIN1TR0T0LUENE 2,6DINITR0T0LUENE DIETHYL PHTHALATE 4CHLDR0PHENYL PHEN FLUORENE 4-NlTROANILINE 0. 8 0. 2 0. 2 0. 4 0. 9 4,6DINITR02METHYLPH •«-D I PHENYL AM INE 4BR0M0PHENYL PHENY CL6BENZENE •PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-NBUTYLPHTHALATE •FLUORANTHENE 0. 1 0. 1 D. 05 0. 7 0. 7 0. 6 1,2-DIPHENYLHYDRAZINE CARBAZOLE PYRENE 0. 6 BUTYLBENZYLPHTHALATE 3,3'CL2BENZIDINE BENZO < A)ANTHRACENE 0. 8 BIS(2ETHYLHEXYL)PHTH CHRYSENE 0. 7 •DI-N-DCTYLPHTHALATE BENZO(B)FLUORANTHE BENZO(K)FLUORANTHE •BENZO(A)PYRENE INDEN0<1,2,3CD)PYR DIBENZD(A,H)ANTHRA BENZO(G, H, DPERYLE Scan Time Ref 782 13:02 3 1. 810 13:30 3 1. 785 13:05 3 1. 791 13:11 3 1. 796 13: 16 3 1. 798 13: 18 3 1. 763 12:43 3 0. 817 13:37 3 1. 0. 7 0. 7 0. 7 0. 5 0. 4 0. 5 RRT 004 040 008 015 022 024 979 049 I T T Me A A A A A A A A 'th BB BB BB BB BB BB BB BB Area(Hght) 21761. 6923. 3045. 2043. 33674. 8215. 7070. 25268. Amount 25. 25. 25. 25. 25. 25. 25. 25. 000 000 000 000 000 000 000 000 PPB PPB PPB PPB PPB PPB PPB PPB 7.Tot 19 19 19 19 19 19 19 19 300015 No 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 ^Jo .51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 ^ 4 P'S 76 77 m/z 204 166 138 198 169 248 284 266 178 178 149 202 77 167 202 149 252 228 149 228 149 252 252 252 276 278 276 c lean T 824 13 827 13 835 13 835 13 836 13 868 14 883 14 899 14 914- 15 918' 15 959 15 1022. 17 839 13 933 15 1044- 17 1098 18 1167 19 1173- 19 1163 19 1180- 19 ] .262 21 1372 . 22 1378- 22 1455' 24 1836- 30 1844- 30 1954* 32 Ret BB BB BB BB Amnt 2! 2: 0. 00 5. 00 25. 00 2; 2: 2: 5. 00 5. 00 5. 00 25. 00 2! 2! 2' 2 2 2 2 2 2 2 2 2 2 2 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 25. 00 2 2 2 2 2 5. 00 5. 00 5. 00 '5. 00 :5. 00 Area G016 D5 PHQIQL -J 100.0^; ( 179712.) 0.3 tio 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 . 00 00 . 00 . 00 . 00 , 00 . 00 . 00 . 00 . 00 . 00 . 00 Amnt 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 Amnt(L) 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 SO. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 80. 00 Sfwm> ?Sll(}''i9^S R. Fac R. 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 992 1. 293 0. 306 1. 110 0. 117 0. 869 1. 108 0. 719 1. 583 1. 337 1. 124 1. 210 1. 224 1. 438 0. 629 0. 876 0. 629 1. 119 1. 006 1. 334 1. 093 0. 620 0. 449 0. 291 0. 596 0. 190 0. 240 0. 146 0. 400 0. 263 0. 275 0. 841 0. 370 0. 128 0. 246 0. 576 0. 317 0. 332 0. 369 1. 064 0. 277 1. 134 1. 413 0. 231 Fac(L) F 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 992 1. 293 0. 306 1. 110 0. 117 0. 869 1. 108 0. 719 1. 583 1. 337 1. 124 1. 210 1. 224 1. 438 0. 629 0. 876 0. 629 1. 119 1. 006 1. 334 1. 093 0. 620 0. 449 0. 291 0. 596 0. 190 0. 240 0. 146 0. 400 0. 263 0. 275 0. 841 0. 370 0. 128 0. 246 0. 576 0. 317 0. 332 0. 369 1. 064 0. 277 1. 134 1. 413 0. 231 ^atio 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 . 00 . 00 . 00 . 00 .00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 300022 Quantitation Report File: BS110994B m Data: BS110994B.TI 11/09/94 10:28:00 ample: SSTD160 290-02-SV80 onds.: RTX-5 O. 25MM X 30M l.OUM 45/4-325620 Formula: X X X Instrument: B Submitted by: Analyst: JAM INST B Weight: Acct. No. 1. 001 AMDUNT=AREA * REF AMNT/(REF AREA • RESP FACT) Resp. fac. from Library Entry No 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 .67 >68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 No 51 52 53 54 ^55 ^ 6 57 58 Name C550 C321 C555 C560 C565 C570 C543 C580 C585 C590 C595 C610 C615 C625 C630 C635 C640 C645 C650 C655 D200 C647 C715 C720 C725 C730 C740 C735 C760 C775 C780 C785 C790 C765 C770 m/z 153 232 184 109 168 165 165 149 •ACENAPHTHENE 0. 8 2. 3. 4, 6-TETRACHLOROPHENOL 8<2, 4DINITR0PHENDL ?<4N I TROPHENOL DIBENZOFURAN 2.4DINITR0T0LUENE 2.6DINITR0T0LUENE DIETHYL PHTHALATE 4CHL0R0PHENYL PHEN FLUORENE 4-NITRDANILINE 0. 8 0. 2 0. 2 0. 4 0. 9 4,6DINITR02METHYLPH •DIPHENYLAMINE 4BR0M0PHENYL PHENY CL6BENZENE •PENTACHLOROPHENOL < PHENANTHRENE ANTHRACENE DI-NBUTYLPHTHALATE •FLUORANTHENE 0. 1 0. 1 D. 05 0. 7 0. 7 0. 6 1,2-DIPHENYLHYDRAZINE CARBAZOLE PYRENE 0. 6 BUTYLBENZYLPHTHALATE 3,3'CL2BENZIDINE BENZO(A)ANTHRACENE 0. B BIS(2ETHYLHEXYL)PHTH CHRYSENE 0. 7 •DI-N-OCTYLPHTHALATE •BENZO(A)PYRENE INDENOd, 2, 3CD)PYR DIBENZO(A,H)ANTHRA BENZO 11275. 38585. 20925. 31218. 24953. 26606. 5253. 6726. 5634. 11506. 1158. 10177. 5724. 4123. 8656. 7634. 6285. 6749. 6861. 6826. 3086. 4918. 2917. 6199. 6378. 7359. 6168. 3317. 2479. 5422. 10522. 3287. 4247. 2454. 7241. 4994. 5190. 17066. 5289. 2485. 4375. 10825. 2651. 3523. 3603. 10456. 2826. 11556. 17369. 913. Amount 20. 000 PPB 20. 000 PPB 20. 000 PPB 20. 000 PPB 20. 000 PPB 20. 000 PPB IO. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 10. 000 PPB 7.Tot 2. 20 2. 20 2. 20 2. 20 2. 20 2. 20 1. 10 10 10 1. 10 10 10 1. 10 1. 10 10 10 10 10 10 1. 10 10 10 10 10 10 1. 10 1. 10 1. 10 1. 10 1. 10 1. 10 1. 10 1. 10 1. 10 1. 10 1. 10 1. 10 1. 10 1. 10 1. 10 1. 10 1. 10 10 10 10 10 10 10 10 10 300029 No 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 i Ret(L) 8:22 10:20 13:00 15: 13 19:36 24:30 6:20 7:54 9: 16 11: 57 14: 11 17: 33 8:05 8:40 7: 55 8: 00 8:06 8: 18 8:23 7: 56 3:21 3:22 8: 38 8:41 8:49 8: 50 9:02 9:03 9: 09 9; 18 9; 38 9: 47 9: 50 9: 59 9; 57 10; 09 JO: 15 10; 22 10; 29 10: 36 11: 11 11:23 11: 43 11; 51 11: 56 12: OS 12: 20 12: 35 12: 46 12; 58 Re )tio 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 , 00 00 . 00 . 00 . 00 , 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 RRT(L) 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 757 0. 944 0. 897 0. 919 1. 091 0. 895 0. 966 1. 036 0. 946 0. 956 0. 968 0. 992 1. 002 0. 948 0. 400 0. 402 1. 032 1. 038 1. 054 1. 056 1. 080 1. 0S2 1. 094 0. 900 0. 932 0. 947 0. 952 0. 966 0. 963 0. 982 0. 992 1. 003 1. 015 1. 026 1. 082 1. 102 0. 901 0. 912 0. 918 0. 933 0. 949 0. 968 0. 982 0. 997 Re itio 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 , 00 , 00 . 00 , 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 Amnt 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 Amnt(L) 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 SZTopi^ R. Fac R. 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 932 1. 193 0. 292 1. 100 0. Ill 0. 816 1. 015 0. 731 1. 535 1. 354 1. 115 1. 197 1. 217 1. 211 0. 547 0. 872 0. 518 1. 100 1. 131 1. 305 1. 094 0. 588 0. 440 0. 281 0. 545 0. 170 0. 220 0. 127 0. 375 0. 259 0. 269 0. 885 0. 274 0. 129 0. 227 0. 561 0. 253 0. 337 0. 344 0. 999 0. 270 1. 105 1. 660 0. 087 Fac(L), F 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 932 1. 193 0. 292 1. 100 0. Ill 0. 816 1. 015 0. 731 1. 535 1. 354 1. 115 1. 197 1. 217 1. 211 0. 547 0. 872 0. 518 1. 100 1. 131 1. 305 1. 094 0. 588 0. 440 0. 281 0. 545 0. 170 0. 220 0. 127 0. 375 0. 259 0. 269 0. 885 0. 274 0. 129 0. 227 0. 561 0. 253 0. 337 0. 344 0. 999 0. 270 1. 105 1. 660 0. 087 ^atio 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 , 00 , 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 300030 Quantitation Report File: BS110994C Data: BS110994C. TI 11/09/94 11:08:00 Sample: SSTD020 2 9 0 - 0 2 - S V l O lends.: RTX-5 0. 25MM X 30M l.OUM 45/4-325^20 Formula: X X X Instrument: B Submitted by: Analyst: JAM INST B Weight: 1.001 Acct. No. : AMOUNT=AREA • REF AMNT/(REF AREA • RESP FACT) Resp. f a c . from L i b r a r y E n t r y No 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 ^ ' ^ fhS 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 No 51 52 53 54 ^ 5 P6 57 58 Name C550 C321 C555 C560 C565 C570 C543 C580 C585 C590 C595 C610 C615 C625 C630 C635 C650 C655 D200 C647 C715 C720 C725 C730 C740 C735 C760 C765 C770 C775 C780 C785 C790 C640 C645 m/z 153 232 184 109 168 165 165 149 •ACENAPHTHENE 0. 8 2.3,4.6-TETRACHLOROPHENOL 8<2, 4DINITR0PHEN0L 8<4NITROPHENOL DIBENZOFURAN 2,4DINITR0T0LUENE 2,6DINITR0T0LUENE DIETHYL PHTHALATE 4CHL0R0PHENYL PHEN FLUORENE 4-NITROANILINE 0. a 0. 2 0. 2 0. 4 0. 9 4,6DINITR02METHYLPH •DIPHENYLAMINE 4BR0M0PHENYL PHENY CL6BENZENE •PENTACHLOROPHENOL < DI-NBUTYLPHTHALATE •FLUORANTHENE 0. 1 0. 1 3. 05 0. 6 1,2-DIPHENYLHYDRAZINE CARBAZOLE PYRENE 0. 6 BUTYLBENZYLPHTHALATE 3,3'CL2BENZIDINE BENZO(A)ANTHRACENE 0. 8 BIS(2ETHYLHEXYL)PHTH CHRYSENE 0. 7 •DI-N-OCTYLPHTHALATE BENZO(B)FLUORANTHE BENZO(K)FLUORANTHE •BENZO(A)PYRENE INDENOd, 2. 3CD)PYR DIBENZO(A,H)ANTHRA BENZO(G, H> DPERYLE PHENANTHRENE ANTHRACENE Scan Time Ref 783 13:03 3 1. 811 13:31 3 1. 786 13:06 3 1. 792 13; 12 3 1. 796 13: 16 3 1. 798 13; 18 3 1. 763 12:43 3 0. 817 13:37 3 1. 0. 7 0. 7 0. 7 0. 5 0. 4 0. 5 0. 7 0. 7 RRT 004 040 008 015 021 023 978 047 T T T ME A A A A A A A A th BB BB BB BB BB BB BB BB Area(H9ht) 9553. 3119. 1100. 686. 14138. 3534. 2928. 10779. Amount 10. 10. 10. 10. 10. 10. 10. 10. 000 000 000 000 000 000 000 000 PPB PPB PPB PPB PPB PPB PPB 7.Tot PPi^AAA 10 10 10 10 10 10 10 J!3.i 300031 No 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 ^Mo 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 ^ 4 | 5 ^76 77 m/z 204 166 138 198 169 248 284 266 149 202 77 167 202 149 252 228 149 228 149 252 252 252 276 278 276 178 178 Scan 825 827 835 835 836 869 884 900 960 1022 839 933 1044 1098 1167 1173 1163 1179 1262 1371 1376 1453 1836 1842 1950 915 918 Ret(L) Ra 13: 13: 13: 13; 13: 13; 12: 13: 13: 13: 13: 13; 13; 14: 14: 15: 16; 17: 13: 15: 17: 18; 19: 19: 19: 19: 21: 03 1. 31 1. 06 1. 12 1. 16 1. 18 1. 43 1. 37 1. 45 1. 47 1. 55 1. 55 1. 56 1. 29 1. 44 1. 00 1. 00 1. 02 1. 59 1. 33 1. 24 1. 18 1. 27 1. 33 1. 23 1. 