SDMS Document 
115549 
ISLAND CHEMICAL COMPANY, INC 
REMEDIAL INVESTIGATION 
ST.CROIX, U.S. VIRGIN ISLANDS 
DRAFT WORK PLAN 
Volume II of II 
Appendices D through 0 
Prepared For 
Island Chemical Company, Inc 
By 
Harding Lawson Associates 
Philadelphia, Pennsylvania 
March 17, 1994 
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00 
cn 
Appendix D 
Rainfall Summary 
• y . 
\WORK\24231\02\WORKPU^N.REP 
HARDING UXWSON ASSOCIATES 
301286 
TABLE 1 
TEMPERATURE AND PRECIPITATION 
[Daia from Alexander Hamilton Field, St. Croix] 
Month 
January 
February---
March 
April 
^lay.---
J :ne 
-•-ly 
f .:?ust 
£ ;ptenber--
C -.tober 
N :venber— 
Diceober— 
Year 
Temperature 
Average 
daily 
maximum 
°F. 
83 
83 
84 
86 
86 
sa 
88 
89 
88 
88 
86 
84 
86 
Average 
daily 
minimum 
"F. 
70 
70 
71 
73 
74 
76 
76 
76 
75 
75 
73 
72 
73 
Average 
maxiaun 
•F. 
86 
86 
86 
88 
89 
90 
90 
91 
91 
90 
89 
• l " 
^92 
Average 
minimum 
•F. 
65 
66 
66 
68 
70 
71 
71 
72 
71 
70 
68 
67 
^64 
Precipitation 
Average 
total 
In. 
2.23 
2.19 
1.73 
2.83 
4.31 
3.10 
3.51 
4.58 
6.65 
5.45 
4.65 
3.34 
44.57 
One year in 10 will have--
Less than--
' In. 
0.50 
.44 
.40 
.55 
.60 , 
.58 
.80 
1.20 
2.20 
1.60 
1.20 
1.00 
34.00 
More than--
In. 
7.2 
s:8 
4.6 
7.6 
8.2 
6.0 
6.6 
8.8 
11.0 
10.2 
9.0 
8.6 
53.8 
Average number of 
days with more 
than one-tenth 
of an inch of 
rainfall 
5 
6 
4 
6 
8 
9 
8 
9 
10 
8 
9 
.9 
91 
Average annual highest temperature. 
Average annual lowest temperature. 
301287 
Appendix E 
Clean Air Act Correspondence 
\WORK\2423l\02\WORKPLAN.REP 
HARDING UVWSON ASSOCIATES 
301288 
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY 
REGION II 
26 FEDERAL PLAZA 
NEW YORK. NEW YORK 
10007 
i/9 
Mr. Harry Sponnoble 
Vice President/General Manager 
Island Chemical Company, Inc. 
P.O. Box 6733 
Christiansted, St. Croix 
U.S. Virgin Islands 00820 
Dear Mr. Sponnoble: 
This Is to inform you that the United States Environmental Protection 
Agency ("EPA"), Region II Office, has completed its review of the 
information you submitted dated April 5, 1979, relative to the chemical 
plant Island Chemical Company, Inc. ("ICCI") recently purchased in 
St. Croix, Virgin Islands. Based upon a review of this material and 
information derived from subsequent telephone discussions with your 
representatives, it 1s the determination of the EPA that this project 
is not subject to Federal Prevention of Significant Air Quality 
Deterioration ("PSD") regulations. The PSD regulations apply to (among 
other sources) any new or modified chemical processing plant with pro-
jected potential (uncontrolled) emissions (In the case of a modification, 
the Increase In potential emissions) of 100 tons per year or more of any 
pollutant regulated under the Clean Air >Act. From information contained 
in the Virgin Islands Department of Conservation and Cultural Affairs 
("VIDCCA") permits to construct for this project, the increase in poten-
tial hydrocarbon emissions were calculated to be less than 100 tons per 
year; therefore, your project is not subject to the PSD regulations. It 
should be mentioned that although this source is not now subject to PSO, 
it may be subject to the PSD regulations In the future; the potential 
emissions associated with this source will be added to the potential 
emissions of any subsequent modiflcation(s) in determining PSD applicability, 
Should you have any questions concerning the contents of this letter, please 
feel free to call Messrs. Kenneth Eng or Gerald DeGaetano at (212) 254-4711 
and (212) 264-4726, respectively. 
