HLA DATA QUALITY ASSURANCE REVIEW SUMMARY 
Semivolatile Organic Compound Analysis 
Case Number: 
Site: 
Contractor Lab: 
Validator: 
QC Reviewer: 
Sample Matrix: 
95020 
Project Number: 
Island Chemical Company 
Pace Incorporated, New Orleans 
Kirsten Meier 
/z^ytyyo^y-y^. 7^y7Zyy<y^ 
Validation Date: 
Review Date: 
Water 
29872 10.1 
11 April, 1995 
^ ~ / y - 9J~ 
Analytical Method: 
SW 846, Method 8270, Pyridine only 
Sample Designations: 
Client ID O^^b Sample ID) 
SO0012 
S00119 
SO0127 
BS0013 
Data for the above samples are: 
[ ] Acceptable for use 
[x] Acceptable for use as qualified 
[ ] Unacceptable for use 
Is action required by the Project Manager? 
Yes 
No[x] 
Comments: 
The investigative samples were validated in accordance with the "USEPA CLP National Functional 
Guidelines for Organic Data Review", February 1994. 
SDMS Document 
115543 
bm_elec.ll 
12291994 1530 
Form BNA l.l 
300689 
Cue Number: 9S020 
PrajeclNumber: 29872 10.1 
Site ID: Island CbcmicaLl Company 
DATA COMPLETENESS CHECKLIST 
[x] 
Included, no problems 
[*] 
Included, problems 
[O] 
Not included 
[NA] 
Not applicable 
Quality Control Sununary 
X 
Case Narrative 
X 
Surrogate Recovery Summary 
* 
MS/MSD Summary 
X 
Reagent Blank Summary 
X 
GC/MS Instrument Performance Summary 
Sample Data 
X 
Chain of Custody Forms 
X 
Holding Times 
* 
Organic Analysis Data Sheets 
X 
Quantitation Reports 
* 
Reconstructed Ion Chromatograms 
X 
Mass Spectra Printouts 
NA 
TIC Mass Spectra Library Searches 
Initial Calibration Data 
X 
Calibration Summary 
X 
Standards Quantitation Reports 
* 
Standards Reconstructed Ion Chromatograms 
Continuing Calibration Data 
* 
Calibration Summary 
X 
Standards Quantitation Reports 
* 
Standards Reconstructed Ion Chromatograms 
"* 
Internal Standards Summary 
Instrument Performance Data 
X 
DFTPP Mass Spectra 
X 
Reconstructed Ion Chromatogram 
X 
DFTPP Mass Listmgs 
bm_elec.ll 
12291994 1530 
2 
FofmBNAl.l 
3 0 0 6 9 0 
Cue Number: 95020 
ProjectNumber: 29872 10.1 
Site ID: bland Chemical Compazy 
Reagent Blank Data 
_x_ 
_x_ 
* 
NA 
Organic Analysis Data Sheets 
Quantitation Reports 
Reconstructed Ion Chromatograms 
Mass Spectra Printouts 
TIC Mass Spectra Library Searches 
Matrix Spike and Matrix Spike Duplicate Data 
* 
Organic Analysis Data Sheets 
X 
Quantitation Reports 
* 
Reconstructed Ion Chromatograms 
Laboratory Control Sample 
NA 
Organic Analysis Data Sheets 
NA 
Quantitation Reports 
NA 
Reconstructed Ion Chromatograms 
NA 
Mass Spectra Printouts 
NA 
TIC Mass Spectra library Searches 
Comments: 
For the instrument B the Reconstructed Ion Chromatograms showed peak areas from the scan 350 and 
higher, while the compound of interest. Pyridine, appears at aproximately scan 210. A visual 
comparison of data for Pyridine was not possible. 
bra_elec.ll 
12291994 1530 
Fomi BNA 1.1 
300691 
Caae Number: 95O20 
ProjectNumber: 29872 10.1 
Site ID: Isbtiid Cbemical Company 
SPECIHC COMMENTS REGARDING ANALYSES 
Ciiain Of Custody 
Were samples properly preserved and received in good condition? 
Yes[x] 
No 
Were custody transfers correctly and completely documented? 
Yes[x] 
No 
Comments: 
None 
Holding Times 
Were sample extractions performed within holding times? 
Yes[x] 
No 
Were sample analyses performed within holding times? 
Yes[x] 
No 
Comments: 
None 
Instrument Tuning 
Did the instrument performance checks meet acceptance criteria? 
Yes[x] 
No 
Were samples analyzed within the 12-hour period following an acceptable performance check? 
Yes[x] 
No 
Conunents: 
None 
boa_elec.il 
12291994 1530 
4 
- 
Foim BNA 1.1 
300692 
Case Number: 95020 
ProjectNumber: 29872 10.1 
Site ID: Island Cbemical Company 
Initial Calibration 
Did the laboratory meet the method requirements regarding the minimum number of calibration standards for an 
acceptable initial calibration? 
Yes[x] 
No 
Did the initial calibration curves meet the linearity criteria for maximum percent relative standard deviation 
(%RSD)? 
Yes[x] 
No 
Did the initial calibration meet the minimum relative response factor (RRF) criteria? 
Yes[x] 
No 
Comments: 
This review is only based on the evaluation of Pyridine. The initial calibration QC criteria were met for 
Pyridine. 
As stated previously, the chromatograms for instrument B do not show the scans for Pyridine and 
N-Nitrosodimethylamine, a visual evaluation was not possible. The possibility that the injection peak or 
other factors might have interfered or affected the quantitation of the target analyte Pyridine, cannot be 
evaluated. 
The concentrations of the initial and continuing standards are listed in the header as twice as high as the 
concentrations used in the quantitation section of the data. The injection volume is not clearly defined, 
but appears, that the same amount of 1.0 ul was used for standards and samples. Since no detections 
of Pyridine were reported, no qualification of data is necessary. 
Continuing Calibration 
Did the continuing calibration curves meet the linearity criteria for maximum percent difference (%D)? 
Yes 
No[x] 
Did the continuing calibration meet the minimum RRF criteria? 
Yes[x] 
No 
Comments: 
This review is only based on the evaluation of Pyridine. 
The continuing calibration on 2-17r95, 14:06, shows a percent difference for Pyridine of 39.2%, 
exceedmg the limit of 25%. Therefore, the result for Pyridine in the associated sample BSOOO was 
qualified as estimated (J). 
As stated previously, the chromatograms for instrument B do not show the scans for Pyridine and 
N-Nitrosodimethylamine, a visual evaluation was not possible. The possibility that the injection peak or 
other factors might have interfered or affected the quantitation of the target analyte Pyridine, cannot be 
evaluated. 
300693 
bna_elec.ll 
12291994 1530 
5 
Form BNA 1.1 
Case Number: 95020 
ProjectNumber: 29872 10.1 
Site ID: Island Cbemical Cotnpany 
Surrogate Recoveries 
Were the surrogate spike recoveries within acceptance limits? 
Yes[x] 
No 
If the spike recoveries were unacceptable, were the samples reanalyzed? 
Yes 
No 
NA[x] 
Comments: 
None 
Matrix Spikes 
Were matrix spike analyses performed at the correct frequency and on a sample matrix representative of the 
samples in the sample delivery group (SDG)? 
Yes[x] 
No 
Were the matrix spike recoveries and relative percent differences (RPDs) within acceptance criteria? 
Yes[x] 
No 
Comments: 
The matrix spikes were performed with a 8270 mixture, which does not include Pyridine. The lab 
provided a summary of matrix spike recoveries, some recoveries were not within 8270 QC limits. 
No qualification of data. 
Internal Standards 
Were the internal standard areas and retention times within the required limits? 
Yes[x] 
No 
If the internal standard requirements were not met, were the samples reanalyzed? 
Yesx[x] 
No 
NA 
Comments: 
No internal standard area and retention time summaries were provided. The associated peak responses 
were compared and the QC criteria were met. No qualification of data. 
300694 
biii_clcc.ll 
12291994 1530 
6 
Form BNA 1.1 
Cue Number: 95020 
Pn>jectNumber: 29872 10.1 
Site ID: Island Cbemical Company 
Blank Analyses 
Were the appropriate number of blank analyses performed? 
Yes[x] 
No 
Were analytes detected in the blanks? 
Yes 
No[x] 
If analytes were detected in the blanks, were the same analytes detected in the associated investigative samples? 
Yes 
No 
NA[x] 
Did the sample results require qualification due to the presence of analytes in the associated blank samples? 
Yes 
No[x] 
Comments: 
This review is only based on the evaluation of Pyridine. The target analyte was not detected in the 
associated prep blanks and qualification of data was not necessary. 
Laboratory Control Samples 
Were laboratory control sample (LCS) analyses performed at the correct frequency? 
Yes 
No 
NA[x] 
Were the LCS recoveries within acceptable limits? 
Yes 
No 
NA[x] 
Comments: 
Not applicable. 
300695 
bai_elcc.ll 
12291994 1530 
7 
Form BNA 1.1 
CaK Number: 95020 
ProjectNumber: 29872 10.1 
Site ID: Isiand Cbemical Company 
Sample Results 
Were target analytes reported in the investigative samples? 
Yes 
No[x] 
Were mass spectra provided for the target analytes detected in the investigative samples? 
Yes 
No 
NA[x] 
Were the mass spectra of acceptable quality and analytes correctly identified? 
Yes 
No 
NA[x] 
Were the quantitated results for target analytes calculated using the appropriate internal standards and were the 
relative retention times (RRTs) acceptable? 
Yes[x] 
No 
Comments: 
As stated previously, the chromatograms for instrument B do not show the scans for Pyridine and 
N-Nitrosodimethylamine, a visual evaluation was not possible. The possibility that the injection peak 
or other factors might have interfered with or affected the quantitation of the target analyte. Pyridine, 
cannot be evaluated. Therefore, the reported results for Pyridine in the investigative samples S00012, 
S00119 and SOO 127 were qualified as estimated (J). 
Tentatively Identifled Compounds 
Were tentatively identified compound (TIC) searches conducted for all sample analyses? 
Yes 
No 
NA[x] 
Were non-target peaks evaluated as required? 
Yes 
No 
Were the TIC mass spectra, searches, identifications, and quantitated results acceptable? 
Yes 
No 
Comments: 
Not applicable. 
bMelecll 
12291994 1530 
8 
Form BNA l.l 
300696 
Case Number: 95020 
ProjectNumber: 29872 10.1 
Site ID: Isbtnd Cbemical Company 
Log Books 
Were sample preparations properly documented and performed in accordance with method protocols? 
Yes[x] 
No 
NA 
Were sample analyses properly documented and performed in accordance with method protocols? 
Yes[x] 
No 
Comments: 
None 
bni_elec.ll 
12291994 1530 
Form BNA 1.1 
300697 
Case Number: 95020 
ProjeaNumber: 29872 10.1 
Site ID: Isbnd ChemicU Cocnpany 
Calculation Checks 
Instrument Tunmg 
m/z of 127, 2-2-95, 9:19, Instrument H 
Relative Abundance: 
Calculation not possible, only relative abimdance was provided 
Initial Calibration 
Std 50, 11/9/94, D5-Phenol 
RRF: 
16823 * 20 = 1.330 
10117x25 
%RSD: 
0.071 *100% = 5.422 
1.309 
Continuing Calibration Std 50, 2-8-95, 11:24, Pyridine 
RRF: 
9392 X 20 = 0.7734 
9715 X 25 
%D: 
0.918 - 0.775 X 100 = 15.58 
0.918 
Surrogate Recovery SO0127, 2-Fluorophenol 
20771 X 20 
= 63.2071 
6911 X 0.951 
63.21 X 100 = 84.28 % recovery 
75 
bna_elec.ll 
12291994 1530 
1 0 
Form BNA 1.1 
300698 
Case Number: 95020 
ProjectNumber: 29872 10.1 
Site ID: Isbmd Chemical Company 
Matrix Spike Recovery 
Detected concentrations not known 
RPD: Batch 12098, Phenol 
2 I 8 - 14 I = -54.54 
I 8 -t- 1 4 I 
Sample Results 
CRQL: Water sample 
Detected Result: No detection 
TIC Result 
Not required 
bai_eleo.ll 
12291994 1530 
H 
Form BNA 1.1 
300699 
Case Number: 95020 
ProjectNumber: 29872 10.1 
Site ID: Island Chemical Cocnpany 
HOLDING TIME QUAUFICATION SUMMARY FORM 
o 
o 
-J 
o 
o 
Sample 
Identification 
Date 
Sampled 
Date 
Prepared 
Date 
Analyzed 
Prep. 
Holding 
Time 
Analysis 
Holding 
Time 
Qualifier 
Comments: None 
lma_elco. 11 
12291994 1530 
12 
Foim BNA l.l 
Case Number: 95020 
ProjectNumber: 29872 10.1 
Site ID: Island Chemical Company 
INITIAL CALIBRATION QUALIFICATION SUMMARY FORM 
Date/Time 
Instrument 
Analyte 
RF 
RSD 
Samples Affected 
Qualifier 
Comments: 
None 
w 
o o 
• J 
o 
i I229I9')4 1530 
13 
FomiBNA l.l 
Case Number: 95020 
ProjectNumber: 29872 10.1 
Site ID: Island Chemical Company 
CONTINUING CALIBRATION QUALIHCATION SUMMARY FORM 
Date/Time 
1 2-17-95, 14:29 
1 ^ 
Instrument 
H 
Analyte 
Pyridine 
RF 
%D 
39.2 
Samples Affected 
BS0013 
Qualifier 
J/UJ 
Comments: 
None 
o 
o 
to 
b™_eIco.ll 
12291994 1530 
14 
Fomi BNA 1.1 
Case Number: 95020 
ProjectNumber: 29872 10.1 
Site ID: bUnd Chemical Cotnpany 
BLANK SUMMARY FORM 
Blank ID 
Analyte 
Blank Result (units) 
Action Level 
• 
Associated Samples 
w 
o o 
•-J 
o 
OJ 
1 
Comments: 
None 
1 
btia elec.ll 
12291994 1.530 
15 
Poem BNA l.l 
Case Number: 95020 
ProjectNumber: 29872 10.1 
Site ID; bbnd Cbemicad Company 
Siunmary and Conclusions 
The analytical results for Pyridine are acceptable for use as qualified. 
The reported results for Pyridme m the investigative samples SO0012, SOO 119 and SOO 127 were 
qualified as estimated (J) since a visual comparison of the peak acquisition was not possible. 
The results for Pyridine in the investigative sample BSO013 was qualified as estimated (J) due to 
exceeding continuing calibration criteria. 
Validator's Signature: 
Validator's Initials: 
QC Reviewer's Signature: 
QC Reviewer's Initials: 
<JLyie^/^ FOA'-C/ 
UK 
<h^^..cyUjy -^, TzyCUT^ 
tlFP 
t 
Validation Date: 
// / i p y j l 
9 - S 
Review Date: 
V- /^ - f J " 
300704 
baa_elec.il 
12291994 1530 
1 6 
Form BNA "l.l 
ENVIRONMENTAL LABORATORIES 
REPORT OF LABORATORY ANALYSIS 
Analytical Results - Semivolatile Organics by Method 8270 
Harding Lawson Associates 
Client ID: S00012 
Description: NA 
Sample ID: VSR-001 
Matrix: Water 
Wet/Dry Basis: NA 
Collected: 01/24/95 
Received: 01/25/95 
Prepared: 01/30/95 
Analyzed: 
Percent Moisture: NA 
CAS No. 
110-86-1 
P a r a m e t e r 
Pyridine 
Concentration, ug/l (ppb) ' 
Detection 
Sample 
Blank 
Limit 
ND 
ND 
10.0 U3 
ND-Not Detected at or above the detection limit stated. 
VALIDATED 
Reviewed By 
/ • ^ ' ^ • ^ 
' ^ ^ - ^ 
Date 
^ ~ l ( - 
f ^ 
201 
161 James Drive West, Suite 100 
St. Rose. LA 70087 
TEL: 504-469-0333 
FAX: 504-469-0555 
An Equal Opportunity Employer 
300705 
ENVIRONMENTAL LABORATORIES 
REPORT OF LABORATORY ANALYSIS 
Analytical Results - Semivolatile Organics by Method 8270 
Harding Lawson Associates 
Client ID: S00119 
Description: NA 
Sample ID: UQB-001 
Matrix: Water 
Wet/Dry Basis: NA 
Collected: 01/19/95 
Received: 01/23/95 
Prepared: 01/24/95 
Analyzed: 02/08/95 
Percent Moisture: NA 
CAS No. 
110-86-1 
P a r a m e t e r 
Pyridine 
Concentration, ug/l (ppb) 
Sample 
ND 
Blank 
ND 
Detection 
Limit 
10.0 
0 3 
ND-Not Detected at or above the detection limit stated. 
VALIDATED 
Reviewed By 
/<^^u-^ 'f€^v-i_ /-
^~ P ~ f J " 
Date 
300706 
202 
161 James Drive West. Suite 100 
St. Rose. LA 70087 
TEL: 504-46 W033 
FAX: 504-469-0555 
An Equal Opportunity Employer 
ENVIRONMENTAL LABORATORIES 
REPORT OF LABORATORY ANALYSIS 
Analytical Results - Semivolatile Organics by Method 8270 
Harding Lawson Associates 
Client ID: S00127 
Description: NA 
Sample ID: VTF-001 
Matrix: Water 
Wet/Dry Basis: NA 
Collected: 01/27/95 
Received: 01/30/95 
Prepared: 02/02/95 
Analyzed: 02/08/95 
Percent Moisture: NA 
CAS No. 
110-86-1 
P a 
r a m e t e r 
Pyridine 
Concentration, ug/l (ppb) 
Sample 
ND 
Blank 
ND 
Detection 
Limit 
10.0 U 2 
ND-Not Detected at or above the detection limit stated. 
Reviewed By 
Date 
VALIDATED 
uyicy. 
yyt.. 
( i - i y 
f ^ 
203 
161 James Drive West, Suite 100 
St. Rose. LA 70087 
TEL: 504-469-0333 
FAX; 504-469-0555 
An Equal Opportunity Employer 
300707 
ENVIRONMENTAL LABORATORIES 
REPORT OF LABORATORY ANALYSIS 
Analytical Results - Semivolatile Organics by Method 8270 
Harding Lawson Associates 
Client ID: BS0013 
Description: NA 
Sample ID: WG-001 
Matrix: Water 
Wet/Dry Basis: NA 
Collected: 01/31/95 
Received: 02/03/95 
Prepared: 02/06/95 
Analyzed: 02/17/95 
Percent Moisture: NA 
CAS No. 
110-86-1 
P a r a m e t e r 
Pyridine 
Concentration, ug/l (ppb) 
Sample 
ND 
Blank 
ND 
Detection 
Limit 
10.0 U3 
ND-Not Detected at or above the detection limit stated. 
VALIDATED 
Reviewed By _
/
^
^
i
^ 
n^<-^ 
Date 
V - / ^ - f o 
204 
161 James Drive West, Suite 100 
SI. Rose. LA 70087 
TEL: 504469O333 
FAX: 504-469-0555 
An Equal-OQOPrtiinittEQmloy.er__ 
300708 
U.S. EPA - CLP 
EPA SAMPLE NO. 
« 
E12022 
INORGANIC ANALYSIS DATA SHEET 
b Name: PACE 
Contract: 
j 
| 
b Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095010 
Matrix (soil/water): SOIL 
Lab Sample ID: VQB002 
Level (low/med): 
LOW 
Date Received: 01/23/95 
% Solids: 
85.7 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
1 
l
l
l
i 
|CAS No. 
1 Analyte jConcentrationjCj Q 
|M j 
1 
1 
1 
Mil 
17429-90-5 {Aluminum | 
12700 | j* 
jP | 
17440-36-0 jAntimony | 
0.88 jBj 
jF j 
17440-38-2 lArsenic j 
0.29 L3T U 
IF 1 
17440-39-3 IBarium 
j 
99.5 | 1 
IP 1 
17440-41-7 IBerylliuml 
0.34 | | 
|F | 
17440-43-9 1 Cadmium | 
1.7 | |* 
IP 1 
17440-70-2 1 Calcium I 
4970 j I* 
jP 1 
17440-47-3 1 Chromium | 
12.9 | j* 
jP | 
17440-48-4 1 Cobalt 
j 
13.6 | | 
|P | 
17440-50-8 1 Copper 
| 
51.7 | | 
|P | 
17439-89-6 [Iron 
| 
24800 j j* 
|P | 
17439-92-1 ILead 
j 
3.4 | j 
|F j 
17439-95-4 jMaqnesiuml 
5360 j j* 
jP j 
17439-96-5 jManqanesel 
858 | | 
|P | 
17439-97-6 jMercury 1 
0.14 | j 
|CV| 
17440-02-0 INickel 
1 
16.0 | j 
jP | 
17440-09-7 jPotassiuml 
936 |B| 
jP | 
17782-49-2 |Selenium 1 
3.3 L»1"N K 
IF | 
17440-22-4 ISilver 
1 
1.2 |U| 
|P | 
17440-23-5 1 Sodium 
| 
908 |B1 
IP j 
17440-28-0 IThallium j 
0.63 jUJ^ 
IF j 
17440-62-2 [Vanadium | 
108 | |* 
IP 1 
17440-66-6 jZinc 
| 
45.4 | j 
jP | 
157-12-5 
1 Cyanide j 
1.2 |U| X 
|AS| 
1 
1 
1 
l
l
l
l 
olor Before: BROWN 
Dior After: YELLOW 
omments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Reviewed By 
Date 
Text:ure: 
MEDIUM 
A r t i f a c t s : YES 
«ed By Q ^ f f ^ 7 ^ 1 / ^ / ? ^ ^ 
FORM I - IN 
300709 
ILMp2.0 
116 
U.S. EPA - CLP 
EPA SAMPLE NO. 
r 
RBSOOl 
INORGANIC ANALYSIS DATA SHEET 
b Name: PACE 
Contract: 
1 
^j 
Lab Code: GULF 
Case No.: HLA 
' SAS No.: 
SDG No.: 095010 
Matrix (soil/water): WATER 
Lab Sample ID: VTX004 
Level (low/med): 
LOW 
Date Received: 02/01/95 
% Solids: 
0.0 
Concentration Units (ug/L or mg/kg dry weight): UG/L 
1 
1 
1 
l
l
l
l 
|CAS No. 
1 Analyte 1 Concentration 1C| Q 
jM | 
1 
1 
1 
l
l
l
l 
17429-90-5 1 Aluminum j 
26.4 IBl 
|P 1 
17440-36-0 jAntimony 1 
1.4 JUIN 
|F | 
17440-38-2 lArsenic 
1 
1.1 IU|W rT IF 1 
17440-39-3 IBarium 
| 
8.8 |U| 
|P 1 
17440-41-7 IBerylliuml 
0.10 1U|N* TT IF 1 
17440-43-9 jCadmium 
1 
3.1 lUl 
|P | 
17440-70-2 ICalcium 
| 
88.5 IBl 
jP | 
17440-47-3 1 Chromium | 
4.1 |U| 
|P j 
17440-48-4 1 Cobalt 
1 
9.5 |UL 
IP I 
17440-50-8 1 Copper 
1 
16.7 |U| 
|P | 
17439-89-6 |Iron 
| 
32.1 |U| 
|P | 
17439-92-1 ILead 
| 
0.50 |U| 
|F | 
17439-95-4 |Magnesium| 
26.0 |U| 
|P | 
17439-96-5 |Manqanese| 
2.6 |U| 
|P | 
17439-97-6 |Mercury 
| 
0.20 |U| 
|CV| 
17440-02-0 INickel 
1 
13.1 lUl 
|P 1 
17440-09-7 1 Potassium! 
526 |UI 
|P j 
17782-49-2 |Selenium | 
1.4 lUjW 3" |F 1 
17440-22-4 ISilver 
| 
5.1 |U| 
|P | 
17440-23-5 jsodium, 
\ 
339 |U| 
|P | 
17440-28-0 IThallium | 
2.7 |U|W 3" 
[F | 
17440-62-2 IVanadium | 
4.5 |U| 
[P | 
17440-66-6 IZinc 
| 
12.1 |B| 
|P | 
157-12-5 
1 Cyanide 
| 
10.0 |Ul 
LAS j 
1 
1 
1 
l
l
l
l 
Color Before: COLORLESS 
Color After: COLORLESS 
Comments: 
Clarity Before: CLEAR 
Clarity After: CLEAR 
VALID 
Reviewed By 
Date 
Texture: 
» 
Artifacts: NO 
y^A/t^^ 
FORM I - 
IN 
300710 
ILM02.0 
1017 
U.S. EPA - CLP 
EPA SAMPLE NO. 
r 
« 
S00118 
INORGANIC ANALYSIS DATA SHEET 
b Name: PACE 
Contract: 
| 
| 
b Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095010 
Matrix (soil/water): WATER 
Lab Sample ID: VQCOOl 
Level (low/med): 
LOW 
Date Received: 01/23/95 
% Solids: 
0.0 
Concentration Units (ug/L or mg/kg dry weight): UG/L 
1 
1 
1 
l
l
l
l 
ICAS No. 
1 Analyte |ConcentrationlC| Q 
|M | 
1 
II 
llll 
17429-90-5 1 Aluminum | 
22.9 |B| 
|P 1 
17440-36-0 lAntimony | 
1.4 |U|N 
|F | 
17440-38-2 lArsenic I 
1.1 |U| 
|F 1 
17440-39-3 IBarium 
| 
8.8 |U| 
|P | 
17440-41-7 IBerylliuml 
0.10 1U|N* 3" |F | 
17440-43-9 1 Cadmium 1 
3.1 |U| 
|P | 
17440-70-2 ICalcium 1 
42.0,IBl 
|P | 
17440-47-3 1 Chromium | 
4.1 |U| 
|P j 
17440-48-4 iCobalt 
j 
9.5 |U1 
LP 1 
17440-50-8 jCopper 
I 
16.7 |U| 
|P I 
17439-89-6 |Iron 
| 
32.1 |U| 
[P | 
17439-92-1 ILead 
1 
0.50 |U| 
|F 1 
17439-95-4 |Magnesium| 
26.0 |U| 
|P | 
17439-96-5 IManganesej 
2.6 1U| 
|P | 
17439-97-6 |Mercury | 
0.20 |U| 
|CV| 
17440-02-0 INickel 
1 
13.1 |U| 
|P I 
17440-09-7 IPotassiumI 
526 |U| 
|P | 
17782-49-2 |Selenium | 
1.4 |U|W X 
IF | 
17440-22-4 ISilver 
1 
5.1 |U| 
|P I 
17440-23-5 ISodium 
1 
339 | UJ- 
|P | 
17440-28-0 IThallium 1 
2.7 lUlW T 
IF | 
17440-62-2 [Vanadium | 
4.5 jUJ 
|P | 
17440-66-6 IZinc 
| 
13.3 |B| 
|P | 
157-12-5 
ICyanide | 
10.0 |U| X 
|AS| 
1 
i 
1 
l
l
l
l 
Color Before: COLORLESS 
Color After: COLORLESS 
Comments: 
Clarity Before: CLEAR 
Clarity After: CLEAR 
Reviewed By 
Date 
Texture: 
Artifacts: NO 
VAW DATED 
% kffyx^. 
^n]'^^ 
FORM I - 
IN 
300711 
ILM02.0 
0018 
U.S. EPA - CLP 
EPA SAMPLE NO. 
€ 
b Name: PACE 
b code: GULF 
Matrix (soil/water): WATER 
Level (low/med): 
LOW 
% Solids: 
0.0 
INORGANIC ANALYSIS DATA SHEET 
Contract: 
Case No.: HLA 
SAS No.: 
I S00119 
SDG No.: 095010 
Lab Sample ID: VQBOOl 
Date Received: 01/23/95 
Concentration Units (ug/L or mg/kg dry weight): UG/L 
1 
1 
ICAS No. 1 
1 
1 
17429-90-5 1 
17440-36-0 1 
17440-38-2 1 
17440-39-3 
17440-41-7 
17440-43-9 
17440-70-2 
17440-47-3 
17440-48-4 
17440-50-8 
17439-89-6 
17439-92-1 
17439-95-4 
17439-96-5 
17439-97-6 
17440-02-0 
17440-09-7 
17782-49-2 
17440-22-4 
17440-23-5 
17440-28-0 
17440-62-2 
17440-66-6 
157-12-5 
1 
Analyte 
Aluminum ! 
Antimony 
Arsenic | 
Barium 
Beryllium 
Cadmium 
Calcium 
Chromium 
Cobalt 
Copper 
Iron 
Lead 
Magnesium 
Manganese 
Mercury 
Nickel 
Potassium 
Selenium 
Silver 
Sodium 
Thallium 
Vanadium 
1 Zinc 
Cyanide 
Concentration | 
22.5 1 
1.4 ! 
1.1 1 
8.8 
0.10 1 
3.1 
132 
4.1 
9.5 
16.7 
95.9 
0.64 
26.0 
4.4 
0.20 
13.1 
526 
1.4 
5.1 
339 
2.7 
1 
4.5 
1 
19.1 
1 
10.0 
1 
C| 
1 
1 
Q 1 
1 
Bl 
U|N 
j 
Uj 
U| 
U|N-' T T 
Ul 
Bj 
Ul 
Ul 
Ul 
Bl 
^sr u 
Ul 
Bl 
Ul 
Ul 
Ul 
Ul 
Ul 
Ul 
U|W J^ 
U| 
IBl 
|U| J-
1 1 
M 1 
P 1 
F 1 
F 1 
P 1 
F 1 
P 1 
P 1 
P 1 
P 1 
P 1 
P 1 
F 1 
P 1 
P 1 
CV| 
P 1 
P 1 
F 1 
P I 
P 1 
|F 1 
|P 1 
|P 1 
|AS| 
Color Before: COLORLESS 
Color After: COLORLESS 
Comments: 
Clarity Before: CLEAR 
Clarity After: CLEAR 
Texture: 
t 
Artifacts: NO 
Reviewed By 
Date — ^MP'-^ 
FORM I - IN 
300712 
ILM02.0 
0S0019 
U.S. EPA - CLP 
EPA SAMPLE NO. 
€ 
SO0120 
INORGANIC ANALYSIS DATA SHEET 
b Name: PACE 
Contract: 
I 
_| 
b Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095010 
Matrix (soil/water): WATER 
Lab Sample ID: VQAOOl 
Level (low/med): 
LOW 
Date Received: 01/23/95 
% solids: 
0.0 
Concentration Units (ug/L or mg/kg dry weight): UG/L 
1 
1 
1 
l
l
l
l 
|CAS No. 