39 1. 02 1. Time R 13: 45 13:47 13: 55 13: 55 13: 56 14:29 14:44 15:00 16:00 17:02 13: 59 15: 33 17: 24 18: 18 19: 27 19: 33 19:23 19:39 21:02 22: 51 22; 56 24; 13 30:36 30: 42 32: 30 15: 15 15: 18 tio RRT(L} 00 1.004 00 1.040 00 1. 003 00 1.015 00 1. 021 00 1.023 00 0. 978 00 1. 047 00 1. 058 00 1.060 00 1.071 00 0.915 00 0. 916 00 0. 952 00 0. 968 00 0. 986 00 1.051 00 1. 119 00 0. 919 00 1.022 00 0. 888 00 0. 934 00 0. 992 00 0. 997 00 0. 989 00 1. 003 00 0. 859 ef 3 3 3 4 4 4 4 4 4 4 4 4 5 5 5 5 5 5 6 6 6 6 6 6 6 4 4 RRT 1. 058 1. 060 1. 071 0. 915 0. 916 0. 952 0. 968 0. 986 1. 051 1. 119 0. 919 1. 022 0. 888 0. 934 0. 992 0. 997 0. 989 1. 003 0. 859 0. 933 0. 936 0. 988 1. 249 1. 253 1. 327 1. 002 1. 005 1 Ratio 00 00 00 00 00 00 00 00 00 , 00 00 , 00 00 , 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 Meth A BB A BB A VB A BB A BB A BB A BB A BB A BB A BB A BB A BB A BB A BB A BB A BV A BB A VB A BB A BV A VB A BB A BB A BB A BB M XXO,i M XX' Amnt 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 Area(Hght) 5345. 11505. 1539. 1896. 6620. 2962. 2889. 1684. 19015. 16186. 11572. 13167. 16994. 8488. 3485. 14398. 11639. 13060. 19173. 13884. 12380. 12605. 13221. 10243. 11093. ihM 15659. "^ 16210. Amnt(L) 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 lo! 00 10. 00 10. 00 10. 00 •^Zli9'i^'^'' Amount 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 10. 000 R. Fac R. F 0. 0. 0. 0. 1. 0. 0. 1. 0. 1. 0. 0. 0. 0. 0, 0 1 1 0 0 1 0 0 1 0 1 1 913 298 105 066 351 338 280 030 511 100 147 121 424 190 , 185 , 108 . 218 . 037 . 741 . 844 . 362 . 680 . 279 . 154 . 933 . 047 . 441 PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB ac(L) 0. 913 0. 298 0. 105 0. 066 1. 351 0. 338 0. 280 1. 030 0. 511 1. 100 0. 147 0. 121 0. 424 0. 190 0. 185 0. 108 1. 218 1. 037 0. 741 0. 844 1. 362 0. 680 0. 279 1. 154 0. 933 1. 047 1. 441 7.Tot 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 Ratio 00 00 00 00 00 00 00 00 00 00 00 00 00 , 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 30003 No 78 79 80 81 82 83 84 85 Ret(L) 22: 51 22: 56 24: 13 30:36 30:42 32: 30 15: 15 15: 18 Ratio 00 00 00 00 00 00 00 00 RRT(L) 0. 933 0. 936 0. 988 1. 249 1. 253 1. 327 1. 002 1. 005 Ratio 00 00 00 00 00 00 00 00 Amnt 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 Amnt(L) 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 10. 00 VTJTP «'^o ^ f l l ^ ' J I I C R. Fac R. 1. 044 0. 931 0. 948 0. 994 0.770 0. 834 1. 003 1. 039 Fac(L) 1. 044 0. 931 0. 948 0. 994 0. 770 0. 834 1. 003 1. 039 Rat: LO 00 00 00 00 00 00 00 00 300033 DATA FROM FILE: BS110994D SCANS -362 TO 1102 ACQUIRED: 11/09/94 11:48:00 CALI: BS110994D ttl SAMPLE: SSTD120 290-02-SU60 CONDS.: RTX-5 .0.25MM X 30M l.OUM 45/4-325(520 INST B CO o o o CO 400 . 6:40 500 _ ?:20 CS50 2-FLUOROPHENOL OG'Ifi D6 PNDIQL 0.6 (SS-5) IOO.O.*: ( 143872.) 10:00 700 _ 11:40 800 . 13:20 900 . 15:00 1000 _ 15:49 BfOBVB i J 0.8 (SS-4) • m m D'l 1..4 DICHLOROBENZENE (IS-1) -&S75 1..2-CL2BENZENE-D4 0.4 (SS-8) :tSSe- D5-NITROBENZENE 0.2 (SS-1) :.I'|i? DO Mi'iPHTHALEME (IS-2) CS25 2-FLUOROBIPHENYL 0.7 (SS-2) CI5Q CHe-ACENAPHTHENE (IS-3) CS55 2.4..6TRIBR0M0PHENnL (SS-6) «j;i;iJaa.--nm,JB]^a,iatiTAiaFhiF ( T S-4 ^ = C53ti D14-P-TERPHENYL 0.5 (SS-3) c5 Co y DATA FROM FILE: BS1109940 SCANS 1102 TO 2000 ACQUIRED: 11/09/94 11:48:00 CALI: BSl109940 ttl SAMPLE: SSTD120 290-02-SU60 CONDS.: RTX-5 0.25MM X 30M l.OUM 45./4-325@20 INST B 1200 . 20:00 1400 _1 23:20 1600 _ 26:40 , - CO o o o CO Ul 1800 30:00 mi - ± 100.0^ ( (IS-5) CI75 D12-PERYLENE (IS-6) 76800.) Quantitation Report File: BS110994D • Data: BS110994D. TI 11/09/94 11:48:00 ample: SSTD120 290-02-SV60 onds.: RTX-5 0. 25MM X 30M l.OUM 45/4-325220 Formula: X X X Instrument: B Submitted by: Analyst: JAM INST B Weight: Acct. No. 1. 001 AMOUNT=AREA • REF AMNT/(REF AREA • RESP FACT) Resp. fac. from Library Entry « No 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 8 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 .42 3 ^44 45 46 47 Name CI 30 CI40 CI50 CI60 CI70 CI75 CS50 CS4 5 CS20 CS25 CS55 CS30 CS70 CS75 C315 C325 C330 C335 C340 C320 C310 C319 C345 C350 C355 C357 C365 C370 C375 C410 C415 C420 C425 C430 C435 C44© C445 C450 C455 C460 C465 C470 C510 C515 C520 C525 C530 0. 6 0. 8 O. 2 0. 7 D4-l,4 DICHLOROBENZENE DS-NAPHTHALENE DIO-ACENAPHTHENE D10-P HENANTHRENE D12-CHRYSENE D12-PERYLENE 2-FLUORDPHENDL D5-PHEN0L D5-NITR0BENZENE 2-FLUOROBIPHENYL 2, 4, 6TRIBR0M0PHEN0L D14-P-TERPHENYL O. 5 2-CHL0R0PHEN0L-D4 0. 8 1.2-CL2BENZENE-D4 0. 4 •PHENOL O. 8 BIS(2CHL0R0ETHYL)E 0.7 2CHL0R0PHEN0L 0. 8 1,3DICHL0R0BENZENE 0.6 •1,4DICHL0R0BENZENE 0.5 ANILINE N-NITROSODIMETHYLAMINE PYRIDINE BENZYL ALCOHOL 1, 2DICHL0R0BENZENE 0. 4 2METHYLPHEN0L 0. 7 2,2'DXYBIS(1CHL0R0PR 4METHYLPHEN0L 0. 6 ?2, 3CD)PYR DIBENZO(A,H)ANTHRA BENZO't')10 60. 00 60. 00 60. 00 60. 00 60. 00 60. 00 60. 00 60. 00 R. Fac R. 1. 017 1. 672 0. 927 0. 894 0. 693 0. 724 1. 147 0. 965 Fac(L) 1. 017 1. 672 0. 927 0. 894 0. 693 0. 724 1. 147 0. 965 Rat: io 00 00 00 00 00 00 00 00 300041 DATA FROM FILE: BS110994E SCANS 367 TO 1107 ACQUIRED: 11/09/94 12:29:00 CALI: BS110994E ttl SAMPLE: SSTDOSO 290-02-SU40 CONDS.: RTX-5 0.25MM X 30H l.OUM 45/4-325520 INST B 400 . 6:40 600 . 10:00 jta 700 _t 11:40 800 _ 13:20 900 . 15:00 1000 . 16:40 co> O) NJi» m -i •^ 100.0^ ( 92800.) CS50 2-FLUOROPHENOL 0.6 (SS-5) €545 D5-PHEN0L 0.8 (SS-4) 'JlOn D'l 1..4 DICHLOROBENZENE (IS-1) CS75 1..2-CL2BENZENE-D4 0.4 (SS-8) •«20 D5-NITR0BENZENE 0.2 (SS-1) ^ = = — C H Q DC NAPHTHALENE (IS-2) CI5£1 Dl 0-ACENAPHTHENE CS25 2-FLUOROBIPHENYL 0.7 (SS-2) (IS-3) CS55 2.. 4. 6TRI BROMOPHENOL (SS-6) kEHENANTHRENE (IS-4) CS30 D14-P-TERPHENYL 0.5 (SS-3) CD vr ^ . y DATA FROM FILE: BSU0994E SCANS 1107 TO 2090 ACQUIRED: 11/99/34 12:29:00 CALI: BS110994E ttl SAMPLE: SSTDO80 290-02-SU40 CONDS.: RTX-5 .0.25MM X 30M l.OUM 45/4-325(?20 INST B CO o o o CO 1200 J 20:00 1400 . 23:20 1600 _i 26:40 1800 . .30:00 m J I J 100.0?; ( (IS-5) 55488.) CI75 D12-PERYLENE (IS-6) Quantitation Report File: BS110994E Data: BS110994E.TI 11/09/94 12: 29:00 ample: SSTDOBO 290-02-SV40 onds.: RTX-5 0. 25MM X 30M l.OUM 45/4-325@20 Formula: X X X Instrument: B Submitted by: Analyst: JAM INST B Weight: Acct. No. 1. 001 AMOUNT=AREA « REF AMNT/(REF AREA • RESP FACT) Resp. fac. from Library Entry No 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 1^^ 'is 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 33 39 40 41 k42 |43 44 45 46 47 Name CI30 CI40 CI50 CI60 CI70 CI75 CS50 CS45 CS20 CS25 CS55 CS30 CS70 CS75 C315 C325 C330 C335 C340 C320 C310 C319 C345 C350 C355 C357 C365 C370 C375 C410 C415 C420 C425 C430 C435 0440 C445 C450 C455 C460 C465 C470 C510 C515 C520 C525 C530 D4-l,4 DICHLOROBENZENE (IS-1) DS-NAPHTHALENE (IS-2) D10-ACENAPHTHENE (IS-3) D10-PHENANTHRENE (IS-4) D12-CHRYSENE (IS-5) D12-PERYLENE (IS-6) 2-FLUOROPHENOL 0.6 (SS-5) D5-PHENDL 0.8 (SS-4> D5-NITR0BENZENE 0.2 (SS-1) 2-FLUOROBIPHENYL 0.7 (SS-2) 2,4,6TRIBROMOPHENOL (SS-6) D14-P-TERPHENYL O. 5 (SS-3) 2-CHL0R0PHEN0L-D4 0.8 (SS-7) 1,2-CL2BENZENE-D4 0.4 (SS-8) •PHENOL O. 8 BIS(2CHL0R0ETHYL)E 0.7 2CHL0R0PHEN0L 0.8 1, 3DICHL0R0BENZENE 0.6 •1,4DICHL0R0BENZENE 0.5 ANILINE N-NITROSODIMETHYLAMINE PYRIDINE BENZYL ALCOHOL 1,2DICHL0R0BENZENE O. 4 2METHYLPHEN0L 0. 7 2,2'0XYBIS(ICHLOROPR 4METHYLPHEN0L S55VX Amount 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 40. 000 R. Fac R. F 0. 0. 0. 0. 1. 0. 0. 1. 0 1 0 0 0 0 0 0 0 1 1 1 0 0 1 0 0 1 0 902 303 155 083 253 368 274 046 513 041 135 136 360 175 187 131 . 978 . 033 . 288 . 017 . 781 . 510 . 448 . 737 . 104 . 087 . 978 PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB ac(L) R 0. 902 0. 303 0. 155 0. 083 1. 253 0. 368 0. 274 1. 046 0. 513 1. 041 0. 135 0. 136 0. 360 0. 175 0. 187 0. 131 0. 978 1. 033 1. 288 1. 017 0. 781 0. 510 1. 448 0. 737 0. 104 1. 087 0. 978 .-— r> r 7.Tot at »nf 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 i o 00 00 00 00 00 00 00 00 00 00 00 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 ' ^48 No 78 79 80 81 82 83 84 85 Ret(L) 19; 41 21: 04 22: 54 23:00 24: 17 30: 42 30: 51 32: 39 Ratio 00 00 00 00 00 00 00 00 RRT(L) 1. 003 0. 859 0. 934 0. 938 0. 990 1. 252 1. 258 1. 332 Ri atio 00 00 00 00 00 00 00 00 Amnt 40. 00 40. 00 40. 00 40. 00 40. 00 40. 00 40. 00 40. 00 Amnt(L) 40. 00 40. 00 40. 00 40. 00 40. 00 40. 00 40. 00 40. 00 syrD ssmiiin R. Fac R. 0. 985 1. 561 1. 008 0. 897 0. 905 0. 916 0. 697 0. 764 Fac(L) 0. 985 1. 561 1. 008 0. 897 0. 905 0.916 0. 697 0. 764 Rat: io 00 00 00 00 00 00 00 00 300049 Initial Calibration Data Instrument Identifier: B Calibration Date: 11/09/94 IN RF: SW(8<) = . 05 , CLP = . 01 OR BELOW 'MAX 7.RSD: SW(^) = 307,«/ CLP = 20. 57. CS50 CS45 CS20 CS25 CS55 CS30 CS70 CS75 C315 C325 C330 C335 C340 C320 C310 C319 C345 C350 C355 C357 ^365 r370 C375 C410 C415 C420 C425 C430 C435 C440 C445 C450 C455 C460 C465 C470 C510 C515 C520 C525 C530 C535 C540 C545 C550 |k321 P555 Compound ., 2-FLUOROPHENOL D5-PHEN0L D5-NITR0BENZENE 2-FLUOROBIPHENYL 0. 0. 0. 0. 2,A, 6TRIBR0M0PHENDL D14-P-TERPHENYL 2-CHL0R0PHEN0L-D4 1,2-CL2BENZENE-D4 •PHENOL BIS(2CHL0R0ETHYL)E 2CHL0R0PHEN0L 1,3DICHL0R0BENZENE •1,4DICHL0R0BENZENE ANILINE 0. 0. 0. 0. 0. 0. 0. 0. 6 8 2 7 5 8 4 8 7 8 6 5 N-NITROSODIMETHYLAMINE PYRIDINE BENZYL ALCOHOL 1,2DICHL0R0BENZENE 2METHYLPHEN0L 0. 0. 2> 2'0XYBIS(1CHL0R0PR 4METHYLPHEN0L S xi^' ^.-ll ^z- 300051 MASS SPECTRUM 11/09/94 9:26:00 + 8:33 SAMPLE: DFTPP 244-92-PERF CONDS.: RTX-5 0.25MM X 30M l.OUM 45/4-325e20 INST B tt512 TO tt514 AUERAGED - «505 Xl.OO DATA: BP110994A tt513 CALI: BP110394A ttl BASE N/Z: 198 RIC: 14672. 