Sincerely yours, 
Meyer 
Director 
Enforcement Division 
• 
cc: 
Mr. Donald C. Francois 
Virgin Islands Department 
of Conservation and Cultural Affairs 
301289 
II D€SCRIPTION OF EQUIPMENT - MAJOR AiND APPLICABLE ITEMS 
AJ Utility Building 
" 1 . 
Boiler: 
Primary 
Make: " 
York-Shipley Inc. 
Pressure: 
150 Ib/in^ 
Blower: 
5 H.P. 
Burner: 
York-Shipley Inc. 
FV-40 
Fuel Consumption: 
#2 Oil 
257.1 Ib/hr (19,700 Btu/lb) 
Sulfur Content: 
Q.1C% 
Sulfur Emissions: 0.41 Ib/hr 
2. 
Boiler: 
Reserve 
Make: 
Llraberto-Girola-Milano 
Pressure; 
16 kg/cm^ 
Btu Rating: 
7,936,000 Btu/hr 
Blower Motor: 
5.9 KH 
feed Water Puip: 
7.5 KW 
Burner: 
Oertli 
Fuel Consumption:. #2 Oil 
402.8 Ib/hr (19,700 Btu/lb) 
Sulfur Content: 
0.16Ji 
Sulfur Emissions: 0.64 Ib/hr 
8. Process Area 
1. ._ 
•' 
V 
Reactor R-l 
Stainless Steel 
Volume: 
1,500 gal. 
Dimensions: 6.5 Ft.die, 10 ft overall height 
Condenser R-l: 15 sq. meter surface area 
Reactor R-4 
Stainless Steel 
Volume: 
1,300 gal. 
Dimensions: 6.0 F t . d i a . , 9 ft. overall height 
2. 
Reactor R-2 
Stainleaa Steel 
Volume: 
1,500 gal. 
Dimensions: 6,5 ft.dia., 10 ft. overall height 
Condenser R-2: 15 m^ surface area 
Flame Front Generator 
MFG. By : John Zink Co. 
Serial #X52932 
Air Orifice: L-l 
Gaa Orifice: 
5/64 
3 012 90 
Carrier: 
Propane 
3. 
Reactor R-101» 
Volume: 
Dimepsions: 
Gloss Lined 
2,000 gal. 
6 ft.dia., 13 ft. overall height 
Condenser E-lOl: 
I6m^ surface area 
Reactor R-102: 
Volume: 
Dimensions: 
Glass lined 
3,000 gallon 
8 ft.dia., 15 ft. overall height 
Condenser E-102: 16m2 surface area 
4. 
Storage Tank:-
Volume: 
Dimensions: 
Reactor R-3 
Stainless Steel 
Volune: 
Dimensions; 
Reactor ,R-5: 
Volume:' 
Dimensions: 
Stainless Steel 
19 m^ 
10 ft.dia., H.'z> ft overall height 
1,500 gallon 
6.5 ft.dia., 10 ft. overall height 
Condenser R-3: 
15 m^ surface area 
Carbon Steel 
1,300 gal. 
i' 
6 ft.diQ.,'9.5 ft. overall height 
301291 
Appendix F 
Cooper Laboratories Geotechnical Investigations 
\WORK\2423l\02\WORKPLA.N.REP 
. HARDING LAWSON ASSOCIATES 
301292 
—I 
Car:::;'c-.in 
Drilling 
Services 
INCORPORATED 
Box A5 
Kincshill 
St. Croix 
V.I. 
00850 
(809) 773-2737 
General Engineering Corp. 