1 Analyte 1 Concentration!Cl Q 
IM | 
1 
I I 
llll 
17429-90-5 1 Aluminum | 
26.7 |B| 
|P 1 
17440-36-0 (Antimony 1 
1.4 |U|N 
|F | 
17440-38-2 lArsenic | 
1.1 |U| 
|F | 
17440-39-3 IBarium 
| 
8.8 |U| 
|P | 
17440-41-7 IBerylliuml 
1.7 1 IN* U T IF 1 
17440-43-9 1 Cadmium | 
3.1 |U| 
|P | 
17440-70-2 ICalcium 1 
55.8 |B| 
|P 1 
17440-47-3 1 Chromium | 
5.6 LB-T U 
IP 1 
17440-48-4 ICobalt 
| 
9.5 |U| 
|P I 
17440-50-8 ICopper 
| 
16.7 1U| 
|P | 
17439-89-6 jlron 
j 
46.3 jB| 
jP j 
17439-92-1 ILead 
j 
0.50 jU| 
|F 1 
17439-95-4 jMaqnesiumj 
32.0 j^T 
\J 
IP 1 
17439-96-5 |Manganese| 
2.6 |U| 
|P I 
17439-97-6 |Mercury | 
0.20 |UI 
|CV| 
17440-02-0 INickel 
1 
13.1 |U1 
|P I 
17440-09-7 jPotassiuml 
526 |U| 
jP I 
17782-49-2 |Selenium | 
1.4 |U| 
|F | 
17440-22-4 ISilver 
| 
5.1 lUI 
IP 1 
17440-23-5 ISodium 
1 
339 |U| 
|P | 
17440-28-0 IThallium 1 
2.7 lUIW T 
IF | 
17440-62-2 IVanadium j 
4.5 jUj 
|P j 
17440-66-6 jZinc 
j 
17.1 |Bj 
jP | 
157-12-5 
jCyanide | 
10.0 jU| 
jASj 
1 
1 
1 
l
l
l
l 
Color Before: COLORLESS 
Color After: COLORLESS 
Comments: 
• 
Clarity Before: CLEAR 
Clarity After: CLEAR 
Texture: 
Artifacts: NO 
Reviewed 
Date 
FORM I - 
IN 
300713 
ILM02.0 
0S0020 
U.S. EPA - CLP 
EPA SAMPLE NO. 
W 
SO0125 
INORGANIC T^ALYSIS DATA SHEET 
b Name: PACE 
Contract: 
| 
| 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095010 
Matrix (soil/water): WATER 
Lab Sample ID: VSIOOl 
Level (low/med): 
LOW 
Date Received: 01/27/95 
% Solids: 
0.0 
Concentration Units (ug/L or mg/kg dry weight): UG/L 
i 
1 
1 
l
l
l
l 
ICAS No. 
1 Analyte |Concentration!Cl Q 
|M 1 
1 
1 
1 
l
l
l
i 
17429-90-5 1 Aluminum 1 
26.3 IB| 
|P | 
17440-36-0 {Antimony { 
1.4 {U{N 
(F { 
{7440-38-2 {Arsenic | 
1.1 |U{ 
|F { 
17440-39-3 IBarium 
j 
8.8 IU! 
IP 1 
17440-41-7 IBerylliuml 
0.10 iU|N* T 
IF | 
17440-43-9 {Cadmium | 
3.1 |U| 
|P | 
17440-70-2 ICalcium | 
56.8 |B| 
|P | 
17440-47-3 1 Chromium { 
5.3 LBT U 
IP { 
17440-48-4 ICobalt 
j 
9.5 1U| 
|P | 
17440-50-8 ICopper 
| 
16.7 |U| 
|P | 
17439-89-6 |Iron 
1 
32.1 |U| 
|P | 
17439-92-1 ILead 
| 
0.86 |>r [>( |F | 
{7439-95-4 {MagnesiumI 
26.0 {U{ 
{P j 
{7439-96-5 {Manganese{ 
2.6 jUj 
IP I 
17439-97-6 |Mercury | 
0.20 |U| 
|CV| 
17440-02-0 {Nickel 
1 
13.1 |U| 
|P | 
17440-09-7 jPotassiuml 
526 {U| 
|P | 
{7782-49-2 {Selenium 1 
1.4 jUj 
jF j 
{7440-22-4 {Silver 
| 
5.1 |U| 
jP j 
17440-23-5 {Sodium 
( 
359 !B{ 
|P | 
17440-28-0 (Thallium | 
2.7 |U|W 3" IF | 
j7440-62-2 {Vanadium { 
4.5 {U{ 
|P { 
{7440-66-6 (Zinc 
| 
12.7 jBj 
|P { 
{57-12-5 
ICyanide j 
10.0 |U{ 
|AS| 
1 
1 
1 
Mil 
Color Before: COLORLESS 
Color After: COLORLESS 
Comments: 
Clarity Before: CLEAR 
Clarity After: CLEAR 
Reviewed By 
Date 
FORM I - IN 
Texture: 
Artifacts: NO 
300714 
ILM02.0 
080021 
HLA DATA QUALITY ASSURANCE REVIEW SL14MARY 
Organochlorine Pesticides and Polychlorinated Biphenyls Analysis 
Case Number : 
C^ ^ Q ) Q 
%fiyi^ CJU^/Y^I>1 fWxy.^^^ 
ProjectNumber 
Z ^ S H Z Z . 
l O - Z . 
Site: 
Contractor Laboratory: P / V C P 
^
^
^
L
n
^
. 
validator 
X . 
i
V
l
^ 
^ 
Validation Date: 3/:g^/q5-
, 
« 
——T 
QC Reviewer ^7>^y^-<y.^ :^. 
> y ^ y 7 y ^ 
Sample Matrix: 
j o - { i , ( | 2 ^ ) 
l J A : f e . - y 5 ) 
Review Date: J y 7 / / 
^ j ~ -
Analytical Method: ^pfi^ ( ^ p 
/Qy, ^ : , > ^ 
. ^ Q , , ; 
Sample Designations: 
C2o<oOI 
C^Z2o7-z. 
(2221^2/^ 
P l o o n l 
D)IZ/4 
P122-2^^-
P200^0 
PZI^ZI 
P3ooo^ 
D ^ n q 
Eiooo^ 
BUo^Z-
RBSOOl 
knoll's 
Son n ^ 
Soo\2n 
S Q O l l ^ 
Data for the above samples are: 
Acceptable for use 
X 
Acceptable for use as qualified 
Unacceptable for use 
Is action required by the Prtrject Manager? 
Yes 
(Noy 
Comments: p^^jtei JU^t^je. JU^i-tlJUx^d^ j y A j y r ^ J^^M, 
\A6^^PfK 
( V K W O ^ 
ocp_l.doc 
10141994 1032 
Form OCP 1.0 
3 0 0 7 1 5 
DATA COMPLETENESS CHECKLIST 
X 
Included, no problems 
* 
Included, problems 
O 
Not included 
NA 
Not applicable 
Quality Control Summary 
X 
Case Narrative 
Surrogate Recovery Summary 
MS/MSD Summary 
X 
Reagent Blank Summary 
Sample Data 
yT* 
Chain of Custody Forms 
^ 
Holding Times 
X 
Organic Anaiysis Data Sheets 
X 
Quantitation Reports 
X 
GC/EC Chromatograms 
y* 
Pesticide/PCB Identification (for positive detections) 
Instrument Calibration and Performance Data 
X 
Initial Calibration Retention Time Summary 
y 
Initial Calibration Response Factor Summary 
• ^ 
Performance Evaluation Mix Summary 
X 
Continuing Calibration Verification Summary 
y 
Analytical Run Sequence Summary 
X 
GPC Calibration and Florisil Cartridge Check Summary 
y 
Pesticide/PCB Standards Quantitation Reports 
X 
Pesticide/PCB Standards GC/EC Chromatograms 
Reagent and Instrument Blank Data 
X 
Organic Analysis Data Sheets 
X 
Quantitation Reports 
X 
GC/EC Chromatograms 
X 
Pesticide/PCB Identification (for positive detections) 
ocp_l.doc 
10141994 1032 
Fonn OCP 1.0 
300716 
Matrix Spike Data 
y 
Organic Analysis Data Sheets 
Quantitation Reports 
X 
GC/EC Chromatograms 
Conunents: 
Fonn OCP IJ) 
ocp_l.doc 
10141994 1032 
3 
300717 
Harding Lawson Associates 
m''. _- j 
Engineering and 
: i I ==.: 1 Environmental Services 
SHEET. 
JOB NO. 
OF 
PROJECT. 
SUBJECT 
m ^ ^ i ^ i ^ d C L i A i ^ d ^ 
Cjyf^A^Oy^^ 
DATE 
S l ^ ^ - I ^ ^ 
COMPUTED BY C\. jJljJdtS^ 
CHECKED BY 
^^JJty^-V? 
53VZ10-0-Zo/oil'^^ 5' 
50012,0 
S O O I I ^ 
S3B\/o,0''0.flDH^'^^ 
^Icoo^ 
5aP)/o-l/oi^f-9^ 
SgPl/22-24/o|25'^r 
SBCz/^--|/oi3 0^F 
50012-5' 
PlOOOl 
Dii2m' 
P12J224-
CZOOOI 
CZZZ02ZL 
C2Z4-26 
\fSlc-ooz-
\/5j:-^o7, 
V5X-003 
VTX-0 0 1 
* 
I ^ 
300718 
• 
SPECinC COMMENTS REGARDING ANALYSES 
Chain Of Custody 
Were samples property pi 
and received in good condition? 
Yesj 
No 
Comments: T^MTCT C%^^ZK^ Jy^^yjL yAy/^^fJi^ 0(yiAji/trx j^J2yUiM>^ oJIrtr^ M J -
2*'6*C^ C^-d^ji^^y£lyru\Jl, CUUi«rxjC&y^y-A^-j^ ± I J L 
C O C ^ . J^iyyUUi^yUy. 
• 
Holding Times 
Were sample extractions performed-within holding times? 
Yes 
( N O ) 
Were sample analyses p^fefuned within holding times? 
(^Yes) 
No 
Comments: 
-A&/Yy\.\lJU O 
2-02*2 1 A T ^ I ^ 
:i2.022.jur^i^ Ji7tA.a^iteJ2_ I c^^x^ y^lA/^ z / ^ 
J^Akriy^ jyrtK>^ OAY^^Y^ jJl^^^^i^ M ^ - l m l oJz O w jd^yycCXliL 
/\lyjrrf\y(<^jy(KAsJL 
( T / U T ) . 
T ^ X C yUiorx^H-UL^l^ (TL y^A)yrA/^^ 
ocp_l.doc 
10141994 1032 
Focrn OCP 1.0 
3 0 0 7 1 9 
Initial Calibration 
Did the laboratory meet the guidelines regarding the minimum number of calibration standards for an acceptable 
initial calibration? 
'YesJ 
No 
Were the calibration standards, analyzed at the correct concentrations? 
/Yes) 
No 
Did the calibration curves meet thejiqearity criteria for maximum percent relative standard deviation (%RSD)? 
Yes 
PNOJ 
Were retention time windosfs-provided and correcUy calculated? 
( Y C ^ 
No 
Were peak resolutions acceptable? 
(Yes) 
No 
Comments: ( I J L ^ jze y ^ n J L 13 - J ^ 
&^ J l i ^ 
C/L AO^yf^^yohy Oliy^JS-VyCji 
Individual Mix Standards (Continuing Calibration) 
Did the individual mix stajjdards meet the linearity criteria for maximum percent difference (%D)? 
(Tes) 
No 
Did the individual mix standanls meet the retention time criteria? 
(Tes) 
No 
Comments: 
|/Uvv>C 
, . 
Form OCP 1.0 
OCp_l.ODC 
10141994 1032 
5 
300720 
Performance Evaluation Mix Standards (Continuing Calibration) 
Did the performance evalu^tien mix standards meet the linearity criteria for maximum percent difference (%D)? 
/Yes) 
No 
Did the performance evaluation mix standards meet the retention time criteria? 
fes) 
No 
Ylmt 
Analytical Sequence 
Were standard and sample^aRglyses performed following the correct analytical sequence? 
Cves) 
No 
yu-Tv^ 
Surrogate Recoveries 
Were the surrogate spike recoveries-w^thin acceptance limits? 
Yes 
(No 
If the spike recoveries w^jcThiacceptable. were the samples reanalyzed? 
Yes) 
No 
Comments: ^IcUvvnilc. S O O I Z O 
O y ^ : k i j L y \ J U W ^ o i ^ > ^ 
( ^ O O I Z J O R ^ ^ 
O d ^ - ^ ^ ^ 
yC7r^jb\^>t^ jduAn<^tu>^ yju^/(r\yiyvJU. $r/}^jML cXji^y^^rr^^/y^pM 
-T^-M^yCicJ^M^ 
300721 
Matrix Spikes 
Were matrix spike analyses performed at the correct firequency and on a sample matrix representative of the 
samples in this sample deUyeiy group (SDG)? 
/Yes) 
No 
Were the matrix spike recoveries and relative percent differences (RPDs) within acceptance criteria? 
(Yes) 
No 
Comments: ]/Y]5 VY^SP 
ym/v^tHwv(u£ trvi 
Blank Analyses 
Were the appropriate numbgiof blank analyses performed? 
/fes) 
No 
Were instrument blanks analyzed at the correct frequency? 
(YesJ 
No 
Were analytes reported in the bla 
Yes 
/No 
If analytes were reported in the blanks, were the same analytes also reported in the associated investigative 
samples? 
. 
Yes 
No 
f^A 
Did the sample results require quajifieation due to the presence of analytes in the associated blank samples? 
Yes 
( N o ) 
Comments: 
YUv^A^ 
ocp_I.doc 
10141994 1032 
FotmOCP 1.0 
300722 
Instrument Performance 
Were the percent breakdowpsJor 4,4'-DDT and endrin correctiy reported? 
( J e s ) 
No 
Were the percent breakdo^nsJor 4.4'-DDT and endrin within acceptance limits? 
(Yes) 
No 
Comments: " j 3 U yjl^^^rtudx^rr- ^^jaeAAvytTOAvC^ (yLoyAt- - ^ ^ ^ 
' l ^ ^ j ^ ^ > V M r ^ ^ ^ ^ 
^^m^\7^ S o o n ? 0<AJI S O D \ \ \ jJy^dxx^yJblJl 0^ Ja^^P/oj^/\A^^^ 
\D% J r t 4,^'-PP^, JlyJywcjd^ U n ^ j M ^ ' 
^^'-PP^aAM>4-H^ 
^^JjCte-^i^, >-jrfviJ4J^ > ^ ^ ^ ^ 
()yy^ y^^AAZl^jT (dy)t^(^XA^^ 
d x S i \ ^ / y A A ^ 66-eiufeei^OAOC^>Zv^^i-e-v^ 
GPC and Florisil Cartridge Check 
Was GPC cleanup performB4^n the sample extracts? 
( j e s j 
No 
Was the GPC column checjc-acceptable? 
(Yes) 
No 
NA 
Was a Florisil cartridge chpck performed? 
(Yes) 
No 
Was the Florisil cartridgepheck acceptable? 
(YesJ 
No 
NA 
YuPAJty 
ocp_l.doc 
^ 
10141994 1032 
8 
_F_onn_0CP_1.0--
300723 
Laboratory Control Samples 
Were LCS analyses perfonped;' 
'Yes) 
No 
Were the LCS recoveries within acceptable limits? 
(Yes) 
No 
NA 
yWe. 
Sample Results 
Were target analytes reported^ the investigative samples? 
(Yes) 
No 
Were chromatograms proyidedsfor all target analytes reported in the investigative samples? 
(jTes^ 
No 
Were chromatograms of apeeptable quality and were analytes correcUy identified? 
(/Qs) 
No 
Were the quantitated results for target analytes calculated using the appropriate standard and were the retention 
times (RTs) acceptable? 
. 
/Yes) 
No 
Comments: T ^ ^ .ymKCl2yyJr S j U i M ^ l y r ^ U i ^ J y X < ^ ^ 
(>L^>WL ££ffet*^T^ 
FoanOCP IS) 
ocp_l.doc 
10141994 1032 
9 
300724 
Calculation Check 
Initial Calibration V T J Z G J ^ 
Retention Time Window: 
%RSD: 
Continuing Calibration 
\ f Z l j ^ ^ l 
^ 
%D:rpB6»08^ 0(^-0g^ jTNjpgmc??^ 
-^ 
;—= 
pr 
-—• 
y - \UU >- 
60 1^ 
1 y-OA^ ii/fy\^'<»y^cr 
Surrogate Recovery] A ^ y y ^ 6 Q Q | H | 
' ' 
0-C?4^ 
XI OO :^ 7- 5"7o : ^ 4,4^ "P; 
Matrix Spike Recovery .5&/yyu*2J2x ^ \ 0 0 0 ^ 
RPD: 
YY15 m^P Ow^^^^^ Urwc^. 
— ^ - j 
X loo r \3^o M^ JIM:^(IZU\-. 
«... 1 A^ 
Fonn OCP ijQ 
10141994 1032 
10 
300725 
Sample Results I _>MtH/y3Xe ^ [ 0 0 0 ^ 
CRQL: 
~ 
% J M U ^ 
- (7-^^jf^^ML QSiQi, 
z^'Z^ y 
Positive Result: 
ocp_l.doc 
FonaOCFIJ) 
10141994 1032 
J J 
300726 
HOLDING TIME QUALIHCATION SUMMARY FORM 
Sample 
Identification 
1 
^XZOZZ. 
Soo|:;..o^^ 
' Date 
Siunpled 
l//q/^^ 
\/7.ol^5' 
Date 
Prepared 
2/^A^ 
2/3/^5-
Date 
Analyzed 
T-Z-Z-o/qS-
z/ll}oi5' 
Prep. 
Holding 
Time 
lO-
7 
Analysis 
Holding 
Time 
0,0 
^-0 
Qualifier 
r/o.:r 
3-/U3-
o 
o 
to 
Comments: 
ocp_l .doc 
1014l9»t 1032 
FcraOCP 1.0 
12 
INITIAL CALIBRATION QUALIFICATION SUMMARY FORM 
Date/Time 
Izlioh^' 
Instrument 
GrCX'^ 
&CX- \S-
Analyte 
P()J)^n.-?>WCy 
"pixdlk^-mcL 
RF 
— 
—• 
7oRSD 
20. S 
20.8 
Samples Affected 
E:I2^)2.Z-, CZOOOl . (ZZlZ02zZ.i 
C224-26, DIIZl^, DI^^^4; 
D1non\ 
Qualifier 
C+/-) 
j/tfT 1 
1 
. . . 
II 
U> 
o o 
V j 
to 
00 
Comments 
: 
oq>._l .doc 
1 
10141994 1032 
13 
FcraOCP 1.0 
CONTINUING CALIBRATION QUALIFICATION SUMMARY FORM 
Date/Time 
f ( M <1A 
V 
Instrument 
VAXLAU-UC/VJ 
Analyte 
w ^ 
OJlZ^OUux^ AJ)^ 
d 
%D 
\JL yvu:^ 
Samples Affected 
- ^ 
.-' 
Qualifier 
1 
bJ 
o o 
<3 
to 
VX) 
Coinmenis 
1 
1 ocp,l.d.« 
i 
10141994 1032 
Fenn OCP 1.0 
14 
BLANK SUMMARY FORM 
Blank ID 
(y\yfr cUskiy^ 
Analyte 
L lAA^ ^ficyy^l^ 
Blank 
Result 
Units 
5x 
Result 
Associated 
Samples 
Qualifier 
1 
to 
o 
o 
U) 
o 
Commcnis: 
ocp_I .doc 
10141994 1032 
Fonn OCP I.O 
15 
Summary and Conclusions 
OiU Acdyx lytjy. 
fi/yini}. 
.>^a(yv\^. AJUACK^ Q M M QCf Mt^^ALy(AA.fi^t(l CX^^"^. 
ay^z^ 
•tL OAJP. AAM-riv, A "P" /^/Kvd? (lJ^:iy^yTiyn^ I H .-kzlj rd/JzkA.(T) X4^ 
-jig. ^ ^ A . -
v ^ 
<Har xikjC-jiXivr 
(Z(y,{Krc/\yr7y-
fUJLy .Xtiy^)^ a " P y 0 / ^ ^ ,i-S^^iiycr\6SKynf^ 
Aly(^.^n^^OAA(^j.fi . 
Zl 
V\L09Ay^ 
C2000I^ C2-Z-02.7_^ C?_2M-^^ P I I 2 l ^ , D]7j2-Zt^ ^/^,./(^ I>l OOO I ^A^vtUL^ 
A-JL 
i/>>.AAv»y i-y* Kyur^ni^xn,^ 
/ or,lPy^^Ar^yMl'/ , Kf^QiyJ^ (J ,>!hnK'j/^^t-Jiy /y"" rn JJ/W^ 
i \^Mif(iy^ 
Validator's Signature: 
Validator's Initials: 
Validation Date: 
3 / 3 0 H S ^ 
QC Reviewer's Signature: 
^ 
•yy-cA^ 
QC Reviewer's Initials 
P^Tr 
Review Date: 
? / 7 / / ? j ~ 
ocp_l.doc 
I0I41994 1032 
16 
Fonn OCP IJ) 
300731 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
Name: G S E L I 
'._ 
Contract: H^JA 
Case No.: HLA 
SAS No.: 
C20001 
Code: PACE 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.0 (g/mL) 5 
% Moisture: 11 
decanted: (Y/N) JJ 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
SDG No.: 95010 
Lab Sample ID: VTXOOl 
Lab File ID: 
Concentrated Extract Volxime: 
Injection Volume: 1^00 (uL) 
GPC Cleanup: 
(Y/N) 
5000 (UL) 
pH: 8.2 
Date Received: 02/01/95 
Date Extracted: 02/03/95 
Date Analyzed: 02/20/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) ^ 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
60-57-1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5 
-alpha-BHC 
-beta-BHC_[ 
delta-BHC 
-gamma-BHC (Lindane) 
-Heptachlor 
\ 
-Aldrin 
-Heptachlor epoxide_ 
-Endosulfan I 
^ 
-Dieldrin 
-4,4' -DDE 
-Endrin 
•Endosulfan II 
-4,4' -DDD 
" 
-Endosulfan sulfate 
-4,4' -DDT 
" 
Methoxychlor__ 
Endrin ketone 
-Endrin Aldehyde_ 
-alpha-Chlordane" 
-gamma-Chlordane" 
-Toxaphene 
' 
—Aroclor-l016_ 
—Arocl or-12 21' 
—Aroclor-1232' 
—Aroclor-1242^ 
—Aroclor-1248^ 
—Aroclor-1254" 
—Aroclor-1260' 
FORM I PEST 
Reviewed By 
Date 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE.NO. 
w 
ame: G S E L I 
IjaB'Code: PACE 
Case No.: HLA 
latrix: (soil/water) SOIL 
sample wt/vol: 
30.0 (g/mL) Q 
i Moisture: 15 
decanted: (Y/N) H 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Contract: HIA. 
SAS No.: 
C22022 
SDG No.: 95010 
Lab Sample ID: 
VTX002 
Lab F i l e ID: 
:oncentrated Extract Volume: 
[njection Volume: 
1.00 
(uL) 
;PC Cleanup: 
(Y/N) 
5000 (uL) 
pH: 9.0 
Date Received: 02/01/95 
Date Extracted: 02/03/95 
Date Analyzed: 02/20/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) E 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
gamma-BHC fLindane) 
76-44-8 
Heptachlor 
3 09-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4, 4'-DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4, 4'-DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4 , 4 ' -DDT 
72-4 3-5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehvde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53 469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
2.0 
2.0 
2.0 
2.0 
2.0 
2.0 
2.0 
2.0 
3.9 
3.9 
3.9 
3.9 
3.9 
3.9 
3.9 
20 
3.9 
3.9 
2.0 
2.0 
200 
39 
79. 
39 
39 
39 
39 
39 
UU" 
U 
U 
U 
U 
U 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
FORM I PEST 
300733 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
Lal^ame: G S E L I 
LM^lode: PACE 
Case No.: HLA 
Contract: HLA 
SAS No.: 
C22426 
SDG No.: 95010 
Matrix: (soil/water) SOIL 
sample wt/vol: 
30.0 (g/mL) 2 
% Moisture: 14 
decanted: (Y/N) H 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Lab Sample ID: VTX003 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: l.OQ (uL) 
GPC Cleanup: 
(Y/N) 
?999 (UL) 
pH: 8.6 
Date Received: 02/01/95 
Date Extracted: 02/03/95 
Date Analyzed: 02/20/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) M 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
60-57-1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4 
5103-71-9 
— 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5— 
-alpha-BHC 
-beta-BHC_^ 
delta-BHC 
-gamma-BHC (Lindane) 
-Heptachlor_] 
-Aldrin 
-Heptachlor epoxide_ 
-Endosulfan I 
-Dieldrin 
-4,4'-DDE 
-Endrin 
-Endosulfan II 
-4,4' -DDD 
" 
-Endosulfan sulfate 
-4,4' -DDT 
'_ 
Methoxychlor_ 
Endrin ketone 
—Endrin Aldehyde_ 
—alpha-Chlordane_ 
—gamma-Chlordane, 
—Toxaphene 
—Aroclor-1016_ 
—Aroclor-1221" 
—Aroclor-1232[ 
—Aroclor-1242]^ 
—Aroclor-1248] 
—Aroclor-1254' 
Aroclor-1260 
FORM I PEST 
Reviewed By 
Date — 
VALID 
300734 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
Lab^Name: G S E L I 
J 
ode: PACE 
Case No.: HLA 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.0 (g/mL) £ 
% Moisture: _§ 
decanted: (Y/N) H 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Contract: HLA 
SAS No.: 
DlOOOl 
SDG No.: 95010 
Lab Sample ID: VSI002 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volvime: 1.00 (uL) 
GPC Cleanup: 
(Y/N) 
5000 (uL) 
pH: 8.3 
Date Received: 01/27/95 
Date Extracted: 02/01/95 
Date Analyzed: 02/21/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
sulfur Cleanup: (Y/N) ^ 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
gamma-BHC (Lindane) 
76-44-8 
Heptachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4 , 4 ' -DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4 , 4 ' -DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4 , 4 ' -DDT 
72-43-5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehyde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
3.6 
3.6 
3.6 
3.6 
3.6 
3.6 
3.6 
19 
3.6 
3.6 
7.2 
7.7 
190 
36 
73, 
36 
36 
36 
36 
36 
uJ-
u 
U 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
^ T 
u 
u 
u 
u 
u 
u 
u 
u 
FORM I PEST 
VA 
Reviewed By _ 
Date 
300735 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
T.ai|iy^=»™*** ^ S E L I 
Contract: 
W 
T.ar) Co 
Matrix 
Sample 
% Mois 
Extrac 
Concer 
Inject 
3PC Cl 
• 
• 
de: PACE 
Case No.: p^^ 
SAS No.! 
HLA 
SDG 
: (soil/wateri SOIL 
Lab Samole ID: 
wt/vol: 
30.0 (q/mL) G 
Lab File ID: 
ture: 17 
decanted: (Y/N) N 
Date Received: 
tion: 
rsepF/Cont/Sonc) 
SONC 
Date Extracted 
itrated Extract Volume: 
5000 (uL) Date Analvzed: 
.ion Volxime: 1.00 (uL) 
Dilution Facto. 
eanup: 
(Y/N^ Y 
pH: 8.8 
Sulfur Cleanup 
CONCENTRATION UNITS: 
CAS NO. 
COMPOUND 
(ug/L or ug/Kg) UG/K 
319-84-6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
qamma-BHC (Lindane) 
76-44-8 
Heptachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4 ,4 ' -DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4 ,4 ' -DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4 ,4 ' -DDT 
72-43 -5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehyde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
FORM I PEST 
Reviewec 
Date 
D11214 
No.: 95010 
VST003 
01/27/?5 
: 02/01/95 
02/?l/95 
r: 
1.00 
: (Y/N) N 
S 
Q 
2.0 
2.0 
2.0 
2.0 
2.0 
2.0 
2.0 
2.0 
4.0 
4.0 
4.0 
4.0 
4.0 
4.0 
4.0 
20 
4.0 
4.0 
2.0 
2.0 
200 
40 
80 
40 
40 
40 
40 
40 
Ml' 
Z^ 'izir^ 
h 
p p p p p p p p p p p p P P P P P P P P P P P P P O t s O 
iyj\XAytz ?/ 
fPT 3/90 
lyZjJ i<^ 
- ' y_ 
30073~r 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
Lal^ ame: G S E L I 
LaBM:ode: PACE 
Case No.: HLA 
Matrix: (soil/water) SOIL 
sample wt/vol: 
30.0 (g/ioL) G 
% Moisture: 12 
decanted: (Y/N) li 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Contract: HLA 
SAS No.: 
D12224 
SDG No.: 95010 
Lab Sample ID: VSI004 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: 1.00 (uL) 
3PC Cleanup: 
(Y/N) 
5000 (uL) 
pH: ?t$ 
Date Received: Ql/27/95 
Date Extracted: 02/01/95 
Date Analyzed: 02/21/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) H 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
60-57-1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5 
alpha-BHC 
beta-BHC_J 
delta-BHC 
—-gamma-BHC (Lindane) 
Heptachlor 
Aldrin 
Heptachlor epoxide_ 
Endosulfan I 
'_ 
Dieldrin 
4,4'-DDE 
Endrin 
Endosulfan II 
4,4'-DDD 
Endosulfan sulfate 
4,4'-DDT 
Methoxychlor 
Endrin ketone 
Endrin Aldehyde, 
alpha-Chlordane' 
gamma-Chlordane^ 
Toxaphene_ 
Aroclor-1016_ 
Aroclor-1221' 
Aroclor-1232] 
Aroclor-1242" 
Aroclor-1248' 
Aroclor-1254] 
Aroclor-1260" 
FORM I PEST 
Reviewed By 
Date 
Urii}A( 
3/90^ 
300737 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
LaK; 
ame: G S E L I 
Code: PACE 
Case No.: HLA 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.0 (g/mL) fi 
% Moisture: Ifi 
decanted: (Y/N) M 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Contract: HLA 
SAS No.: 
D20020 
SDG No.: 95010 
Lab Sample ID: VOB003 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: 1.00 (uL) 
3PC Cleanup: 
(Y/N) 
50Q9 (UL) 
pH: 8.3 
Date Received: 01/23/95 
Date Extracted: 01/25/95 
Date Analyzed: 02/03/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) li 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
6 0 - 5 7 - 1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5— 
-alpha-BHC 
-beta-BHcJ 
delta-BHC 
-gamma-BHC (Lindane) 
-Heptachlor 
-Aldrin 
-Heptachlor epoxide, 
-Endosulfan I 
] 
-Dieldrin 
-4,4'-DDE 
-Endrin 
-Endosulfan II_ 
-4,4' -DDD 
-Endosulfan sulfate, 
-4,4' -DDT 
Methoxychlor_ 
Endrin ketone 
-Endrin Aldehyde, 
-alpha-Chlordane] 
-gamma-chlordane] 
-Toxaphene, 
—Aroclor-1016_ 
—Ar OC 1 or-12 21] 
—Aroclor-1232] 
—Aroclor-1242] 
—Aroclor-1248] 
—Aroclor-1254" 
Aroclor-1260 
Reviewed By 
FORM I PE«Ete 
3 / 9 0 
300738 
u a ^ I a m e : G S E L I 
C<alRc 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
C o n t r a c t : 
HLA 
SAS N o . : 
EPA SAMPLE NO. 