100. On 138 50.0- # SI *•>'» 4^ ^ F/3 7'7 127 51 59 I 110 1UL_ 9G ii; - r - - | r 141 It" 186 T—'—r .173 . il—M- 296 -T-+-H M >24 M 1 — ' I ' l — ' — r M/Z 100.0 50 100 150 200 >50.0- \ 442 255 275 -i—"—r 296 423 M/Z 250 sfi0 • T — < — I — . — I — t — j — I — I — I — ^ — , — I — . — r 350 i 400 -1 T'-i 1 1 r'"-!—I r- 450 2480. r 2480. TIC 11/09/94 9:26:00 SAMPLE: DFTPP 244-92-PERF CONDS.: RTX-5 0.25MM X 30M RANGE: G 1.. 700 LABEL: N 100.0-1 RIC CO o o o cn CO DATA: BP110994Jrtt512 SCANS 495 TO 545 CALI: BP110994A ttl l.OUM 45/4-325@20 INST B 0, 4.0 QUAN: A O.. 1.0 J O BASE: U 20.. 3 513 23630. k 497 500 502 505 507 509 k. 513 52; 525 523 534 538 500 8:20 510 3:30 520 8:40 530 8:!=!0 541 543 540 9:00 SCAN TIME 100.0 n •iM. y f'1/2 100.0 -1 =10.0 - CO o o o , cn if^ I :-M MASS SPECTRUM 11/16/34 11:22:00 + 8:28 SAMPLE: DFTPP 244-92-PERF CONDS.: RTX-5 U.25MMX30M l.OUM 45/4- tt507 TO #503 AUERAGED - #500 Xl.OO DATA: BPl116940 tt508 CALI: BP111694D ttl BASE M/Z: 198 RIC: 11792. je20 INST B f H JiL Z'i iU I ' l l uu.. 255 L 'M/Z 250 . !•; fz- 133 # 4^ # Ur 119 117 186 141 16r 179 4 - •MS ;224 1 00 150 -, ! -1 r"-i r-"| -t—I r ' |'. 'I • [ 200 44 V'-HK 1—'—r "1—'—r 365 —t— 423 I i-IMfl 350 400 r 1758. r 1758. 450 RK DATA: BP111694D #507 CALI: BP111694D ttl SCANS 490 TO 540 11/16/94 11:22:00 SAMPLE: DFTPP 244-y2-PERF CMNDS.: PTK-5 0.25MM X SGM l.OUM 45/4-325@20 INST B RANGE: G 100.0- RIC J.Q1 ^90 8:10 700 LABEL: H 0.- 4.0 QUAN: A O,. 1.0 J O BASE: U 20. 49;: ^03 — 1 - 505 o; 20 21184. 513 ilG 520 52; 526 530 __533 535 539 510 8:30 520 8:40 530 8:50 540 SCAN 9:00 TIME 0 Mass L 11/16/ .Samp 1 e jfconds. #507 59 44rj Mass 39? 40? 50? 51? 52? 57? 63? 69 74 75 76 77 78 79 SO 81 93 98 i 99 ^ 107 108 110 111 117 127 128 129 141 167 175 179 186 187 196 198 199 204 205 206 207 217 221 224 ^ 225 " 227 244 255 256 274 • 275 ist 94 11: 22: 00 + ; DFTPP 244- : RT 8: 28 92-PERF X-5 0. 25riM X 30M to #509 B'verag s S S s S s s s B S s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s s 0, 00 7. RA I 3. 24 0. 17 9. 27 44. 54 2. 10 2. 22 1. 71 53. 24 2. 73 6. 37 1. 82 50. 11 2. 22. 3. 13 1. 71 2. 39 4. 15 1. 93 1. 93 10. 75 1. 48 24. 40 3. 01 5. 35 49. 15 2. 62 15. 93 1. 59 4. 39 1. 54 2. 33 10. 98 3. 53 5. 46 100. 00 7. 05 1. 82 4. 95 20. 14 1. 88 5. 63 7. 79 10. 64 1. 76 4. 15 9. 33 39. 59 5. 86 3. 92 22. 53 Data; Cali: 1. OUM BP111694D # 508 BP111694D # 1 45/4-325'220 ed - #500 XI. 00 0. n t e ri. 57. 3. 163. 7S3. 37. 39. 30. 936. 48. 112. 32. 881. 39. 55. 30. 42. 73. 34. 34. 189. 26. 429. 53. 94. 864. 46. 280. 28. 86. 27. 41. 193. 62. 96. 1758. 124. 32. 87. 354. 33. 99. 137. 187. 31. 73. 164. 696. 103. 69. 396. Minima Max i.Tia Mass 276 296 365 423 441 442 443 Min Inten: # 0 7. RA In S 3. 47 S 5. 01 S 1. 32 S 2. 16 S 7. 57 S 52. 96 S 10. 92 Base m/z; 198 RIC: 11792. INST B o 61, 83. 32. 38. 133. 931. 192. 300056 GC/MS Tuning and Mass Calibration DECAFLUGROTRIPHENYLPHOSPHINE Case Number: Laboratory; GULF Contract: I n s t ID: 13 Sens D a t e : i : / 1 6 / ? 4 Sens TiiTie: 1 1 : 2 2 : 0 0 Lab ID: DP11.16?'^D Call Date: 10/02.''9i Ar:alyst: JAM Data release authorized bq: M/E . Ion Abundance Criteria Spec # 507 51 30 to 60/1 of mass 198 63 less than 2.7. of mass 69 69 mass 69 relative abundance 70 less than 2% of mass 69 127 40 TO 607 of mass 193 197 less than 17, of mass 198 198 base peak. 100A relative abundance 199 5 TO 9/: of mass 198 275 10 TO 30/; of mass 193 365 greater than 1/1 of mass 198 441 less than mass 443 442 greater than 407. of mass 193 443 17 TO 23/: of mass 442 1 - value in parenthesis is 7. of mass 69 2 - value in parenthesis is 7. of mass 442 44. 0, 53. 0. 49. 0. 100. 7. 22. 1 7. 52. 10. 54 00 24 00 15 00 00 05 53 82 57 96 92 ( 0. ( 0. <20. 00) 00) 63) 1 1 2 300057 DATA FROM FILE: BS111694A SCANS 368 TO 1181 ACQUIRED: il/lP./94 n:44:rifi CALI: BS111694A ttl SAMPLE: SSTDOSO 290-02-SU25 CONDS.: RTX-5 0.25MM X 30M l.OUM 45/4-.325(?20 INST B 400 . 6:40 500 J 8:20 600 _f 10:00 700 11:40 800 13:20 900 . 15:00 o^ 1000 - Oj 16:40 cn 00 m J j_ CS50 2-FLUOROPHENOL 0.6 (SS-5) -^ 100.0;; ( 65408.) €S4&- D5-PHEN0L 0.8 .•v> M ^ ^ .DATA FROM FILE: BSl11694A SCANS llOl TO 2100 ACQUIRED: 11/16/94 11:44:90 CALI: BSl11694A #1 SAMPLE: SSTD050 290-02-SU25 CONDS.: RTX-5 0.25MM X 30M l.OUM 45/4-325220 INST B 1200 . 20:00 1400 J 23:20 1600 4 26:40 1800 30:00 2000 J CO o o 33:20 cn M i 100.0;; ( 41344.) i:i7Ci DJ-^-CHRYSENE (IS-5) CI75 D12-PERYLENE (IS-6) Quantitation Report File; BS111694A # ^ ^ c ; Data; BS111694A. TI 1/16/94 11:44:00 Sample; SSTD050 290-02-SV25 Conds.: RTX-5 O. 25MM X 30M l.OUM 45/4-325©20 Formula: X X X Instrument; B Submitted by; Analijst; JAM INST B Weight: Acct. No. 1. 000 AMOUNT=AREA • REF AMNT/(REF AREA • RESP FACT) Resp. fac. from Library Entrg • No 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 |41 '42 43 44 45 46 47 Name CI 30 CI40 CI 50 CI60 CI70 CI75 CS50 CS45 CS20 CS25 CS55 CS30 CS70 CS75 C315 C325 C330 C335 C340 C320 C310 C319 C345 C350 C355 C357 C370 C375 C410 C415 C420 C425 C430 C435 C440 C445 C450 C455 C460 C465 C470 C510 C515 C520 C525 C530 C535 0. 6 0. 8 0. 2 0. 7 5 8 4 D4-l,4 DICHLOROBENZENE DS-NAPHTHALENE DIO-ACENAPHTHENE DIO-PHENANTHRENE D12-CHRYSENE D12-PERYLENE 2-FLUOROPHENOL D5-PHEN0L D5-NITR0BENZENE 2-FLUOROBIPHENYL 2.4.6TRIBROMOPHENOL D14-P-TERPHENYL 2-CHL0R0PHEN0L-D4 1.2-CL2BENZENE-D4 •PHENOL BIS(2CHL0R0ETHYL)E 2CHL0R0PHEN0L 1.3DICHLOROBENZENE •1,4DICHL0R0BENZENE ANILINE N-NITROSODIMETHYLAMINE PYRIDINE BENZYL ALCOHOL 1,2DICHL0R0BENZENE O. 2METHYLPHEN0L O. 2.2'0XYBIS(1CHL0R0PR &NITROSOPROPYLAMINE O. HEXACHLOROETHANE NITROBENZENE ISOPHORONE •2-NITROPHENOL 2, 4-DIMETHYLPHENOL BENZOIC ACID BIS(2CHL0R0ETH0XY) O. 0, O. 0. 8 0. 7 O. 8 O. 6 O. 5 0. O. O. 0. 0. (IS-1) (13-2) (IS-3) (IS-4) (IS-5) (IS-6) (SS-5) (SS-4) (SS-1) (SS-2) (SS-6) (SS-3) (SS-7) (SS-8) 4 7 5 3 2 4 1 n O. •2.4DICHL0R0PHEN0L 0. 1. 2. 4TRICHL0R0BENZ 0. NAPHTHALENE 0. 4-CHLOROANILINE •CL6BUTADIENE •4CHL0R03METHYLPHEN 0. 2METHYLNAPHTHALENE 0. S^^ '^S 49 50 C540 C545 C550 m/z 152 136 164 188 240 264 112 99 82 172 330 244 132 152 94 93 128 146 146 93 74 79 108 146 108 45 70 117 77 82 139 107 122 93 162 180 128 127 225 107 142 237 196 196 162 65 163 152 138 153 ACENAPHTHYLENE 3-NITROANILINE •ACENAPHTHENE Scan -501 • 616 775 908 1170 1456 383 473 554 712 847 1049 484 518 • 474- 480- 485 497" 502- 475- 210 209 516- 519" 527- 528 541- 547 556 575 584 586- 598- 594 605 612 618 624 632 666 679 698 707 • 711 ' 723 736 751 762 773 778 Time 8; 21 10; 16 12; 55 15:08 19: 30 24: 16 6: 23 7: 53 9: 14 11; 52 14; 07 17: 29 8:04 8: 38 7: 54 8: 00 8: 05 8: 17 8: 22 7: 55 3: 30 3: 29 8:36 8:39 8:47 8: 48 9:01 9: 07 9: 16 9: 35 9:44 9: 46 9: 58 9: 54 10: 05 10; 12 10; 18 10:24 10: 32 11: 06 11: 19 11: 38 11:47 11: 51 12: 03 12: 16 12: 31 12: 42 12; 53 12: 58 Ref 1 2 3 4 5 6 1 1 2 3 3 5 2 2 2 2 2 2 2 2 2 2 2 2 2 3 3 3 3 3 3 3 3 3 0. 0. 0. 0. 1. 0. 0. 1. 0. 0. 0. 0. 1. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. o. 0. 0. 0. 0. 0. 0. 0. 0, 1. 1. 3 0. e RRT 000 000 000 000 000 000 764 944 899 919 093 897 966 034 946 958 968 992 002 948 419 417 030 036 052 054 080 092 903 933 948 951 971 964 982 994 003 013 026 081 102 901 912 917 933 950 969 983 997 004 Meth A BB A BB A BB A BB A BB A BD A BB A BV A BB A BB A BB A BB A BB A BB A BB A VB A BB A BV A VB A BV A BB A BB A BV A BB A VB A BB A BB A BB A BB A BB A BB A BB A BV A BB A BB A BB A BB A BV A BB A BB A BB A BB A BV A VB A BB A BB A BB A BB A BB A BB Area(Hght) 9825. 33034. 19628. 32470. 24774. 2634S. 11257. 16300. 13607. 25926. 3003. 24041. 13097. 9059. 20198. 16165. 12870. 14449. 15532. 20145. 7190. 10826. 7483. 14161. 12697. 21195. 8642. 5597. 14385. 28080. 7623. 9516. 5217. 17511. 10839. 12273. 34625. 11660. 5531. 10929. 24900. 6486. 8103. 8568. 22917. 7637. 26920. 36463. 2105. 21149. SfTO(pS-i' 3/liU^U Amount 20. 000 20. 000 20. 000 20. 000 20. 000 20. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB 7Tot 0. 0. 0. 0. 0. 0. 95 95 95 95 95 95 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 . 19 . 19 , 19 , 19 300061 No 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 43 49 50 \ Re- 8: 10: 12: 15: 19: 24: 6; 7: 9; 11: 14: 17: 8; 8; 7: 8; 8; 8: 8: 7; 3; 3: 8: 8: 8: 8: 9; 9; 9: 9; 9: 9; 9: 9: 10: 10: 10; 10; 10: 11: 11: 11; 11: 11; 12; 12; 12; 12; 12: 12; b(L) : 21 : 16 55 08 30 16 23 53 14 52 07 29 04 38 54 00 05 17 22 55 30 29 36 39 47 48 01 07 16 35 44 46 58 54 05 12 18 24 32 06 19 38 47 51 03 16 31 42 53 58 R, atio . 00 . 00 00 . 00 . 00 00 00 , 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 RRT(L) 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 764 0. 944 0. 899 0. 919 1. 093 0. 897 0. 966 1. 034 0. 946 0. 958 0. 968 0. 992 1. 002 0. 948 0. 419 0. 417 1. 030 1. 036 1. 052 1. 054 1. 080 1. 092 0. 903 0. 933 0. 948 0. 951 0. 971 0. 964 0. 982 0. 994 1. 003 1. 013 1. 026 1. 081 1. 102 0. 901 0. 912 0. 917 0. 933 0. 950 0. 969 0. 983 0. 997 1. 004 R, atio 00 00 00 00 00 00 00 , 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 •00 oo 00 00 00 00 00 00 00 00 00 00 00 00 0 0 00 00 00 00 00 00 00 00 00 00 00 00 00 Amnt 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 • 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 Amnt(L) 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 Sfroosp m lli^U R. Fac R. 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 917 1. 327 0. 330 1. 057 0. 122 0. 776 1. 066 0. 738 1. 645 1. 316 1. 048 1. 177 1. 265 1. 640 0. 585 0. 882 0. 609 1. 153 1. 034 1. 726 0. 704 0. 456 0. 348 0. 680 0. 185 0. 230 0. 126 0. 424 0. 262 0. 297 0. 839 0. 282 0. 134 0. 265 0. 603 0. 264 0. 330 0. 349 0. 934 0. 311 1. 097 1. 486 0. 086 0. 862 Fac(L) 1. 1. 1. 1. 1. 1. 0. 1. 0. 1. 0. 0. 1. 0. 1. 1. 1. 1. 1. 1. 0. 0. 0. 1. 1. 1. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 1. 1. 0. 0. 000 000 000 000 000 000 917 327 330 057 122 776 066 738 645 316 048 177 265 640 585 882 609 153 034 726 704 456 348 680 185 230 126 424 262 297 839 282 134 265 603 264 330 349 934 311 097 486 086 862 - - Rat — - io 00 , 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 , 00 00 .00 00 300062 Quantitation Report File; BS111694A .Data; BS111694A. TI )l 1/16/94 11:44:00 Sample: SSTD050 290-02-SV25 Conds.: RTX-5 O. 25MM X 30M l.OUM 45/4-325@20 Formula; X X X Instrument; B Submitted by: Analyst: JAM INST B Weigh t; Acct. No. 1. 000 AMOUNT=AREA • REF AMNT/(REF AREA • RESP FACT) Resp. fac. from Library Entry No 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 No 51 52 53 p4 '55 56 57 58 Name C321 C555 C560 C565 C570 C543 C580 C5B5 C590 C595 C610 C615 C625 C630 C635 C640 C645 C650 C655 D200 C647 C715 C720 C725 C730 C740 C735 C760 C765 C770 C775 C780 C785 C790 C365 m/z 232 184 109 168 165 165 149 204 2.3.4.6-TETRACHLOROPHENOL S<2. 4DINITR0PHEN0L 8<4N I TROPHENOL DIBENZOFURAN 2.4DINITR0TOLUENE 2,6DINITR0T0LUENE DIETHYL PHTHALATE 4CHL0R0PHENYL PHEN FLUORENE 4-NITROANILINE 0. 8 0. 2 0. 2 0. 4 0. 9 4.6DINITR02METHYLPH •DIPHENYLAMINE 4BR0M0PHENYL PHENY CL6BENZENE •PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-NBUTYLPHTHALATE •FLUORANTHENE 0. 1 0. 1 0. 05 0. 7 0. 7 0. 6 1. 2-DIPHENYLHYDRAZINE CARBAZOLE PYRENE 0. 6 BUTYLBENZYLPHTHALATE 3.3'CL2BENZIDINE BENZO(A)ANTHRACENE 0. 8 BIS(2ETHYLHEXYL)PHTH CHRYSENE 0. 7 •DI-N-OCTYLPHTHALATE BENZO(B)FLUORANTHE BENZO(K)FLUORANTHE •BENZO(A)PYRENE INDEN0(1,2, 3CD)PYR DIBENZO(A. H)ANTHRA BENZO((?. H. DPERYLE 4METHYLPHEN0L Scan Time Ref 806 13:26 3 1. 782 13:02 3 1. 787 13:07 3 1. 792 13; 12 3 1. 794 13; 14 3 1. 759 12:39 3 0. 813 13:33 3 1. 820 13:40 3 1. 0. 7 0. 7 0. 7 0. 5 0. 4 0. 5 0. 6 RRT 040 009 015 022 025 979 049 058 T T T T Me A A A A A A A A - >th BB BB BB BB BB DB BB DD Area(Hght) 8056. 3006. 2123. 33620. 8401. 6798. 25861. 12997. Amount 25. 25. 25. 25. 25. 25. 25. 25. 000 000 000 000 000 000 000 000 PPB PPB PPB PPB PPB PPB PPB PPB 7.Tot 19 19 19 19 19 19 19 19 300063 No 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 No 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 75 76 77 m/z : 166 138 198 169 248 234 266 178 178 149 202 77 167 202 149 252 228 149 228 149 252 252 252 276 278 276 108 Scan 823 830 831 832 864 879 895 910 914 955 1018 835 928 1040 1094 1162 1167 1158 1174 1255 1360 1366 1440 1815 1822 : 1927 540 Time Ref 13: 43 13; 50 13; 51 13; 52 14; 24 14; 39 14; 55 15: 10 15: 14 15; 55 16; 58 13; 55 15; 28 17; 20 18: 14 19: 22 19: 27 19; 18 19; 34 20; 55 22; 40 22; 46 24; 00 30; 15 30; 22 32; 07 9; 00 Ret(L) Ratio RRT(L) 13:26 13:02 13: 07 13: 12 13; 14 12: 39 13: 33 13; 40 13; 43 13; 50 13; 51 13: 52 14; 24 14; 39 14; 55 15; 10 15; 14 15: 55 16: 58 13; 55 15; 28 17; 20 IS; 14 19; 22 19; 27 19; 18 19; 34 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 040 1. 009 1. 015 1. 022 1. 025 0. 979 1. 049 1. 058 1. 062 1. 071 0. 915 0. 916 0. 952 0. 968 0. 986 1. 002 1. 007 1. 052 1. 121 0. 920 1. 022 0. 889 0. 935 0. 993 0. 997 0. 990 1. 003 3 3 4 4 4 4 4 4 4 4 4 4 4 5 5 5 5 5 5 6 6 6 6 6 6 6 1 RRT 1. 062 1. 07 1 0. 915 0. 916 0. 952 0. 968 0. 986 1. 002 1. 007 1. 052 1. 121 0. 920 1. 022 0. 889 0. 935 0. 993 0. 997 0. 990 1. 003 0. 862 0. 934 0. 938 0. 989 1. 247 1. 251 1. 323 1. 078 1 Ratio 1. 00 00 00 00 00 00 00 00 00 00 00 00 00 . 00 , 00 . 00 , 00 , 00 , 00 , 00 , 00 . 00 , 00 . 00 , 00 . 00 . oo Meth A BB A VB A BB A BB A BB A BB A BB A BV A VB A BB A. BB A BB A BB A BB A BB A BB A BV A BB A VB A BB A BV A VB A BB A BB A BB A BB A Bm-'i Amnt 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 ^ Area(H9ht) 26765. 2536. 4763. 13204. 7648. 7474. 4974. 39916. 40182. 45559. 39629. 34947. 14584. 41417. 19095. 6377. 32715. 27463. 30125. 45164. 33056. 28720. 29173. 31601. 24105. 26716. /?t/'^12756. Amnt(L) 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. OO syfo9tp tSlllUHA Amount 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 R. Fac R. F 0. 0. 0. 1. 0. 0. 1. 0. 1. 0. 0. 0. 0. 0. 0. 0. 0. 1, 0, 0 0. 1 0 0 1. 0 0 328 < 123 1 087 ( 370 342 1 277 054 530 091 103 117 325 188 184 123 983 990 122 .976 . 861 , 359 . 337 . 617 . 206 , 056 . 887 . 973 PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB ac(L) 0. 328 0. 123 D. 087 1. 370 D. 342 0. 277 1. 054 0. 530 1. 091 0. 103 0. 117 0. 325 0. 188 0. 184 0. 123 0. 983 0. 990 1. 122 0. 976 0. 861 0. 359 1. 337 0. 617 0. 206 1. 056 0. 887 0. 973 7.Tot 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 Ratio 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 . 00 00 , 00 . 00 . 00 . 00 . 00 . 00 , 00 , 00 , 00 , 00 ^3 00064 • ^ - - - - No 78 79 80 81 82 83 84 85 Ret(L) 20; 55 22; 40 22:46 24; 00 30; 15 30: 22 32: 07 9:00 Ratio 00 00 00 00 00 00 00 00 RRT(L) 0. 862 0. 934 0. 938 0. 989 1. 247 1. 251 1. 323 1. 078 Ratio 00 00 00 00 00 00 00 00 Amnt 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 Amnt(L) 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 Xnvayp SfllUlHA R. Fac R. 1. 371 1. 004 0. 872 0. 886 0. 960 0. 732 0. 811 1. 039 Fac(L) 1. 371 1. 004 0. 872 0. 886 0. 960 0. 732 0. 811 1. 039 Rat io 0 0 00 00 00 00 00 00 00 300065 C a l i b r a t i on Check m Instrument Identifier; B balibration Date; 08/20/94 Standard File; DS111694A Date; 11/16/94 Time; 11: MIN RF; SW(.?<) = . 05 CLP MAX .7.D: SW(^) = 307. CLP Compound 44: 00 = .01 OR = 257. Mean RF(I) BELOW RF(0) 7. D CS50 CS45 CS20 CS25 CS55 CS30 CS70 CS75 2-FLUOROPHENOL D5-PHEN0L D5-NITR0BENZENE 2-FLUOROBIPHENYL 0. 6 O. 8 0. 2 0. 7 2.4.6TRIBROMOPHENOL D14-P-TERPHENYL 0. 5 2-CHL0R0PHEN0L-D4 0. 8 1.2-CL2BENZENE-D4 0. 4 C315 •PHENOL 0. 8 C325 BIS(2CHL0R0ETHYL)E 0.7 C330 2CHL0R0PHEN0L 0. 8 C335 1,3DICHL0R0BENZENE 0.6 C340 •I.4DICHL0R0BENZENE 0.5 C320 ANILINE N-NITROSODIMETHYLAMINE PYRIDINE BENZYL ALCOHOL 1,2DICHLOROBENZENE O. 4 2METHYLPHEN0L 0. 7 C310 C319 »P345 ^350 •7:355 C357 C365 4METHYLPHEN0L 0. 6 C370 &NITROSOPROPYLAMINE 0. 5 C375 C410 C415 C420 C425 C430 C435 0. 3 0. 2 0. 4 0. 1 C450 C455 C520 C525 C530 X535 ^540 :545 0. 3 0. 2 0. 2 O. 7 HEXACHLOROETHANE NITROBENZENE ISOPHORONE •2-NITROPHENOL 2.4-DIMETHYLPHENOL 0. 2 BENZOIC ACID BIS(2CHL0R0ETH0XY) C440 •2,4DICHL0R0PHEN0L C445 1,2.4TRICHLOROBENZ NAPHTHALENE 4-CHLaROANILINE C460 •CL6BUTADIENE C465 «4CHL0R03METHYLPHEN 0. 2 C470 2METHYLNAPHTHALENE 0. 4 C510 S DATA FROM FILE: SUUNSOl SCANS 1094 TO 2100 ACQUIRED: 11/16./94 15:50:00 CALI: SUUNSOl #1 SAMPLE: PT-1/110434 WATER HLA . CONDS.: RTX-5 0.25MM X 30M l.OUM 45/4-325(520 INST B 1200 _ 20:00 L 1400 - 23:20 ^ B - - r •i _L J 100.0;^ ( 31328.) CI70 D12-CHRYSENE (IS-5) CI75 D12-PERYLENE (IS-5) 1500 25:40 I 3 1800 _* 30:00 2000 33:20 ?ri CJ o o o vJ CO Quantitation Report File; SVUNSOl ^Wa 3ta; SVUNSOl. TI /16/94 15; 50; 00 ample; PT-1/H0494 Conds. : RTX-5 0. 25MM Formula: S S W Submitted by; WATER X 30M HLA 1.OUM 45/4-325020 Instrument: B Analyst: JAM INST B Weight: Acct. No. ; 1. 000 10966 AMOUNT=AREA • REF AMNT/(REF AREA • RESP FACT) Resp. fac. from Library Entry No 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 I'' ^ 7 No 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 No 1 2 i^ P4 5 Name CI 30 CI40 CI 50 CI60 CI70 CI75 CS50 CS45 CS20 CS25 CS55 CS30 CS70 CS75 C720 C740 C760 m/z 152 136 164 188 240 264 112 99 82 172 330 244 132 152 149 149 149 D4-1.4 DICHLOROBENZENE DS-NAPHTHALENE D10-ACENAPHTHENE D10-PHENANTHRENE D12-CHRYSENE D12-PERYLENE 2-FLUOROPHENOL D5-PHEN0L D5-NITR0BENZENE 2-FLUOROBIPHENYL 0. 6 0. 8 0. 2 0. 7 2.4.6TRIBR0M0PHEN0L D14-P-TERPHENYL 0. 5 2-CHL0RQPHEN0L-D4 0. 8 1.2-CL2BENZENE-D4 0. 4 BUTYLBENZYLPHTHALATE BIS(2ETHYLHEXYL)PHTH •DI-N-OCTYLPHTHALATE Scan Time R 494 - 8;14 614 10; 14 774 12;54 907 15:07 1168 19:28 1453 24;13 363 6; 03 464 7:44 550 9;10 711 11;51 846 14:06 1048 17:28 475 7; 55 5 1 2 - 8:32 1092 18;12 1156 19;16 1253 20;53 !ef 1 2 3 4 5 6 1 1 2 3 3 5 1 1 5 5 6 Ret(L) Ratio RRT(L) Ri 8; 2 1 0. 99 1. 000 10; 16 1. 00 1. 000 12:55 1.00 1.000 15; OS 1. 00 1. 000 19; 30 1. 00 1. 000 RRT 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 735 0. 939 0. 896 0. 919 1. 093 0. 897 0. 962 1. 036 0. 935 0. 990 0. 862 atio 00 , 00 . 00 . 00 . 00 (IS-1) (IS-2) (IS-3) (IS-4) (IS-5) (IS-6) (SS-5) (SS-4) (SS-1) (SS-2) (SS-6) (SS-3) (SS-7) (SS-8) Meth A BB A BB A BB A BB A BB A BB A BB A BB A BB A BB A BB A BE A BB A BB A VV A BB A BB Amnt 20. 00 20. 00 20. 00 20. 00 20. 00 Area(Hght) 8553. 30853. 18061. 29565. 23933. 24679. 22400. 35340. 19002. 36462. 7357. 36651. 26356. 9537. 2220. 3837. 2308. Amnt(L) R 20. 00 20. 00 20. 00 20. 00 20. 00 Amount 20. 000 20. 000 20. 000 20. 000 20. 000 20. 000 57. 145 62. 263 37. 380 33. 210 66. 561 39. 452 58. 883 30. 233 3. COS 3. 616 1. 364 ;. Fac R. F 1. 000 1. 000 1. 000 1. 000 1. 000 PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB ac(L) 1. 000 1. 000 1. 000 1. 000 1. 000 7.Tot 3. 3. 3. 3. 3. 3. 11. 12. 7. 7. 12. 7. 11. 5. 0. 0. 0. Rat 1. 1. 1 1 1 86 86 86 86 86 86 03 02 21 37 85 61 37 84 5S 70 26 i 0 . 00 , 00 . 00 . 00 . 