D21921 
:ode: PACE 
C a s e N o . : HLA 
M a t r i x : 
( s o i l / w a t e r ) 
SOIL 
Sample w t / v o l : 
3 0 . 0 
(g/mL) fi 
i M o i s t u r e : 
12 
d e c a n t e d : 
(Y/N) li 
S x t r a c t i o n : 
( S e p F / C o n t / S o n c ) 
SONC 
SDG No.: 95010 
Lab Sample ID: VOB004 
Lab File ID: 
:;oncentrated Extract Volume: 
Cnjection Volume: 1.00 (uL) 
;PC Cleanup: 
(Y/N) 
5000 (uL) 
pH: 8.8 
Date Received: 01/23/95 
Date Extracted: 01/25/95 
Date Analyzed: 02/03/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) li_ 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
319-85-7 
319-86-8 
5 8 - 8 9 - 9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
6 0 - 5 7 - 1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5 
-alpha-BHC 
-beta-BHC_] 
delta-BHC 
-gamma-BHC (Lindane) 
-Heptachlor 
\ 
-Aldrin 
-Heptachlor epoxide, 
-Endosulfan I 
] 
-Dieldrin 
-4,4'-DDE 
-Endrin 
-Endosulfan II 
-4,4' -DDD 
-Endosulfan sulfate 
-4,4' -DDT 
Methoxychlor_ 
Endrin ketone 
-Endrin Aldehyde, 
-alpha-Chlordane] 
-gamma-Chlordane, 
-Toxaphene, 
-Aroclor-1016_ 
—Aroclor-1221, 
—Aroclor-1232] 
—Aroclor-1242] 
—Aroclor-1248] 
—Aroclor-12 54] 
—Aroclor-12 60* 
FORM I PEST 
Reviewed By 
Date 
300739 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
La|^ ame: G S E L I 
Lab Code: PACE 
Case No.: HLA 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.0 (g/mL) fi 
% Moisture: H 
decanted: (Y/N) li 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Contract: HLA 
SAS No.: 
D30002^ 
SDG No.: 95010 
Lab Sample ID: VOA002 
Lab File ID: 
Concentrated Extract Volume: 
Injection Voltime: l.OO (uL) 
GPC Cleanup: 
(Y/N) 
5000 (uL) 
pH: 7.9 
Date Received: 01/23/95 
Date Extracted: 01/25/95 
Date Analyzed: 02/03/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) H 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
qamma-BHC (Lindane) 
76-44-8 
Heptachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4,4'-DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4, 4'-DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4,4'-DDT 
72-43-5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehvde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
3.7 
3.7 
3.7 
3.7 
3.7 
3.7 
3.7 
19 
3.7 
3.7 
1.9 
1.9 
190 
37 
74 
37 
1 
37 
37 
i 
37 
37 
U 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
FORM I PEST 
Reviewed By 
Date — 
^3/90^ 
3 0 0 7 4 0 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
L g ^ ame: G S E L I 
Lab Code: PACE 
Case No.: HLA 
!4atrix: (soil/water) SOIL 
sample wt/vol: 
30.0 (g/mL) fi 
I Moisture: 12 
decanted: (Y/N) li ; 
Extraction: 
(SepF/Cont/Sonc) 
SONg 
Contract: HLA 
SAS No.: 
D31719 
SDG No.: 95010 
Lab Sample ID: VOA003 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: 1.00 (uL) 
3PC Cleanup: 
(Y/N) Y 
?999 (UL) 
pH: 8.5 
Date Received: 01/23/95 
Date Extracted: 01/25/95 
Date Analyzed: 02/03/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) li__ 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
60-57-1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4—— 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5— 
-alpha-BHC 
-beta-BHC_] 
delta-BHC 
-gamma-BHC (Lindane) 
-Heptachlor 
[ 
-Aldrin 
-Heptachlor epoxide, 
-Endosulfan I 
] 
-Dieldrin 
-4,4'-DDE 
-Endrin 
-Endosulfan II 
-4,4'-DDD 
-Endosulfan sulfate 
-4,4'-DDT 
Methoxychlor__ 
Endrin ketone 
-Endrin Aldehyde, 
-alpha-Chlordane] 
-gamma-Chlordane] 
-Toxaphene 
- -Aroc 1 or-1016, 
—Aroclor-12 21] 
—Aroclor-1232] 
—Aroclor-1242] 
—Aroclor-1248] 
—Aroclor-1254] 
Aroclor-12 60' 
FORM I 
PEST 
Reviewed By 
Date 
3/90 
300741 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
:.agteT ame: G s E L I 
Lab Code: PACE 
Case No.: HLA 
Matrix: (soil/water) SOIL 
Seunple wt/vol: 
30.0 (g/mL) fi 
% Moisture: _7 
decanted: (Y/N) li 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Contract: HLA 
SAS No.: 
E10005 
SDG No.: 95010 
Lab Sample ID: VOC003 
Lab File ID: 
Concentrated Extract Volume: 
Injection Voltime: 1.00 (uL) 
3PC Cleanup: 
(Y/N) 
5000 (uL) 
pH: 8.1 
Date Received: 01/23/95 
Date Extracted: 01/25/95 
Date Analyzed: 02/03/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) li 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6— 
319-85-7— 
319-86-8— 
58-89-9 
76-44-8 
3 0 9 - 0 0 - 2 — 
1 0 2 4 - 5 7 - 3 -
9 5 9 - 9 8 - 8 — 
6 0 - 5 7 - 1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1 0 3 1 - 0 7 - 8 -
50-29-3 
72-43-5 
53494-70-5 
7 4 2 1 - 9 3 - 4 -
5 1 0 3 - 7 1 - 9 -
5 1 0 3 - 7 4 - 2 -
8 0 0 1 - 3 5 - 2 -
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5 
alpha-BHC 
beta-BHC_] 
delta-BHC 
-gamma-BHC 
(Lindane) 
- H e p t a c h l o r 
-Aldrin 
-Heptachlor epoxide, 
-Endosulfan I 
-Dieldrin 
-4,4'-DDE 
-Endrin 
-Endosulfan II 
-4,4'-DDD 
-Endosulfan sulfate 
-4,4' -DDT 
Methoxychlor_ 
Endrin ketone 
-Endrin Aldehyde, 
-alpha-Chlordane, 
-gamma-Chlordane, 
-Toxaphene, 
Aroclor-1016, 
Aroclor-1221] 
Aroclor-1232] 
Aroclor-1242] 
A r o c l o r - 1 2 4 8] 
Aroclor-1254] 
Aroclor-1260' 
FORM I 
PEST 
Reviewed By 
Date 
300742 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
"W 
ame: G S E L I 
Leib Code: PACE 
Case No.: HIA 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.0 (g/mL) fi 
% Moisture: 14 
decanted: (Y/N) H 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Contract: HLA 
SAS No.: 
E12022 
SDG No.: 95010 
Lab Sample ID: VOB002 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volxime: 1.00 (uL) 
SPC Cleanup: 
(Y/N) 
5000 (UL) 
pH: 8.7 
Date Received: 01/23/95 
Date Extracted: 02/03/95 
Date Analyzed: 02/20/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) M 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
qamma-BHC (Lindane) 
76-44-8 
H e p t a c h l o r 
309-00-2 
A l d r i n 
1024-57-3 
H e p t a c h l o r 
epoxide 
959-98-8 
Endosulfan I 
60-57-1 
D i e l d r i n 
72-55-9 
4 , 4 ' -DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan 
I I 
72-54-8 
4 , 4 ' -DDD 
1031-07-8 
Endosulfan 
s u l f a t e 
50-29-3 
4 ,4 ' -DDT 
72-43-5 
Methoxychlor 
53494-70-5 
E n d r i n k e t o n e 
7421-93-4 
Endrin Aldehvde 
5103-71-9 
a l p h a - C h l o r d a n e 
5103-74-2 
gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
A r o c l o r - 1 0 1 6 
11104-28-2 
A r o c l o r - 1 2 2 1 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
A r o c l o r - 1 2 4 8 
11097-69-1 
Aroclor-1254 
1 1 0 9 6 - 8 2 - 5 
A r o c l o r - 1 2 6 0 
2 . 0 
2 . 0 
2 . 0 
2 . 0 
2 . 0 
2 . 0 
2 . 0 
2 . 0 
3 . 8 
3 . 8 
3 . 8 
3 . 8 
3 . 8 
3 . 8 
3 . 8 
20 
3 . 8 
3 . 8 
2 . 0 
2 . 0 
200 
38 
77' 
38 
38 
38 
38 
38 
U T 
U T 
U T 
U T 
U T 
U T 
uT 
U T 
uT 
U T 
U T 
U T 
U T 
U T 
U T 
U T 
U T 
U T 
U T 
U T 
uT 
uT 
uT 
U T 
U T 
U T 
U T 
U T 
FORM I PEST 
Reviewed By 
Date r 
3/90 
300743 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
L a J ^ 
Name: G S E L I 
Lffl^Code: PACE 
Case No.: HLA 
Matrix: (soil/water) WATER 
Sample wt/vol: 
1000 
(g/mL) ML 
% Moisture: 
decanted: (Y/N) _ 
Extraction: 
(SepF/Cont/Sonc) 
CONT 
Contract: HLA 
SAS No.: 
RBSOOl 
SDG No.: 95010 
Lab Sample ID: VTX004 
Lab File ID: 
Concentrated Extract Volxime: 
Injection Volxime: 
1.00 (uL) 
SPC Cleanup: 
(Y/N) li 
2000 (uL) 
pH: ?.$ 
Date Received: 
02/01/95 
Date Extracted: 02/01/95 
Date Analyzed: 
02/03/95 
Dilution Factor: 
1.00 
• 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) li 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/L 
319-84-6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
gamma-BHC (Lindane) 
76-44-8 
Heptachlor 
3 09-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4, 4'-DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4 , 4 ' -DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4,4 • -DDT 
72-43-5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehyde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.020 
0.020 
0.020 
0.020 
0.020 
0.020 
0.020 
0.10 
0.020 
0.020 
0.010 
0.010 
1.0 
0.20 
0.40 
0.20 
0.20 
0.20 
0.20 
0.20 
U 
U 
u 
U 
U 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
FORM I PEST 
Reviewed By 
Date 
^ 7 ^ 
300744 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
ame: G S E L I 
Lab Code: PACE 
Case No.: HLA 
Matrix: (soil/water) WATER 
Sample wt/vol: 
1000 
(g/mL) ML 
% Moisture: 
decanted: (Y/N) _ 
Extraction: 
(SepF/Cont/Sonc) 
CONT 
Contract: HLA 
SAS No.: 
S00118 
SDG No.: 95010 
Lab Sample ID: VOCOOl 
Lab File ID: 
Concentrated Extract Volxime: 
I n j e c t i o n Volxime: 
1.00 
(uL) 
GPC Cleanup: 
(Y/N) li 
2000 (uL) 
pH: 6.9 
Date Received: 01/23/95 
Date Extracted: 01/24/95 
Date Analyzed: Ql/27/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) N 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/L 
319-84-6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
qamma-BHC (Lindane) 
76-44-8 
Heptachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4,4'-DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4,4'-DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4 .4 ' -DDT 
72-4 3-5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehvde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.020 
0.020 
0.020 
0.020 
0.020 
0.020 
0.020 
0.10 
0.020 
0.020 
0.010 
0.010 
1.0 
0.20 
0.40 
0.20 
0.20 
0.20 
0.20 
0.20 
U 
U 
U 
U 
U 
U 
U 
U 
U 
U 
U 
U 
U 
U 
U 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
FORM I PEST 
Reviewed By 
Date 
300745 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
La|^ 
LaR 
ame: G S E L I 
La^Xode: PACE 
Case No.: HLA 
Matrix: (soil/water) WATER 
sample wt/vol: 
1000 
(g/mL) ML 
% Moisture: 
decanted: (Y/N) _ 
Extraction: 
(SepF/Cont/Sonc) 
CONT 
Contract: HLA 
SAS No.: 
S00119 r 
SDG No.: 95010 
Lab Sample ID: VOBOOl 
Lab File ID: 
Concentrated Extract Volxime: 
Injection Volxime: 1.00 (uL) 
GPC Cleanup: 
(Y/N) li 
2000 (uL) 
pH: 6.8 
Date Received: 01/23/95 
Date Extracted: 01/24/95 
Date Analyzed: 01/27/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
sulfur Cleanup: (Y/N) li 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/L 
319-84-6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
gamma-BHC (Lindane) 
76-44-8 
Heptachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4,4'-DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
• 
4,4'-DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4,4'-DDT 
72-43-5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehvde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.020 
0.020 
0.020 
0.020 
0.020 
0.020 
0.020 
0.10 
0.020 
0.020 
0.010 
0.010 
1.0 
0.20 
0.40 
0.20 
0.20 
0.20 
0.20 
0.20 
U 
u 
u 
U 
U 
U 
U 
U 
U 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
V 
FORM I PEST 
Reviewed By 
Date — 
L. 
300746 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
^ 
Name: G S E L I 
Lab Code: PACE 
Case No.: HLA 
Matrix: (soil/water) WATER 
Sample wt/vol: 
1000 
(g/mL) ML 
% Moisture: 
decanted: (Y/N) _ 
Extraction: 
(SepF/Cont/Sonc) 
CONT 
Contract: HLA 
SAS No.: 
S00120 
SDG No.: 95010 
Lab Sample ID: VOAOOl 
Lab File ID: 
Concentrated Extract Volxime: 
Injection Volxme: 1.00 
(uL) 
GPC Cleanup: 
(Y/N) N 
2000 (uL) 
pH: 
7.1 
Date Received: 01/23/95 
Date Extracted: 01/24/95 
Date Analyzed: 02/03/95 
Dilution Factor: 
1.00 
Sulfur Cleanup: (Y/N) N _ 
CAS NO. 
COMPOUND 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/L 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
60-57-1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5 
-alpha-BHC 
-beta-BHCj; 
delta-BHC 
-gamma-BHC (Lindane) 
-Heptachlor 
-Aldrin 
-Heptachlor epoxide, 
-Endosulfan I 
-Dieldrin 
-4,4'-DDE 
-Endrin 
-Endosulfan II 
-4,4' -DDD 
] 
•Endosulfan sulfate 
•4,4' -DDT 
] 
Methoxychlor 
Endrin ketone 
-Endrin Aldehyde, 
-alpha-Chlordane, 
-gamma-Chlordane, 
-Toxaphene 
-Aroclor-1016_ 
-Aroclor-1221] 
-Aroclor-1232] 
-Aroclor-1242] 
-Aroclor-1248] 
-Aroclor-1254] 
-Aroclor-12 60' 
0 . 0 1 0 
0 . 0 1 0 
0 . 0 1 0 
0 . 0 1 0 
0 . 0 1 0 
0 . 0 1 0 
0 . 0 1 0 
0 . 0 1 0 
0 . 0 2 0 
0 . 0 2 0 
0 . 0 2 0 
0 . 0 2 0 
0 . 0 2 0 
0 . 0 2 0 
0 . 0 2 0 
0 . 1 0 
0 . 0 2 0 
0 . 0 2 4 
0 . 0 1 0 
0 . 0 1 0 
1.0 
0 . 2 0 
0 . 4 0 
0 . 2 0 
0 . 2 0 
0 . 2 0 
0 . 2 0 
0 . 2 0 
U 
U 
U 
U 
U 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
Reviewed By 
FORM I PEST Date 
^ 
IDATED 
• - r •• 111- • 
^ ' ^ ' ^ ^ - ^ ' ^ y 
:^l^ll±^L_y/9o 
300747 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
# 
Name: G S E L I 
Lab Code: PACE 
Case No.: HLA 
Matrix: (soil/water) WATER 
Sample wt/vol: 
600.0 
(g/mL) ML 
% Moisture: 
decanted: (Y/N) _ 
Extraction: 
(SepF/Cont/Sonc) 
CONT 
Contract: HLA 
SAS No.: 
SO0120RE 
SDG No.: 95010 
Lab Sample ID: VOAOOIRE 
Lab File ID: 
Concentrated Extract Volxime: 
Injection Volxime: l.OO 
(uL) 
GPC Cleanup: 
(Y/N) N 
2000 (uL) 
pH: 
7.1 
Date Received: 01/23/95 
Date Extracted: 02/08/95 
Date Analyzed: 02/11/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) N, 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/L 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
60-57-1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5 
-alpha-BHC 
-beta-BHC_] 
delta-BHC 
-gamma-BHC (Lindane), 
-Heptachlor 
-Aldrin 
-Heptachlor epoxide, 
•Endosulfan I 
•Dieldrin 
-4,4' -DDE 
-Endrin 
•Endosulfan II 
•4,4' -DDD 
-Endosulfan sulfate 
-4,4' -DDT 
_" 
Methoxychlor 
Endrin ketone 
—Endrin Aldehyde, 
—alpha-Chlordane, 
—gamma-Chlordane, 
—Toxaphene 
—Aroclor-1016, 
—Aroclor-1221, 
—Aroclor-1232_ 
—Aroclor-1242_ 
—Aroclor-1248, 
—Aroclor-12 54, 
—Aroclor-1260 
0 . 0 1 7 
0 . 0 1 7 
0 . 0 1 7 
0 . 0 1 7 
0 . 0 2 5 
0 . 0 1 7 
0 . 0 1 7 
0 . 0 1 7 
0 . 0 3 3 
0 . 0 3 3 
0 . 0 3 3 
0 . 0 3 3 
0 . 0 3 3 
0 . 0 3 3 
0 . 0 3 3 
0 . 1 7 
0 . 0 3 3 
0 . 0 3 3 
0 . 0 1 7 
0 . 0 1 7 
1.7 
0 . 3 3 
0 . 6 7 
0 . 3 3 
0 . 3 3 
0 . 3 3 
0 . 3 3 
0 . 3 3 
U J 
U T 
U T 
U T 
yr 
U T 
uT 
uT 
U T 
UT 
U T 
UT 
U T 
U T 
UT 
UT 
UT 
uT 
UJ 
UT 
UT 
uT 
UT 
uT 
uT 
uT 
uT 
uT 
V 
FORM I 
PEST 
Reviewed By 
Date 
V 
3/90 
300748 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
Name: G S E L I 
Xode: PACE 
Case No.: HLA 
Matrix: (soil/water) WATER 
Sample wt/vol: 
1000 
(g/mL) ML 
% Moisture: 
decanted: (Y/N) _ 
Extraction: 
(SepF/Cont/Sonc) 
CONT 
Contract: HLA 
SAS No.: 
S00125 
SDG No.: 95010 
Lab Sample ID: VSIOOl 
Lab File ID: 
Concentrated Extract Volxime: 
Injection Volxime: 1.00 (uL) 
GPC Cleanup: 
(Y/N) li 
2000 (uL) 
pH: 6.6 
Date Received: 01/27/95 
Date Extracted: 01/30/95 
Date Analyzed: 02/03/95 
Dilution Factor: 
i.oo 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) li 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/L 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
6 0 - 5 7 - 1 
72-55-9 
7 2 - 2 0 - 8 
33213-65-9 
7 2 - 5 4 - 8 
1031-07-8 
50-29-3 
7 2 - 4 3 - 5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5 
-alpha-BHC 
-beta-BHCj; 
delta-BHC 
-gamma-BHC (Lindane) 
-Heptachlor 
-Aldrin 
-Heptachlor epoxide, 
•Endosulfan I 
] 
- D i e l d r i n 
- 4 , 4 ' -DDE 
-Endrin 
-Endosulfan 
I I 
- 4 , 4 ' -DDD 
] 
-Endosulfan 
s u l f a t e 
- 4 , 4 ' -DDT 
] 
Methoxychlor__ 
Endrin k e t o n e 
—Endrin Aldehyde_ 
—alpha-Chlordane, 
—gamma-Chlordane, 
—Toxaphene, 
—Aroclor-1016, 
—Aroclor-12 21] 
—Aroclor-1232] 
—Aroclor-1242] 
—Aroclor-1248] 
—Aroclor-1254] 
—Aroclor-12 60' 
.010 
.010 
.010 
.010 
.010 
.010 
.010 
.010 
.020 
.020 
.020 
.020 
.020 
.020 
.020 
0.10 
.020 
.020 
.010 
.010 
1.0 
0.20 
0.40 
0.20 
0.20 
0.20 
0.20 
0.20 
u u u u u u u u u u u u u u u u u u u u u u u u u u u u 
FORM I 
PEST 
VALIDATED 
Reviewed By ^ - - f ^ t y X 2 • U/]; r t - b O 
Date 
/ Z ^ / ^ r 
3/90 
300749 
HLA DATA QUALTTY ASSURANCE REVIEW SUMMARY 
Organochlorine Pesticides and Polychlorinated Biphenyls Analysis 
Case Number: 
Site: 
Contractor Lab: 
Validator: 
QC Reviewer: 
Sample Matrix: 
95020 
Island Chemical Company 
Pace Environmental Laboratories, 
Kirsten Meier 
T^TAyy^y^^ ?^^<u^ 
water and soil 
Project Number: 
St. Rosa, LA 
Validation Date: 
Review Date: 
29872 10.2 
28 March 1995 
V - ( S - f S -
Analytical Method: 
Low Level Pest/PCB 
Sample Designations: 
RBSO/012495 * 
(SO0012) 
SBF3/12-14/012495 
(F31214) 
SBCl/0-1/012795 
(ClOOOl) 
SBD4/0-1/012795 
(D40001) 
SBBI/0-1/013195 
(BlOOOl) 
SBF2/12-15/012495 
(F21215) 
SBF3/18-20/012495 
(F31820) 
SBCl/16-18/012795 
(C11618) 
SBD4/14-16/012795 
(D41416) 
SBBl/6-8/013195 
(B16008) 
SBF2/18-20/012495 
(F21820) 
SBBl/24-26/013195 
(B12426) 
SBCl/18-20/012795 
(C11820) 
SBD4/20-22/012795 
(D42022) 
SBB101/0-1/013I95 
(BlOlOl) 
SBF3/0-1/012495 
(F30001) 
RBSO/012795 * 
(SO0127) 
SBCl/20-22/012795 
(C12022) 
RBSO/013195 * 
(BSO013) 
* = aqueous sample 
( ) = Lab sample ID 
Data for the above samples are: 
[ ] Acceptable for use 
[x] Acceptable for use as qualified 
[ ] Unacceptable for use 
Is action required by the Project Manager? 
Yes 
No[x] 
Comments: 
The investigative samples were analyzed using the Low Concentration SOW for Pesticides/PCB and the 
analytical data were reviewed in accordance with the Functional Guidelines, February 1994. 
The investigative sample RBSO/012395 was requested for analysis on the Chain of Custody, the lab 
propped the sample as VTE-001, but then the lab was requested not to analyze this sample. 
ocp_elec.ll 
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300750 
Cue Number: 9)020 
Project hfumber: 29S72 10.2 
Site ID: Isbnd CbcmioU Company 
DATA COMPLETENESS CHECKLIST 
[x] 
Included, no problems 
[*] 
Included, problems 
[O] 
Not included 
[NA] 
Not applicable 
Quality Control Summary 
X 
Case Narrative 
* 
Surrogate Recovery Summary 
* 
MS/MSD Summary 
X 
Reagent Blank Summary 
Sample Data 
* 
Chain of Custody Forms 
* 
Holding Times 
X 
Organic Analysis Data Sheets 
X 
Quantitation Reports 
X 
GC/EC Chromatograms 
X 
Pesticide/PCB Identification (for positive detections) 
Instrument Calibration and Performance Data 
X 
Initial Calibration Retention Time Summary 
* 
Initial Calibration Response Factor Summary 
X 
Performance Evaluation Mix Summary 
X 
Continuing Calibration Verification Summary 
X 
Analytical Run Sequence Summary 
X 
GPC Calibration and Florisil Cartridge Check Summary 
X 
Pesticide/PCB Standards Quantitation Reports 
X 
Pesticide/PCB Standards GC/EC Chromatograms 
Reagent and Instrument Blank Data 
X 
Organic Analysis Data Sheets 
X 
Quantitation Reports 
X 
GC/EC Chromatograms 
X 
Pesticide/PCB Identification (for positive detections) 
ocp_clcc. 11 
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300751 
Cue Number: 95020 
Project Number. 29872 10.2 
Site ID: bland CheniicBl Coinpanjr 
Matrix Spike/LCS Data 
* 
Organic Analysis Data Sheets 
X 
Quantitation Reports 
X 
GC/EC Chromatograms 
Comments: 
None 
ocp_el6C.ll 
12291994 1530 
Fonn OCP 1.1 
300752 
Cue Number: 95020 
Project Number: 29872 10.2 
Site ID: hbnd CfaemioU Company 
SPECIHC COMMENTS REGARDING ANALYSES 
Chain Of Custody 
Were samples properly preserved and received in good condition? 
Yes[x] 
No 
Comments: 
The Chain of Custodies submitted are not signed and dated by the lab upon sample receipt. No 
qualification of data. 
Holding Times 
Were sample extractions performed within holding times? 
Yes 
No[x] 
Were sample analyses performed within holding times? 
Yes[x] 
No 
Comments: 
Due to low surrogate recoveries the investigative samples RBSO/012495 and RBSO/012795 were re-
extracted on 2-20-94, 17 and 20 days past their hold time. Therefore, the results for these samples 
were qualified as estimated (J). 
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Form OCP 1.1 
300753 
Cue Number: 95020 
Project Number: 29872 10.2 
Sile ID: Island Cbemical Company 
Initial Calibration 
Did the laboratory meet the guidelines regarding the minimum number of calibration standards for an acceptable 
initial calibration? 
Yes[x] 
No 
Were the calibration standards analyzed at the correct concentrations? 
Yes[x] 
No 
Did the calibration curves meet the linearity criteria for maximum percent relative standard deviation (%RSD)? 
Yes 
No[x] 
Were retention time windows provided and correctly calculated? 
Yes[x] 
No 
Were peak resolutions acceptable? 
Yes[x] 
No 
Comments: 
The compound alpha-BHC in the initial calibration on 2-10-94 has a 20.8% RSD, exceeding the criteria 
of 209S. Therefore, the result for alpha-BHC in the investigative samples SBF2/12-15/012495 
(F21215), SBF2/18-20/012495 (F21820), SBF3/0-I/012495 (F30001), SBCl/0-1/012795 (ClOOOl), 
SBCl/16-18/012795 (C11618), SBCl/18-20/012795 (CI1820), SBCl/20-22/012795 (C12022), SBD4/0-
1/012795 (D40001), SBD4/14-16/012795 (D41416), SBD4/20-22/012795 (D42022) aud RBSO/013195 
(BSO013) were qualified as estimated (J). 
Individual Mix Standards (Continuing Calibration) 
Did the individual mix standards meet the linearity criteria for maximum percent difference (%D)? 
Yes[x] 
No 
Did the individual mix standards meet the retention time criteria? 
Yes[x] 
No 
Comments: 
None 
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Form.OCP-1.1.. 
300754 
Case Nunber: 95020 
Project Number: 29872 10.2 
Sile ID: bland Chemiod Cotnpai^ 
Performance Evaluation Mix Standards (Continuing Calibration) 
Did the performance evaluation mix standards meet the linearity criteria for maximum percent difference (%D)? 
Yes[x] 
No 
Did the performance evaluation mix standards meet the retention time criteria? 
Yes[x] 
No 
Comments: 
None 
Analytical Sequence 
Were standard and sample analyses performed following the correct analytical sequence? 
Yes[x] 
No 
Comments: 
None 
300755 
ocp_elec.ll 
12291994 1530 
Form OCP 1.1 
CaM Number: 95020 
Project Number: 29872 10.2 
Site DD: bbmd Chemical CompaiQr 
Surrogate Recoveries 
Were the surrogate spike recoveries within acceptance limits? 
Yes 
No[x] 
If the spike recoveries were unacceptable, were the samples reanalyzed? 
Yes 
No[x] 
Comments: 
The following surrogate recoveries outside the required 60-150% were reported: 
Sample ID 
RBSO/012495 * (SO0012) 
RBSO/012795 * (SO0127) 
SBBl/6-8/013195 (B16008) 
SBCl/0-1/012795 (ClOOOl) 
SBF2/12-15/012495 (F21215) 
SBF3/0-1/012495 (F30001) 
SBF3/0-1/012495MS (F30001MS) 
SBF3/0-1/012495MSD (KJOOOIMSD) 
TCXl 
15% 
56% 
TCX2 
50% 
48% 
14% 
56% 
50% 
DCBl 
52% 
49% 
16% 
2850% 
3400% 
3550% 
DCB2 
51% 
46% 
19% 
156% 
Therefore, the results in the above listed investigative samples were qualified as estimated (J). 
The prep bench sheet lists the surrogate standard ID, but not the concentration. When assuming that 
the lab used 20 ug/I surrogate as listed in the SOW Low Concentration Pest/PCB, then the surrogate 
recoveries calculate to the values the lab reported. No qualification of data. 
300756 
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12291994 1530 
Form OCP 1.1 
Caae Number: 95020 
Project Nunber. 29872 10.2 
Site ID: bbnd Cbenucal Oxnpary 
Matrix Spikes 
Were matrix spike analyses performed at the correct frequency and on a sample matrix representative of the 
samples in this sample deliveiy group (SDG)? 
Yes[x] 
No 
Were the matrix spike recoveries and relative percent differences (RPDs) within acceptance criteria? 
Yes 
No[x] 
Comments: 
The Low Level Method does not require matrix spike analyses, and the regular method recommends 
not to qualify on matrix spike recoveries alone. However, the matrix spikes performed were requested 
by the client and therefore it seems important to make an evaluation based on matrix spike recoveries. 
The Endrin recovery was -13% in the MS and MSD samples. The recovery for 4,4'-DDT was 152% 
in the MSD sample. It appears, that the sample matrix is interfering with the detection of Endrin, 
therefore^the non-detections of Endrin in the investigative samples were rejected (R), and reported 
detections are qualified as estimated (J). No detections were reported for 4,4'-DDT, therefore an 
estimated (J) qualification of 4,4'-DDT detections is not necessary. 
Blank Analyses 
Were the appropriate number of blank analyses performed? 
Yes[x] 
No 
Were instrument blanks analyzed at the correct frequency? 
Yes[x] 
No 
Were analytes reported in the blanks? 
Yes 
No[x] 
If analytes were reported in the blanks, were the same analytes also reported in the associated investigative 
samples? 
Yes 
No[x] 
Did the sample results require qualification due to the presence of analytes in the associated blank samples? 
Yes 
No[x] 
Comments: 
None 
300757 
. y 
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12291994 1530 
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Case Number: 95020 
Project Number: 29872 10.2 
Site ID: bland CbemiaU Cotnpany 
Instrument Performance 
Were the percent breakdowns for 4,4'-DDT and endrin correctly reported? 
Yes[x] 
No 
Were the percent breakdowns for 4,4'-DDT and endrin within acceptance limits? 
Yes[x] 
No 
Comments: 
None 
GPC and Florisil Cartridge Check 
Was GPC cleanup performed on the sample extracts? 
Yes[x] 
No 
Was the GPC column check acceptable? 
Yes[x] 
No 
NA 
Was a Florisil cartridge check performed? 
Yes[x] 
No 
Was the Florisil cartridge check acceptable? 
Yes[x] 
No 
NA 
Comments: 
None 
300758 
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Form OCP I.I 
Case Number 95020 
Project Number: 29872 10.2 
Site ID: bland Cbemioal Company 
Laboratory Control Samples 
Were LCS analyses performed? 
Yes[x] 
No 
Were the LCS recoveries within acceptable limits? 
Yes 
No[x] 
NA 
Comments: 
For the blank spike performed on 2-16-94, the recovery for Heptachlor Epoxide was 73%, below the 
required 74%. Therefore, the results for Heptachlor Epoxide in the investigative samples were 
qualified as estimated (J). 
Sample Results 
Were target analytes repiorted in the investigative samples? 
Yes[x] 
No 
Were chromatograms provided for all target analytes reported in the investigative samples? 
Yes[x] 
No 
Were chromatograms of acceptable quality and were analytes correctly identified? 
Yes[x] 
No 
Were the quantitated results for target analytes calculated using the appropriate standard and were the retention 
times (RTs) acceptable? 
Yes[x] 
No 
Comments: 
The analytical instrument is set up in such way, that the raw data concentration haJs been adjusted for 
extract volume, GPC factor, soil sample amount and percent moisture and lists the concentration in 
ug/kg (ppb-dry). A more standard approach is to have the raw data in ug/l, then concentrations can be 
more easily compared to each other. No qualification of data. 