00 300074 No R e t ( L ) R a t i o RRT(L) R a t i o 6 \ 7 's 9 10 11 12 13 14 15 16 17 24: 6; 7; 9; 11; 14; 17; B: 8; 18; 19: 20: 16 23 53 14 52 07 29 04 38 14 18 55 1. 0. 0. 0. 1. 1. 1. 0. 0. 1. 1. 1. 00 95 98 99 00 00 00 98 99 00 00 00 1. 0. 0. 0. 0. 1. 0. 0. 1. 0. O. 0. 000 764 944 899 919 093 897 966 034 935 990 862 1. 0. 0. 00 96 99 00 00 00 00 00 00 00 OO 00 Amnt 20. 57. 62. 37. 38. 66. 39. 58. 30. 3. 3. 1. 00 15 26 33 21 56 45 89 23 01 62 36 A m n t ( L ) R.Fac R . F a c ( L ) R a t i o 20. 25. 25. 25. 25. 25. 25. 25. 25. 25. 25. 25. 00 00 00 00 00 00 00 00 00 00 00 00 1. 2. 3. 0. 1. 0. 1. 2. 0. 0. 0. 0. 000 095 306 493 615 326 225 512 892 074 128 075 1. 0. 1. 0. 1. 0. 0. 1. 0. 0. 0. 1. 000 917 327 330 057 122 776 066 738 617 887 371 1. 2. 2. 1. 1. C . 1. 1. 0. 0. 0. 00 29 49 50 53 66 58 36 21 12 14 05 300075 TARGET COMPOUND COMPARISON COMPOUND: C720 BUTYLBENZYLPHTHALATE RAW DATA: SUUNSOl #1092 ll/16.'-94 15:50 SAMPLE: PT-1/110494 WATER HLA CONDS.: RTX-5 0.25MM X 30M l.OUM 45/4-325520 BASE M/Z: INST B 149 RIC: 1352. 48.2-1 24.1 1 — ' i ' I I I I I I I I I I I ' I I I I I I ! I I I I I I I I I I I I ' I I — l l l l — l — T ' I ' ' ' ' I 482. I I I I I I I I I I I I I I I I I I I I ' ' I I ' ENHANCED DATA: SUUNSOl #1092 BASE M/Z: 149 RIC: 902. i < . •-' 13.7 r ' I I I I I I - r - l — l l l l — r — 1 — r - 1 I ' ' ' ' I ' I ' ' I I I I I I I — I I I I I I — r - 1—I I I I I I I I I I I I I I I I I I I I I I I I I I I' I I" I I I I I I I * ' LIBRARY FILE: SN #52 BASE M/Z: 149 RIC: 2940. 100.0-1 50.0- -I i r ^ r I I I I I I I I I I I I I I I I I'l I I I ' ' I r - r - A I I r I ' ' I I ' I I I I ' I ' I r 1000. I I I I I — 1 1 I I I I I I I I I I I I I I I I I I 1 1 ' I ' I M/Z 40 100.0- 50.0-* =10 60 ;-;o 100 120 140 150 160 180 200 0.0- -50=0- co g-100.0-' o -J a\ I 100.0- 83. bn 41.3-1 M.7-] 37.4- TARGET COMPOUND COMPARISON COMPOUND: C740 BIS(2ETHYLHEXYL)PHTH RAW DATA: SUUNSOl #1156 11/16/94 15:50 SAMPLE: PT-1/110494 WATER HLA ;.: RTX-5 0.25MM X 30M l.OUM 45/4-325@20 BASE M/Z: INST B 149 RIC: 4056. J L ; CO 1 o I o i - J •>J M/Z 100.0- 50. 0d 0.0 -50. 0-" -100.0 - i — 1 — I — 1 — I — I — I — I — I 1 I I 1 I I I r ENHANCED DATA: SUUNSOl #1155 1338. — 1 — 1 — I — I — I — I — I — I BASE M/Z: 149 - 1 — I — I — I — 1 — I — I — I — 1 - ^ RIC: 3200. I ' I - • — I — > — r - i — I — I — I — r 1—'—r -I 1 1 1 1 1 r- LIBRARY FILE: SN #56 BASE M/Z: 149 RIC: 1586. - • — i — ' — r - 1 — I — ' — I — ' — r " 1 — < — r 50 100 150 200 - I — I — I — I — 1 250 1118. r 1000. 28.2-] 14.IT 22.1-: 11.0-: TARGET COMPOUND COMPARISON COMPOUND: C750 $0I-N-OCTYLPHTHALATE RAW DATA: SUUNSOl #1253 11/16/94 15:50 SAMPLE: PT-1/110494 WATER HLA CONDS.: RTX-5 0.25MM X 30M l.OUM 45/4-3251220 BASE M/Z: 149 INST B RIC: 528. ^ i I - I — I — I — I — p — i — I — I — r — ] — I — r — I — I — p — 1 — I I I — I — I — I — r — 1 — | — i — i — i — i — r — i — i — r — i — [ • • i • i — r - - 1 — I — T — r * - i — I — I — r - ENHANCED DATA: SUUNS01 #1253 BASE M/Z: 149 RIC: 471. jl.fc. X 1 - I — r - H — I — I — I — I — I — T - ' T — I — 1 — I — I — I — T " ^ — ' — ' — ' — I — ' — ' — ' — ' — I — ' — ' — ' — ' — I — ' — ' " - ' ' — ' " - I — I — I — I — I — I — I — r - " 1 — I — I — I — I — I — I — I 1 — H - ] — I — I — r - 100.0- 50.0-: LIBRARY FILE: SN #57 BASE M/Z: 149 RIC: 1110. 1000. - I — I — I — I — 1 — I — 1 — 1 — I — I — I — I — I — I — I — I — I — I — I — I — I — I — I — I — I — 1 — I — I — I — I — I — 1 — 1 — I — I — I — I — I — I — I — I — r - - I — I — I — I — I — I — I — I — I — I — r ' ' I — I — r - CO o o o 00 M/Z 40 100.0- 50.0-: 0.0- -50.0- F:0 hy 80 100 120 •100. 0-' 140 150 DATA FROM FILE: SUUNS02 SCANS 355 TO 1095 ACQUIRED: 11/16/94 16:31:00 CALI: SUUNS02 #1 SAMPLE: PT-2/110494 WATER HLA CONDS.: RTX-5 0.25MM X 30M 1.0UM 45/4-325520 INST B 400 _, 6:40 5uti 3:20 600 . 10:00 700 11:40 800 13:20 900 _: 15:00 CO o o o •J vo 1000 _ 16:40 W I CS50 2-FLUOROPHENOL - - . . J z m . m ( 71680.) U.b >:.bb-.j) JLS45 c^rPmumPHEmM 'Wlsz-?^ GI30 D4-1..4 DICHLOROBENZENE (IS-1) CS75 1.. 2-CL2BENZEHE-D4 0.4 (SS-8) CS20 D5-NITROBENZENE 0.2 (SS-1) CI40 DS-NAPHTHALENE I'l'^y-i CS25 2-FLUOROBIPHENYL 0.7 (SS-2) CI50 DIO-ACENAPHTHENE (IS-3) 2.. 4,. 5TRI BROMOPHENOL CI50 DIO-PHENANTHRENE (SS-6) (IS-4) H5590 D14-P-TERPHENYL 0.5 (SS-3) li^ DATA FROM FILE: SUUNS02 SCANS 1095 TO 2100 ACQUIRED: 11/16/94 16:31:00 CALI: SUUNS02 #1 SAMPLE: PT-2/110494 WATER HLA CONDS.: RTX-5 0.25MM X SOM l.OUM 45/4-325520 INST B CO o o o CO o I _L ± 1200 . 20:00 1400 _ 23:20 1600 _ 25:40 1800 _ 30:00 2000 . 33:20 ffl -• 100.0;^ ( 29564.) CI70 D12-CHRYSENE (IS-5) CI75 D12-PERYLENE (IS-6) Quantitation Report File: SVUNS02 u, m Data; SVUNS02. TI 1/16/94 16;31;00 ample; PT-2/110494 WATER Conds.: RTX-5 0. 25MM X SOM Formula; S S W Submitted by; HLA 1.OUM 45/4-325t20 Instrument: B Analyst; JAM INST B Weight; 1. 000 Acct. No. : 10966 AMOUNT=AREA • REF AMNT/(REF AREA • RESP FACT) Resp. fac. from Library Entry No 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 ho 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 No 1 2 3 4 5 6 ^ 7 Pe 9 Name CI30 CI40 CI 50 CI 60 CI70 CI75 CS50 CS45 CS20 CS25 CS55 CS30 CS70 CS75 C740 D4-1.4 DICHLOROBENZENE DS-NAPHTHALENE DIO-ACENAPHTHENE DIO-PHENANTHRENE D12-CHRYSENE D12-PERYLENE 2-FLUOROPHENOL D5-PHEN0L D5-NITROBENZENE 2-FLUOROBIPHENYL 0. 6 0. 8 0. 2 0. 7 2,4.6TRIBROMOPHENOL D14-P-TERPHENYL 0. 5 2-CHL0R0PHEN0L-D4 0. 8 1,2-CL2BENZENE-D4 0. 4 BIS(2ETHYLHEXYL)PHTH m/z Scan Time Ref 152 136 164 188 240 264 112 99 82 172 330 244 132 152 149 495/ 8; 15 1 614 10;14 2 774 12;54 3 907 15; 07 4 1168 19:28 5 1453 24: 13 6 363 6; 08 1 466 7; 46 1 551 9;11 2 712 11:52 3 846 14:06 3 104S 17:2S 5 478 7;58 1 513' 8:33 1 1156 19: 16 5 RRT 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 743 0. 941 0. 897 0. 920 1. 093 0. 897 0. 966 1. 036 0. 990 Ret(L) Ratio RRT(L) Ratio S; 21 10: 16 12; 55 15; 08 19; 30 24: 16 6; 23 7: 53 9; 14 0.99 1.000 1. 1. 00 1. 000 1. 1.00 1.000 1. 1. 00 1. 000 1, 1. 00 1. 000 1, 1.00 1.000 1. 1 0. 96 0. 764 0 [ 0. 99 0. 944 1 0. 99 0. 899 1 00 00 00 00 , 00 . 00 . 97 . 00 . 00 (IS-1) (13-2) (IS-3) (IB-4) (IS-5) (IS-6) (SS-5) (SS-4) (SS-1) (SS-2) (SS-6) (SS-3) (SS-7) (SS-8) Meth A BB A BB A BB A BB A BB A BB A BB A BB A BB A BB A BB A BB A BB A BB A BB Amnt 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 62. 27 66. 78 39. 21 Area(Hght) 8633. 32871. 18538. 31305. 24671. 27222. 24637. 38259. 21234. 33195. 8053. 40723. 29560. 9629. 7559. Amnt(L) F 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 25. 00 25. 00 25. 00 Amount 20. 000 20. 000 20. 000 20. 000 20. 000 20. 000 62. 270 66. 782 39. 206 33. 996 70. 983 42. 524 64. 216 30. 242 6. 910 !. Fac R. F 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 2. 283 3. 545 0. 517 . PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB ac(L) 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 917 1. 327 0. 330 •/;Tot 3. 69 3. 69 3. 69 3. 69 3. 69 3. 69 11. 49 12. 32 7. 23 7. 19 13. 09 7. 84 11. 85 5, 53 1. 27 Ratio 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 2. 49 2. 67 1. 57 300081 No 10 i^ b 13 14 15 Ret(L) 11; 52 14; 07 17:29 8:04 8; 33 19: IS Ratio 1. 00 1. 00 1. 00 0. 99 0. 99 1. 00 RRT(L) 0. 919 1. 093 0. 897 0. 966 1. 034 0. 990 Ratio 1. 00 1. 00 1. 00 1. C>0 1. 00 1. 00 Amnt 39. 00 70. 98 42. 52 64. 22 30. 24 6. 91 Amnt(L) 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 R. Fac R 1. 648 0. 348 1. 321 2. 739 0. 892 0. 245 Fac(L) 1. 057 0. 122 0. 776 1. 066 0. 738 0. S87 Ratio 1. 56 2. 1. c. 1. o 84 70 57 21 2S 300082 100.0- 50.0- - y ^ r - j 44.2- TARGET COMPOUND COMPARISON COMPOUND: C740 BIS(2ETHYLHEXYL)PHTH RAW DATA: SUUNS02 #1156 11/16.--94 16:31 SAMPLE: PT-2/110494 WATER HLA CONDS.: RTX-5 0.25MM X 30M l.OUM 45/4-325520 - r ^ — r 1—I—r BASE M.--Z: 149 RIC: 9600. INST B ENHANCED DATA: SUUNS02 #1155 — I — I — , — j — I — 1 — I — f - BASE M/Z: 149 - 1 1 1 1 1 1 1 1 1 H 1 - RIC: - r ' I '•• I • -p",—r 1 — y ^ — I — I — I — I — I — I - T 1 r 1 — • — I — ' — r 36. i ' l ' i I Q C . 52.0-1 16.0- LIBRARY FILE: SN #55 1—I—I—'—I—'—r M/Z 100.0- 50.0- 0.0- w -50.0- o o l O -100.0- 00 I col I I I 1 1 -•—r 1—'—r BASE M/Z: 149 RIC: 1586, "1 I I ' r 1—I—1—'—r 100 150 200 250 I II r 1000. 1—'—!—'—T DATA FROM FILE: SUUNS03 SCANS 353 TO 1093 ACQUIRED: 11/16/94 17:11:00 CALI: SUUNS03 #1 SAMPLE: PT-3/110494 WATER HLA CONDS.: RTX-5 0.25MM X 30M l.OUM 45/4-325520 INST B 400 _ 6:40 - 500 . S:2M 500 10:00 700 . 11:40 300 . 13:20 300 . 15:00 CO o o o 00 1000 16:48 'Effi CS50 2-FLUOROPHENOL 0.6 (SS-5) 100.0' 49654.) C^a^ 2 ^ 5 « a E N 0 L - D 4 2 ? ^ ^ ^ ^ CI30 D4-1..4 DICHLOROBENZENE (IS-1) CS75 1.2-CL2BENZENE-D4 0.4 (SS-S) CS20 D5-NITROBENZENE 0.2 (SS-1) CI40 DS-NAPHTHALENE (IS-2) CS25 2-FLUOROBIPHENYL 0.7 ( ' - 1 ' - , - ' • • ' t -€150 DIO-ACENAPHTHENE :is-3) CS55 2.. 4.. 5TRI BROMOPHENOL (SS-6) CI60 DIO-PHENANTHRENE (IS-4) - ^ c^ x" CS30 ni4-P-TERPHENYL 0.5 (SS-3) CJ o o o 00 cn DATA FROM FILE: SUUNS03 SCANS 1093 TO 2100 ACQUIRED: 11/16/94 17:11:00 CALI: SUUNS03 #1 SAMPLE: PT-3/110434 WATER HLA CONDS.: RTX-5 0.25MM X SOM l.OUM 45/4-325520 INST B 1200 J 20:00 1 23:20 1500 . 26:40 1800 _. .30:fiH 33:20 ffflg J -J 100.0" ( 25312.) CI70 D12-CHRYSENE (IS-5) CI75 D12-PERYLENE (IS-6) Quantitation Report File; SVUNS03 ^^ra ata; SVUNS03. TI /16/94 17; 11: 00 ^mple; PT-3/110494 Conds. : RTX-5 0. 251- Formula; S S W Submitted by; WATER HLA X SOM l.OUM 45/4-325^20 Instrument; 3 Analyst; JAM INST B Weight; 1. 000 Acct. No. ; 10966 AMOUNT=AREA • REF AMNT/(REF AREA • RESP FACT) Resp. fac. from Library Entry No 1 c 3 4 5 6 7 8 9 10 11 12 13 14 15 Name CI 30 CI40 CI 50 CI60 CI 70 CI75 CS50 CS45 CS20 CS25 CS55 CS30 CS70 CS75 C740 D4-1.4 DICHLOROBENZENE DS-NAPHTHALENE D10-ACENAPHTHENE DIO-PHENANTHRENE D12-CHRYSENE D12-PERYLENE 2-FLUDROPHENOL D5-PHEN0L D5-NITR0BENZENE 2-FLUCROBIPHENYL 2.4.6TRIBROMOPHENOL D14-P-TERPHENYL 0.5 2-CHL0R0PHEN0L-D4 0.8 1.2-CL2BENZENE-D4 0.4 BIS(2ETHYLHEXYL)PHTH 0. 0. O. 0. (IS-1) (IS-2) (IS-3) (IS-4) (IS-5) (IS-6) (SS-5) (SS-4) (SS-1) (SS-2) (SS-6) (SS-3) (SS-7) (SS-S) m/z Scan Time Ref RRT Meth 1 C 3 4 5 6 7 8 9 10 11 12 13 14 15 152 136 164 IBS 240 264 112 99 B2 172 330 244 132 152 149 493' 613 773 906 1167 1452 363 464 549 711 845 1047 475 512 ' 1155 8; 13 10; 13 12: 53 15: 06 19: 27 24; 12 6; 03 7; 44 9: 09 11; 51 14; 05 17; 27 7; 55 B; 32 19; 15 1 2 3 4 6 1 1 2 3 3 C= 1 1 000 000 000 000 000 1. 000 0. 736 O. 941 O. 896 0. 920 1. 093 0. 897 0. 963 1. 039 0. 990 A BB A BB A BB A BE A BB A BB A BB A BB A BB A BB A BB A BB A BB A BB A BB Area(Hght) 6628. 25909. 14867. 23577. 20228. 22239. 14690. 26120. 14770. 26604. 5185. 31551. 18906. 6546. Amount 20. 000 PPB 20. 0(D0 PPB 20. 000 PPB 20. 000 PPB 20.000 PPB 20. 000 PPB 48. 360 PPB 59. 385 PPB 34. 599 PPB 33. 869 PPB 56. 988 PPB 40.183 PPB 53. 496 PPB 26. 778 PPB 4. 462 PPB •/.Tot 4. 13 4. 18 4. 18 4. 18 4. 18 4. 18 10. 11 12. 42 7. 24 7. 08 11. 92 8. 40 11. 19 5. 60 0. 93 No Ret(L) Ratio RRT(L) Ratio 1 8; 21 0. 98 1. 000 1. 00 2 ,10: 16 1. 00 1. 000 1. 00 3 12; 5J 1.00 1.000 1.00 4 5 6 7 8 15: 19; 24; 6; 7; OS 30 16 23 53 1. 1. 1. 0. 0. 00 00 00 95 9S 1. 1. 1. 0. 0. 000 000 000 764 944 1. 1. 1. 0. 1. 00 00 00 96 00 9; 14 0. 99 O. 899 1. 00 Amnt 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 48. 36 59. 33 34. 60 Amnt(L) R. Fac R.Fac(L) Ratio 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 25. 00 25. 00 25. 00 1. 000 000 000 000 000 1. 000 1. 773 3. 153 0. 456 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 917 1. 327 0. 330 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 93 2. 38 1. 38 300086 No 10 (11 12 13 14 15 Ret(L) 11: 52 14; 07 17:29 8: 04 8; 38 19; 18 Ratio 1. 00 1. 00 1. 00 0. 98 0. 99 1. 00 RRT(L) 0. 919 1. 093 0. 897 0. 966 1. 034 0. 990 Ratio 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Amnt 33. 87 56. 99 40. IS 53. 50 26. 78 4. 46 Amnt(L) 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 R. Fac R. 1. 432 0. 279 1. 248 2. 282 0. 790 0. 153 Fac(L) 1. 057 0. 122 0. 776 1. 066 0. 738 0. 887 Ratio 1. 35 2. 2S 1. 61 2. 14 1. 07 0. IS 300087 100.0- !^fi.0- 43.7- TARGET COMPOUND COMPARISON COMPOUND: C740 BIS(2ETHYLHEXYL)PHTH RAW DATA: SUUNSOS #1155 11/15/94 17:11 SAMPLE: PT-3/110434 WATER HLA CONDS.: RTX-5 0.25MM X SOM l.OUM 45/4-325520 BASE M/Z: 149 INST B •y-' 1 — ' — I — ' ' 1 " ' I — I 1 — > — I — r - * 1 — • — I — T - ' - T — I — I — ' \ — ' — I — ' 1 — ' — I — f - Rlf ENHANCED DATA: SUUNSOS #1155 '• r " ' I - I — r 4912. I ' r BASE M/Z: 149 RIC: 4296. _- i COO IC"-".'. r 1474. 1 — I — I — 1 — r 1 I — I — I — I — I — I — I — r 59.2^ 29.5- y.o- 0.0- » grl00.0-^ O CO 1 00 LIBRARY FILE: SN #56 1 — I — I — 1 — I — I — I — I — I — I — I — ' j — ' I — ' I <~ M/Z 50 100 100.0-1 50.0- 1 i\ BASE M/Z: 149 ;IC: 1585. -T 1 ' ] ' I 1 r-"-] > 1 > 1 > 1 1 1 1 1 > \ 1 1 1 1 1 1 1 1 1—Y" 150 200 250 100.0-1 50.0 M/Z 100.0 50.0 MASS SPECTRUM 11/29/94 13:42:00 + 8 : 5 0 SAMPLE: DFTPP 244-92-PERF CONDS.: RTX-5 0.25MM X SOM l.OUM 45/4-325520 #529 TO #531 AUERAGED - #525 Xl.OO DATA: BP112994E #530 CALI: BP112934E #1 INST B BASE M/Z: 198 RIC: 13840. 2204. 2204. 250 400 450 RIC 11/29/94 13:42:00 SAMPLE: DFTPP 244-92-PERF CONDS.: RTX-5 0.25MM X SON RANGE: G 1.. 70© LABEL: N 100.0-1 DATA: BP112994E #529 CALI: BP112994E #1 l.OUM 45/4-325520 INST B 0.. 4.0 QUAN: A O. l.O J O 530 SCANS 515 TO 565 BASE: U 20. RIC o o o CO o 22880. 517 \ 554 520 8:40 530 3:50 540 S'.Qf. 550 9:10 560 9:20 SCAN TIME • ' Mass List Data; 11/29/94 13:42:00 + 8:50 Cali: Sample: DFTPP 244-92-PERF Conds.: RTX-5 0. 25MM X SOM l.OUM #529 to #531 averaged - #525 XI. 00 BP112994E BP112994E 530 1 39 443 Mass O. 00 7. RA O. Inten. Minima Max ima Mass 45/4-325(520 Min Inten; # 0 7. RA Base RIC; m/ z; 198 13840. INST B 0. Inten. 39? 50? 51? 52? 57? 63? 69 74 75 77 78 79 80 81 93 98 99 101 107 108 110 111 117 127 128 129 130 148 167 179 180 186 187 196 198 199 204 205 206 207 217 221 224 225 227 244 255 256 258 S S S S S S S S S S S S S S S S S S S S S S S S s s s s s s s s s s s s s s s s s s s s 5 s s s s s 7. 32. 1. 2. 1. 43. 18 53 53 18 18 36 24 09 5. 94 42, 1 83 95 54 59 13 86 18 1. 1. 2. 2. 2. 1. 41 1. 59 11. 43 2. 59 24. 05 2. 27 5. 90 42. 29 2. 04 16. 42 1. 18 1. 41 4. 08 3. 09 1. 41 10. 84 3. 40 2. 27 100. 00 7. 3. 2. 23. 03 45 36 00 99 5. 94 5. 54 11. 30 3. 09 4. 40 8. \2. 6. 1. 80 47 13 23 5. 49 48. 166. 717. 26. 48. 30. 953. 46. 131. 944. 43. 34. 35. 47. 63. 48. 31. 35. 252. 57. 530. 50. 130. 932. 45. 362. 26. 31. 90. 68. 31. 239. 75. 50. 2204. 155. 76. 52. 507. 66. 131. 122. 249. 68. 97. 194. 936. 135. 27. 121. 275 276 296 365 423 441? 442? 443? S S S S S S S S 23. 09 4. 31 4. 40 1. 91 2. 68 6. 40 49. 09 9. 53 509. -95. 97. 42. 59. 141. 1082. 210. 300091 GC/MS Tuning and Mass Calibration DECAFLUOROTRIPHENYLPHOSPHINE Case Number: Laboratory; GULF Contract: Inst ID; B Sens Date; 11/29/94 Sens Time; 13:42:00 Lab ID: BP112994E Cali Date; 10/02/91 Analyst: JAM Data release authorized by: M/E Ion Abundance Criteria Spec # 529 51 30 to 607. of mass 198 68 less than 27. of mass 69 69 mass 69 relative abundance 70 less than 27. of mass 69 127 4,0 TO 607. of mass 198 197 less than 17. of mass 198 198 base peak. 1007. relative abundance 199 5 TO 97. of mass 198 275 10 TO 307. of mass 198 365 greater than 17. of mass 198 441 less than mass 443 442 greater than 407. of mass 198 443 17 TO 237. of mass 442 1 - value in parenthesis is 7. of mass 69 2 - value in parenthesis is '/. of mass 442 32. 53 - 0. 00 43. 24 0. 00 42. 29 • 0. 00- 100. 00- 7. 0 3 " 23. 09" 1. 9 1 - 6. 40- 49. 09 . 9. 53 • ( ( 0. 00) 0. 00) (19. 41) 1 1 2 300092 DATA FROM FILE: BS112994A SCANS 395 TO 1120 ACQUIRED: 11./29/94 14:06:R0 CALI: BS112994A #1 SAMPLE: SSTDOSO 29O-02-SU25 CONDS.: RTX-5 0.25MMX.30M l.OUM 45/4-32.5520 INST P 400 _r 6:40 500 8:20 600 10:00 700 _ 11:40 800 _ 13:20 900 . 15:00 1000 16:40 col o, OU.1..00. _L CS50 2-FLUOROPHENOL 0.6 (SS-5) 100.0;^ ( 80256.) mrS'-imMOPHEKL-D^-VmiTy eK:0 D 4 - L 4 DICHLOROBENZENE (IS-1) — e 5 7 5 - 1;2-CL2BENZENE-D4 0.4 (SS-8) C570 D5-NITROBENZENE 0.2 (SS-1) &I40—DS-NAPHTHALENE (IS-2) CS2.' 1=; 9-•FLUOROBIPHENYL 0.7 (SS-2: CI50 DIO-ACENAPHTHENE CS55 2.4.6TRIBROMOPHENOL (SS-6) -&im- DIO-PHENANTHRENE (IS-4) (IS-3) CS30 D14-P-TERPHENYL 0.5 (SS-3) DATA FROM FILE: BSl12994A SCANS 1120 TO 2232 ACQUIRED: 11/29/94 14:06:00 CALI: BS112994A #1 SAMPLE: SSTD050 290-02-SU25 CONDS.: RTX-5 0.25MMX30M l.OUM 45/4-325520 INST B 1200 _ 20:00 1400 23:20 1600 _ 26:40 1800 _ 30:00 : _L 100. o;^ ( 51072.) CI70 D12-CHRYSENE (IS-5) CI75 D12-PERYLENE (IS-6) r 2000 _ 33:20 CO o o o vo Quantitation Report File; BS112994A € ata; BS112994A.TI 1/29/94 14: 06: 00 Sample: SSTD050 290-02-SV25 Conds.: RTX-5 0. 25MM X SOM l.OUM 45/4-325(220 Formula; X X X Instrument: B Submitted by; Analyst: JAM INST B Weight: 1. 001 Acct. No. ; AMOUNT=AREA • REF AMNT/(REF AREA • RESP FACT) Resp. fac. from Library Entry m m No 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 (16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 |41 h2 A3 AA 45 46 47 Name CI 30 CI40 CI50 CI60 CI70 CI75 CS45 CS20 CS25 CS55 CS30 CS75 C315 C325 C330 C320 C310 C319 C345 C350 C355 C357 C370 C375 C410 C415 C420 C425 C430 C435 C440 C445 C450 C455 C460 C465 C470 C510 C515 C520 C525 C530 C535 C540 C54 5 C550 C321 D4-1.4 DICHLOROBENZENE DS-NAPHTHALENE D10-ACENAPHTHENE D10-PHENANTHRENE D12-CHRYSENE D12-PERYLENE D5-PHEN0L D5-NITR0BENZENE 2-FLUOROBIPHENYL 2.4.6TRIBROMOPHENOL 0. B 0. 2 O. 7 O. 0. 0. 0. 0. O. 0. O. O. O. O. 4 7 5 3 Cm A 1 D14-P-TERPHENYL 0.5 1. 2-CL2BENZENE-D4 0. 4 •PHENOL O. B BIS(2CHL0R0ETHYL)E 0.7 2CHL0R0PHEN0L O. B ANILINE N-NITROSODIMETHYLAMINE PYRIDINE BENZYL ALCOHOL 1.2DICHL0R0BENZENE 0. 2METHYLPHEN0L O. 2.2'0XYBIS(1CHL0R0PR 855 56 57 58 Name C570 C543 C5S0 C585 C590 C595 C615 C625 C630 C635 C650 C655 D200 C647 C715 C720 C725 C730 C740 C735 C760 C765 C770 C775 C780 C785 C790 CS70 CS50 C335 C340 C365 C595 C640 C645 m/z 165 165 149 204 166 138 169 248 2.4DINITR0T0LUENE 2.6DINITR0T0LUENE DIETHYL PHTHALATE 4CHLOROPHENYL PHEN FLUORENE 4-NITROANILINE •DIPHENYLAMINE 4BR0M0PHENYL PHENY CL6BENZENE •PENTACHLOROPHENOL DI-NBUTYLPHTHALATE •FLUORANTHENE 0. 2 0. 2 0. 4 0. 9 0. 1 0. 1 0. 05 0. 6 1.2-DIPHENYLHYDRAZINE CARBAZOLE PYRENE 0. 6 BUTYLBENZYLPHTHALATE 3.3'CL2BENZIDINE BENZO(A)ANTHRACENE 0. 8 BIS(2ETHYLHEXYL)PHTH CHRYSENE 0. 7 •DI-N-OCTYLPHTHALATE BENZO(B)FLUORANTHE BENZO(K)FLUORANTHE •BENZO(A)PYRENE INDEN0(1,2. 3CD)PYR DIBENZ0(A, H)ANTHRA BENZO(G. H, DPERYLE 2-CHL0R0PHEN0L-D4 2-FLUOROPHENOL 1,3DICHL0R0BENZENE •1.4DICHL0R0BENZENE 4METHYLPHEN0L 4-NITROANILINE PHENANTHRENE ANTHRACENE Scan Time Ref 813 13:33 3 1. 777 12:57 3 0. 831 13:51 3 1. 840 14:00 3 1. 844 14:04 3 1. 851 14; 11 3 1. 852 14; 12 4 0. 884 14:44 4 0. 0. 7 0. 7 0. 7 0. 5 0. 4 0. 5 0. 8 0. 6 0. 6 0. 5 0. 6 0. 7 0. 7 RRT 023 977 045 057 062 070 917 952 T T T (SS-7) (SS-5) T T Meth A BD A BB A BV A BB A BV A BB A BB A BB Area(Hght) 10653. 7473. 36320. 19472. 37353. 2953. 18803. 11064. Amount 25. 25. 25. 25. 25. 25. 25. 25. 000 000 000 000 000 000 000 000 _ PPB PPB PPB PPB PPB PPB PPB PPB •/.Tot 1. 