300759 
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• 
• 
Caae Number: 95020 
Project Number: 29872 10.2 
Site ID: bland Chemical Cotnpany 
Calculation Check 
Initial Calibration 
Retention Time Window: were provided by lab, no calculation necessary 
%RSD: 2-10-95, DB-608, alpha BHC 
. 1466015 X 100 = 20.765% 
7060000 
Continuing Calibration, 2-2-95, 12:19, DB-1701, alpha BHC 
%D: 0.009-0.010 
x 100 = 11.11% 
0.009 
Surrogate Recovery, ClOOOl (VTF002), TCX 
190902 X 5000 x 2 
= 10.402 ug/kg 
7460000 x 30 X 0.82 
A 100% recovery of the surrogate would result in 
0.2 ng/ml X 0.2 ml X 5000 ul x 2 = 16.26 ug/kg 
30 g X 1 ul X 0.82 
therefore, 10.402 ug/kg = 63.97% surrogate recovery 
Matrix Spike Recovery, F30001MSD, 4,4'-DDT 
58.4 X 100 = 152.48% 
38.3 
RPD: for 126% and 152% is 18.7%RPD 
300760 
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Form OCP l.l 
Case Number: 95020 
Project Number: 29872 10.2 
Site ID: bland Cbemical Cofnpoi^ 
Sample Results 
CRQL: 
Positive Result: F30001, alpha Chlordane 
65946 X 5000 x 2 
= 3.89 
6480000 X 1 X 30x 0.87 
ocp_elcc. 11 
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Form OCP 1.1 
300761 
Case Number: 95020 
Project Number: 29872 10.2 
Site ID: bbuvl Chemical Company 
HOLDING TIME QUALIHCATIGN SUMMARY FORM 
OJ 
o 
o 
to 
Sample 
Identification 
RBSO/012495 RE 
RBSO/012795 RE 
Date 
Sampled 
1/24/94 
1/27/94 
Date 
Prepared 
2/20/94 
2/20/94 
Date 
Analyzed 
2/21/94 
2/21/94 
Prep. 
Holding 
Time 
27 days 
24 days 
Analysis 
Holding 
Time 
1 
1 
Qualifier 
J/UJ 
J/UJ 
Comments: 
None 
ocp_eleo.ll 
12291994 1530 
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Form OCP 1.1 
Case Number: 95020 
Project Number: 29872 10.2 
Site ID: btand Cbemioal Company 
INITIAL CALIBRATION QUALIFICATION SUMMARY FORM 
Date/Time 
2/10/94 
Instrument 
Analyte 
alpha BHC 
RF 
RSD 
20.8 % 
Samples Affected 
SBF2/12-15/012495 (F21215), SBF2/18-20/012495 (F21820), SBF3/0-
1/012495 (F30001), SBCl/0-1/012795 (ClOOOl), SBCl/16-18/012795 
(C11618), SBCl/18-20/012795 (C11820), SBCl/20-22/012795 (C12022), 
SBD4/0-1/012795 (D40001), SBD4/14-16/012795 (D41416), SBD4/20-
22/012795 (D42022), RBSO/013195 (BSO013) 
Qualifier 
J/UJ 
w 
o 
o 
Comments: 
None 
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Case Number: 95020 
Project Number: 29872 10.2 
Site ID: bland Chemical Company 
CONTINUING CALIBRATION QUALIHCATION SUMMARY FORM 
Date/Time 
Instrument 
Analyte 
>. 
%D 
Samples Affected 
Qualifier 
o 
2 
Comments: 
a\ 
None 
it:> 
ocp_elcc. 11 
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FomlOCP 1.1 
Case Number: 95020 
Project Number: 29872 10.2 
Site ID: bland Chemical Company 
BLANK SUMMARY FORM 
o 
o 
CJl 
Blank ID 
Analyte 
• 
Blank 
Result 
Units 
5 x 
Result 
Associated 
Samples 
Qualifier 
Comments: None 
ocp_clcc.ll 
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Form OCP l.l 
Case Number: 95020 
Project Number. 29872 10.2 
Site ID: bbnd Cbemical Cocnpany 
Summary and Conclusions 
The analytical results for the Pesticide/PCBs low level analyses are accetable for use as qualified. 
The results for the reanalyses of the investigative samples RBSO/012495 and RBSO/012795 were 
qualified as estimated (J) since the prep for these samples exceeded the hold time. 
The results for alpha-BHC in the investigative samples SBF2/12-15/012495 (F21215), SBF2/18-
20/012495 (F21820), SBF3/0-1/012495 (F30001), SBCl/0-1/012795 (ClOOOl), SBCl/16-18/012795 
(C11618), SBCl/18-20/012795 (C11820), SBCl/20-22/012795 (C12022), SBD4/0-1/012795 (D40001), 
SBD4/14-16/012795 (D41416), SBD4/20-22/012795 (D42022), and RBSO/013195 (BSO013) were 
qulifies as estimated (J) since the %RSD was exceede in the initial calibration. 
The results for the investigative samples RBSO/012495 (SO0012), RBSO/012795 (SO0I27), SBBl/6-
8/013195 (B16008), SBCl/0-1/012795 (C10001),SBF2/12-15/012495(F21215), and SBF3/0-1/012495 
(F30001) were qualified as estimated due to surrogate recoveries exceeding the QC criteria. 
Due to the negative recovery of Endrin in the matrix spike and matrix spike duplicate, the detection of 
Endrin in the investigative samples were qualified as estimated (J), while non-detections were rejected 
(R). 
The recovery of Heptachlor epoxide in the LCS sample was below the QC criteria. Therefore, the 
results for Heptachlor epoxide in the investigative samples were qualified as estimated (J). 
Validator's Signature: 
/ < i ^ V6w H y y C A ^ 
Validator's Initials: 
U M 
Validation Date: 
3 - 2 ^ - i S 
QC Reviewer's Signature: ^TPt^yLe/ ^ 
y y C A y / x . ^ 
QC Reviewer's Initials: 
M.PP 
Review Date: V - C - 
I T 
ocp_clcc. 11 
12291994 1530 
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Form OCP 1.1 
300766 
ID 
PESTICIDE ORGAMICS AMALYSIS DATA SHEET 
EPA SAMPLE MO. 
Lab Name: (? S E L I 
Code: PACE 
Case No.: HIA, 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.0 (g/mL) fi 
% Moisture: 12 
decanted: (Y/N) H 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Contract: HLA 
SAS No.: 
BlOOOl 
SDG No.: 95020 
Lab Sample ID: 
W G 0 0 2 
Lab File ID: 
Concentrated Extract Voliime: 
Injection Volume: 1.00 (uL) 
GPC Cleanup: (Y/N) 
5000 (UL) 
pH: 8.6 
Date Received: 
02/03/95 
Date Extracted: 02/06/95 
Date Analyzed: 
03/04/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) H 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) yg/Kg 
• 
3 1 9 - 8 4 - 6 — 
3 1 9 - 8 5 - 7 — 
3 1 9 - 8 6 - 8 — 
58-89-9 
76-44-8 
3 0 9 - 0 0 - 2 — 
1 0 2 4 - 5 7 - 3 -
9 5 9 - 9 8 - 8 — 
6 0 - 5 7 - 1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1 0 3 1 - 0 7 - 8 -
50-29-3 
72-43-5 
53494-70-5 
7 4 2 1 - 9 3 - 4 -
5 1 0 3 - 7 1 - 9 -
5 1 0 3 - 7 4 - 2 -
8 0 0 1 - 3 5 - 2 -
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5 
alpha-BHC 
beta-BHC_^ 
delta-BHC 
-gamma-BHC (Lindane) 
>Heptachlor 
-Aldrin 
-Heptachlor epoxide, 
-Endosulfan I 
~_ 
-Dieldrin 
-4,4* -DDE 
-Endrin 
-Endosulfan II 
•4,4' -DDD 
-Endosulfan sulfate 
-4,4' -DDT 
—Methoxychlbr__ 
-Endrin ketone 
—Endrin Aldehyde, 
—alpha-Chlordane_ 
—g2unma-Chlordane_ 
—Toxaphene 
—Aroclor-1016_ 
—Aroclor-12 21" 
—Aroclor-12 3 2^ 
—Aroclor-1242_ 
—Aroclor-1248^ 
—Aroclor-1254_ 
—Aroclor-1260 
_ 3 0 0 7 6 7 
VALIDATED; 
FORM I PEST Frv. 
Date 
d By yu^i^^h^ej^Q 
2-2e-fs 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
9D 
Neune: G S E L I 
Code: £A2E 
Case No.: HLA 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.o (g/mL) fi 
% Moisture: Ifi 
decanted: (Y/N) H 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Contract: HLA 
SAS No.: 
BlOlOl 
SDG No.: 95020 
Lab Sample ID: 
W G 0 0 4 
Lab Pile ID: 
Concentrated Extract Volume: 
Injection Volume: 1.00 (uL) 
GPC Cleanup: 
(Y/N) X 
5000 (uL) 
pH: 9.^ 
Date Received: 
02/03/95 
Date Extracted: 02/p6/95 
Date Analyzed: 
03/04/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) H 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
319-85-7 
319-86-8 
5 8 - 8 9 - 9 
7 6 - 4 4 - 8 
309-00-2 
1024-57-3 
959-98-8 
6 0 - 5 7 - 1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
7 2 - 4 3 - 5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
•' 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5 
-alpha-BHC 
-beta-BHC_2 
delta-BHC 
-gamma-BHC (Lindane) 
-Heptachlor 
-Aldrin 
-Heptachlor epoxide, 
-Endosulfan I 
~_ 
-Dieldrin 
-4,4*-DDE 
-Endrin 
-Endosulfan II 
-4,4 • -DDD 
-Endosulfan sulfate 
-4,4'-DDT. 
— M e t h o x y c h l o r 
Endrin ketone 
—Endrin Aldehyde, 
—alpha-Chlordane. 
—geunma-Chlordane' 
—Toxaphene. 
—Aroclor-1016_ 
—Aroclor-12 21] 
—Aroclor-1232] 
—Aroclor-1242] 
—Aroclor-1248] 
—Aroclor-1254] 
Aroclor-12 60' 
300768 
VALIDATED 
FORM I PEST Re-
Date 
J By 1^4^ 
S-Z^-fS 
ID 
PESTICIDE ORGANICS AMALYSIS DATA SHEET 
EPA SAMPLE NO. 
^ b Name: G S E L I 
Contract: HLA 
Case No.: HLA 
SAS No.: 
B12426 
Code: PACE 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.0 (g/mL) fi 
% Moisture: 12 
decanted: (Y/N) fi 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
SDG No.: 95020 
Lab Sample ID: WG005 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: 1.00 (uL) 
GPC Cleanup: 
(Y/N) X 
5000 (uL) 
pH: g.g 
Date Received: 02/03/95 
Date Extracted: 02/06/95 
Date Analyzed: 03/04/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) ^ 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) Vg/Kg 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
60-57-1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5— 
•alpha-BHC 
-beta-BHC_2 
delta-BHC 
-gamma-BHC (Lindane) 
-Heptachlor 
[ 
-Aldrin 
-Heptachlor epoxide, 
-Endosulfan I 
] 
-Dieldrin 
-4,4* -DDE 
•Endrin 
-Endosulfan II 
-4,4 • -DDD 
-Endosulfan sulfate 
•4,4' -DDT 
] 
—Methoxychlor_ 
—Endrin ketone 
—Endrin Aldehyde, 
—alpha-Chlordane] 
—gamma-Chlordane] 
-Toxaphene, 
—Aroclor-1016_ 
—Aroclor-1221] 
—Aroclor-1232] 
—Aroclor-1242] 
—Aroclor-1248] 
—Aroclor-1254' 
Aroclor-12 60 
2 . 1 
2 . 1 
2 . 1 
2 . 1 
2 . 1 
2 . 1 
2 . 1 
2 . 1 
4 . 1 
4 . 1 
4 . 1 
4 . 1 
4 . 1 
4 . 1 
4 . 1 
2 1 
4 . 1 
4 . 1 
2 . 1 
2 . 1 
10 
4 1 
&2 
4 1 
4 1 
4 1 
4 1 
4 1 
U 
U 
U 
U 
U 
U 
U J 
U 
U 
U 
JITK 
u u u u u u u u u u u u 
u u u u u 
300769 
VALIDATED 
FORM I PEST 
Revic.vcd By 
77^hy\ KiA.e7^/Qn 
Date 
3-2^-^.5 
ID 
PESTICIDE ORGAMICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
# 
Name: g S E L I 
Contract: HLA 
Case No.: HLA 
SAS No.: 
B16008 
Lab Code: PACE 
Matrix: (soil/water) S O I L 
Sample wt/vol: 
30.0 (g/mL) fi 
% Moisture: 2fi 
decanted: (Y/N) H 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
SDG No.: 95020 
Lab Sample ID: WG003 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: 1.00 (uL) 
GPC Cleanup: 
(Y/N) ^ 
5Q00 (UL) 
pH: 
9,2 
Date Received: 02/03/95 
Date Extracted: 02/06/95 
Date Analyzed: 03/04/95 
Dilution Factor: 
l.OO 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) 1L_ 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
60-57-1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5 
-alpha-BHC 
-beta-BHCj; 
delta-BHC 
-geunma-BHC (Lindane) 
-Heptachl or 
' 
-Aldrin 
-Heptachlor epoxide, 
-Endosulfan I 
] 
-Dieldrin 
-4,4' -DDE 
-Endrin 
-Endosulfan II 
-4,4' -DDD 
-Endosulfan sulfate 
-4,4' -DDT 
Methoxychlor_ 
Endrin ketone 
—Endrin Aldehyde, 
—alpha-Chlordane] 
—gamma-Chlordane, 
—Toxaphene 
—Aroclor-1016_ 
—Aroclor-12 21, 
—Aroclor-1232] 
—Aroclor-124 2, 
—Aroclor-1248, 
—Aroclor-1254] 
—Aroclor-1260 
300770 
FORM I PEST 
Revic 
Date 
VALI DATED" 
t'O^Uty^ ^ ' ^ - / ^ . 
?d By 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
elm 
Name: G s E L I 
Contract: fflLA. 
Case No.: HLA, 
SAS No.: 
BS0013 
Code: PACE 
Matrix: (soil/water) WATER 
Saunple w t / v o l : 
1000 
(g/mL) ML 
% Moisture: 
decanted: (Y/N) _ 
Extraction: 
(SepF/Cont/Sonc) 
CONT 
SDG No.: 95020 
Lab Sample ID: WGOOl 
Lab File ID: 
Concentrated Extract Volvune: 
Injection Volume: 1.00 (uL) 
GPC Cleanup: 
(Y/N) H 
2000 (UL) 
pH: $,9 
Date Received: 02/03/95 
Date Extracted: 02/06/95 
Date Analyzed: 02/16/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) H 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) 12S/L. 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
60-57-1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5— 
-—alpha-BHC 
beta-BHC " 
delta-BHC 
-gamma-BHC (Lindane) 
-Heptachlor 
-Aldrin 
-Heptachlor epoxide, 
-Endosulfan I 
] 
-Dieldrin 
-4,4'-DDE 
-Endrin 
-Endosulfan II 
•4,4' -DDD, 
-Endosulfan sulfate 
-4,4' -DDT 
Methoxychlor_ 
-—Endrin ketone 
-Endrin Aldehyde. 
—alpha-Chlordane] 
—gamma-Chlordane] 
—Toxaphene. 
—Aroclor-1016, 
—Aroclor-122l] 
—Aroclor-1232] 
—Aroclor-1242] 
—Aroclor-1248] 
—Aroclor-1254" 
Aroclor-1260 
.010 
.010 
.010 
.010 
.010 
.010 
.010 
.010 
.020 
.020 
.020 
.020 
.020 
.020 
.020 
0.10 
.020 
.020 
.010 
.010 
1.0 
0.20 
6.40 
0.20 
0.20 
0.20 
0.20 
0.20 
U J 
u u u u u 
UJ 
u u u 
u u u u u u u u u u u u u u u u u 
3 0 0 7 7 1 
FORM I PEST 
VALIDATED 
Revicv.cd By 
f^^orc-z^,^ 
Date 
3 ^ 2 y-fsS" 
hj^i/SO.^ 
ID J 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
i 
Name: G S E L I 
Code: PfrCE 
Case No.: HLA 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.0 (g/mL) fi 
% Moisture: Ifi 
decanted: (Y/N) li 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Contract: HLA 
SAS No.: 
ClOOOl 
SDG No.: 95020 
Lab Sample ID: VTF002 
Lab File ID: 
Concentrated Extract Volume: 
Injection volume: 1.00 (uL) 
GPC Cleanups 
(Y/N) I 
5000 (UL) 
pH: 10.4 
Date Received: 01/30/95 
Date Extracted: 02/03/95 
Date Analyzed: 02/20/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) H 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) Vg/Kg 
319-84-6 
aloha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
aamma-BHC (Lindane) 
76-44-8 
Heotachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4.4'-DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4. 4'-DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4.4'-DDT 
72-43 -5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehvde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
2.1 
2.1 
2.1 
2.1 
2.1 
2.1 
2.1 
2.1 
4.0 
4.0 
4.0 
4.0 
4.0 
4.0 
4.0 
21 
4.0 
4.0 
2.1 
2.1 
210 
40 
.81 
40 
40 
40 
40 
40 
u:] 
[ 
U 
U 
U 
U 
U 
U 
U 
UV/ 
U3 
yK 
U3 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
UV 
r 
U3 
FORM I PEST Re. 
Date 
300772 
VALIDATEp;; ~ 
..J Ey 
IZ:;W /WeY 3/90 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE MO. 
Name: g g E L I 
Contract: HLA 
C11618 
Code: PACE 
Case No.: HLA 
SAS No.: 
SDG No.: 95020 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.o (g/mL) fi 
% Moisture: 12 
decanted: (Y/N) fi 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Lab Sample ID: VTF003 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: 1.00 (uL) 
GPC Cleanup: 
(Y/N) X 
5000 (UL) 
pH: 9tQ 
Date Received: 01/30/95 
Date Extracted: 02/03/95 
Date Analyzed: 02/20/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) fi 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
' 
aaunma-BHC (Lindane) 
76-44 -8 
Heptachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4.4'-DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4.4'-DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4 .4 • -DDT 
72-43-5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehvde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
'• 
gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
1 11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
3.7 
3.7 
3.7 
3.7 
3.7 
3.7 
3.7 
19 
3.7 
3.7 
1.9 
1.9 
190 
37 
75 
' 37 
37 
37 
37 
37 
UJ 
U 
u 
u 
u 
u 
UJ 
u 
u 
u 
^ R 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
iu 
!u 
u 
300773 
FORM I 
PEST 
VALIDATE^-. 
Revic.vcd By I ' ^ J e ^ 
\{M.<Ly^ 
90 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE N O ; 
• 
Name: g S E L I 
Lab Code: PACE 
Case No.: 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.0 (g/mL) fi 
% Moisture: Ifi 
decanted: (Y/N) fi 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Contract: ULL. 
SAS No.: 
C11820 
SDG No.: 25020 
Lab Sample ID: VTF004 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: 1.00 (uL) 
GPC Cleanup: 
(Y/N) X 
5000 (uL) 
pH: 9.2 
Date Received: 01/30/95 
Date Extracted: 02/03/95 
Date Analyzed: 02/20/95 
Dilution Factor: 
1^Op 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) fi 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) Vg/Kg 
319-84-6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
qaunma-BHC (Lindaine) 
76-44-8 
Heptachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4,4'-DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4,4'-DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4.4'-DDT 
72-43-5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehvde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
gaunma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
2.1 
2.1 
2.1 
2.1 
2.1 
2.1 
2.1 
2.1 
4.0 
4.0 
4.0 
4.0 
4.0 
4.0 
4.0 
21 
4.0 
4.0 
2.1 
2.1 
210 
40 
81 
40 
40 
40 
40 
40 
UJ 
u 
u 
u 
u 
u 
UJ 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
FORM I PEST^^ • 
Date 
VALIDATED^ 
Z ' 2 2 - 1 S 
3/90 
300774 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
Name: G s E L l 
Lab Code: PACE 
Case No.: HIA 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.0 
(g/mL) fi^ 
% Moisture: 15 
decanted: (Y/N) fi 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Contract: filA. 
SAS No.: 
C12022 
SDG No.: 95020 
Lab Sample ID: 
VTF005 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: 
1.00 
(uL) 
GPC Cleanup: 
(Y/N) X 
5000 
(UL) 
pH: 
9»5 
Date Received: 
01/30/95 
Date Extracted: 02/03/95 
Date Analyzed: 
02/20/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) fi 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
60-57-1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5 
-alpha-BHC 
-beta-BHC_] 
delta-BHC 
-gamma-BHC (Lindane), 
•Heptachlor 
•Aldrin 
•Heptachlor epoxide, 
•Endosulfan I 
•Dieldrin 
-4,4' -DDE 
-Endrin 
-Endosulfan II 
-4,4' -DDD_! 
] 
-Endosulfan sulfate 
-4,4' -DDT 
] 
Methoxychlor_ 
Endrin ketone 
-Endrin Aldehyde, 
-alpha-Chlordane] 
•gamma-Chlordane] 
-Toxaphene 
] 
—Aroclor-1016, 
—Aroclor-12 21] 
—Aroclor-1232] 
—Aroclor-1242] 
—Aroclor-1248] 
—Aroclor-1254] 
—Aroclor-12 60" 
FORM I PES'fevi 
Date 
300775 
VALIDATED' 
.vcd By 
\''6yz>4c^ 
lUytiy'^'. 3/ao 
ID 
PESTICIDE ORGAMICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
Lab Name: G S E L I 
Contract: HLA 
Case No.: HLA 
SAS No.: 
D40001 
Code: PACE 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.0 (g/mL) fi 
% Moisture: 22 
decanted: (Y/N) fi 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
SDG No.: 95020 
Lab Sample ID: VTFQ06 
Lab File ID: 
Concentrated Extract Voliu&e: 
Injection Volume: l.OO (uL) 
GPC Cleanup: 
(Y/N) X 
5000 (UL) 
pH: 
9.g 
Date Received: 01/30/95 
Date Extracted: 02/03/95 
Date Analyzed: 02/20/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) fi^ 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) Vg/Kg 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
7 6 - 4 4 - 8 
309-00-2 
1024-57-3 
959-98-8 
6 0 - 5 7 - 1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
7 2 - 4 3 - 5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5 
-alpha-BHC 
-beta-BHC_] 
delta-BHC 
•gamma-BHC (Lindane) 
•Heptachlor 
\ 
-Aldrin 
-Heptachlor epoxide, 
-Endosulfan I 
] 
-Dieldrin 
-4,4'-DDE 
-Endrin 
-Endosulfan II 
-4,4' -DDD 
] 
-Endosulfan sulfate 
-4,4' -DDT 
] 
Methoxychlor 
Endrin ketone 
-Endrin Aldehyde, 
-alpha-Chlordane, 
-gaunma-Chlordane, 
-Toxaphene 
—Aroclor-1016, 
—Aroclor-12 21] 
—Aroclor-1232] 
—Aroclor-1242] 
—Aroclor-1248] 
—Aroclor-1254] 
-—Aroclor-12 60' 
300776 
FORM I PEST "^ 
Date 
I ' C y ' k ^ hi^^^^<^-/wQQ 
By %'28-^S 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
9 
Naune: G S E L I 
Contract: HLA 
D41416 
Lab Code: PACE 
Case No.: HLA 
SAS No.: 
SDG No.: 95020 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.0 (g/mL) fi 
* Moisture: 14 
decanted: (Y/N) fi 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Lab Sample ID: VTF007 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: 1.00 (uL) 
GPC Cleanup: (Y/N) 
5000 (UL) 
pH: 9»9 
Date Received: 01/30/95 
Date Extracted: 02/03/95 
Date Analyzed: 02/20/95 
Dilution Factor: 1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) fi 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
319-85-7 
319-86-8--
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
60-57-1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5— 
-alpha-BHC 
-beta-BHC_] 
delta-BHC 
-gamma-BHC (Lindane) 
-Heptachlor 
-Aldrin 
-Heptachlor epoxide, 
-Endosulfan I 
] 
-Dieldrin 
-4,4'-DDE 
-Endrin 
-Endosulfan II 
-4,4' -DDD, 
-Endosulfan sulfate 
-4,4' -DDT, 
Mcthoxychlor_ 
Endrin ketone 
—Endrin Aldehyde, 
—alpha-Chlordane] 
—gamma-Chlordane] 
—Toxaphene 
—Aroclor-1016. 
—Aroclor-12 21] 
—Aroclor-1232] 
—Aroclor-1242] 
—Aroclor-1248] 
—Aroclor-1254" 
Aroclor-1260 
300777 
FORM I PEST 
VALIDATEDJ 
J 
Reviewed By 
Date_^ll^ll£ 
^ ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
Lab 
Name: G S E L I 
Contract: fiLJL 
Case No.: HLA 
SAS No.: 
D42022 
Code: PACE 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.0 (g/mL) fi 
% Moisture: 15 
decanted: (Y/N) fi 
Extraction: 
(SepF/Cont/Sonc) 
gONC 
SDG No.: 95020 
Lab Saunple ID: VTFOOS 
Lab File ID: 
Concentrated Extract Volume: 
Injection Voltu&e: l.OQ (uL) 
GPC Cleanup: 
(Y/N) X 
5000 (uL) 
pH: 9.9 
Date Received: 01/30/95 
Date Extracted: 02/03/95 
Date Analyzed: 02/20/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) fi 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) Vg/Kg 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
6 0 - 5 7 - 1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
1 1 0 9 6 - 8 2 - 5 — 
-alpha-BHC 
-beta-BHC_] 
delta-BHC 
-gamma-BHC (Lindane) 
-Heptachlor 
\ 
-Aldrin 
-Heptachlor epoxide. 
-Endosulfan I 
] 
-Dieldrin 
-4,4'-DDE 
-Endrin 
-Endosulfan II_ 
•4,4' -DDD 
-Endosulfan sulfate 
-4,4' -DDT, 
Methoxychlor_ 
Endrin ketone 
-Endrin Aldehyde, 
—alpha-Chlordane] 
—geunma-Chlordane] 
—Toxaphene. 
—Aroclor-1016, 
—Aroclor-1221] 
—Aroclor-1232] 
—Aroclor-1242] 
—Aroclor-1248] 
—Aroclor-1254] 
Aroclor-1260" 
FORM I PEST 
Revic 
Date 
VALID 
wed By 
300778 
rrED 
-5-;;y-K 
y/ro-
ID 
PESTICIDE ORGAMICS AMALYSIS DATA SHEET 
EPA SAMPLE.NO, 
Jgb 
^Hb 
Name: G S E L I 
Code: PACE 
Case Mo.: HLA 
Matrix: (soil/water) S O I L 
Sample wt/vol: 
30.0 (g/mL) fi 
% Moisture: JZ 
decanted: (Y/N) fi 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Contract: fiXA. 
SAS No.: 
F21215 
SDG No.: 25020 
Lab Sample ID: VSR002 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: 1.00 (uL) 
GPC Cleanup: 
(Y/N) X 
5000 (UL) 
pH: 5.9 
Date Received: 01/27/95 
Date Extracted: 02/03/95 
Date Analyzed: 02/22/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) fi 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 
959-98-8 
60-57-1 
72-55-9 
72-20-8 
33213-65-9 
72-54-8 
1031-07-8 
50-29-3 
72-43-5 
53494-70-5 
7421-93-4 
5103-71-9 
5103-74-2 
8001-35-2 
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5 
-alpha-BHC 
•beta-BHCJ" 
delta-BHC 
.gamma-BHC (Lindane) 
-Heptachlor 
\ 
-Aldrin 
-Heptachlor epoxide, 
-Endosulfan I 
] 
-Dieldrin 
-4,4' -DDE_ 
-Endrin 
-Endosulfan II 
-4,4'-DDD 
-Endosulfan sulfate 
•4,4' -DDT, 
Methoxychlor_ 
-—Endrin ketone 
—Endrin Aldehyde, 
—alpha-Chlordane] 
—gamma-Chlordane, 
—Toxaphene, 
—Aroclor-1016_ 
—Aroclor-12 21] 
—Aroclor-1232] 
—Aroclor-1242] 
—Aroclor-1248] 
—Aroclor-1254, 
—Aroclor-12 60' 
300779 
FORM I PEST 
VA 
Reviewed By 
kjdcy^ 
Date 
-^'-^8~'^S 
V^° 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
Lab 
Name: G S E L I 
Contract: HLA 
Case Mo.: HLA^ 
SAS No.: 
F21820 
Code: SLSZ 
Matrix: (soil/water) S O I L 
Sample wt/vol: 
30.0 (g/mL) fi 
% Moisture: 14 
decanted: (Y/N) N 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
SDG No.: 95020 
Lab Sample ID: VSR003 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: 1.00 (uL) 
GPC Cleanup: 
(Y/N) X 
5000 (UL) 
pH: 7.0 
Date Received: 01/27/95 
Date Extracted: 02/03/95 
Date Analyzed: 02/22/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) fi 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
gamma-BHC (Lindane) 
76-44-8 
Heptachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4,4'-DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4,4'-DDD 
1031-07-8- 
Endosulfan sulfate 
50-29-3 
4,4'-DDT 
72-43-5-^ 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehyde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
geunma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
2,0 
2.0 
2.0 
2.0 
2.0 
2.0 
2.0 
2.0 
3.8 
3.8 
3.8 
3,8 
3.8 
3.8 
3.8 
20 
3.8 
3.8 
2.0 
2.0 
200 
3.8 
77 
38 
38 
38 
38 
38 
UJ 
U 
U 
U 
U 
U 
U3 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
300780 
FORM I PEST 
Revic.vcd By 
Date 
— 
VALIDATED 
|o^>^^t/L lUy.^/90 
3-28-9-^ 
ID 
PESTICIDE ORGAMICS ANALYSIS DATA SHEET 
lAh Na 
fPb> Cc 
Matrix 
Sample 
% Mois 
Extrac 
Concen 
Inject 
GPC Cl 
# 
me: G S E L I 
Contract: HLA 
de: PACE 
Case No.: HLA 
SAS No.: 
SDG 
: (soil/water) SOIL 
Lab Samole ID: 
wt/vol: 
30.0 (g/mL) g ... 
Lab File ID: 
ture: 13 
decanted: (Y/N) N 
Date Received: 
tion: 
(SeoF/Cont/Sonc) 
SONC 
Date Extracted 
itrated Extract Volume: 
5000 (uLi 
Date Analyzed: 
,ion Volume: 1.00 (uL) 
Dilution Facto: 
eanup: 
fY/N^ Y 
pH: 6.4 
Sulfur Cleanup 
CONCENTRATION UNITS: 
CAS NO. 
COMPOUND 
(ug/L or ug/Kg) Vg/K< 
319-84 -6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9— 
cramma-BHC (Lindane) 
76-44-8 
Heptachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4,4 • -DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4,4'-DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4,4 ' -DDT 
72-43-5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehvde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
EPA SAMPLE NO. 