19 19 19 19 19 19 19 19 300098 No 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 S3 84 85 No 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 75 76 77 m/z 284 266 149 202 77 167 202 149 252 228 149 228 149 252 252 252 276 278 276 132 112 146 146 108 138 178 178 ( 3can 900 917 975 1041- 855 950 1063- 1119 1196 1204- ; 1 192 1211 • ; 1303 ; 1423- ; Time Ref 15; 00 15; 17 16; 15 17; 21 14; 15 15; 50 17: 43 18; 39 19; 56 20: 04 19: 52 20; 11 21:43 23; 43 1430- 23; 50 1515- 25; 15 1942. ; 1950- ; 2069- ; 503 404- 516- 521' 557' 851' : 931- : 935 • : 32; 22 32; 30 34; 29 8; 23 6: 44 8: 36 8: 41 9; 17 14: 11 15; 31 15: 35 Ret(L) Ratio RRT(L) 13: 12; 13; 14; 14: 14; 14; 14: 15; 15; 16; 17; 14; 15; 17; 18; 19: 20; 19; 20; 21; 23; 23; 25; 32; 32; 34; 33 57 51 00 04 11 12 44 00 17 15 21 15 50 43 39 56 04 52 11 43 43 50 15 22 30 29 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 023 0. 977 1. 045 1. 057 1. 062 1. 070 0. 917 0. 952 0. 969 0. 987 1. 050 1. 121 0. 920 1. 023 0. 881 0. 927 0. 991 0. 998 0. 98S 1. 003 0. 851 0. 929 0. 933 0. 989 1. 263 1. 273 1. 351 4 4 4 4 4 4 5 5 5 5 5 5 6 6 6 6 6 6 6 3 4 4 RRT 0. 969 0. 987 1. 050 1. 121 0. 920 1. 023 0. 881 0. 927 0. 991 0. 998 O. 988 1. 003 0. 851 0. 929 0. 933 0. 989 1. 268 1. 273 1. 351 0. 967 0. 777 0. 992 1. 002 1. 071 1. 070 1. 002 1. 006 1 Ratio 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 . 00 00 00 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 M( A A A A A A A A A A A A A A A A 5th BB BB BB DB BB BB BB BB BB BV BB VB BB BV VB BB A^BB A A A A A A A A A A BB BB BB BV BV VB BB BB BV VB Amnt 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 2; 2! C t 2! 2: c < 2: 2: 2; c < 2'. 2! 2: 2; 2; 2 2 2 2 2 3. 00 3. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 5. 00 Area(Hght) 12313. 7195. 61832. 55245. 43523. 15293. 55762. 26958. 11843. 46619. 33752. 43740. 59613. 40859. 40800. 40205. 40611. 32940. 33937. 17468. 13404. 19579. 22565. 15891. 2953. 50504. 59788. \ Amnt(L) 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 Amount 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 25. 000 R. Fac R. F 0. 0. 1. 0. 1. 0. 0. 0. 0. 0. 1. 1. 0. 0. 1. 0. 0. 1. 0. 0. 1. 0. 0. 0 0 0 0 309 217 055 566 085 086 350 206 229 134 152 029 811 285 250 604 265 045 869' 981 331 . 912 . 911 . 898 , 907 , 735 . 758 PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB PPB ac (L) 0. 309 0. 217 1. 055 0. 566 1. 085 0. 086 0. 350 0. 206 0. 229 0. 134 1. 152 1. 029 0. 811 0. 285 1. 250 0. 604 0. 265 1. 045 0. 869 0. 981 1. 331 0. 912 0. 911 0. 898 0. 907 0. 735 0. 758 Rat: rot 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19 Lo 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 . 00 . 00 . 00 . 00 , 00 . 00 300099 No 78 79 80 81 82 83 84 85 Ret(L) 8: 23 6; 44 8: 36 8; 41 9: 17 14: 11 15: 31 15: 35 R. atio 00 00 00 00 00 00 00 00 RRT(L) 0. 967 0. 777 0. 992 1. 002 1. 071 1. 070 1. 002 i. 006 R, ati 00 00 00 00 00 00 00 00 Amnt 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 Amnt(L) 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 R. Fac R. 1. 043 0. 800 1. 169 1. 347 0. 949 0. 086 0. 941 1. 114 Fac(L) 1. 0. 1. 1. 0. 0. 0. 1. 043 800 169 347 949 086 941 114 Rat io . 00 00 00 00 00 00 00 00 300100 Calibration Check # : Instrument Identifier; B alibration Date: 08/20/94 Standard File; BS112994A Date; 11/29/94 Time; 15:37:00 MIN RF: SW(?<) = . 05 CLP = . 01 OR MAX 7.D; SW(^) = 307. CLP = 257. . Mean Compound RF(I) BELOW RF(0) 7. D « ii CS50 CS45 CS20 CS25 CS55 CS30 CS70 CS75 C315 C325 C330 C335 C340 C320 C310 C319 .C345 350 355 C357 C365 C370 C375 C410 C415 C420 C425 C430 C435 C440 C445 C450 C455 C460 C465 C470 C510 C515 C520 C525 C530 C535 540 545 C550 C321 C555 0. 0. O. 0. 2-FLUOROPHENOL D5-PHEN0L D5-NITR0BENZENE 2-FLUOROBIPHENYL 2.4.6TRIBR0MOPHENOL D14-P-TERPHENYL 0. 5 2-CHL0R0PHEN0L-D4 0. 8 1. 2-CL2BENZENE-D4 0. 4 •PHENOL 0. 8 BIS(2CHL0R0ETHYL)E 0.7 2CHL0R0PHEN0L O. 8 1.3DICHL0R0BENZENE O. 6 •1.4DICHL0R0BENZENE 0.5 ANILINE N-NITROSODIMETHYLAMINE PYRIDINE BENZYL ALCOHOL 1,2DICHL0R0BENZENE 0.4 2METHYLPHEN0L 0. 7 2.2'0XYBIS(1CHL0R0PR 4METHYLPHEN0L O. 8 DATA FROM FILE: SU11271WB1 SCANS 373 TO 1113 ACQUIRED: 11/29/94 20:46:00 CALI: SU11271WB1 #1 SAMPLE: SBLKW WATER-11271WB1 CONDS.: RTX-5 0.25MM X SOM l.OUM 45/4-325520 INST B 400 -I 6:40 r 500 . 8:20 •r 600 _/' 10:00 ( 700 J 11:40 800 Jt 13:20 900 J 15:00 1000 J 16:40 -^' i I ± CS50 2-FLUOROPHENOL 0.6 (SS-5) 100.0.^ 45632.) - ^^-^^ P ^ - ™° ^ CS70 ^^^^-cfeftHEN0L-D4 0.8 (SS-7) CI30 04-1,4 DICHLOROBENZENE (IS-1) CS75 1,2-CL2BENZENE-D4 0.4 (SS-8) CS20 D5-HITROBENZENE 0.2 (SS-1) CI40 DS-NAPHTHALENE (IS-2) CS25 2-FLUOROBIPHENYL CI50 DIO-ACENAPHTHENE (IS-3) CS55 2.4,6TRIBROMOPHENOL (SS-6) • CI60 DIO-PHENANTHRENE RRT(L) 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 777 0. 944 0. 901 0. 919 1. 091 O. 888 0. 967 0. 946 0. 969 1. 002 1. 075 0. 994 1. 077 1. 004 1. 023 0. 987 0. 881 0. 988 1. 033 1. 014 lef 2 2 3 3 4 5 5 1 3 RRT 0. 992 1. 082 1. 004 1. 025 0. 990 0. 882 0. 987 1. 035 1. 021 Ratio 0. 00 00 00 00 00 00 97 00 00 00 00 00 00 00 00 00 00 , 00 00 00 , 00 , 00 , 00 , 00 . 00 . 01 Meth A BB A BB A BB A BB A BV A BV A BB A BV A BB Amnt 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 55. 19 51. 83 38. 94 38. 31 63. 47 31. 66 59. 80 41. 00 56. 62 30. 29 30. 42 35. 23 69. 16 41. 36 38. 56 18. 85 43. 21 21. 47 33. 20 65. 08 Area(Hght) Amount 15595. 25035. 39562. 13257. 4329. 81509. 28153. 12543. 7465. Amnt(L) 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 35. 232 PPB 69. 164 PPB 41. 365 PPB 38. 558 PPB 18. 846 PPB 43. 2< 37 PPB 21. 474 PPB 33. 2< D2 PPB 65. 081 PPB R. Fac R. 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 1. 767 2. 234 0. 420 1. 623 0. 374 1. 077 2. 494 2. 211 2. 407 1. 632 0. 723 0. 419 0. 673 1. 424 0. 477 0. 101 2. 160 0. 746 0. 977 0. 269 Fac(L) 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. BOO 1. 078 0. 269 1. 059 0. 147 0. 851 1. 043 1. 348 1. 063 1. 347 0. 594 0. 298 0. 243 0. 861 0. 309 0. 134 1. 250 0. 869 0. 735 0. 103 7.1 3. 7. 4. 3. 1. 4. 2. 3. 6. Rat: 1. 1. 1. 1. 1. 1. 2. 2. 1. 1. 2. 1. 2. 1. 2. 1. 1. 1. 2. 1. 1. 0. 1. 0. 1. 2, rot 58 03 21 92 92 39 18 38 62 LO 00 00 00 00 00 00 21 07 56 53 54 27 39 64 26 21 22 41 77 65 54 75 73 86 33 60 300111 o ° I-* to DATA FROM FILE: SULINS05MSR SCANS 379 TO 1114 ACQUIRED: 11/29/94 22:14:00 CALI: SUUNS05MSR #1 SAMPLE: MS/110494 WATER HLA CONDS.: RTX-5 0.25MN X SOM l.OUM 45/4-325520 INST B 400 J 6:40 500 . 8:20 600 J 10:00 700 4 11:40 800 Zh- 13:20 i 7 900 - 15:00 1000 J 16:40 m i I CS50 2-FLUOROPHENOL O.b (bb-5) 100.0."; ( 75776.) 0G16 05-^^^Sh 0 CnLORiMN£-DV 0.8 (SS-7) -wee- 04-1..4 DICHLOROBENZENE (IS-1) CS75 1,2-CL2BENZENE-D4 0.4 (SS-8) CS20 D5-NITROBENZENE 0.2 (SS-1) CI40 DS-NAPHTHALENE (IS-2) CS25 2-FLUOROBIPHENYL 0.7 (SS-2) CISe DIQ-ACENAPHTHENE (IS-3) CS55 2.4,6TRIBROMOPHENOL (SS-6) CI60 DIO-PHENANTHRENE (IS-4) T ^ Q D14-P-TERPHENYL 0.5 (SS-3) / CO o o l-» M CO DATA FROM FILE: SUUNS05MSR SCANS 1114 TO 2232 ACQUIRED: 11/29/94 22:14:00 CALI: SUUNS05MSR #1 SAMPLE: MS/110494 WATER HLA CONDS.: RTX-5 0.25MM X SOM l.OUM 45/4-325520 INST B 1200 . 20:00 1400 J 23:20 1600 J 26:40 1800 . 30:00 2000 . 33:20 -"^0 - 0 E ± J_ 100.0;; ( 27168.) CI70 D12-CHRYSENE (IS-5) CI75 D12-PERYLENE (IS-6) Quantitation Report File: SVUNS05MSR Data: SVUNS05MSR. TI 1/29/94 22: 14: 00 ample: MS/110494 WATER HLA Conds.: RTX-5 0. 25MM X SOM l.OUM 45/4-325620 Formula: S S W Instrument: B Submitted by: Analyst; JAM INST B Weight: Acct. No. : 1. 000 11271 AMOUNT=AREA • REF AMNT/(REF AREA • RESP FACT) Resp. fac. from Library Entry No 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 i ^ ^ >17 IS 19 20 21 22 23 24 25 26 No 1 2 3 4 5 6 7 8 9 10 11 12 J^ |l4 ^15 16 17 Name CI30 CI40 CI50 CI60 CI70 CI75 CS50 CS45 CS20 CS25 CS55 CS30 CS70 C315 C330 C340 C370 C445 C465 C550 C570 C635 C715 C740 CS75 C560 m/z 152 136 164 188 240 264 112 99 82 172 330 244 132 94 128 146 70 D4-l,4 DICHLOROBENZENE D8-NAPHTHALENE DIO-ACENAPHTHENE D10-PHENANTHRENE D12-CHRYSENE D12-PERYLENE 2-FLUOROPHENOL D5-PHEN0L D5-NITR0BENZENE 2-FLUOROBIPHENYL 0. 6 0. 8 0. 2 0. 7 2,4,6TRIBROMOPHENOL D14-P-TERPHENYL 0. 5 2-CHL0R0PHENDL-D4 0. 8 •PHENOL " 2CHL0R0PHEN0L y 0, 8 0. 8 • 1,4DICHL0R0BENZENE'0. 5 8 C . 2. 2. 4. 4. 3. 4. 6. 3. 5. 3. 5. 2. 3. 300118 ot 16 16 16 16 16 16 74 71 85 15 69 55 38 97 39 66 18 1 • No 18 1^*^ '20 21 22 23 24 25 26 No 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 .16 ^ 7 IS 19 20 21 22 23 24 25 26 m/z £ 180 107 153 165 266 Jean Time R 629 10:29 685 11:25 798 13: 18 814 13:34 918 15: 18 202 1064 17:44 149 1191 19:51 152 109 Ret(L) 8: 40 10:35 13: 15 15:29 20: 07 25:32 6: 44 8: 11 9: 32 12: 11 14:27 17: 52 8:23 8: 12 8: 24 8:41 9: 19 10: 31 11: 24 13: 18 13:33 15: 17 17:43 19: 52 8: 57 13:26 532 8: 52 811 13:31 Ratic 0. 99 1. 00 1. 00 1. 00 1. 00 1. 00 0. 96 0. 99 0. 99 1. 00 1. 00 1. 00 0. 99 0. 99 0. 99 0. 99 0. 99 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 0. 99 1. 01 > RRT(L) 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 777 0. 944 0. 901 0. 919 1. 091 0. 888 0. 967 0. 946 0. 969 1. 002 1. 075 0. 994 1. 077 1. 004 1. 023 0. 987 0. 881 0. 988 1. 033 1. 014 :ef 2 2 3 3 4 5 5 1 3 RRT 0. 992 1. 080 1. 004 1. 024 0. 987 0. 882 0. 987 1. 035 1. 020 Ratio 0. 00 00 00 00 00 00 97 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 , 00 . 00 . 00 . 01 Meth A BV A BB A DB A BB A BB A BB A BB A BV A BB Amnt 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 43. 85 43. 57 35. 60 38. 38 61. 90 32. 88 49. 75 36. 72 49. 81 24. 57 29. 40 28. 85 64. 31 40. 72 39. 64 38. 50 42. 69 6. 62 30. 53 66. 66 Area(Hght) Amoun 13794. 25146. 40771. 14267. 8992. 84001. 9060. 12220. 8004. Amnt(L) 20. 00 20. 00 20. 00 20. 00 20. 00 20. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. OO 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 25. 00 t 28. 847 PPB 64. 307 PPB 40. 72 1 PPB 39. 639 PPB 38. 497 PPB 42. 687 PPB 6. 62 30. 52 :5 PPB :6 PPB 66. 658 PPB R. Fac R. 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 1. 403 1. 878 0. 384 / 1. 626 0. 365 1. 119 2. 075 1. 980 2. 117 1. 324 0. 699 0. 343 0. 626 1. 402 0. 491 0. 206 2. 134 0. 230 0. 898 0. 275 Fac(L) 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000 0. 800 1. 078 0. 269 1. 059 0. 147 0. 851 1. 043 1. 348 1. 063 1. 347 0. 594 0. 298 0. 243 0. 861 0. 309 0. 134 1. 250 0. 869 0. 735 0. 103 7.1 3. 6. 4. , 4. 4. 4. 0. 3. 7. Rat: 2. 0 1 2 rot 12 95 40 29 16 62 72 30 21 Lo 00 00 00 00 00 00 75 74 42 54 48 32 99 47 99 98 18 15 57 63 59 54 , 71 . 26 , 22 . 67 300119 CO o o l-> O E P I S O 0 E U X £ ^ T U X K J ^ l i k l ^ BATCH # PATH RECEIVED H js^?; M ^ ^ LIMS # l09,LoU) ETC/GULF SOUTH f ^ /f^^'^ Cy-^l^A-'J SAMPLE EXTRACTION/ANALYSIS LOG EXTRACTION DATE_|X:;:Ji:l:V:i_ PAGE 1 OF REVIEWED BY EXTRACTION TECHS: SDG/RG # OP PEST() TPH ( ) OTHER ( ) FRACTION: SV y " PEST/PCB ( ) PROTOCOL 3/90 ( ) SW846 (/pP ( ) MOD CAL ( ) OTHER ( ) EXTRACTION: CLLE (vTsonlc ( ) Shaker ( ) Sox()SepFon() NOTE r^ y GULF SOCHH ID XO'K^OVJSS- LLNJP-OI U L M P ' O S t-LOD'O ULDL-O\ tcCC -O 1 CLCfO-6l L L I O - P - O I ( i . N j S r O l a\)^-6S -tM>o'^—©-6^ LLfO«?>^0(<' L\^]W^1(^ MATRIX/ LEVEL V L v r . oJ/c pH - - ]/ % MOIST « V DWF • * \ ^ k 1 ANfT EXIP /qce) \ V 1 / -/5(5 II INITIAL EXTRN VOL mis l-p y ^ 6.fi ao I'O ^ . / . c Q.- II GPC INIT VOL ml V _^ - - ' . > ^ V GPC FINAL VOL ml - ^ y — — ' V — • - ^ = ^ V 1 VOL TAKEN FOR SV/P :\ Zy — — f— , \ . ^ , - ~ s L _ n\ AL/FL INIT VOL ml — ^ ^ — - — V - _aU_ IX AiyFL FINAL VOL ml \ \ -.y — ' si ) < FINAL PROCESS VOL ml 1-0 A S..0 •3-0 1-0 \ ^ 1 l-d I SPIKING SURR VOL ul lOO \ \ y VOLUMES MATRIX SPIKE VOL ul •— 1 1 / i 1 ( ANALYSIS 1 1 DILUTK5N RATIO ^ 0 > " / 1 ANAL DATE /i//(r nh j ' i ANAL INfT 0^ r i- 1 i QLF NF I 1 1 > . SURROGATE ID ^ " 7 7 " " 3 U-^'')'V»SS CONC SURROGATE SPIKER M z i VERIFIER REAGENT LOT #'S MATRIX SPIKE ID; A MATRIX SPIKE SPIKER CH2CI2 KLAZA] ACETONE HEXANE ALUMINA MATRIX SPIKE VERIRER, FLORISIL NOTES AND COMMENTS; X A L \ ^ ^ (V V ^ ^ f e V ^ ' S K ^ A p L ^ ( ^ (X:z>(=: U3(LL- d r - o r e f i c - y d ^ . Q S A ' L S -^<^(^A^hZZ BCTXM.W11 y CO o o H aWi ETC/Gm.F SOUTH SAMPLE EXTRACTION/ANALYSIS LOG f^c^ /N'/^ CQ^Ljj^^ • t c UTU EPISODE UN-? ,UC1^ /ytC^C^Ll wo BATCH # / / ^ " 7 / DATE RECEIVED ' ^5^ / •/, /9^ f? "^ / ^^^IMS # U I:i-3p4- SDG/RG # REVIEWED BY EXTRACTION TECHS: EXTRACTION DATE PAGE 1 OF \ zgL FRACTION: SV PES OP PEST( TPH () OTHER ( ) • ^ B ( ) PROTOCOL 3/90 ( ) SW846 (-f PP ( ) MOD CAL ( ) OTHER ( ) EXTRACTION: CLLE (-ySonte ( ) Shaker ( ) Sox ( ) Sep Fun ( ) NOTE GULF SOUTH ID n s i i u ^ & i (li^^l^OOSl MS--' I L U ^ S l|^•^l LO nrvSO ^ U f J S - o C o m%e^ U N J S - 0 > t € bcs- or ee U c v ; - to \ U C 7 ^ > 0 1 U n ^ T ^ - o ( U T U - A ^ S(P'.VJ3.CAV^O ^ ( ' - pH ^ ) % MOIST - > > . ; DWF 1 • V , / 1 AMT IcxiO ..X. / r y ^ ' \ C_5...>-> II INITIAL EXTRN VOL mis III GPC INIT VOL ml VI GPC FINAL VOL ml • VII VOL TAKEN FOR SV/P .. VIII AI7FL INIT VOL mt IX AiyPL FINAL VOL ml X FINAL PROCESS VOL ml i.O c — • W O SPIKING VOLUMES SURR VOL ul \eo _ 1 MATRIX SPIKE VOL ul g'JS N / • • V v ^ I'O'O • ANALYSIS DILUTION RATIO J^O i iJo M ANAL DATE n\)-^ 1 — •f: " / ; i i " / ? « ' ANAL INIT C ^ Fj • V ' ^ f r QLF NF / / I ) ( 1 1 —ni.M, 7^ 1 SURROGATE ID i ^ * ^ I- C f i -'S\fS'3 cONC SURROGATE SPIKER ^ " ^ VERIFIER y [ y j REAGENT LOT #"S CH2Clgo'X.3^l ACETONE MATRIX SPIKE ID: A y ) ' ~ } Z > S ' ^ ' h [ ^ ' \ Z l S 0 B ^ A ' 7 - ' ^ ' ~ \ . 'RfZ^fA.'Zi'^'^^ ^ MATRIX SPIKE VERIHER. HEXANE ALUMINA FLORISIL MATRIX SPIKE SPIKER h ^ I NOTES AND COMMENTS: KXTKK.Wtl ^ .jwM^ a w . . t n Ltiti.HiJtinj:ti'i-AL UASOHJ\-T .3.1 CC/MS IMSTRCTKCNT OPERATIONS LOGSHEET BEMl-VOLATILES pa^e I o£ ;' \m¥'^ O - O "O Analyst! CD 00 Project 1,1). • (client/case/sdg) : tn A Date: U. •hjlf Instrument: Standard Data Acqulaltlon Faranetera for Beni-Volatiles: GC Conditions Flow rate Head pressure paWaai Injector temp. Injector mode GC desciptors GC program • 3.5 ml/min HS Conditions 30 Psi Fused Silica Capillary. 30m X 0.?2ww. l.Oum film ?5.0 Scan range: 35-500 amu Scan rate : 1 s/scan EM voltage : _ 2 2 £ ^ _ _ Mod SplltJ.ess- samPleaSV. DFTPP^UM 45 MmlnV to 300 P 12/rnin (optiwizedl Non-standard'Conditiona t " Maihtananca/Problems t (IQ-*^.^ /*«vm<, A-^-JI.. 0^*^^.^ 4z/»yir4.sf- Fomastar Files » •- Original Data Filed wittn -• Standard identifications « Spike Amounts: Targets: 3 y»-»>- /•..-/ is: .3?^P-l^/• /XTV/tt/ DFTPP; J H'f-rx-y//ti Today's .Responee Factora: • l-i-f-'f, ^ . f f l Definition of Status/Comraents Column on Run Log (page 2 ) ! ^.........analysis passed all criteria - not ^applicable CO ...carry-over or contamination suspected DVlevel.'.'.dilution required/suggested level -tiara *•:•...':. ME. sample matrix effect (also indicate OC excursions, for example, IS2t, SS2t, etc.) RE.......i.re-extraction required RR. rerun required TD/level...too dilute/suggested fevel 11111111111 1 IM^^l^ o H ^ - ^ ^ ' T * " EHVl«0>mEMTAL LABORATORY QC/MS INSTRaUBNT OPERATIONS LOGSHEET Analyst '.(LjUM. Date ! i i / n / t y - SEMI-VOtATILES RRF of the day : /0'fj> l^.lf^l Perf. s t d . + 12 hrs. ; f l } page 2 of 2 Are runs within tine liaits? rtM NO (If no, circle outliers) 300122 page 1 of 2 _ ; - w , « - »/.j.A-.' iriT ji-BJlATIOHa LOGSHEET -— SEMI-VOLATILES O O Analyst: ^ m f " tUiateaaaea/Probleaa i . ^ ^ yexaastar rilss i fiy//d>1/.~S/it- Original Data Filed witht '••••- . •taadard Ideotlfleations t Spike Aaountai. . . . Targets; af^-y^.svi*-hri- IS: i'yj~i\-Jy£*lt;^> DFTPP; i<^y>s Reapoaaa Factors:_;:^ ^ - 8«{iaition of Btatua/ComHenta Column on Run Log (paga 3)i <• nS?^aoo?i?^bl«'' ' " "it"i» HE sample -atrix effect (also indicate QC CO...::::: :carry?Sier or contamination suspected REi. . • re^exIraCtion^re^Jr^d'' '"*' "'^' ^^'''' BVlevel.. .dilution required/suggested levSl S!!!.. Z . . rerSn re^irSd ^ TD/level...too dilute/suggested fevel mzm-: yyzA ty-' aavr BOOTH ENVIRONMENTAL LABORATORY sc/vs XMSTROMZKT OPERATIONS LOGSHEET — BEKI-VOLATILKB page 2 ot 2 Analyst •#f RRF of the day Date . 1 o CD TXHS f ' » f.w/- ^.vr iv.ci ' ii'.if ir.y li OP >- >• JJ^ / t 1 p "hhi FILE ID d f l l t l l ' l i i S J h p n t A S C i l t i i l f SJlHI-Cii^ ^ l a ^ l i d ejimne ~~~~~~-~.,_^ "~ • Perf. Std. CLIENT ID + 12 h r s . (dil) erTfr j/rotrp tSsioii-f rjToo-H- frrciTf- snc^rf ^~^^_^ ~"^--~.^^ : ^':- AMT INJ ;2^ - - , ^ 1 QLF 1 *^<^^V ( I f MOLT FACT I \ 1.8 AR - - — - - - \ no, • RT - - .- - - • - X circle outliers) BUR REC ^ ^ - - - y N, N STATUS/ COMMENTS y ] \ T^.A J \ \ \ \ TAPE ?yf? 300123 o o o o as aULi SOUTH ENVIfiOKHENTAL LABORATORY GC/MS INSTRDMENT OPERATIONS LOGSHEET SEMI-VOLATILES Analyst: 'T OzM^ry Date: 11 M izi_ Instrument: A. cn Project I.D.-(client/case/sdg):_ CD Standard Data Acquisition Parameters for Serai-Volatiles: GC Conditions Flow rate Head pressure Column Injector temp. Injector mode- GC desciptors GC program •3.5 ml/mifi 30 psi Fused Silica Capillary. 3Qni x 0.32mm. l.Oum film 2 50 Mod Splitless sample°SV. DFTPP^UM 45 (4minr to 300 P 12/min (optimized) MS Conditions Scan range: 35-500 amu Scan rate : 1 s/scan EM voltage: /i- '1 (J page 1 .; 2 J Non-standard Conditions : Maintenance/Problems : Formaster F i l e s . : BSllU-A.Aj^ Original Data Filed with!_tl£/£. standard I d e n t i f i c a t i o n s ( Spike Amounts: _ , Targets: .2?<;»-»'^-y/>i- ' lS:__Xrtz2±LkylllUiL. DFTPP: D'/'/-'f)-yyy/ Today's Response Factors! I.'ij-I'. °-77 7 Definition of Status/Cosments Column on Run I.og (paga 2)i ^.........analysis passed all criteria ME.- sample matrix effect (also indicate QC - not applicable excursions, for example, IS2t, SS2f', etc.) CO .carry-over or contamination suspected RE..........re-extraction required •?' DL/level. .'.dilution required/suggested level RR rerun required TD/level...too dilute/suggested I'evel IS m llli j.-S;-x-:-;-:-i:: m evur SOOTH ENVIRONMENTAL LABORATORY GC/MS INSTRUMENT OPERATIONS LOGSHEET Analyst • . Q . / H ^ Z y RRF of the day SEMI-VOLATILES page 2 of 2 D O ( 3 O O ".1 O a t e TIME ll'.fi. C n:oi ' ir.HZ JV.To ir-.ie' ir.rt H J I n : i i '• OP ;>«>- ^ • i r - . ?. Q k 1 f _^ •.mil) FILE ID 9/'ll/i^VP SriiiiitA r/Ufictio -Vuac^^B rv-Ucxne J V U f t f t n S V I d t C i u i ^ r i / ^A<^ 1 fVUfJJti'i- f i / l 4 M J t i ~~~ _ _ P e r f . S t d . -t- 12 h r s . CLIENT ID ( d i l ) e n f r syroiii' I ; K J ' I 6 C O L r.is-^ t/Litj- imcL. i',T.y S A . . . ' i - » i - O t , f . i r /£/iu.- itiOL !',ir f S u t ^ P T - i / l l a i i i fir-il IKUM n - s l n i ^ t f l i ~~~'——-.^__ ~~~--—-— ' ••. ir. AMT INJ 2 ^ yi u ''A U U V , . . . l ^ - . 1 1 - QC BATCH r^ - iicr> \ / t O l t t y -^-^^^ 1 M l • 1 QLF / ) rfo r " r." r.' / \ 1 1 ^ ^ . , { l i MULT FACT / / 2 S - -r -?/- 2 / ' 1 1 1 > I . S AR — - y Ly - y i^ ^-^ .. no. RT - - ^ ' ^ ^ y -_ ^ • ^ c i r c l e o u t l i e r s ) SUR REC - — 01.. (?'- e>L f t , • ^ ^ ^ ^ -- ^ STATUS/ COMMENTS ^ \^ y y y .y y ^ ^ y \ ^ TAPE (flTf 1 1 - •-- •J(^m 9 4 J Vj V ± ^ ^