F30001 
NO.: 25020 
VSR004 
01/27/95 
: 02/03/25 
02/22/95 
r: 
1.00 
: (VN) V 
5 
Q 
2.0 
2.0 
2.0 
2.0 
2.0 
2.0 
2.0 
2.0 
3.8 
3.8 
5.0 
3.8 
3.8 
3.8 
3.8 
20 
3.8 
4.0 
3.9 
4.1 
200 
38 
76 
38 
38 
38 
38 
38 
UD-
U 
U 
U 
U 
u 
u 
u 
u 
u 
P 
u 
u 
u 
u 
u 
u 
p 
p 
p 
u 
u 
u 
u 
u 
u 
U\ / 
UJ 
—---
FORM I PEST pev;„ 
Date 
3 0 0 7 8 1 
^/AUDATED 
d By 
iTu^itrui \Uy^Gy 
3/90 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
Lab 
Name: G S E L I 
Contract: HLA 
F31214 
Code: £2^fi£_ 
Case No,: HLJ^ 
SAS No.: 
SDG No.: 95020 
Matrix: (soil/water) SOIL 
Sample wt/vol: 
30.0 (g/mL) fi 
% Moisture: H 
decanted: (Y/N) U. 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
Lab Sample ID: VSR007 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: 1.00 (uL) 
GPC Cleanup: 
(Y/N) 
5000 (UL) 
pH: 9.5 
Date Received: 01/27/95 
Date Extracted: 02/03/95 
Date Analyzed: 03/04/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) fi 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) UG/KG 
319-84-6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
gamma-BHC (Lindane) 
76-44-8 
Heptachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4 .4 ' -DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4,4 ' -DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4,4 ' -DDT 
72-43-5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehvde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
—gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
3.7 
3.7 
3.7 
3.7 
3.7 
3.7 
3.7 
19 
3.7 
3.7 
1.9 
1.9 
190 
37 
74 
37 
37 
37 
37 
37 
U 
U 
U 
U 
U 
U 
U3 
U 
U 
U 
U 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
300782 
FORM I PEST 
Revic.vcd By 
Date — 
VALIjDATED. 
;d By 
l^^'^'kt^ riUt7'K/<in 
3-^^ - i s 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO, 
Name: G S E L I 
Contract: HIA. 
Case No.: HLA 
SAS No.: 
F31820 
Code: PACE 
Matrix: (soil/water) S O I L 
Sample wt/vol: 
30.o (g/mL) fi 
% Moisture: H 
decanted: (Y/N) fi 
Extraction: 
(SepF/Cont/Sonc) 
SONC 
SDG No.: 95020 
Lab Sample ID: VSR009 
Lab File ID: 
Concentrated Extract Volume: 
Injection Vol\ame: l.OO (uL) 
GPC Cleanup: 
(Y/N) X 
5000 (uL) 
pH: 8.6 
Date Received: 01/27/95 
Date Extracted: 02/03/95 
Date Analyzed: 03/04/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) fi 
Q -
CONCENTRATION UNITS: 
(ug/L or ug/Kg) Vg/Kg 
319-84-6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
gamma-BHC (Lindane) 
76-44-8 
Heptachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4,4 ' -DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4,4 • -DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4,4 • -DDT 
72-43-5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
—Endrin Aldehyde 
5103-71-9 
alpha-Chlordane ^ 
5103-74-2 
gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
1.9 
3.7 
3.7 
3.7 
3.7 
3.7 
3.7 
3.7 
19 
3.7 
3.7 
1.9 
1.9 
190 
37 
74 
37 
37 
37 
37 
37 
U 
U 
U 
U 
U 
U 
UJ 
U 
U 
U 
U 
U 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
300783 
FORM I PEST 
ncS( 
Date ... 
''ALIDATED 
-J By 
IT/^icn. tU7<L^^.^Q 
'2>-7-S-^3 
ID 
PESTICIDE ORGAMICS AMALYSIS DATA SHEET 
EPA SAMPLE NO. 
Name: G S E L I 
Contract: HLA 
Case No.: HLA_ 
SAS No.: 
S00012 
Lab Code: PACE 
Matrix: (soil/water) WATER 
Sample wt/vol: 
1000 
(g/mL) ML 
% Moisture: 
decanted: (Y/N) _ 
Extraction: 
(SepF/Cont/Sonc) 
CONT 
SDG No.: 95020 
Lab Sample ID: VSROOl 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volime: 1.00 (uL) 
GPC Cleanup: 
(Y/N) fi 
2000 (UL) 
pH: 7.0 
Date Received: 01/27/95 
Date Extracted: 01/30/95 
Date Analyzed: 02/03/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) fi 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) Vg/L 
319-84 -6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
gamma-BHC (Lindane) 
76-4 4-8 
Heptachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4,4'-DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4,4 ' -DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4 ,4 ' -DDT 
72-43 -5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehvde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
' 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.020 
0.020 
0.020 
0.020 
0.020 
0.020 
0.020 
0.10 
0.020 
0.020 
0.010 
0.010 
1.0 
0.20 
'0.40 
0.20 
0.20 
0.20 
0.20 
0.20 
UZ 
f 
u 
u 
u 
u 
u 
u 
u 
ui/ 
UJ 
UJ 
U 
U 
U 
U 
U 
u 
u 
D 
U 
U 
U 
U 
U 
U 
u / 
ua 1 
300784 
VAU 
FORM I PEST 
F.'. 
:--; By 
Date 
ipATEa^ 
JZrUv^ YJLMA 3/90 
l>'2^-'iS 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
Name: G s E L I 
Contract: HLA 
Case No.: HLA 
SAS No.: 
S00012RE 
Lab Code: PACE 
Matrix: (soil/water) WATER 
Sample wt/vol: 
420.0 (g/mL) ML 
% Moisture: 
decanted: (Y/N) _ 
Extraction: 
(SepF/Cont/Sonc) 
CONT 
SDG No.: 95020 
Lab Sample ID: VSROOIRE 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: 1.00 (uL) 
GPC Cleanup: 
(Y/N) fi 
2000 (uL) 
pH: 7.0 
Date Received: 01/27/95 
Date Extracted: 02/20/95 
Date Analyzed: 02/21/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) fi__ 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) Vg/L 
• 
319-84-6 
319-85-7 
319-86-8 
58-89-9 
76-44-8 
309-00-2 
1024-57-3 — 
959-98-8 
6 0 - 5 7 - 1 
72-55-9 
72-20-8 
3 3 2 1 3 - 6 5 - 9 -
72-54-8 
1031-07-8— 
50-29-3 
72-43-5 
53494-70-5 
7 4 2 1 - 9 3 - 4 -
5 1 0 3 - 7 1 - 9 -
5 1 0 3 - 7 4 - 2 -
8 0 0 1 - 3 5 - 2 -
12674-11-2 
11104-28-2 
11141-16-5 
53469-21-9 
12672-29-6 
11097-69-1 
11096-82-5 
—alpha-BHC 
—beta-BHC_] 
delta-BHC 
-gamma-BHC (Lindane) 
-Heptachlor 
-Aldrin 
-Heptachlor epoxide, 
-Endosulfan I 
] 
-Dieldrin 
-4,4' -DDE 
-Endrin 
. 
-Endosulfan II 
-4,4' -DDD 
-Endosulfan sulfate 
-4,4' -DDT. 
Methoxychlor__ 
Endrin ketone 
—Endrin Aldehyde, 
—alpha-Chlordane] 
—gamma-chlordane, 
—Toxaphene, 
—Aroclor-1016. 
—Aroclor-1221] 
—Aroclor-1232. 
—Aroclor-1242. 
—Aroclor-1248] 
—Aroclor-1254 
Aroclor-1260 
0.024 
0.024 
0.024 
0.024 
0.024 
0.024 
0.024 
0.024 
0.048 
0.048 
0.048 
0.048 
0.048 
0.048 
0.048 
0.24 
0.048 
0.048 
0.024 
0.024 
2.4 
0.48 
6.95 
0.48 
0.48 
0.48 
0.48 
0.48 
UJ 
u u u u u u u 
Uil/ 
U J 
\;3l 
U J 
u u u u u u u u u u u u u u u 
U j V 
3 0 0 7 8 5 
FORM I PEST 
Pf 
Date 
VALIDATED 
By JZ^m 
2 , ^ ^ - f S 
3/50" 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
LS 
Name: G S E L I 
Contract: HIA. 
SO0127 
Code: PACE 
Case No.: HIA, 
SAS No.: 
Matrix: (soil/water) WATER 
Sample wt/vol: 
1000 
(g/mL) ML 
% Moisture: 
decanted: (Y/N) 
Extraction: 
(SepF/Cont/Sonc) 
CONT 
SDG No.: 95020 
Lab Sample ID: VTFOOl 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volume: 1.00 (uL) 
GPC Cleanup: 
(Y/N) fi 
2000 (UL) 
pH: 5.9 
Date Received: 01/30/95 
Date Extracted: 02/01/95 
Date Analyzed: 02/03/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
sulfur Cleanup: (Y/N) fi 
Q 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) Vg/L 
319-84-6 
alpha-BHC 
319-8 5-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9— 
—gamma-BHC (Lindane) 
76-44-8 
Heptachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4 ,4 ' -DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4,4'-DDD 
1031-07-8-r 
Endosulfan sulfate 
50-29-3 
4,4 • -DDT 
72-43-5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehvde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
gamma-Chlordane 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.010 
0.020 
0.020 
0.020 
0.020 
0.020 
0.020 
0.020 
0.10 
0.020 
0.020 
0.010 
0.010 
1.0 
0,.20 
0.40 
0.20 
0.20 
0.20 
0.20 
0.20 
30 
\32 
U 
U 
U 
U 
U 
U 
U 
ui 
/ 
U J 
jtrR 
ua 
u 
u 
u 
u 
u 
u 
u 
ul 
u 
u 
u 
u 
u 
u 
Ul 
/ 
ua 
0786 
VALIDATED 
FORM I PEST 
R-
Dale 
By yrjz-r-c 
37^0-
3-2^~^S 
ID 
PESTICIDE ORGANICS ANALYSIS DATA SHEET 
EPA SAMPLE NO. 
^ 3 
sff 
Name: G S E L I 
Contract: HLA 
Case No.: HLA_ 
SAS No.: 
SO0127RE 
Code: PACE 
Matrix: (soil/water) H&IES 
Sample wt/vol: 
490.o (g/mL) M L 
% Moisture: 
decanted: (Y/N) _ 
Extraction: 
(SepF/Cont/Sonc) 
gONT 
SDG No.: 25020 
Lab Sample ID: VTFOOIRE 
Lab File ID: 
Concentrated Extract Volume: 
Injection Volvme: l.QQ (uL) 
GPC Cleanup: 
(Y/N) fi 
2000 (UL) 
pH: 5.9 
Date Received: 01/30/95 
Date Extracted: 02/20/95 
Date Analyzed: 02/21/95 
Dilution Factor: 
1.00 
CAS NO. 
COMPOUND 
Sulfur Cleanup: (Y/N) fi 
CONCENTRATION UNITS: 
(ug/L or ug/Kg) Vg/L 
319-84-6 
alpha-BHC 
319-85-7 
beta-BHC 
319-86-8 
delta-BHC 
58-89-9 
gamma-BHC (Lindane) 
76-44 -8 
Heptachlor 
309-00-2 
Aldrin 
1024-57-3 
Heptachlor epoxide 
959-98-8 
Endosulfan I 
60-57-1 
Dieldrin 
72-55-9 
4,4 ' -DDE 
72-20-8 
Endrin 
33213-65-9 
Endosulfan II 
72-54-8 
4,4 ' -DDD 
1031-07-8 
Endosulfan sulfate 
50-29-3 
4,4'-DDT 
72-43 -5 
Methoxychlor 
53494-70-5 
Endrin ketone 
7421-93-4 
Endrin Aldehvde 
5103-71-9 
alpha-Chlordane 
5103-74-2 
gamma-Chlordahe 
8001-35-2 
Toxaphene 
12674-11-2 
Aroclor-1016 
11104-28-2 
Aroclor-1221 
11141-16-5 
Aroclor-1232 
53469-21-9 
Aroclor-1242 
12672-29-6 
Aroclor-1248 
11097-69-1 
Aroclor-1254 
11096-82-5 
Aroclor-1260 
0.020 
0.020 
0.020 
0.020 
0.020 
0.020 
0.020 
0.020 
0.041 
0.041 
0.041 
0.041 
0.041 
0.041 
0.041 
0.20 
0.041 
0.041 
0.020 
0.020 
2.0 
0.41 
0.82 
0.41 
0.41 
0.41 
0.41 
0.41 
ua 
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300787 
VAL! 
FORM I PEST 
El 
Rev:_v.cd By _ 
Date 
l:ihjA 
3/90 
HLA DATA QUALITY ASSURANCE REVIEW SUMMARY 
Metals Analysis 
Case Number : 
^ I ^ Q | Q 
Project Number 2 ' ^ ^ I Z . ] O - Z 
Site: 
J L & w l 
r L ^ \ . ^ S ^ 
r ^ W j O / ^ . 
Contractor Laboratory: 
p / ^ C g ' 
^ lXP/£-
^Jzih^ 
Validator 
X 
U / J ^ c t t ^ 
Validation Date: 
QC Reviewer 'T^tTTCy ^ 
P^yTiTTc^ 
Review Date: 
v / p / f -r^ 
Sample Matrix: 
;
j
^ ( j Z ) 
VJcifjl^ 
(^^ 
EPA CL? vn c-ickH^ sovj^ yvl jL^.uxAM ^ Ci^y^JJi 
Analytical Methods: 
Sample Designations: 
OATZZLOZ-L. 
CZ-LiJrZLo 
Dlonri 1 
Dl iT-iU-
Dl^^'7_4-
VZnni^n 
D Z i q Z I 
D2>r)0nz. 
V2\n\Oi 
B l O o n ^ 
£12-02-2-
r\Z/0r)/Ol 
RBSOO/ 
SoonS 
S00ll(^ 
f>oo\7n 
SOO\ZS' 
Data for the above samples are: 
Acceptable for use 
^ 
Acceptable for use as qualified 
Unacceptable for use 
Is action required by the Preject Manager? 
Yes 
(No) 
Comments: 
1^ tyy\ cWc it^o.\ 
^ U i V c M lo c J". 
IDCt_l.dOC 
1Q141994 1035 
Form M E T I J 
300788 
DATA COMPLETENESS CHECKLIST 
X 
Included, no problems 
* 
Included, problems 
O 
Not included 
NA 
Not applicable 
Quality Control Summary 
X 
Case Narrative 
^ 
Chain of Custody Forms 
y 
Cover Page 
^ 
Holding Times 
X 
Inorganic Analysis Data Sheets 
X 
Initial and Continuing Calibration Summary 
y 
ICP and AA CRDL Check Standard Summary 
y 
Linear Range Verification Standard Summary 
j(f- 
Calibration and Preparation Blank Summary 
A 
ICP Interference Check Sample Summary 
•% 
Matrix Spike Summary 
i t 
Post Digestion Spike Sample Summary 
^ 
Duplicate Sample Simimary 
^ 
Laboratory Control Sample Sununary 
t^^A 
Method of Standard Additions Summary 
/ 
ICP Serial Dilution Summary 
Y 
Quarteriy Instrument Detection Limits Siunmary 
X 
Annual Interelement Correction Factors Summary 
X 
Quarteriy ICP Linear Range Summary 
X 
Sample Preparation Log Summary 
X 
Sample Analysis Rim Log Summary 
Sample Raw Data 
X 
ICP Raw Data 
X 
GFAA Raw Data 
X 
Mercury Raw Data 
X 
Cyanide Raw Data 
Comments: 
met \jdac 
101419^1035 
2 
Fom. MET 1.0 
300789 
SPECmC COMMENTS REGARDING ANALYSES 
Chain Of Custody 
Were samples property preserved aB4.^eived in good condition? 
Yes (No, 
Were custody transfers COTiecthr and completely documented? 
(Yes/ 
No 
Comments: " T ^ 
^ C Z 6 jU^^SCuudZli^ jt^^ofetCCnj' y^^^y^^c^^^y^^ ^ 
> ^ i / > ' * Y ^ 
lAuo-Axt^ oJUi MiA^^fll^^ J l ^ 
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Holding Times 
</ 
U 
' 
M 
Were sample preparations and analyses, performed within holding times? 
Yes Qfo) 
y7Xy\yyy\^cJi j^Oyy^^jJU^ ju>^\x OA^^iXcvi^^ yQ^euz^z)Jlji IH-' (f^yA 
YVOXA^CAAKoN 
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Harding Lawson Associates 
->-=—= Engineering and 
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SHEET 
OF 
JOB NO. 
PROJECT 
JM'UOyX.d CJUvd.JLy^dy^ f.ir»*^'y<!t^^ 
SUBJECT 
DATE 
3l^'^^|H9 
COMPUTED BY ( ^ . [ J l L i J t t ^ 
CHECKED BY 
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300791 
Instrument Calibration 
Were instruments caiibrat^M^y and each time that sample analyses were performed? 
(Yes\ 
No 
Were the instruments calibpt^ using the minimum required numbers of blanks and standards? 
/Yes) 
No 
For the GFAA methods wa§_Dne standard analyzed at the Conttact Required Detection Limit (CRDL)? 
/Yes) 
No 
For the applicable method^^^td. the correlation coefficients meet the minimum requirement of 0.995? 
(Vesy No 
NA 
For the cyanide analyses wjis-a. midrange standard distilled and analyzed? 
(Yes/ 
No 
Comments: 
— ^ 
"fiimALy 
Initial and Continuing Calibration Verification 
Were the calibration standards and blanks analyzed at the required frequencies? 
/Yesj 
No 
Were the standard recoverjeswithin QC limits? 
(^^es) 
No 
Comments: 
yVvc 
10141994 1035 
4 
^^"^ ^ ^ ^ *-^ 
300792 
CRDL Standards 
Were CRDL standards (CRI-and CRA) analyzed at the required frequency? 
(Yes/ 
No 
Were the ICP standards (Ot^analyzed at the required levels? 
(Yes} 
No 
For the low concentration.method, were the^CRDL results acceptable? 
Yes 
No 
( N A ) 
Comments: 
yitvAiy 
Matrix Spike 
Were matrix spike analyses performed at the correct frequency and on a sample matrix representative of the 
samples in this SDG? 
^_.^^ 
(Yes) 
No 
Were field or rinse blanks used forthe spike analysis sample? 
Yes 
TNO) 
Were the matrix spike recoveries within acceptance criteria? 
Yes 
( N O ) 
Were post-digestion spikes performed wherMc^uired? 
Yes 
No 
QiAj 
Comments: " J ^ 
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5 
. • - - - . 
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: 
300793 
Laboratory Control Sample 
Were laboratory control s^mijle analyses performed at the required frequency? 
Were laboratory control sample r^oxMy results acceptable? 
Yes 
T N O ) 
Comments: ( J U T 
\ Z O . O } % 
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J i ; ^ i ^ ju&(V\yuL^ydiyi~ ( f ^ ^ 
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ICP Interference Check Sample 
Were ICP interference ch^ek-samples (ICS) analysed at the required frequency? 
T Y C S ) 
NO 
Were the ICS recovery mieria met? 
CYQSA 
NO 
Were results greater than the IDL rcpoited for elements not present in the ICS solution? 
. ^ - ^ ^ ^ 
y 
'•Or 
& ) 
(
^ 
y ^ H r f 
tlohy 
Were negative results with absolute values greater than the IDL reported for elements not present in the ICS 
solution? 
^ - ^ ^ - - v 
(&\0r.Ff 
y,hr 
Were the concentrations o p n ^ s in the investigative samples similar to the concentrations of the ICS solution? 
! ^ 
Mfr 
i h h s 
Did the sample results require quaJifjcation due to interference problems? 
Yes ( ^ o j 
Comments: 
yi»w^ 
met_l Joe 
10141994 1035 
FOOT MET 
IJJ 
3 0 0 7 9 4 
Duplicate Sample Results 
Were duplicate sample apalyses performed at the required frequency? 
CY"esj 
No 
Did the duplicate sample.»9tilt;s meet acceptance criteria? 
(jTes) 
No 
: (UAC 
Comments: fjLu(XJ6uX<lV^At^y^l/0-tnA. JtO/wi-^C^tiL-yUdLLfctJ^ 
Were preparation and caUbnition blank analyses performed at the required frequency? 
(Yes) 
No 
Were elements reported in the bl^)ks>at levels above the CRDL? 
Yes 
Qio) 
Were elements reported iJHha.bIanks at levels between the IDL and the CRDL? 
(Yes) 
No 
Were negative results with.absolute values greater than the IDL reported in the blanks? 
(Yes) 
No 
If analytes were reported in the blanks, were the same analytes also reported for the associated investigative 
samples? 
^ 
Yes; 
No 
yvuixK^t^ 
^ 0{A\yLLC-, 
Did the sample results rea)UK>qualincation due to the presence of analytes in the associated blank samples? 
Comments: 
{ I j A y i ^ 
'^ 
" ^ 2 ^ ^ ^ ^ 
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^ 
^ 
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0 ^ 
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10141994 1035 
Foim MET 
Ii) 
3 0 0 7 9 5 
Harding Lawson Associates 
. •_ _ Engineering and 
s ; ~ 1? Environmental Services 
SHEET 
OF 
PROJECT. 
SUBJECT 
JOB NO. 
DATE 
COMPUTED BY 
CHECKED BY 
^
^
^ 
[Dx^/V2Jlut«staL XsiA'AyJji ' ^ X A i x S I ^ 
^QC 
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300796 
ICP Serial Dilution 
Were serial dilution analvsesfierformed at the required fr^uency? 
Cyesj 
No 
For analytes with concentrations greater than 50 times the IDL, were the percent differences within acceptance 
criteria? 
^ - > . 
(j'es) 
No 
Comments: 
IW^ 
GFAA QC 
Were duplicate injections peiformed for each GFAA sample analysis? 
( Y ^ 
No 
For results greater than theCWDL were the percent RSD results calculated correcdy and within control limits? 
(YeO 
No 
NA 
Were the GFAA analytical spike ^pest-digestion spike) recoveries within acceptance criteria? 
Yes 
(^o) 
If the GFAA analytical spike recoveries were not acceptable, were samples diluted and reanalyzed when 
required? 
^—^^ 
(Y^ 
^° 
Was tiie method of stand^xl-afMitions (MSA) used for GFAA analysis when required? 
Yes ) 
No ("H^A^^^-oJ^v^) 
When MSA analyses were performed, weretha correlation coefficients and spiking levels acceptable? 
Yes 
No Q^J^ 
Comments: Y b ^ - d-ZifUyd^J^-r^ A - ^ J y j L 
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8 
^ ° ^ *^^ ^-^ 
3 0 0 7 9 7 
Harding Lawson Associates 
• - . _- J Engineering and 
' " ; = 1 1 
Environmental Services 
SHEET 
OF 
PROJECT. 
SUBJECT 
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£10005' 
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133.0 
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JOB NO. 
DATE 3M/35: 
COMPUTED BYC 
CHECKED BY 
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300798 
fuJh 
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• - . _ - J Engineering and 
: s : =r 11 Environmental Services 
SHEET 
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DATE ^/W^r 
COMPUTED BY 
CHECKED BY 
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300799 
ICP Interelement Correction Factors 
Were annual interelement correction factors provided for each instrument used for sample analysis and were they 
current? 
fYes j 
No 
Comments: 
yu^ 
ICP Linear Ranges 
Were linear ranges providoLfor each instrument used for sample analysis and were they current? 
(Yes) 
No 
f 
Was a quarterly linear range>^rification analysis performed and if so, were the results acceptable? 
(Y£) No 
For the low concentration method was a linear range standard analysis performed as required, and if so, were the 
results acceptable? 
^—^ 
Yes 
No 
( N A ) 
Conunents: 
^ & v a 
Log Books 
Were all sample preparations-m-operly documented and performed in accordance with method protocols? 
(Yes") 
No 
Were all sample analyses jweperly documented and performed in accordance with metiiod protocols? 
(Ves^ 
No 
Comments: 
vW^ 
mct_laloc 
10141994 1035 
Q 
Form MET 1^ 
300800 
Sample Results 
Were target analytes reporte44n the investigative samples? 
(Yes) 
No 
Were the quantitated resitifs-lqr target analytes calculated and reported correctiy? 
(Yes) 
No 
NA 
For the applicable methods, were peak integrations performed correctiy? 
Yes 
No 
( N A ) 
Were detection limits provjd^ for tiie reported target analytes. and if so, were tiiey current and acceptable? 
(Yes) 
No 
Comments: 
tUn^ 
met Ixloc 
I014I994 1035 
10 
Fonn MET 1.0 
300801 
HOLDING TIME QUALIFICATION SUMMARY FORM 
u> 
o 
o 
00 
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Sample 
Identification 
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Blank ID 
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(units) 
Action Level 
Associated Samples 
Qualifier 
PBS 
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12 A 
F O T I M E T I . O 
BLANK SUMMARY FORM 
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Blank ID 
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10141994 1035 
\23 
FcraMETI.O 
Summary and Conclusions 
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Validation Date: 
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101419»4 1035 
13 
Fonn .MET 1.0 
300805 
_ Harding Lawson Associates 
CUCCT 
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=^ Engineering and 
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300806 
1^1 
U.S. EPA - CLP 
EPA SAMPLE NO. 
9 
C20001 
INORGANIC ANALYSIS DATA SHEET 
b Name: PACE 
Contract: 
| 
j 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095010 
Matrix (soil/water): SOIL 
Lab Sample ID: VTXOOl 
Level (low/med): 
LOW 
Date Received: 02/01/95 
% Solids: 
88.9 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
i 
1 
l
l
l
l 
jCAS No. 
1 Analyte |Concentration|C| Q 
jM | 
1 
I
I 
l
l
l
l 
17429-90-5 1 Aluminum | 
14700 II* 
IP 1 
17440-36-0 lAntimony | 
1.3 1 |W J" |F | 
17440-38-2 (Arsenic | 
1.5 | ^ 
1/ |F | 
17440-39-3 (Barium 
( 
112 II 
IP 1 
17440-41-7 IBerylliuml 
0.34 | I 
|F | 
17440-43-9 1 cadmium | 
3.0 | I* 
|P 1 
17440-70-2 ICalcium 1 
71800 | |* 
|P | 
17440-47-3 1 Chromium | 
18.9 | |* 
|P 1 
17440-48-4 ICobalt 
| 
12.4 | | 
|P | 
17440-50-8 ICopper 
| 
50.9 | | 
|P | 
17439-89-6 (Iron 
j 
26300 | j* 
|P 1 
17439-92-1 ILead 
| 
31.2 | | 
|F | 
17439-95-4 |Maqnesium| 
7650 1 1 * 
IP 1 
17439-96-5 |Manqanesel 
689 j j 
jP j 
17439-97-6 |Mercury | 
0.27 1 I 
ICVj 
17440-02-0 (Nickel 
1 
15.6 1 ( 
|P 1 
17440-09-7 JPotassiuml 
2460 | | 
|P 1 
(7782-49-2 | Selenium | 
3.1 UB-fN R 
|F ( 
(7440-22-4 (Silver 
( 
1.1 (U( 
IP ( 
(7440-23-5 (Sodium 
1 
416 (B| 
(P ( 
(7440-28-0 (Thallium ( 
0.61 (U(W J~ (F ( 
(7440-62-2 (Vanadium ( 
65.6 ( |* 
|P | 
(7440-66-6 IZinc 
| 
182 | j 
|P | 
(57-12-5 
(Cyanide | 
l.l (U( 3" (AS( 
1 
1 
1 
l
l
l
l 
Color Before: BROWN 
Color After: YELLOW 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
V 
Reviewed By 
Date 
FORM I - IN 
Texture: 
COARSE 
Artifacts: YES 
./iLfJTvLl. 
JA 
Z7^^5^ 
300807 
ILM02.0 
080005 
m 
b N2uae: PACE 
Lab Code: GULF 
Matrix (soil/water): SOIL 
Level (low/med): 
LOW 
% Solids: 
83.9 
U.S. EPA - CLP 
1 
INORGANIC ANALYSIS PATA SHEET 
Contract: 
Case No.: HLA 
SAS No.: 
EPA SAMPLE NO. 
C22022 
SDG No.: 095010 
Lab Sample ID: VTX002 
Date Received: 02/01/95 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
1 
l
l
l
i 
(CAS No. 
( Analyte (Concentration(C| Q 
(M ( 
1 
1 
1 
Mil 
(7429-90-5 (Aluminum ( 
11700 ( (* 
(P ( 
(7440-36-0 (Antimony ( 
0.33 (U|W 3" |F | 
17440-38-2 lArsenic | 
0.34 l.B-r IX IF 1 
17440-39-3 IBarium 
| 
106 1 J 
LP 1 
17440-41-7 IBerylliuml 
0.33 | t 
|F | 
17440-43-9 (Cadmium | 
1.9 | |* 
|P | 
17440-70-2 ICalcium 1 
12100 1 1 * 
IP 1 
17440-47-3 1 Chromium | 
18.8 | |* 
|P | 
17440-48-4 ICobalt 
| 
15.2 | | 
|P | 
(7440-50-8 ICopper 
| 
47.8 | | 
|P | 
17439-89-6 (Iron 
1 
20800 | |* 
|P | 
(7439-92-1 (Lead 
( 
3.9 | | 
(F | 
(7439-95-4 (Maqnesium( 
6290 ( 1 * 
|P | 
17439-96-5 |Manganese] 
291 | | 
|P | 
17439-97-6 [Mercury | 
0.14 | | 
(CV( 
(7440-02-0 (Nickel 
( 
12.5 ( ( 
(P ( 
(7440-09-7 (Potassium( 
1250 II 
IP 1 
17782-49-2 |Selenium | 
3.3 (JUfN K 
IF | 
(7440-22-4 (Silver 
| 
1.2 (Ui 
|P ( 
(7440-23-5 (Sodium 
( 
965 (B| 
(P ( 
(7440-28-0 (Thallium ( 
0.64 (U| 
|F | 
17440-62-2 IVanadium | 
90.0 | |* 
|P | 
(7440-66-6 (Zinc 
| 
45.8 i | 
|P ( 
157-12-5 
ICyanide | 
1.2 |U| X 
|AS| 
1 
t 
1 
i
l
l
! 
Color Before: BROWN 
Color After: YELLOW 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
MEDIUM 
Artifacts: YES 
I T ^ l ^ ^ ^ 
FORM I - 
IN 
300808 
ILM02.0 
030006 
U.S. EPA - CLP 
EPA SAMPLE NO. 
C22426 
INORGANIC ANALYSIS DATA SHEET 
b Name: PACE 
Contract: 
| 
l 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095010 
Matrix (soil/water): SOIL 
Lab Sample ID: VTX003 
Level (low/med): 
LOW 
Date Received: 02/01/95 
% Solids: 
86.0 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
ICAS No. 1 
1 
1 
17429-90-5 1 
17440-36-0 1 
17440-38-2 1 
17440-39-3 
17440-41-7 
17440-43-9 
17440-70-2 
17440-47-3 
17440-48-4 
17440-50-8 
17439-89-6 
17439-92-1 
17439-95-4 
17439-96-5 
17439-97-6 
17440-02-0 
17440-09-7 
17782-49-2 
17440-22-4 
17440-23-5 
17440-28-0 
17440-62-2 
17440-66-6 
157-12-5 
1 
1 
Analyte 1 
1 
Aluminum 1 
Antimony 
Arsenic 
Barium 
Beryllium 
Cadmium 
Calcium 
Chromiiim 
Cobalt 
Copper 
Iron 
Lead 
Magnesium 
Manganese 
Mercury 
Nickel 
Potassium 
Selenium 
Silver 
1 Sodium 
Thallium 
IVanadium 
[ Zinc 
1 Cyanide 
Concentration 
9980 
0.33 
0.91 
67.8 
0.36 
2.0 
5680 
18.6 
12.6 
47.1 
24500 
3.2 
5110 
354 
0.12 
14.1 
1040 
1 
0.33 
1 
1.2 
1 
586 
1 
0.63 
1 
131 
1 
50.9 
1 
1.1 
1 
C| 
1 
1 
Q 
1 1 
1* 
1 
U|W 
LBT r 1 
U 1 
1 
1 
1 
1* 
1* 
* 
* 
• * 
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IB 
Ur'NW R 
IU 
IB 
|U W X 
1 * 
|U r 
M 1 
P 1 
F 1 
F 1 
P 1 
F 1 
P 1 
P 1 
P 1 
P 1 
P 1 
P 1 
F 1 
P 1 
P 1 
CV| 
P 1 
|P 1 
|F 1 
|P 1 
|P 1 
|F 1 
|P 1 
|P 1 
(AS( 
1 1 
Color Before: BROWN 
Color After: YELLOW 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Reviewed By 
Date 
Texture: 
COARSE 
Artifacts: YES 
VAU DATED . 
FORM I - IN 
3 0 0 8 0 9 
ILM02.0 
080007 
•
^ 
Name: PACE 
Lab Code: GULF 
Matrix (soil/water): SOIL 
Level (low/med): 
LOW 
% Solids: 
90.9 
U.S. EPA - CLP 
1 
INORGANIC ANALYSIS DATA SHEET 
Contract: 
Case No.: HLA 
SAS No.: 
EPA SAMPLE NO. 
DlOOOl 
SDG No.: 095010 
Lab Sample ID: VSI002 
Date Received: 01/27/95 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
I 
1 
l
l
l
l 
(CAS No. 
1 Analyte |Concentration|C| Q 
|M | 
1 
1 
1 
l
l
l
l 
17429-90-5 1 Aluminum 1 
16100 1 1 * 
IP 1 
17440-36-0 lAntimony | 
0.31 |U|W T 
IF I 
17440-38-2 (Arsenic | 
1.2 (^ 
|^ IF | 
17440-39-3 IBarium 
| 
132 ( ( 
IP 1 
17440-41-7 IBerylliuml 
0.35 | | 
|F | 
17440-43-9 1 Cadmium ( 
2.8 ( (* 
(PI 
17440-70-2 ICalcium 1 
84500 | |* 
|P | 
17440-47-3 1 Chromium | 
19.8 | |* 
|P | 
17440-48-4 1 Cobalti 
| 
16.1 | I 
|P I 
17440-50-8 ICopper 
1 
45.1 1 1 
|P 1 
17439-89-6 (Iron 
| 
25400 | |* 
|P | 
17439-92-1 ILead 
| 
6.8 (I 
|F | 
17439-95-4 |Magnesium( 
8540 ( |* 
|P | 
17439-96-5 |Manqanese| 
976 | | 
|P | 
17439-97-6 [Mercury 1 
0.26 | | 
|CV| 
(7440-02-0 INickel 
| 
15.6 | | 
|P | 
17440-09-7 [Potassiuml 
1940 II 
IP 1 
[7782-49-2 [Selenium | 
3.1 UJfN R 
[F | 
17440-22-4 [Silver 
[ 
1.1 [Ul 
IP] 
[7440-23-5 [Sodium 
I 
557 [Bl 
[P [ 
[7440-28-0 [Thallium 1 
0.59 |U|W X 
|F [ 
(7440-62-2 [Vanadium [ 
99.4 | (* 
(P ( 
[7440-66-6 IZinc 
| 
89.5 | ( 
[P [ 
[57-12-5 
[Cyanide | 
1.1 |U| X 
|AS| 
1 
1 
1 
l
l
l
l 
Color Before: BROWN 
Color After: YELLOW 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Reviewed By 
Date 
Texture: 
COARSE 
Artifacts: YES 
FORM I - 
IN 
300810 
ILM02.0 
OSO'008 
U.S. EPA - CLP 
EPA SAMPLE NO. 
I 
m 
D11214 
INORGANIC ANALYSIS DATA SHEET 
b Name: PACE 
Contract: 
1 
1 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095010 
Matrix (soil/water): SOIL 
Lab Sample ID: VSI003 
Level (low/med): 
LOW 
Date Received: 01/27/95 
% Solids: 
82.9 
concentration Units (ug/L or mg/kg dry weight): MG/KG 
CAS No, 
7429-
7440-
7440-
7440-
7440-
7440-
7440-
7440-
7440-
7440-
7439-
7439-
7439-
7439-
7439-
7440-
7440-
7782-
7440-
7440-
7440-
7440-
7440-
-90-
•36-
-38-
-39-
-41-
-43-
•70-
-47-
-48-
-50-
-89-
-92-
-95-
-96-
-97-
-02-
-09-
-49-
-22-
-23-
-28-
-62-
-66-
-5 
-0 
•2 
-3 
-7 
-9 
-2 
-3 
-4 
-8 
-6 
-1 
-4 
-5 
-6 
-0 
-7 
-2 
-4 
-5 
-0 
-2 
-6 
57-12-5 
Analyte 
Aluminum 
Antimony 
Arsenic 
Barium 
Beryllium 
Cadmium 
Calcium 
Chromium 
Cobalt 
Copper 
Iron 
Lead 
Magnesium 
Manganese 
Mercury 
Nickel 
Potassium 
Selenium 
Silver 
Sodium 
Thallium 
Vanadium 
Zinc 
Cyanide 
Concentration 
13400 
0.46 
0.80 
187 
0.34 
3.5 
14700 
25.4 
23.0 
50.4 
32700 
4.7 
7320 
2070 
0.14 
20.9 
1250 
0.34 
1.2 
1200 
0.65 
194 
50.3 
1.2 
l ^ Z Q . 
1 
B|W 
1 
1 
1* 
U^NW R 
yi 
Bl 
Ul 
UJ 
r 
M 
F_ 
F_ 
P_ 
F_ 
P_ 
P_ 
P_ 
P 
P 
P 
F 
P 
P 
CV 
P 
P_ 
P 
F 
P 
P 
AS 
Color Before: BROWN 
Color After: YELLOW 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Reviewed By 
Date 
Texture: 
COARSE 
Artifacts: YES 
VAIIDATE 
%
^ 
]ArUA( 
FORM I - 
IN 
300811 
ILM02.0 
080009 
# 
b Name: PACE 
Lab Code: GULF 
Matrix (soil/water): SOIL 
Level (low/med): 
LOW 
% Solids: 
87.5 
U.S. EPA - CLP 
1 
INORGANIC ANALYSIS DATA SHEET 
Contract: 
Case No.: HLA 
SAS No.: 
EPA SAMPLE NO. 
D12224 
SDG No.: 095010 
Lab Sample ID: VSI004 
Date Received: 01/27/95 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
[CAS No. 
1 
1 
17429-90-5 1 
17440-36-0 
17440-38-2 
17440-39-3 
17440-41-7 
[7440-43-9 
17440-70-2 
17440-47-3 
(7440-48-4 
(7440-50-8 
(7439-89-6 
[7439-92-1 
[7439-95-4 
17439-96-5 
17439-97-6 
[7440-02-0 
[7440-09-7 
[7782-49-2 
[7440-22-4 
17440-23-5 
[7440-28-0 
[7440-62-2 
[7440-66-6 
(57-12-5 
1 
Analyte 
Aluminum 
Antimony 
Arsenic 
Barium 
Beryllium 
Cadmium 
Calcium 
Chromium 
Cobalt 
Copper 
Iron 
Lead 
Magnesium 
Manganese 
Mercury 
Nickel 
Potassium 
Selenium 
Silver 
Sodium 
Thallium 
Vanadium 
(Zinc 
Cyanide 
1 
Concentration 
16300 
0.45 
0.33 
121 
0.24 
3.4 
5820 
19.9 
15.2 
50.4 
33200 
2.9 
6700 
940 
0.11 
22.6 
1000 
0.32 
1.2 
1120 
1 
0.62 
1 
157 
1 
59.3 
1 
1.1 
1 
c\ 
1 
Q 
1* 
BIW 
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1 
1 
1* 
1* 
1* 
1 
1 
1 * 
1 
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1 
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1* 
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1 
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1 
p 1 
F 1 
F 1 
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F 1 
P 1 
P 1 
P 1 
P 1 
P 1 
P 1 
F I 
P 1 
P 1 
CV| 
P 1 
P 1 
|F [ 
|P 1 
|P 1 
|F 1 
|P 1 
|P 1 
|AS| 
Color Before: BROWN 
Color After: YELLOW 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Reviewed By 
Date 
FORM I - IN 
Texture: 
COARSE 
Artifacts: YES 
'bAk\^^ 
300812 
ILM02.0 
080010 
U.S. EPA - CLP 
EPA SAMPLE NO. 
^kib 
D20020 
INORGANIC ANALYSIS DATA SHEET 
Name: PACE 
Contract: 
I 
| 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095010 
Matrix (soil/water): SOIL 
Lab Sample ID: VQB003 
Level (low/med): 
LOW 
Date Received: 01/23/95 
% Solids: 
80.3 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
[CAS No. 
1 
1 
[7429-90-5 1 
17440-36-0 
[7440-38-2 
[7440-39-3 
[7440-41-7 
[7440-43-9 
[7440-70-2 
[7440-47-3 
[7440-48-4 
[7440-50-8 
[7439-89-6 
17439-92-1 
17439-95-4 
[7439-96-5 
[7439-97-6 
17440-02-0 
[7440-09-7 
[7782-49-2 
[7440-22-4 
[7440-23-5 
[7440-28-0 
[7440-62-2 
[7440-66-6 
[57-12-5 
1 
Analyte 
Aluminum i 
Antimony 
Arsenic 
Barium 
[ 
Beryllium( 
Cadmium 
Calcium 
Chromium 
Cobalt 
Copper 
Iron 
Lead 
Magnesium 
Manganese 
Mercury 
Nickel 
Potassium 
Selenium 
[Silver 
Sodium 
(Thallium 
[Vanadium 
1 Zinc 
1 Cyanide 
1 
Concentration 
18400 
0.35 
1.5 
98.3 
0.37 
1.9 
60600 
22.1 
18.9 
51.7 
26700 
5.9 
7530 
842 
0.15 
18.2 
2090 
3.5 
1.3 
558 
1 
0.67 
1 
116 
I 
66.3 
1 
1.2 
1 
C| 
1 
1 
Q 1 
1 
1* 
U|W 
LBt r 
\A 
1 
1 
1* 
1* 
1* 
1 
1 
1* 
1 . 
1* 
1 
1 1 
1 i 
LH1N R 
lUI 
IBl 
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1 1* 
1 1 
1U[ zr 
1 1 
M 1 
P 1 
F 1 
F 1 
P 1 
F [ 
P 1 
P 1 
P 1 
P 1 
P 1 
P 1 
F 1 
P 1 
P 1 
CV| 
P 1 
P 1 
F I 
|P 1 
|P 1 
|F 1 
|P 1 
|P 1 
|AS| 
1 1 
Color Before: BROWN 
Color After: YELLOW 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Reviewed By 
Date 
Texture: 
FINE 
Artifacts: YES 
VALIDATED 
FORM I - IN 
300813 
ILM02.0 
080011 
^^0) Name: PACE 
Lab Code: GULF 
Matrix (soil/water): SOIL 
Level (low/med): 
LOW 
% Solids: 
88.2 
U.S. EPA - CLP 
1 
INORGANIC ANALYSIS DATA SHEET 
Contract: 
Case No.: HLA 
SAS No.: 
EPA SAMPLE NO. 
D21921 
SDG No.: 095010 
Lab Sample ID: VQB004 
Date Received: 01/23/95 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
1 
l
l
l
l 
[CAS No. 
1 Analyte |ConcentrationlCl Q 
IM 1 
1 
1 
i 
l
l
l
l 
[7429-90-5 (Aluminum | 
10700 j (* 
|P 1 
17440-36-0 (Antimony | 
0.48 |B|W cr IF 1 
17440-38-2 (Arsenic ( 
0.66 [M- M 
IF 1 
17440-39-3 (Barium 
1 
131 11 
IP 1 
[7440-41-7 IBerylliuml 
0.26 | | 
|F | 
[7440-43-9 (Cadmium | 
2.6 | |* 
|P | 
[7440-70-2 ICalcium | 
5700 | |* 
[P | 
17440-47-3 1 Chromium [ 
19.9 | |* 
|P | 
[7440-48-4 (Cobalt 
| 
16.0 | | 
|P | 
[7440-50-8 [Copper 
1 
47.7 1 1 
[P [ 
[7439-89-6 [Iron 
I 
27400 [ [* 
|P [ 
[7439-92-1 ILead 
1 
4.0 II 
IF 1 
[7439-95-4 [MagnesiumI 
5480 | |* 
[P | 
[7439-96-5 |Manqanese| 
755 1 [ 
[PI 
[7439-97-6 [Mercury [ 
0.13 | [ 
|CV| 
[7440-02-0 (Nickel 
| 
16.7 | | 
|P [ 
[7440-09-7 [Potassiuml 
985 |B| 
|P | 
[7782-49-2 | Selenium | 
0.32 IJJtKW R |F | 
[7440-22-4 (Silver 
[ 
1.2 |U| 
|P [ 
[7440-23-5 (Sodium 
1 
780 |B| 
[P | 
[7440-28-0 [Thallium 1 
0.61 |U| 
IF | 
[7440-62-2 (Vanadium | 
141 [ |* 
jP ( 
(7440-66-6 (Zinc 
[ 
50.5 [ | 
[P | 
[57-12-5 
ICyanide ( 
1.1 |U| -J" |AS[ 
1 
1 
1 
l
l
l
l 
Color Before: BROWN 
Color After: YELLOW 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
MEDIUM 
Artifacts: YES 
VALIDATED). 
i%Mrf 
Reviewed By •—/ r -ii ».••• 
D=.e 
ZZM^ 
iMh-. 
FORM I - 
IN 
300814 
ILM02.0 
uS0012 
m 
b Name: PACE 
"Lab Code: GULF 
Matrix (soil/water): SOIL 
Level (low/med): 
LOW 
% Solids: 
88.7 
U.S. EPA - CLP 
1 
INORGANIC ANALYSIS DATA SHEET 
Contract: 
Case No.: HLA 
SAS No.: 
EPA SAMPLE NO. 
D30002 
SDG No.: 095010 
Lab Sample ID: VQA002 
Date Received: 01/23/95 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
I CAS No. 
[ 
1 
1 
(7429-90-5 1 
(7440-36-0 ( 
(7440-38-2 1 
(7440-39-3 ( 
(7440-41-7 
(7440-43-9 
(7440-70-2 
(7440-47-3 
[7440-48-4 
(7440-50-8 
17439-89-6 
17439-92-1 
[7439-95-4 
(7439-96-5 
(7439-97-6 
(7440-02-0 
(7440-09-7 
[7782-49-2 
(7440-22-4 
[7440-23-5 
(7440-28-0 
17440-62-2 
(7440-66-6 
(57-12-5 
1 
Analyte i 
Alviminum | 
Antimony | 
Arsenic [ 
Barium 
Beryllium 
Cadmium 
Calcium 
Chromium 
Cobalt 
Copper 
Iron 
Lead 
Magnesium 
Manganese 
Mercury 
Nickel 
Potassium 
Selenium 
Silver 
Sodium 
Thallium 
Vanadium 
1 Zinc 
1 Cyanide 
1 
Concentration 
12800 
0.32 
0.67 
99.7 
0.38 
1.7 
21900 
20.4 
15.4 
62.2 
23600 
5.4 
6250 
589 
0.13 
20.5 
1280 
3.2 
1.1 
497 
( 
0.61 
1 
98.1 
1 
56.7 
1 
1.1 
1 
1 
C| 
1 .. 
1 
Q 1 
1 
1* 
1 
U|MW 
^ 
f T 
M 
1 
1 
1* 
1* 
1* 
1 
1 
1* 
1 
1* 
1 
1 1 
1 1 
1 1 
U^N K 
lUI 
[Bl 
|U[W X 
1 1* 
1 1 
|U[ J" 
1 1 
M 1 
P 1 
F 1 
F 1 
P 1 
F 1 
P 1 
P I 
P 1 
P 1 
P 1 
P 1 
F 1 
P 1 
P 1 
CV( 
P 1 
P 1 
F 1 
|P 1 
[P 1 
(F 1 
[P 1 
[P 1 
|AS| 
Color Before: BROWN 
Color After: YELLOW 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
MEDIUM 
Artifacts: YES 
Reviewed 
Date 
^ o^. Cp^jrj^7>(t^1^ 
FORM I - IN 
300815 
ILM02.0 
080013 
U.S. EPA - CLP 
EPA SAMPLE NO. 
m 
b Name: PACE 
Lab Code: GULF 
Matrix (soil/water): SOIL 
Level (low/med): 
LOW 
% Solids: 
INORGANIC ANALYSIS DATA SHEET 
Contract: 
Case No.: HLA 
SAS No.: 
1 D31719 
SDG No.: 095010 
Lab Sample ID: VQA003 
Date Received: 01/23/95 
87.8 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
i 
1 
1 
l
l
l
l 
|CAS No. 
1 Analyte 1ConcentrationlCl Q 
|M 1 
1 
1 
i 
l
l
l
l 
17429-90-5 1 Aluminum | 
9350 | I* 
IP 1 
17440-36-0 lAntimony 1 
0.32 |U|W T 
[F I 
17440-38-2 [Arsenic | 
0.40 O f 
\j{ [F | 
17440-39-3 I Barium 
| 
140 II 
|P 1 
[7440-41-7 IBerylliuml 
0.30 | 1 
IF ( 
17440-43-9 (Cadmium ( 
1.6 1 1* 
IP 1 
17440-70-2 ICalcium 1 
4640 | I* 
[P [ 
17440-47-3 1 Chromium | 
18.0 I I* 
|P 1 
(7440-48-4 ICobalt 
1 
12.2 I I 
|P ( 
17440-50-8 (Copper 
| 
39.7 I I 
|P I 
[7439-89-6 [Iron 
| 
25000 | I* 
|P 1 
17439-92-1 JLead 
| 
3.9 j 1 
[F [ 
17439-95-4 [Magnesium( 
4340 [ 1 * 
|P [ 
(7439-96-5 (Manganesej 
1020 [ J 
|P I 
[7439-97-6 [Mercury | 
0.14 [ I 
|CV[ 
[7440-02-0 [Nickel 
j 
14.7 [ [ 
|P [ 
[7440-09-7 IPotassiumI 
602 IB| 
|P [ 
17782-49-2 [Selenium | 
0.32 UtJfNW R [F [ 
(7440-22-4 [Silver 
| 
1.2 [U| 
[P ( 
17440-23-5 (Sodium 
( 
610 (B( 
[P | 
17440-28-0 (Thallium ( 
0.62 (U[ 
[F [ 
[7440-62-2 [Vanadium [ 
137 | [* 
|P 1 
[7440-66-6 [Zinc 
| 
56.7 [ | 
|P [ 
[57-12-5 
(Cyanide [ 
1.1 [U| ;r [AS( 
1 
1
1 
l
l
l
l 
Color Before: BROWN 
Color After: YELLOW 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
Artifacts: YES 
Reviewed By ^ - ^ T H T P 
P- W V ^ M T , 
Date 
MMS^IZZZ 
FORM I - 
IN 
300816 
ILM02.0 
080014 
# 
b Neme: PACE 
Lab Code: GULF 
Matrix (soil/water): SOIL 
Level (low/med): 
LOW 
% Solids: 
92.9 
U.S. EPA - CLP 
1 
INORGANIC ANALYSIS DATA SHEET 
Contract: 
Case No.: HLA 
SAS No.: 
EPA SAMPLE NO. 
E10005 
SDG No.: 095010 
Lab Sample ID: VQC003 
Date Received: 01/23/95 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
1 
l
l
l
l 
(CAS No. 
1 Analyte (Concentration 1C| Q 
IM | 
1 
II 
llll 
17429-90-5 1 Aluminum 1 
16900 1 |* 
IP 1 
17440-36-0 lAntimony 1 
0.54 |B1W X 
IF 1 
17440-38-2 lArsenic | 
1.7 l.Br U 
IF 1 
(7440-39-3 IBarium 
| 
60.1 1 j 
IP 1 
(7440-41-7 IBerylliuml 
0.30 | | 
[F [ 
[7440-43-9 [Cadmium | 
4.0 | |* 
[P [ 
17440-70-2 ICalcium | 
35200 | [* 
|P ( 
(7440-47-3 (Chromium | 
17.5 | |* 
|P | 
17440-48-4 [Cobalt: 
1 
16.8 | | 
|P | 
[7440-50-8 ICopper 
| 
43.4 [ | 
[P [ 
(7439-89-6 [Iron 
1 
32200 | [* 
|P | 
17439-92-1 ILead 
[ 
89.9 | [ 
[F ( 
[7439-95-4 |Maqnesium| 
7920 | [* 
(P | 
17439-96-5 |Manganese[ 
791 | I 
|P I 
[7439-97-6 [Mercury [ 
0.11 |U| 
|CV| 
[7440-02-0 [Nickel 
| 
16.8 11 
|P [ 
(7440-09-7 [Potassiuml 
1470 [ [ 
|P [ 
17782-49-2 |Selenium [ 
3.0 UJfN K 
IF [ 
[7440-22-4 [Silver 
1 
1.1 |U| 
[P 1 
17440-23-5 ISodium 
[ 
358 |B| 
[P [ 
[7440-28-0 (Thallium [ 
0.58 [U( 
[F [ 
[7440-62-2 [Vanadium | 
88.0 | [* 
(P [ 
(7440-66-6 (Zinc 
[ 
555 [ [ 
|P | 
[57-12-5 
[Cyanide | 
1.1 |U| X 
iAS[ 
1 
1 
1 
l
l
l
l 
Color Before: BROWN 
Color After: YELLOW 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
Artifacts: YES 
Reviewed By 
Date 
FORM I - 
IN 
300817 
ILM02.0 
080015 
HLA DATA QUALITY ASSURANCE REVIEW SUMMARY 
Metals Analysis 
Case Number: 
95020 
Project Number: 
29872 10.2 
Site: 
Island Chemical Company 
Contractor Lab: 
Pace Environmental Laboratories, 
Validator: 
Kirsten Meier 
QC Reviewer: 
^AHA^yTct^ 7<^. ^ ^ y y T y i A 
St. Rosa, LA 
Validation Date: 
31 March 1995 
Review Date: 
^ ~ ^ " ? T^ 
Sample Matrix: 
water and soil 
Analytical Method: 
CLP metals, including Cyanide 
Sample Designations: 
RBSO/012495 * 
(SO0012) 
SBF3/12-14/012495 
(F31214) 
SBCl/0-1/012795 
(ClOOOl) 
SBD4/0-1/012795 
(D40001) 
SBBl/0-1/013195 
(BlOOOl) 
SBF2/12-15/012495 
(F21215) 
SBF3/18-20/012495 
(F31820) 
SBCl/16-18/012795 
(C11618) 
SBD4/14-16/012795 
(D41416) 
SBBl/6-8/013195 
(B16008) 
SBF2/18-20/012495 
(F21820) 
SBBl/24-26/013195 
(B12426) 
SBCl/18-20/012795 
(Cll820) 
SBD4/20-22/012795 
(D42022) 
SBBlOl/0-1/013195 
(BlOlOl) 
SBF3/0-1/012495 
(F30001) 
RBSO/012795 * 
(SO0127) 
SBCl/20-22/012795 
(C12022) 
RBSO/013195 * 
(BS0013) 
* = aqueous sample 
( ) = Sample ID on Form I 
Data for the above samples are: 
[ ] 
Acceptable for use 
[x] 
Acceptable for use as qualified 
[ ] 
Unacceptable for use 
Is action required by the Project Manager? 
Yes 
No[x] 
Comments: 
The investigative sample were analyzed following the CLP ILM02.0 methods and the data was 
reviewed in accordance with the Functional Guidelines, February 1994. Calibration requirements for 
mercury were obtained from the July, 1988 version of the Functional Guidelines. 
The metals Antimony, Arsenic, Beryllium, Lead, Selenium and Thallium were analyzed by GFAA. 
Ilict_elec. 11 
12291994 0940 
300818 
Form MET 1.1 
, CaK Numlier: 95020 
Projea Number: 29872 10.2 
Site ID: bbnd Cbemical Company 
DATA COMPLETENESS CHECKLIST 
[x] 
Included, no problems 
[*] 
Included, problems 
[O] 
Not included 
[NA] 
Not applicable 
Quality Control Summary 
X 
Case Narrative 
* 
Chain of Custody Forms 
X 
Cover Page 
X 
Holding Times 
X 
Inorganic Analysis Data Sheets 
* 
Initial and Continuing Calibration Summary 
^x 
ICP and AA CRDL Check Standard Summary 
X 
Linear Range Verification Standard Summaiy 
* 
Calibration and Preparation Blank Summaiy 
X 
ICP Interference Check Sample Summary 
* 
Matrix Spike Summary 
* 
Post Digestion Spike Sample Summary 
* 
Duplicate Sample Summary 
* 
Laboratory Control Sample Sunimaiy 
x 
Method of Standard Additions Summary 
* 
ICP Serial Dilution Summary 
X 
Quarterly Instrument Detection Limits Summaiy 
X 
Annual Interelement Correction Factors Summary 
X 
Quarterly ICP Linear Range Summary 
X 
Sample Preparation Log Summary 
* 
Sample Analysis Run Log Summary 
Sample Raw Data 
X 
ICP Raw Data 
* 
GFAA Raw Data 
X 
Mercury Raw Data 
X 
Cyanide Raw Data 
Comments: 
None 
mct_ekc.ll 
12291994 0940 
2 
FotmMETl.l 
300819 
I Caie Number: 95020 
Project Number 29872 10.2 
Site ID: Island Chemical Company 
SPECIHC COMMENTS REGARDDSTG ANALYSES 
Chain Of Custody 
Were samples properly preserved and received in good condition? 
Yes[x] 
No 
Were custody transfers correctly and completely documented? 
Yes[x] 
No 
Comments: 
The submitted Chain of Custody forms were not signed and dated by the lab. No qualification of data. 
Holding Times 
Were sample preparations and analyses performed within holding times? 
Yes[x] 
No . 
Comments: 
None 
mct_tlec.ll 
12291994 0940 
3 
Fonn MET 1.1 
300820 
iCaae Number 95020 
Project Nunber 29872 10.2 
Site ID: bland Cbemical Company 
Instrument Calibration 
Were instruments calibrated daily and each time that sample analyses were performed? 
Yes[x] 
No 
Were the instruments calibrated using the minimum required numbers of blanks and standards? 
Yes[x] 
No 
For the GFAA methods was one standard analyzed at the Contract Required Detection Limit (CRDL)? 
Yes[x] 
No 
For the applicable methods did the correlation coefficients meet the minimum requirement of 0.995? 
Yes[x] 
No 
NA 
For the cyanide analyses was a midrange standard distilled and analyzed? 
Yes[x] 
No 
NA 
Comments: 
For the GFAA calibrations the lab chose non-linear correlation, the correlation coefficients were 
> 0.995 for this type of calibration. No qualification of data. 
Initial and Continuing Calibration Verification 
Were the calibration standards and blanks analyzed at the required frequencies? 
Yes[x] 
No 
Were the standard recoveries within QC limits? 
Yes[x] 
No 
Comments: 
On Form II (page 080028) the cyanide ICV recovery is listed as 55%; that is a typo, the true 
concentration is 20 ug/l which results in 110% recovery. No qualification of data. 
metelec.ll 
12291994 0940 
4 
Fonn MET 1.1 
300821 
Cue Number. 95020 
Project Number 29872 10.2 
Sits ID: bland Cbemical Company 
CRDL Standards 
Were CRDL standards (CRI and CRA) analyzed at the required frequency? 
Yes[x] 
No 
Were the ICP standards (CRI) analyzed at the required levels? 
Yes[x] 
No 
For the low concentration method, were the CRDL results acceptable? 
Yes 
No 
NA[x] 
Comments: 
None 
Matrix Spike 
Were matrix spike analyses performed at the correct frequency and on a sample matrix representative of the 
samples in this SDG? 
Yes 
No[x] 
Were field or rinse blanks used for the spike analysis sample? 
Yes 
No[x] 
Were the matrix spike recoveries within acceptance criteria? 
Yes 
No[x] 
Were post-digestion spikes performed when required? 
Yes[x] 
No 
NA 
Comments: 
For Mercury the matrix spikes were performed on samples not belonging to this SDG. No further 
qualification of data. 
The soil spike recoveries for Cyanide were 58.7%, 71.2%, and 0% recovery. Therefore, detections of 
Cyanide reported in the investigative soil samples were qualified as estimated (J), while non-detections 
were rejected (R). 
roct_elec.ll 
12291994 0940 
5 
Fonn MET l.l 
300822 
Cue Number 95020 
Project Number 29872 10.2 
Site ID: bbnd Cbetmod Company 
The following analytes had soil spike recoveries outside the QC criteria of 75-125% 
Analyte 
Antimony 
Arsenic 
Cadmium 
Copper 
Lead 
Selenium 
Vanadium 
% Recovery 
17.9 
0 
68.4 
26.1 
62 
25 
132.3 
Qualifier 
J/R 
J/R 
J/UJ 
J/R 
J/UJ 
J./R 
J/-
Therefore, the qualifiers listed in the above table were applied to all of the associated investigative soil 
samples. 
The post digestion spike recoveries for Cadmium (63.4%), Copper (75.2%) and Vanadium (71.9%) 
were low, however qualification under the Functional Guidelines is not necessary. 
The water spike reoveries for antimony (127.7%) and beiyllium (74%) were outside the acceptance 
range. Therefore, the detections of antimony and beryllium inthe investigative water samples were 
qualified as estimated (J). Non-detected beryllium results were qualified as estimated (UJ), while non-
detected antimony results are acceptable and not qualified. 
met_elec.ll 
12291994 0940 
Fonn MET 1.1 
300823 
Caae Number 95020 
Project Numhcn 29872 10.2 
Site ID: bbnd Cbemical Conxparty 
Laboratory Control Sample 
Were laboratoiy control sample analyses performed at the required frequency? 
Yes[x] 
No 
Were laboratory control sample recovery results acceptable? 
Yes 
No[x] 
Comments: 
The aqueous LCS recovery for Potassium was 120.6%, exceeding the limit of 120.0%. Therefore, 
detections of Potassium in the investigative water samples were qualified as estimated (J). 
The soil LCS recovery for Cyanide was 11.4 mg/kg, below the limit of 30 mg/kg and represents a 
recovery of 15.4%. In accordance with the functional guidelines, the soil Cyanide data is unusable and 
was rejected (R). 
ICP Interference Check Sample 
Were ICP interference check samples (ICS) analysed at the required frequency? 
Yes[x] 
No 
Were the ICS recovery criteria met? 
Yes[x] 
No 
Were results greater than the IDL reported for elements not present in the ICS solution? 
Yes[x] 
No 
Were negative results with absolute values greater than the IDL reported for elements not present in the ICS 
solution? 
Yes[x] 
No 
Were the concentrations of metals in the investigative samples similar to the concentrations of the ICS solution? 
Yes 
No[x] 
Did the sample results require qualification due to interference problems? 
Yes 
No[x] 
Comments: 
None 
iDCt_elec.il 
12291994 0940 
7 
' 
J 
W U «J *• "* 
Fonn MET 1.1 
300824 
Cue Number: 95020 
Project Number 29872 10.2 
Sile ID: bbnd Cbemical Company 
Duplicate Sample Results 
Were duplicate sample analyses performed at the required frequency? 
Yes[x] 
No 
Did the duplicate sample results meet acceptance criteria? 
Yes 
No[x] 
Comments: 
The following analytes exceeded the criteria for duplicate analysis: 
Alumium (22.9% RPD), Cadmium (75.3% RPD), Chromium (29.1% RPD), Copper (39.6% RPD), 
Iron (63.2% RPD), Lead (145.5% RPD), Nickel (>lxCRDL) and Zinc (55.1% RPD). Therefore, the 
results for these analytes in the investigative soil samples were qualified as estimated (J). 
Blank Analyses 
Were preparation and calibration blank analyses performed at the required frequency? 
Yes[x] 
No 
Were elements reported in the blanks at levels above the CRDL? 
Yes 
No[x] 
Were elements reported in the blanks at levels between the IDL and the CRDL? 
Yes[x] 
No 
Were negative results with absolute values greater than the IDL reported in the blanks? 
Yes[x] 
No 
If analytes were reported in the blanks, were the same analytes also reported for the associated investigative 
samples? 
Yes[x] 
No 
Did the sample results require qualification due to the presence of analytes in the associated blank samples? 
Yes[x] 
No 
Comments: 
See table "Blank Summary Form" for blank contamination and qualifiers added. 
inct_eWc.ll 
^ 
12291994 0940 
8 
FormMEri.l 
300825 
Cue Number: 95020 
Project Number 29872 10.2 
Site ID: bbmd Chemical Company 
ICP Serial DUution 
Were serial dilution analyses performed at the required frequency? 
Yes[x] 
No 
For analytes with concentrations greater than 50 times the IDL, were the percent differences within acceptance 
criteria? 
Yes 
No[x] 
Comments: 
The duplicate analysis for Zinc resulted in 11.0% difference, outside the QC criteria of 10%. 
Therefore, the results for Zinc in the investigative samples were qualified as estimated (J). 
GFAAQC 
Were duplicate injections performed for each GFAA sample analysis? 
Yes[x] 
No 
For results greater than the CRDL were the percent RSD results calculated correctly and within control limits? 
Yes[x] 
No 
NA 
Were the GFAA analytical spike (post-digestion spike) recoveries within acceptance criteria? 
Yes 
No[x] 
If the GFAA analytical spike recoveries were not acceptable, were samples diluted and reanalyzed when 
required? 
Yes 
No[x] 
Was the method of standard additions (MSA) used for GFAA analysis when required? 
Yes[x] 
No 
When MSA analyses were performed, were the correlation coefficients and spiking levels acceptable? 
Yes[x] 
No 
Comments: 
For the following analytes the analytical spike recovery exceeded the criteria of 85-115% and the 
samples were not reanalyzed at a dilution: 
metelec.ll 
- 
- - 
~^ 
12291994 0940 
9 
' 
FonnMETl.l 
300826 
Owe Number 95020 
Project Nunber: 29872 10.2 
Site ID: bbnd Chemical Cotnpai^ 
Analyte 
Antimony 
Arsenic 
Arsenic 
Lead 
Lead 
Lead 
Lead 
Selenium 
Selenium 
Selenium 
Selenium 
Selenium 
Selenium 
Selenium 
Selenium 
Selenium 
Selenium 
Thallium 
Thallium 
Thallium 
Sample ID 
SO0127 
C11820 
D42022 
F21820 
F31820 
ClOOOl 
B16008 
F21820 
F31214 
F31820 
ClOOOl 
C11618 
C11820 
D42022 
BlOOOl 
B16008 
B12426 
S00012 
S00127 
BS0013 
Spike Recovery 
81.3 
121.5 
118.1 
84.1 
81.2 
80.0 
81.2 
72.5 
45.8 
79.0 
76.2 
77.9 
84.3 
79.3 
78.0 
53.0 
47.3 
81.8 
81.0 
79.3 
Qualifier 
J/UJ 
J/-
J/-
J/UJ 
J/UJ 
J/UJ 
J/UJ 
J/UJ 
J/UJ 
J/UJ 
J/UJ 
J/UJ 
J/UJ 
J/UJ 
J/UJ 
J/UJ 
J/UJ 
J/UJ 
J/UJ 
J/UJ 
The above listed qualifiers were applied to the appropriate analytes in the associated investigative 
samples. 
ii*t_elcc.ll 
12291994 0940 
10 
FormMEri.l 
300827 
•Caje Number 95020 
Project Number 29872 10.2 
Sile ID: bbnl Chemical Company 
ICP Interelement Correction Factors 
Were annual interelement correction factors provided for each instrument used for sample analysis and were 
they current? 
Yes[x] 
No 
Comments: 
None 
ICP Linear Ranges 
Were linear ranges provided for each instrument used for sample analysis and were they current? 
Yes[x] 
No 
Was a quarterly linear range verification analysis performed and if so, were the results acceptable? 
Yes[x] 
No 
For the low concentration method was a linear range standard analysis performed as required, and if so, were 
the results acceptable? 
Yes 
No 
NA[x] 
Comments: 
None 
Log Books 
Were all sample preparations properly documented and performed in accordance with method protocols? 
Yes[x] 
No 
Were all sample analyses properly documented and performed in accordance with method protocols? 
Yes 
No[x] 
Comments: 
For the GFAA analyses the date and time when the standards were prepped was not noted on the raw 
data. No qualification of data. 
mct_clec.ll 
12291994 0940 
H 
Fonn MET 1.1 
300828 
'Cue Number: 95020 
Project Nunber 29872 10.2 
Sile ID: bbnd Chemical Company 
Sample Results 
Were target analytes reported in the investigative samples? 
Yes[x] 
No 
Were the quantitated results for target analytes calculated and reported correctly? 
Yes[x] 
No 
NA 
For the applicable methods, were peak measurements performed correctly? 
Yes 
No 
NA[x] 
Were detection limits provided for the reported target analytes, and if so, were they current and acceptable? 
Yes[x] 
No 
Comments: 
None 
metelec.ll 
' 
12291994 0940 
1 2 
iFonnMETLl 
300829 
Que Number: 95020 
Project Number: 29872 10.2 
Sile ID: bbnd Chemical Company 
HOLDING TIME QUALIFICATION SUMMARY FORM 
o 
o 
00 
o 
Sample 
Identification 
Analyte 
. 
Date 
Sampled 
Date 
Prepared 
Date 
Analyzed 
Analysis 
Holding 
Time 
Qualifier 
Comments: 
None 
mel_ctco.ll 
12291994 0940 
13 
FomiMEr 1.1 
Cue Number: 95O20 
Project Number: 29872 10.2 
Sile ID: bland Chemical Company 
BLANK SUMMARY FORM 
Blank ID 
ICB 
CCB 
C C B 
ICB 
CCB 
ICB 
CCB 
CCB 
Prep Blank Water 
Prep Blank Water 
Prep Blank Soil 
Analyte 
Chronuum 
Lead 
Magnesium 
Selenium 
Alumium 
Arsenic 
Beryllium 
Copper 
Beryllium 
Lead 
Zinc 
Blank Result 
[ug/l] 
4.1 
1.9 
27.8 
-1.5 
-21.1 
2.4 
0.1 
-19.9 
0.804 
0.970 
2.291 mg/kg 
Action Level 
4.1 mg/kg or 20.5 ug/l 
1.9 mg/kg or 9.5 ug/l 
27.8 mg/kg or 139 ug/l 
1.5 mg/kg or 7.5 ug/l 
21.1 mg/kg or 105.5 ug/l 
2.4 mg/kg or 12 ug/l 
O.I mg/kg or 0.5 ug/l 
19.9 mg/kg or 99.5 ug/l 
4.02 ug/l 
4.85 ug/l 
11.455 mg/kg 
Associated Samples 
all investigative samples 
all investigative samples 
all investigative samples 
all investigative samples 
all investigative samples 
all investigative samples 
all investigative samples 
all investigative samples 
all water samples 
all water samples 
all soil samples 
Qualifier 
U 
U 
U 
U 
U 
u 
u 
u 
u 
u 
u 
Comments: 
^ 
Detections of the listed analytes in the investigative sample below the action level were qualified as undetected (U) due to blank contamination. 
w 
o o 
00 
w 
TOl_eleo.ll 
12391994 0940 
14 
Forni MET l.l 
' Cue Number: 95020 
Project Number: 29872 10.2 
Sile ID: bbuxl Chemical Company 
Summary and Conclusions 
The analytical results for the metal analyses are acceptable for use as qualified. 
The data for Mercury was rejected (R) in accordance with the Functional Guidelines, because the initial 
calibration was performed with less standards than the method requires. 
Due to low spike recoveries, the detections of Antimony, Arsenic, Copper, Selenium and Cyanide 
reported in the investigative samples were qualified as estimated (J), while non-detections were rejected 
(R). 
Due to low spike recoveries, the results for Cadmium and Lead in the investigative samples were 
qualified as estimated (J). 
Due to high spike recoveries,the detections of Vanadium in the investigative samples were qualified as 
estimated (J). 
Detections of Potassium in the investigative samples were qualified as estimated (J), since the LCS 
recovery exceeded the upper QC limit. 
The results for Mercury in the soil investigative samples were rejected (R), due to very low recovery of 
the soil LCS. 
The soil results for the analytes Alumium, Cadmium, Chromium, Copper, Iron, Lead, Nickel and Zinc 
were qualified as estimated (J), because the duplicate analysis exceeded the QC criteria. 
Blank contamination was observed for several analytes and detections in the investigative samples below 
the action level were qualified as undetected (U). See table "Blank Summary Form" for detailed 
information. 
The results for Zinc in the investigative samples were qualified as estimated (J), since the duplicate 
analysis ecxeeded the QC criteria. 
The analytical spike recoveries for several analytes did not meet the QC criteria and the results for 
these analytes were qualified. See table in report for details. 
Validator's Signature: 
[i^y-> WvL 
l U A c X ^ 
Validator's Initials: 
1 / H 
• 
Validation Date: 3 - 3 / - - ^ 
QC Reviewer's Signature: ^^?t<^,y^^ y=>. y y C / y ^ 
QC Reviewer's Initials: 
P ^ P P 
Review Date: 
i - Q . - 
f T 
mct_elcc.ll 
12291994 0940 
15 
Form MET l.l 
300832 
t^ b Name: PACE 
Lab Code: GULF 
Matrix (soil/water): SOIL 
Level (low/med): 
LOW 
% Solids: 
81.4 
U.S. EPA - CLP 
1 
INORGANIC ANALYSIS DATA SHEET 
Contract: 
Case No.: HIA 
SAS No.: 
EPA SAMPLE NO. 
BlOOOl 
SDG No.: 095020 
Lab Sample ID: WG002 
Date Received: 02/03/95 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
l
.
l 
l
l
l
l 
|CAS No. 
1 Analyte |ConcentrationjC| 
Q 
jM | 
1 
1 
1 
I
I
I
! 
17429-90-5 1 Aluminum | 
23300 | | * J 
|P j 
17440-36-0 lAntimony | 
0.34 UJIN'R 
|F | 
17440-38-2 lArsenic 
1 
0.27 L»|NR 
|F | 
17440-39-3 1 Barium 
| 
197 I I 
IP 1 
17440-41-7 1 Beryllium! 
0.32 | j 
|F | 
17440-43-9 1 Cadmium 
| 
2.8 j |N*:J 
|P | 
17440-70-2 ICalcium 
| 
17800 | j 
jP | 
17440-47-3 1 Chromium j 
19.9 | |* 3 
jP j 
17440-48-4 ICobalt 
| 
29.6 | | 
|P j 
17440-50-8 ICopper 
| 
54.5 | jN*3 
jP | 
17439-89-6 |Iron 
\ 
32100 | I* U 
IP | 
17439-92-1 ILead 
| 
3.4 | |NS*:7 
|F | 
17439-95-4 |Maqnesium| 
7260 I I 
jP 1 
17439-96-5 |Manganese| 
1860 | | 
|P | 
17439-97-6 |Mercury 
| 
0.29 | | 
|CV| 
17440-02-0 INickel 
1 
19.2 1 1* a 
|P | 
17440-09-7 IPotassiumI 
4180 I I 
IP 1 
17782-49-2 | Selenium ] 
0.34 |JB1NWR 
IF 1 
17440-22-4 ISilver 
| 
1.3 |U| 
|P | 
17440-23-5 ISodium 
| 
575 |B| 
|P | 
17440-28-0 (Thallium 1 
0.66 jUj 
|F | 
17440-62-2 IVanadium | 
109 | JNJ 
jP j 
17440-66-6 IZinc 
| 
72.7 | |E*J 
|P 1 
157-12-5 
ICyanide 
| 
1.2 
|J»iNR 
|AS| 
1 
1 
1 
l
l
l
l 
Color Before: BROWN 
Color After: BROWN 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
Artifacts: YES 
^ 
Lo>'^ 
/ALIDATED 
• - y 
jAjs.f<;>VL tUy.(. 
FORM I - 
IN 
300833 
ILM02.0 
080005 
t ab Name: PACE 
Lab Code: GULF 
Matrix (soil/water): SOIL 
Level (low/med): 
LOW 
% Solids: 
83.9 
U.S. EPA - CLP 
1 
INORGANIC ANALYSIS DATA SHEET 
Contract: 
Case No.: HLA 
SAS No.: 
EPA SAMPLE NO. 
I BlOlOl 
I 
SDG No.: 095020 
Lab Sample ID: WG004 
Date Received: 02/03/95 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
jCAS No. 
i Analyte jConcentration!cj Q 
JM j 
17429-90-5 1 Aluminum 1 
28200 1 I*J 
JJ> 1 
17440-36-0 lAntimony j 
0.33 UJ1NR 
IF | 
17440-38-2 lArsenic | 
1.5 tBlN^R IF 1 
17440-39-3 IBarium 
| 
268 1 | 
jp 1 
17440-41-7 IBerylliuml 
0.58 | | 
|F | 
17440-43-9 1 Cadmium 1 
3.1 | |N*a 
IP | 
17440-70-2 ICalcium | 
12200 j | 
jP 1 
17440-47-3 1 Chromium I 
21.911*.7 
|P1 
17440-48-4 ICobalt 
1 
31.7 1 | 
IP 1 
17440-50-8 ICopper 
1 
58.4 1 IN*"! IP ! 
17439-89-6 1 Iron 
| 
37000 1 | * tl 
IP | 
17439-92-1 ILead 
| 
7.1 1 |N*-3 
|F 1 
17439-95-4 IMaqnesium! 
7760 1 | 
|P 1 
17439-96-5 jManqanesel 
2100 II 
|P | 
17439-97-6 [Mercury | 
0.12 |U| 
|CV| 
17440-02-0 INickel 
| 
24.7 | |*3 
|P | 
17440-09-7 IPotassiumI 
4330 II 
IP 1 
17782-49-2 |Selenium j 
3.3 1-^1 N-R 
|F | 
17440-22-4 ISilver 
1 
L.2 |U| 
|P | 
17440-23-5 ISodium 
1 
702 1B| 
|P 1 
17440-28-0 IThallium 1 
0.64 lUl 
|F I 
17440-62-2 IVanadium | 
110 j jN 7 
|P | 
17440-66-6 IZinc 
| 
3620 1 1E*3 
|P 1 
157-12-5 
ICyanide | 
1.2 IITINR 
1AS| 
Color Before: BROWN 
Color After: BROWN 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
Artifacts: YES 
VALIDATED 
Revic.vcd By 
\<7A-yP(yVL 
k x / ^ 
Date 
-?--;^rf^ 
FORM I - 
IN 
300834 
ILM02.0 
0S0003 
U.S. EPA - CLP 
EPA SAMPLE NO. 
« 
1 B12426 
1 
INORGANIC ANALYSIS DATA SHEET 
Tab Name: PACE 
Contract: 
1 
1 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095020 
Matrix (soil/water): SOIL 
Lab Sample ID: WG005 
Level (low/med): 
LOW 
Date Received: 02/03/95 
% Solids: 
80.7 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
1 
l
l
l
l 
ICAS No. 
1 Analyte |ConcentrationlC| Q 
IM | 
1 
1 
1 
l
l
l
l 
17429-90-5 1 Aluminum | 
17600 | |*7 
|P 1 
17440-36-0 lAntimony | 
0.35 |if1NK 
IF | 
17440-38-2 lArsenic I 
0.27 lyjNR 
|F j 
17440-39-3 IBarium 
1 
87.4 1 1 
IP 1 
17440-41-7 IBerylliuml 
0.36 | | 
IF | 
17440-43-9 1 Cadmium I 
3.0 | |N*3 
|P I 
17440-70-2 ICalcium 1 
6550 | | 
IP 1 
17440-47-3 1 Chromium 1 
28.2 1 1*J 
IP 1 
17440-48-4 ICobalt 
| 
16.4 | | 
IP | 
17440-50-8 ICopper 
| 
47.3 1 IN*!! 
|P 1 
17439-89-6 1 Iron 
1- 
33100 | 1 * r; 
|P 1 
17439-92-1 ILead 
| 
2.8 | |N*3 
|F | 
17439-95-4 |MagnesiumI 
7070 | | 
|P 1 
17439-96-5 |Manganese| 
545 | | 
IP | 
17439-97-6 1 Mercury | 
0.12 |U| 
|CV1 
17440-02-0 INickel 
| 
18.1 1 1 * :7 
|P I 
17440-09-7 IPotassiumI 
1130 |B| 
IP 1 
17782-49-2 | Selenium I 
0.35 IJBINWR 
IF 1 
17440-22-4 ISilver 
1 
1.3 |U| 
|P | 
17440-23-5 ISodium 
| 
1220 IBl 
IP 1 
17440-28-0 IThallium | 
0.67 |U1 
IF 1 
17440-62-2 IVanadium 1 
162 | \UT 
|P 1 
17440-66-6 IZinc 
| 
53.6 | IE*J J^P 1 
157-12-5 
ICyanide 1 
1.2 l-t^fNR. 
1AS| 
1 
1 
1 
l
l
l
l 
Color Before: BROWN 
Color After: BROWN 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
Artifacts: YES 
Pevis'.ved By 
Date . . — ^ 
VALIDATED 
l/(y~,K>tyL 
h/jy. 
3-3>l~-lS_ 
FORM I - 
IN 
300835 
ILM02.0 
nPnno*:» 
U.S. EPA - CLP 
EPA SAMPLE NO. 
% 
B16008 
INORGANIC ANALYSIS DATA SHEET 
b Name: PACE 
Contract: 
1 
j 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095020 
Matrix (soil/water): SOIL 
Lab Sample ID: WG003 
Level (low/med): 
LOW 
Date Received: 02/03/95 
% Solids: 
72.3 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
1 
l
l
l
l 
|CAS No. 
1 Analyte |ConcentrationlC| 
Q 
|M | 
1 
1 
1 
l
l
l
l 
17429-90-5 1 Aluminum 1 
26400 1 1*3" 
|P 1 
17440-36-0 lAntimony 1 
0.39 I^INR 
IF 1 
17440-38-2 lArsenic 
| 
0.30 UriNK 
IF 1 
17440-39-3 IBarium 
| 
111 I I 
IP 1 
17440-41-7 IBerylliuml 
0.35 1 | 
IF | 
17440-43-9 1 Cadmium 
| 
3.8 | |N*J 
|P 1 
17440-70-2 ICalcium 
| 
35400 | | 
|P | 
17440-47-3 1 Chromium | 
27.2 | | * 3 
IP 1 
17440-48-4 ICobalt 
1 
18.7 1 1 
IP | 
17440-50-8 ICopper 
1 
60.2 1 |N*X T 1 P 1 
17439-89-6 |Iron 
| 
39500 | 1*3 
|P 1 
17439-92-1 ILead 
| 
1.8 
| INW*!;^ |F | 
17439-95-4 |Magnesiuml 
10800 | 1 
|P 1 
17439-96-5 jManganesej 
739 | | 
|P | 
17439-97-6 |Mercury 
| 
0.16 | | 
1CV| 
17440-02-0 INickel 
1 
18.9 | | * 3 
IP 1 
17440-09-7 IPotassiumI 
2520 1 1 
IP 1 
17782-49-2 | Selenium | 
0.39 lU^NWR 
|F | 
17440-22-4 ISilver 
| 
1.4 
1U| 
IP 1 
17440-23-5 1 Sodium 
| 
2140 j | 
IP | 
17440-28-0 l.Thallium 1 
0.75 |U| 
|F 1 
17440-62-2 (Vanadium | 
165 ( (N3 
(P | 
(7440-66-6 jzinc 
j 
76.3 | |E*3 
IP 1 
157-12-5 
ICyanide 
| 
1.4 
|^NT?. 
|AS| 
1 
1 
1 
l
l
l
l 
Color Before: BROWN 
Color After: BROWN 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
Artifacts: YES 
VALIDATED 
Rev:-'.'.'cd By 
Date, 
3 - 3 ^ - 
f ^ 
k ^ ' ^ y ^ 
c 
FORM I - 
IN 
300836 
; ILM02.0 
080008 
U.S. EPAX--CLP: 
1 ^ A r 
INORGANIC ANALYSISIDATA SHEET 
EPA SAMPLE NO. 
Name: PACE 
Lab Code: GULF 
Case No.: HLA 
Contract: 
SAS No.: 
I 
I BS0013 
SDG No.: 095020 
Lab Sample ID: WGOOl 
Date Received: 02/03/95 
Matrix (soil/water): WATER 
Level (low/med): 
LOW 
% Solids: 
0.0 
/[ 
Concentration Units (ug/L omng/kg dry weight) : UG/L 
1 
1 
1 
II 
II 
ICAS No. 
1 Analyte |Concentration 1c1 Q 
IM | 
1 
1 
1 
l
l
l
l 
(7429-90-5 (Aluminum ( 
54.2 |c/l 
IP ( 
17440-36-0 lAntimony ( 
0.28 (UIN 
(F ( 
(7440-38-2 (Arsenic [ 
0.22 (UI 
|F | 
17440-39-3 IBarium 
I 
1.8 |U1 
IPI 
17440-41-7 IBerylliuml 
0.02 |U|N*:r 
IF I 
17440-43-9 (Cadmium I 
0.62 1U| 
IP 1 
17440-70-2 ICalcium 1 
- 11.9 |B| 
IP 1 
17440-47-3 (Chromium ( 
1.4 (^C 
IP 1 
17440-48-4 (Cobalt 
1 
1.9 (Uj 
(P I 
[7440-50-8 (Copper 
( 
3.3 1U| 
(P | 
17439-89-6 |Iron 
| 
6.4 1U| 
|P I 
(7439-92-1 (Lead 
( 
0.14 (^IC/ 
(F ( 
17439-95-4 [MagnesiumI 
5.2 (Ul 
IP [ 
(7439-96-5 (Manganese( 
0.52 (Uj 
|P I 
[7439-97-6 [Mercury ( 
0.20 |U| 
|CV| 
[7440-02-0 [Nickel 
1 
2.6 [Ul 
[P I 
[7440-09-7 [Potassixml 
105 |UI 
|P I 
[7782-49-2 [Selenium [ 
0.28 [Ul 
IF 1 
17440-22-4 [Silver 
[ 
1.0 |U| 
IP I 
[7440-23-5 [Sodium 
1 
67.9 |U| 
|P I 
[7440-28-0 [Thallium 1 
0.54 lUIWJ 
IF | 
17440-62-2 IVanadium | 
0.90 1U| 
|P I 
[7440-66-6 [Zinc 
j 
2.4 |B| 
|P [ 
[57-12-5 
ICyanide 1 
10.0 |U| 
|AS| 
1 
1 
1 
II 
I I 
Color Before: COLORLESS 
Color After: COLORLESS 
Conments: 
Clarity Before: CLEAR 
Clarity After: CLEAR 
• 
Texture: 
Artifacts: NO 
VALlDATEp^ 
••y 
LaltJ 
3 -Ayj-'IS 
FORM I - IN 
300837 
j ILM02.0 
0S0009 
U.S. EPA - CLP 
EPA SAMPLE NO. 
% 
1 ClOOOl 1 
INORGANIC ANALYSIS DATA SHEET 
ab Name: PACE 
Contract: 
| 
1 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095020 
Matrix (soil/water): SOIL 
Lab Sample ID: VTF002 
Level (low/med): 
LOW 
Date Received: 01/3 0/95 
% Solids: 
81.6 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
jCAS No. 
j Analyte jconcentrationjcj Q JM 1 
17429-90-5 1 Aluminum [ 
22200 1 1*3 [P 1 
17440-36-0 lAntimony 1 
0.42 1B|N3 1F| 
17440-38-2 [Arsenic [ 
0.27 I^INPv 
IF | 
[7440-39-3 [Barium 
[ 
119 [ J 
[P 1 
i 7440-41-7 IBerylliuml 
0.03 \y^HA 
\F \ 
17440-43-9 1 Cadmium 1 
3.5 1 [N*:] [P [ 
17440-70-2 ICalcium 1 
37500 1 | 
[P [ 
[7440-47-3 [Chromium [ 
22.6 | 1*3 |P 1 
17440-48-4 ICobalt 
| 
18.9 1 | 
IP 1 
17440-50-8 [Copper 
[ 
54.8 | IN*3 |P | 
[7439-89-6 1 Iron 
1 
31400 1 |*3 [P 1 
17439-92-1 ILead 
[ 
0.23 LBlNW* C3 |F [ 
[7439-95-4 [MagnesiumI 
9000 | | 
IP | 
17439-96-5 |Manganese! 
812 11 
IP | 
17439-97-6 [Mercury [ 
0.15 | | 
ICVl 
17440-02-0 INickel 
| 
16.2 1 |*3 |P 1 
17440-09-7 IPotassiumI 
2720 1 | 
IP 1 
17782-49-2 1 Selenium 1 
0.34 |^NW R IF [ 
[7440-22-4 [Silver 
[ 
1.2 [Ul 
IP | 
17440-23-5 ISodium 
[ 
2430 I I 
|P 1 
17440-28-0 IThallium 1 
0.66 1U| 
[F 1 
17440-62-2 IVanadium | 
112 | IN 3 
|P 1 
17440-66-6 IZinc 
| 
5790 [ [E*3 |P | 
[57-12-5 
[Cyanide | 
1.2 I^NK |AS1 
Color Before: BROWN 
Color After: BROWN 
Comments: 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
Artifacts: NO 
VALIDATED 
Rev.c'.ved By 
l/^Tyfo^ ky^ty 
Date 
^ - 3 { ' 9 y 
FORM I - IN 
300838 
ILM02.0 
oeooK 
U.S. EPA - CLP 
EPA SAMPLE NO. 
m 
C11618 
INORGANIC ANALYSIS DATA SHEET 
ab Name: PACE 
Contract: 
1 
1 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095020 
Matrix (soil/water): SOIL 
Lab Sample ID: VTF003 
Level (low/med): 
LOW 
Date Received: 01/30/95 
% Solids: 
87.5 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
1 
M i l 
|CAS No. 
1 Analyte (Concentration!C| 
Q 
IM | 
1 
1 
1 
l
l
l
l 
17429-90-5 lAluminum 1 
12900 | 1*3 
IP 1 
17440-36-0 lAntimony | 
0.32 IWiNR 
IF 1 
17440-38-2 lArsenic 
| 
0.25 liMNR 
IF 1 
17440-39-3 IBarium 
| 
98.3 | I 
IP 1 
17440-41-7 IBerylliuml 
0.02 IXI U 
IF 1 
17440-43-9 1 Cadmium 
! 
1.5 1 |N*3 
|P I 
17440-70-2 ICalcium 
1 
7490 1 1 
|P 1 
17440-47-3 1 Chromium | 
8.8 | | * J 
IP 1 
17440-48-4 ICobalt 
| 
11.0 |B1 
IP | 
17440-50-8 ICopper 
1 
27.9 | |N*:j 
|P 1 
17439-89-6 (Iron 
1 
19700 | 1*3 
|P 1 
17439-92-1 ILead 
1 
0.12 l^N* 03 
IF 1 
17439-95-4 IMagnesiuml 
4730 | 1 
IP | 
17439-96-5 1 Manganese| 
672 1 1 
|P | 
17439-97-6 1 Mercury 
1 
0.14 1 1 
|CV| 
17440-02-0 INickel 
1 
10.4 1 | * 3 
J P | 
17440-09-7 IPotassiumI 
729 |B( 
[P 1 
17782-49-2 I Selenium I 
0.32 IJB1NWR 
|F | 
[7440-22-4 [Silver 
I 
1.2 
[Ul 
|P 1 
[7440-23-5 ISodium 
| 
1210 | 1 
IP 1 
17440-28-0 IThallium 1 
0.62 lUl 
IF 1 
17440-62-2 IVanadium 1 
78.9 | IN3 
|P I 
17440-66-6 IZinc 
1 
35.1 1 1E*3 
|P 1 
157-12-5 
ICyanide 
1 
1.1 LiJIN'R 
|AS| 
1 
1 
1 
l
l
l
l 
Color Before: BROWN 
Color After: BROWN 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
Artifacts: YES 
Revicv/ed By 
Date . 
VALIDATED ^ ^ 
"^'V- f^ 
FORM I - 
IN 
300839 
ILM02.0 
osooii 
U.S. EPA - CLP 
EPA SAMPLE NO. 
% 
C11820 
1 
INORGANIC ANALYSIS DATA SHEET 
| 
I 
b Name: PACE 
Contract: 
1 
, 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095020 
Matrix (soil/water): SOIL 
Lab Sample ID: VTF004 
Level (low/med): 
LOW 
Date Received: 01/3 0/95 
% Solids: 
82.2 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
ICAS No. 
17429-90-5 
17440-36-0 
17440-38-2 
[7440-39-3 
[7440-41-7 
[7440-43-9 
[7440-70-2 
17440-47-3 
17440-48-4 
17440-50-8 
17439-89-6 
17439-92-1 
17439-95-4 
17439-96-5 
17439-97-6 
[7440-02-0 
17440-09-7 
17782-49-2 
[7440-22-4 
[7440-23-5 
17440-28-0 
17440-62-2 
17440-66-6 
[57-12-5 
1 
Analyte 
Aluminum 
Antimony 
Arsenic 
Barium 
Beryllium 
Cadmium 
Calcium 
Chromium 
Cobalt 
Copper 
Iron 
Lead 
Magnesium 
Manganese 
Mercury 
Nickel 
Potassium 
Selenium 
Silver 
Sodium 
Thallium 
Vanadium 
Zinc 
Cyanide 
Concentration 
12400 
0.34 
0.27 
128 
0.15 
1.6 
6680 
11.1 
12.1 
35.1 
21800 
0.66 
4790 
902 
0.14 
12.9 
597 
0.34 
1.2 
1050 
0.66 
93.1 
37.1 
c 
IJ-j 
^ 
1 
^ 
B 
L^n 
1 
1 
IB 
xr 
u 
B 
|U 
1 
1 
1.2 Ijy 
1 
Q 
*3 
N K 
NWR 
MB 
N*3 
* J 
N*3 
* :i 
MN*U3 
*:i 
NWR 
N 3 
E*3 
[NR 
M 1 
P 1 
F 1 
F 1 
P 1 
F 1 
P 1 
P 1 
P 1 
P 1 
P 1 
P 1 
F 1 
P 1 
P 1 
cvi 
P 1 
P 1 
F 1 
P 1 
P 1 
F 1 
P 1 
P 1 
ASl 
Color Before: BROWN 
Color After: BROWN 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
Artifacts: YES 
VALIDATED, 
Reviewed By 
l/eA^4^^^ h(U,i 
Date 
3-;^^-?-^ 
FORM I - IN 
300840 
ILM02.0 
080012 
U.S. EPA - CLP 
EPA SAMPLE NO. 
# 
INORGANIC ANALYSIS DATA SHEET 
1 
1 
j C12022 
i 
b Name: PACE 
Contract: 
j 
j 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095020 
Matrix (soil/water): SOIL 
Lab Sample ID: VTF005 
Level (low/med): 
LOW 
Date Received: 01/30/95 
% Solids: 
85.2 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
1 
l
l
l
l 
ICAS No. 
1 Analyte |ConcentrationlC| Q 
IM 1 
1 
1 
1 
l l l l 
17429-90-5 lAluminum | 
20600 | 1*3 
|P I 
17440-36-0 lAntimony [ 
0.33 [jy|NR 
[F | 
17440-38-2 lArsenic I 
1.3 l-EHNj^R 
IF 1 
17440-39-3 IBarium 
[ 
101 [ [ 
|P [ 
[7440-41-7 IBerylliuml 
0.50 [ [ 
[F | 
[7440-43-9 (Cadmium | 
2.1 [ |N*3 
|P I 
[7440-70-2 [Calcium 1 
133000 | [ 
[P | 
[7440-47-3 [Chromium 1 
30.1 [ |*3 
IP [ 
[7440-48-4 (Cobalt 
( 
12.5 [ ( 
(P | 
[7440-50-8 [Copper 
| 
38.4 ( 1N*3 
IP 1 
17439-89-6 (Iron 
| 
22400 | 1*3 
|P I 
17439-92-1 ILead 
1 
4.5 1 1NS*3 |F 1 
[7439-95-4 [MagnesiumI 
9290 [ [ 
|P | 
[7439-96-5 [Manganese[ 
604 [ 1 
|P 1 
17439-97-6 [Mercury [ 
0.28 1 1 
ICVI 
17440-02-0 INickel 
| 
21.8 | |*:7 
|P I 
17440-09-7 IPotassiumI 
3370 [ [ 
|P [ 
[7782-49-2 [Selenium [ 
3.3 1«1NR 
IF 1 
17440-22-4 ISilver 
[ 
1.2 |U| 
|P | 
17440-23-5 ISodium 
| 
510 1B| 
|P 1 
[7440-28-0 IThallium 1 
0.63 |U| 
|F | 
17440-62-2 IVanadium 1 
73.8 | |N:J 
IP | 
17440-66-6 IZinc. 
| 
61.6' [ 1E* 3" |P 1 
[57-12-5 
[Cyanide [ 
1.2 [jy^NR 
1 AS 1 
1 
1 
1 
l l l l 
Color Before: BROWN 
Color After: BROWN 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
Artifacts: YES 
VALIDATED 
Reviev/ed By 
\ / y ^ U y ^ ^ fty^'e . 
Date 
FORM I - 
IN 
5'3( - f 5 
r 
300841 
ILM02.0 
080013 
U.S. EPA - CLP 
EPA SAMPLE NO. 
tL b Name: PACE 
Lab Code: GULF 
INORGANIC ANALYSIS DATA SHEET 
Contract: 
Case No.: HLA 
SAS No.: 
1 D40001 
I 
SDG No.: 095020 
Matrix (soil/water): SOIL 
Level (low/med): 
LOW 
% Solids: 
70.8 
Lab Sample ID: VTF006 
Date Received: 01/30/95 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
jCAS No. 
j Analyte jconcentrationjcj Q 
JM j 
[7429-90-5 lAluminum | 
25000 1 | * 3" 
IP 1 
17440-36-0 lAntimony | 
0.40 |.U-|NR 
IF 1 
17440-38-2 lArsenic 1 
1.1 I^N^R 
|F [ 
[7440-39-3 [Barium 
[ 
274 1 | 
|P 1 
17440-41-7 IBerylliuml 
0.44 | | 
IF | 
17440-43-9 1 Cadmium I 
3.4 1 1N* "3 IP 1 
[7440-70-2 ICalcium I 
65200 | [ 
[PI 
[7440-47-3 [Chromium | 
28.1 | |*3- 
[P 1 
[7440-48-4 [Cobalt 
[ 
20.5 [ | 
JJP | 
17440-50-8 ICopper 
I 
57.1 | |N*3 
(P | 
17439-89-6 | Iron 
| 
37300 I [ * rr 
|P I 
[7439-92-1 [Lead 
[ 
3.5 [ |N* 3 
|F | 
17439-95-4 [MagnesiumI 
13900 | 1 
IP 1 
17439-96-5 IManqanesel 
1040 | [ 
|P 1 
17439-97-6 |Mercury | 
0.33 [ [ 
[CVI 
17440-02-0 [Nickel 
1 
17.6 | |*J 
|P | 
[7440-09-7 [Potassiuml 
1640 | [ 
|P 1 
17782-49-2 1 Selenium [ 
4.0 [JBIN R 
|F [ 
J7440-22-4 (Silver 
[ 
1.4 |U1 
|P | 
17440-23-5 ISodium 
| 
1510 j [ 
|P | 
[7440-28-0 [Thallium 1 
0.76 [Ul 
IF 1 
17440-62-2 [Vanadium [ 
155 | [NJ 
|P 1 
17440-66-6 IZinc 
| 
59.0 1 1E*3 
IP 1 
157-12-5 
ICyanide | 
1.4 UriNR 
1AS| 
1 
I I 
l l l l 
Color Before: BROWN 
Color After: BROWN 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
Artifacts: YES 
Revic 
Date 
FORM I - 
IN 
VALIDATED , . 
•ved By 
lAA^Ityyi 
(U<<Ly^ 
Z~^( - 7 S 
300842 
ILM02.0 
08001 
U.S. EPA - CLP 
EPA SAMPLE NO. 
I 
I 
1 D41416 
I 
I 
I 
INORGANIC ANALYSIS DATA SHEET 
!ab Name: PACE 
Contract: 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095020 
Matrix (soil/water): SOIL 
Lab Sample ID: VTF007 
Level (low/med): 
LOW 
Date Received: 01/3 0/95 
% Solids: 
86.1 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
1 
l
l
l
l 
ICAS No. 
1 Analyte 1 Concentration]C1 Q 
IM 1 
1 
1 
1 - 
II 
I I 
17429-90-5 [Aluminum | 
18000 1 1*3 
IP 1 
[7440-36-0 [Antimony [ 
0.33 [JJ-INR 
|F 1 
[7440-38-2 lArsenic I 
1.6 |^|N^R |F | 
[7440-39-3 [Barium 
[ 
44.1 [B[ 
|P 1 
[7440-41-7 IBerylliuml 
0.37 | | 
[F | 
17440-43-9 1 Cadmium 1 
3.1 | 1N*3 
|P 1 
[7440-70-2 [Calcium [ 
6450 | [ 
|P [ 
[7440-47-3 [Chromium 1 
24.1 1 |* J 
IP | 
17440-48-4 ICobalt 
1 
8.1 IBl 
IP 1 
17440-50-8 ICopper 
( 
39.9 | IN*J 
|P | 
17439-89-6 1 Iron 
1 
31300 [ 1*3" 
|P 1 
[7439-92-1 [Lead 
1 
2.0 101 N*7 
IF 1 
17439-95-4 [Magnesium] 
7700 | [ 
IP 1 
17439-96-5 IManqanesel 
216 11 
|P 1 
17439-97-6 |Mercury | 
0.14 [ 1 
ICVj 
17440-02-0 INickel 
| 
11.6 | 1*J 
|P 1 
17440-09-7 IPotassiumI 
1190 [ [ 
[P [ 
[7782-49-2 | Selenium | 
3.3 U»TN/^ 
[F | 
17440-22-4 [Silver 
[ 
1.2 |U| 
|P [ 
[7440-23-5 ISodium 
1 
1660 1 | 
|P 1 
17440-28-0 IThallium 1 
0.63 |U| 
|F | 
17440-62-2 IVanadium 1 
131 1 |NJ 
|P 1 
[7440-66-6 [Zinc 
| 
51.2 | |E*J 
|P | 
157-12-5 
ICyanide 1 
1.1 1JJ1NR 
1AS| 
1 
1 
1 
l
l
l
l 
Color Before: BROWN 
Color After: BROWN 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
» 
Artifacts: YES 
VALIDATED 
Reviewed By 
FORM I - 
IN 
300843 
ILM02.C 
080015 
U.S. EPA - CLP 
EPA SAMPLE NO. 
« 
D42022 
I 
INORGANIC ANALYSIS DATA SHEET 
1 
I 
b Name: PACE 
Contract: 
I 
| 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095020 
Matrix (soil/water): SOIL 
Lab Sample ID: VTF008 
Level (low/med): 
LOW 
Date Received: 01/3 0/95 
% Solids: 
. 85.5 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
1 
l
l
l
l 
|CAS No. 
1 Analyte [ConcentrationlC| Q 
|M | 
1 
1 
1 
l
l
l
l 
17429-90-5 [Aluminum 1 
13000 1 1 * T 
|P 1 
17440-36-0 lAntimony | 
0.33 I^NR 
|F | 
[7440-38-2 [Arsenic I 
0.26 [iMNWR 
IF 1 
[7440-39-3 [Barium 
| 
105 [ [ 
[P [ 
17440-41-7 IBerylliuml 
0.24 | I 
|F | 
[7440-43-9 [Cadmium [ 
2.2 [ |N*3 
[P 1 
[7440-70-2 [Calcium [ 
6350 | 1 
IP 1 
17440-47-3 (Chromium | 
18.9 | |* J 
|P 1 
17440-48-4 ICobalt 
1 
15.9 11 
IP | 
[7440-50-8 [Copper 
[ 
34.6 [ |N*:r 
|P 1 
17439-89-6 [Iron 
1 
26800 I I * CT |P I 
17439-92-1 ILead 
| 
1.9 1 |N*3 
|F 1 
17439-95-4 |Magnesium] 
5140 | [ 
[P ] 
17439-96-5 |Manganese| 
1100 11 
|P I 
17439-97-6 ]Mercury | 
0.28 ] ] 
ICV] 
17440-02-0 INickel 
1 
17.1 | |* J 
IP | 
17440-09-7 (Potassiuml 
919 |B| 
[P | 
17782-49-2 |Selenium | 
0.33 IXINWR 
IF 1 
17440-22-4 ISilver 
1 
1.2 |U1 
|P | 
17440-23-5 (Sodium 
| 
775 |B| 
|P | 
[7440-28-0 IThallium 1 
0.63 lUl 
IF | 
17440-62-2 IVanadium ] 
126 I [N 3 
|P ] 
17440-66-6 IZinc 
( 
43.5 I 1E*^ |P 1 
157-12-5 
ICyanide | 
1.2 m-lNB. 
IAS] 
1 
1 
1 
l l l l 
Color Before: BROWN 
Color After: BROWN 
Conunents: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Reviev/ed By 
Date ..I 
Texture: 
COARSE 
Artifacts: YES 
VALIDATED 
3'1>I - ^ S 
ky/cy^ 
FORM I - 
IN 
300844 
ILM02.0 
080016 
U.S. EPA - CLP 
EPA SAMPLE NO. 
^^t< 
ab Name: PACE 
Lab Code: GULF 
INORGANIC ANALYSIS DATA SHEET 
Contract: 
Case No.: HLA 
SAS No.: 
1 F21215 
1 
I 
I 
SDG No.: 095020 
Matrix (soil/water): SOIL 
Level (low/med): 
LOW 
% Solids: 
93.1 
Lab Sample ID: VSR002 
Date Received: 01/27/95 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
1 
l
l
l
l 
ICAS No. 
1 Analyte |Concentration!C| 
Q 
IM 1 
1 
1 
1 
l
l
l
l 
17429-90-5 lAluminum | 
15500 I 1*3 
IP 1 
17440-36-0 JAntimony 1 
0.30 m'lNR 
|F 1 
[7440-38-2 [Arsenic 
I 
1.7 [.BINi/R 
[F 1 
17440-39-3 IBarium 
1 
153 1 1 
[ P I 
[7440-41-7 IBerylliuml 
0.36 [ [ 
|F [ 
[7440-43-9 [Cadmium 
] 
2.6 | |N*3 
|P 1 
17440-70-2 ICalcium 
| 
9870 1 1 
|P I 
[7440-47-3 [Chromium | 
18.7 | 1*7 
|P | 
17440-48-4 ICobalt 
| 
16.0 ] 1 
|P I 
17440-50-8 ICopper 
] 
52.2 I IN*3 
IP ] 
17439-89-6 |Iron 
j 
29500 1 1*3 
IP | 
17439-92-1 ILead 
| 
3.3 | ]N*3 
IF ] 
17439-95-4 IMagnesiuml 
6200 1 1 
|P I 
17439-96-5 |Manganese] 
915 | I 
IP I 
17439-97-6 |Mercury 
| 
0.13 ] ] 
ICV] 
17440-02-0 INickel 
| 
15.4 I I * J 
|P I 
17440-09-7 IPotassiumI 
1090 | 1 
|P ] 
17782-49-2 ] Selenium ] 
3.0 IJTINR 
IF ] 
17440-22-4 ISilver 
1 
1.1 |U] 
IP 1 
17440-23-5 ISodium 
1 
1140 | | 
IP | 
17440-28-0 IThallium 1 
0.58 IU] 
IF ] 
17440-62-2 IVanadium ] 
144 | |N J 
IP | 
17440-66-6 IZinc 
| 
48.5 1 |E*7 
|P | 
157-12-5 
ICyanide 
] 
1.1 IJ^INR 
|AS| 
1 
1 
1 
l
l
l
l 
Color Before: BROWN 
Color After: BROWN 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
T^exture: 
COARSE 
Artifacts: YES 
Reviewed By 
Date .. 
..••• 
VALIDATED 
Z'l^c^S 
FORM I - 
IN 
300845 
ILM02.0 
08001 
^Bra 
U.S. EPA - CLP 
EPA SAMPLE NO. 
1 
INORGANIC ANALYSIS DATA SHEET 
b Name: PACE 
Contract: 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
Matrix (soil/water): SOIL 
Level (low/med): 
LOW 
% Solids: 
86.0 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
I 
I 
I F21820 
I 
I 
I 
SDG No.: 095020 
Lab Sample ID: VSR003 
Date Received: 01/27/95 
1 
1 
ICAS No. 1 
1 
1 
17429-90-5 1 
17440-36-0 1 
17440-38-2 1 
[7440-39-3 1 
17440-41-7 1 
[7440-43-9 1 
[7440-70-2 1 
[7440-47-3 
(7440-48-4 
[7440-50-8 
[7439-89-6 
[7439-92-1 
[7439-95-4 
[7439-96-5 
[7439-97-6 
[7440-02-0 
[7440-09-7 
[7782-49-2 
[7440-22-4 
17440-23-5 
[7440-28-0 
[7440-62-2 
[7440-66-6 
157-12-5 
1 
Analyte j 
Aluminum | 
Antimony ] 
Arsenic 
Barium 
\ 
Beryllium] 
Cadmium | 
Calcium 
Chromium 
Cobalt 
Copper 
Iron 
Lead 
Magnesium 
Manganese 
Mercury 
Nickel 
Potassium 
Selenium 
ISilver 
]Sodium 
Thallium 
jVanadium 
1 Zinc 
1 Cyanide 
1 
Concentration 
18600 
0.33 
0.26 
95.9 
0.36 
3.5 
6480 
28.3 
17.5 
57.3 
39500 
1.2 
7570 
646 
0.14 
19.2 
1 
1050 
[ 
0.33 
1 
1.2 
1 
1290 
1 
0.63 
1 
171 
1 
58.5 
] 
1.2 
1 
1 
1 
C| Q 
1 
1 
1 
1* 3 
J^JINR 
i 
Jy-INR 
1 
1 
]N*3 
1 
l*J 
1 
1N*3 
1*3 
|NW*i;3 
1 
1 
1 
l*J 
Bl 
l-yiNWR 
IU] 
1 1 
|U| 
( INJ 
[ |E*3 
I^NR 
1 1 
M 1 
P 1 
F 1 
F I 
P 1 
F I 
P 1 
P 1 
P 1 
P 1 
P 1 
P 1 
F 1 
P 1 
P 1 
CV| 
P 1 
P 1 
F 1 
P 1 
P 1 
F 1 
IP 1 
P 1 
[AS] 
1 1 
Color Before: BROWN 
Color After: BROWN 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
Artifacts: YES 
FORM I - IN 
Reviewed By 
Date .. 
7" 
VALi^TED 
7>'Z(- f S 
300846 
ILM02.C 
08001 
# 
b Name: PACE 
Lab Code: GULF 
U.S. EPA - CLP 
1 
INORGANIC ANALYSIS DATA SHEET 
Contract: 
Case No.: HLA 
SAS No.: 
EPA SAMPLE NO. 
I 
F30001 
1 
I 
SDG No.: 095020 
Matrix (soil/water): SOIL 
Level (low/med): 
LOW 
% Solids: 
86.9 
Lab Sample ID: VSR004 
Date Received: 01/27/95 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 
1 
1 
l
l
l
l 
|CAS No. 
1 Analyte |ConcentrationlCl Q 
IM 1 
1 
1 
1 
I
I
I
) 
[7429-90-5 [Aluminum [ 
17300 1 1*3 
IP 1 
17440-36-0 lAntimony | 
0.32 iJtTlNR 
]F ] 
17440-38-2 (Arsenic | 
0.25 |>W1NR 
|F | 
17440-39-3 IBarium 
| 
112 11 
IP 1 
17440-41-7 IBerylliuml 
0.21 IB] 
IF 1 
17440-43-9 1 Cadmium | 
6.4 ] 1N*J 
|P | 
17440-70-2 ICalcium 1 
60000 | ] 
IP ] 
17440-47-3 1 Chromium 1 
30.4 1 |* 3 
|P 1 
[7440-48-4 [Cobalt 
I 
17.6 [ | 
IP ] 
[7440-50-8 [Copper 
| 
141 [ |N*3 
|P j 
17439-89-6 ]Iron 
] 
63400 I I* J 
IP I 
17439-92-1 ILead 
] 
3.0 | INS*3 IF ] 
17439-95-4 iMagnesium] 
7480 1 | 
|P | 
17439-96-5 IManganese] 
888 1 1 
|P ] 
17439-97-6 |Mercury ] 
0.27 1 | 
ICV] 
[7440-02-0 [Nickel 
1 
26.9 [ \ * 3 
IP 1 
17440-09-7 [Potassiuml 
2530 | 1 
|P | 
17782-49-2 ]Selenium ] 
0.32 pBtNK 
|F | 
17440-22-4 ISilver 
1 
1.2 |U1 
|P | 
17440-23-5 1 Sodium 
] 
385 IB] 
IP ] 
17440-28-0 IThallium | 
0.62 |U| 
|F 1 
17440-62-2 IVanadium | 
99.2 1 IN 3 
]P ] 
17440-66-6 IZinc 
] 
479 1 ]E*3 
IP ] 
157-12-5 
ICyanide | 
1.1 UMNR 
|AS| 
1 
1 
1 
l
l
l
l 
Color Before: BROWN 
Color After: BROWN 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
» 
Artifacts: YES 
VALIDATED 
ne\/iijv:ed By 
I ' a y - i / c ^ kU-tP 
Date 
"^-^^-^s 
FORM I - 
IN 
300847 
ILM02.0 
080019 
% 
U.S. EPA - CLP 
EPA SAMPLE NO. 
1 
INORGANIC ANALYSIS DATA SHEET 
] 
] 
b Name: PACE 
Contract: 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
Matrix (soil/water): SOIL 
Level (low/med): 
LOW 
% Solids: 
89.1 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
1 F31214 
1 
I 
I 
SDG No.: 095020 
Lab Sample ID: VSR007 
Date Received: 01/27/95 
1 
1 
1 
Mil 
|CAS No. 
1 Analyte |Concentration!C] 
Q 
IM ] 
1 
1 
1 
l
l
l
l 
[7429-90-5 [Aluminum [ 
18800 [ 1*3 
IP 1 
17440-36-0 lAntimony | 
0.31 [.HINR 
[F [ 
[7440-38-2 [Arsenic 
[ 
1.2 
lBr\UtJtfR 
|F | 
[7440-39-3 [Barium 
[ 
177 [ ( 
IP 1 
17440-41-7 IBerylliuml 
0.36 | [ 
[F [ 
[7440-43-9 [Cadmium 
[ 
3.0 [ [N*3 
IP 1 
17440-70-2 ICalcium 
| 
25000 | | 
IP ] 
[7440-47-3 [Chromium [ 
19.6 [ | * 3 
[P | 
17440-48-4 ICobalt 
] 
17.8 ] ] 
|P ] 
17440-50-8 ICopper 
1 
56.1 1 |N*3 
IP 1 
17439-89-6 |Iron 
] 
33900 ] 1*3 
]P 1 
17439-92-1 ILead 
1 
3.2 1 IN*3 
|F 1 
17439-95-4 (Magnesium( 
7870 ] ] 
]P | 
17439-96-5 |Manganese| 
1240 | 1 
|P 1 
17439-97-6 ]Mercury 
] 
0.11 ]U] 
ICV] 
17440-02-0 INickel 
1 
17.3 1 1*3 
|P 1 
17440-09-7 [Potassiuml 
1380 1 | 
IP 1 
17782-49-2 | Selenium | 
0.31 i;»1NWR 
|F 1 
17440-22-4 ISilver 
| 
1.1 lUl 
IP 1 
17440-23-5 ISodium 
I 
1450 | 1 
|P ] 
17440-28-0 IThallium ] 
0.61 ]U] 
IF 1 
17440-62-2 IVanadium I 
172 | INJ 
|P | 
17440-66-6 IZinc 
| 
60.5 | |E*J 
IP ] 
157-12-5 
ICyanide 
| 
1.1 UJ1NR 
1AS| 
1 
1 
1 
l
l
l
l 
Color Before: BROWN 
Color After: BROWN 
Comments: 
ROCKS 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
Artifacts: YES 
VALIDATED 
Rev;^'.vcd By 
Date 
I DATED 
. 
3-3/ - ^ s 
FORM I - 
IN 
300848 
ILM02.0 
08002 
U.S. EPA - CLP 
EPA SAMPLE NO. 
# 
F31820 
INORGANIC ANALYSIS DATA SHEET 
| 
b Name: PACE 
Contract: 
j 
] 
Lab Code: GULF 
Case No.: HLA 
SAS No.: 
SDG No.: 095020 
Matrix (soil/water): SOIL 
Lab Sample ID: VSR009 
Level (low/med): 
LOW 
Date Received: 01/27/95 
% Solids: 
89.3 
Concentration Units (ug/L or mg/kg dry weight): MG/KG 
|CAS No. 
1 7 4 2 9 - 9 0 - 5 
1 7 4 4 0 - 3 6 - 0 
1 7 4 4 0 - 3 8 - 2 
1 7 4 4 0 - 3 9 - 3 
1 7 4 4 0 - 4 1 - 7 
[ 7 4 4 0 - 4 3 - 9 
1 7 4 4 0 - 7 0 - 2 
1 7 4 4 0 - 4 7 - 3 
[ 7 4 4 0 - 4 8 - 4 
( 7 4 4 0 - 5 0 - 8 
( 7 4 3 9 - 8 9 - 6 
[ 7 4 3 9 - 9 2 - 1 
( 7 4 3 9 - 9 5 - 4 
1 7 4 3 9 - 9 6 - 5 
1 7 4 3 9 - 9 7 - 6 
1 7 4 4 0 - 0 2 - 0 
[ 7 4 4 0 - 0 9 - 7 
[ 7 7 8 2 - 4 9 - 2 
[ 7 4 4 0 - 2 2 - 4 
[ 7 4 4 0 - 2 3 - 5 
[ 7 4 4 0 - 2 8 - 0 
1 7 4 4 0 - 6 2 - 2 
1 7 4 4 0 - 6 6 - 6 
1 5 7 - 1 2 - 5 
A n a l y t e 
Aluminum 
A n t i m o n y 
A r s e n i c 
B a r i u m 
B e r y l l i u m 
Cadmium 
C a l c i u m 
Chromium 
C o b a l t 
C o p p e r 
I r o n 
Lead 
Magnesium 
M a n g a n e s e 
M e r c u r y 
N i c k e l 
P o t a s s i u m 
S e l e n i u m 
S i l v e r -
Sodium 
T h a l l i u m 
Vanadium 
Z i n c 
i C y a n i d e 
C o n c e n t r a t i o n 
14700 
0 . 3 1 
0 . 2 5 
1 
|C 
.l_ 
1 
UB1 
[XT 
5 6 . 3 1 
0 . 0 5 \y 
2 . 9 1 
9520 1 
2 5 . 3 1 
1 2 . 3 1 
4 2 . 0 1 
31900 1 
0 . 2 9 \y 
6520 1 
385 1 
0 . 1 1 
|U 
1 3 . 6 1 
855 
0 . 3 1 
1.1 
7 3 1 
0 . 6 0 
IB 
1^ 
|U 
IB 
|U 
151 1 
1 
5 4 . 6 1 
1 
1.1 \y 
A . 
Q 
* J 
NR 
NR 
U 
N * J 
*3 
N * J 
* 3 
NW*i;3 
* 3 
INWR 
N 3 
E*3 
NR 
M 1 
P 1 
F 1 
F 1 
P 1 
F 1 
P 1 
P 1 
P 1 
P 1 
P 1 
P 1 
F 1 
P 1 
P 1 
CVI 
P 1 
P 1 
F 1 
P 1 
P 1 
F 1 
P 1 
P 1 
AS] 
Color Before: BROWN 
Color After: BROWN 
Comments: 
Clarity Before: 
Clarity After: CLEAR 
Texture: 
COARSE 
Artifacts: YES 
Reviewed By 
Date .-• m 
VALIDATED 
3 - 3 / - f ^ 
FORM I - 
IN 
300849 
ILM02.0 
080021 
Name: PACE 
Lab code: GULF 
Matrix (soil/water): WATER 
Level (low/med): 
LCW 
% Solids: 
0.0 
U.S. EPA" -- -CLP 
INORGANIC ANALYSIS DATA SHEET 
Contract: 
Case No.: HLA 
SAS No.: 
EPA SAMPLE NO. 
I S00012 
I 
I. 
SDG No.: 095020 
Lab Sample ID: VSROOl 
Date Received: 01/27/95 
Concentration Units (ug/L ornng/kg dry weight): UG/L 
^ < # 
1 
1 
1 
l
l
l
l 
ICAS No. 
1 Analyte ]Concentration]C] Q 
jM | 
1 
1 
1 
l
l
l
l 
17429-90-5 lAluminum ] 
25.1 \ y \ u 
IP 1 
17440-36-0 [Antimony [ 
1.4 |U|N 
|F | 
[7440-38-2 (Arsenic [ 
1.1 1U| 
jF I 
17440-39-3 IBarium 
[ 
8.8 IU| 
|P | 
[7440-41-7 (Beryllium] 
0.10 |U|N*3 
IF I 
17440-43-9 1 Cadmium | 
3.1 |U| 
IP ] 
17440-70-2 ICalcium ] 
80.4 IB] 
jP ] 
17440-47-3 1 Chromium I 
5.6 \ ^ o 
|p ] 
[7440-48-4 ICobalt 
] 
9.5 IU] 
|P ] 
17440-50-8 ICopper 
| 
16.7 |U| 
|P | 
17439-89-6 I Iron 
1 
36.1 IB] 
|P 1 
17439-92-1 [Lead 
1 
0.50 |U| 
jF ] 
17439-95-4 (MagnesiumI 
26.0 |U| 
jP | 
17439-96-5 |Manganese[ 
2.6 [U] 
IP ] 
17439-97-6 |Mercury | 
0.20 lUl 
ICVI 
17440-02-0 INickel 
1 
13.1 IU] 
|P ] 
17440-09-7 IPotassiumI 
526 IU] 
IP 1 
17782-49-2 |Selenium | 
1.4 IU] 
jF | 
17440-22-4 ISilver 
1 
5.1 ]U] 
|P ] 
[7440-23-5 (Sodium 
1 
339 IU] 
|P ] 
17440-28-0 [Thallium 1 
2.7 1U]WJ 
jF | 
17440-62-2 IVanadium I 
4.5 ]U] 
|P ] 
(7440-66-6 tZinc 
| 
7.6 IB] 
|P ] 
[57-12-5 
(Cyanide j 
10.0 ]U| 
|AS| 
1 
1 
1 
l
l
l
l 
Color Before: COLORLESS 
Color After: COLORLESS 
Comments: 
Clarity Before: CLEAR 
Clarity After: CLEAR 
Texture: 
Artifacts: NO 
VALIDATED 
Date 
' yy-'T^ 
Uui hy/(y^ 
FORM I - 
IN 
300850 
ILM02.0 
0S0022 
Name: PACE 
Lab Code: GULF 
U.S. EPA --CLP-
1 
• 
" ^ " 
INORGANIC ANALYSIS-DATA SHEET 
Contract: 
Case No.: HLA 
SAS No.: 
EPA SAMPLE NO. 
S00127 
SDG No.: 095020 
Matrix (soil/water): WATER 
Level (low/med): 
LOW 
% Solids: 
0.0 
Lab Sample ID: VTFOOl 
Date Received: 01/30/95 
-m 
Concentration Units (ug/L or mg/kg dry weight): UG/L 
CAS No. 
7429-90-5 
7440-36-0 
7440-38-2 
7440-39-3 
7440-41-7 
7440-43-9 
7440-70-2 
7440-47-3 
7440-48-4 
7440-50-8 
7439-89-6 
7439-92-1 
7439-95-4 
7439-96-5 
7439-97-6 
7440-02-0 
7440-09-7 
7782-49-2 
7440-22-4 
7440-23-5 
7440-28-0 
7440-62-2 
7440-66-6 
57-12-5 
Analyte 
Aluminum 
Antimony 
Arsenic 
Barium 
Beryllium 
Cadmium 
Calcium 
Chromixam 
Cobalt 
Copper 
Iron 
Lead 
Magnesium 
Manganese 
Mercury 
Nickel 
Potassium 
Selenium 
Silver 
Sodium' 
Thallium 
Vanadium 
Zinc 
Cyanide 
Concentration 
20.9 
1.4 
1.1 
8.8 
0.10 
3.1 
38.8 
4.7 
9.5 
16.7 
32.1 
0.50 
28.0 
2.6 
0.20 
13.1 
526 
1.4 
5.1 
339 
2.7 
4.5 
13.9 
10.0 
I 
|C] 
Q 
1 
1 1 
1 
\mnu 
1 
IUINW3 
IU] 
lUI 
1 
| U | N * 3 
lUI 
lUl 
i ^ ^ y 
(Ul 
lui 
lUI 
IU( 
lB^L/ 
|U( 
(U[ 
IU] 
(U( 
|U( 
|U( 
|U( 
(UIW3 
[Ul 
IBl 
|U( 
1 1 
M 1 
p 1 
F 1 
F 1 
P 1 
F 1 
P 1 
P 1 
P 1 
P 1 
P 
P 
F 
P 
P 
CV 
P 
P 
F 
P 
P 
|F 
|P 
|P 
]AS 
l _ 
olor Before: COLORLESS 
Dior After: COLORLESS 
omments: 
Clarity Before: CLEAR 
Clarity After: CLEAR 
Texture: 
Artifacts: NO 
FORM I - IN.--
i/tilis 
rALlPATED 
' ^ y - 3 y ^ 3 
3 0 0 8 5 1 
ILM02.0 
080023