P.O. Box A59 
Christiansted, St. Croix 
May 12, 1979 
CDS Job 1119^12 
ATTEN'TION: Mr. John HcCallum 
REFERENCE: Subsurface Investigation - Proposed Cooper Laboratories 
Plant Expansion, Estate Bethlehem, St. Croix 
Dear Sirs: 
Enclosed herewith please find our soil engineering report 
for the above project. 
Based on the available soils information it appears that 
footing foundations are feasible for the support of the proposed units. 
Specific recommendations are included in the body of the report. 
Should you have any questions with regard to this report, 
please do not hesitate to contact us. 
Very truly yours, 
CARiaSEAN DRIU-ING SERVICES, INC. 
Joseph M./Lasero 
Registered Professional Engineer' 260E 
JMC:fs 
/ 
/ 
301293 
;and and water borinjs / diamond core drilling / soils / concrete / csphalt / chemical grouting / piezor-.e:er '.-::c!irtJcn 
SOIL REPORT 
SJcSURFACE INVESTIGATION - PROPOSED COOPER 
LA5JRATCRIES PLANT EXPANSION, ESTATE BETH^E.-iEM 
ST. CROIX, U.S.V.l, 
INTRODUCTION 
The subsurface investigation for the proposed Cooper Laboratories 
Plant Expansion, Estate Bethlehem, St. Croix has been completed. Three (3) 
soil borings were performed at the site and the results of these borings, to-
gether with a location diagram are included in this report. 
It is our understanding that the proposed expansion will occupy 
an area of 33 ft. by 17 ft. with various units including a large class reactor 
having an estimated total weight (including internals) iof 35 tons. Other 
units will have minor loads. 
The purpose of this report is to describe the soil conditions as 
encountered in the borings, to analyze and evaluate the boring and test data 
obtained, and to submit recommendations regarding feasible foundation design 
and construction. 
SUBSURFACE INVESTIGATION PROCEDURES 
The soil borings were performed using a trailer-mounted drilling 
rig equipped with a hydraulic head used.in the drilling and sampling opera-
tions. Also used was a truck mounted rig for deeper holes. The boreholes 
were advanced using continuous flight hollowstem augers and representatiive 
samples were obtained by means of split-barrel sampling procedures in accor-
301294 
; C A R I B a e A N D B I U L I H C S E R V I C E S . I N C . 
^ 
CDS Job j^-795:2 
Page 2 
dance with ASTM Specifications D-15S6. 
In the split-barrel sampling procedure, standard penetration 
resistance values (blows per foot of a 140 lb. hammer falling 30" on a 2" 
O.D. split-barrel sampler) were obtained. These resistance values are an 
indication of the relative density of predominantly granular soil in piace. 
All soil samples obtained in the field were labeled, sealed 
and forwarded to the laboratory for further examination and testing. 
TESTING PROGRAM 
Due to the nature of the soil's encountered a limited laboratory 
testing program was implemented.. The program consisted;of reclassification 
of the samples and determination of the natural moisture content. The ..re-
sults of all tests performed are shown on the boring logs opposite the cor-
responding samples. 
Careful boring logs were kept in the field, where the soil 
samples were classified in accordance with the Unified Soil Classification 
System. After completion of the testing program, the smaples were again 
examined and the field classifications revised where necessary. 
SOIL CONDITIONS 
The site is located in an alluvium valley formed on the Kings-
hill Formation of Lower Miocene Age. Sediments were derived from the north 
range and consist of fine sands, sandy clays and silty gravels. Variable 
stratification is present indicating braided stream deposition. 
301295 
iziz^!nn;^i;izzzz^^^ni!^ziii^zrzr CARI6BCAM ORI>.I.INC SERVICES, INC.izi^zzmzziiizmz^ni^rirzz^z^r^^^iizzi 
CDS Job /;79512 
Page 3 
From a sciis engineering viewpoint, the upper surface soils 
(below existing coricrete slab at B-I and B-2) at all boring locations 
consist of either stiff silty clay or silty sand with variable percen-
tages of clay to an average depth of rom 1.5 to 2.5 ft. Below this 
surface layer, medium dense to dense silty sand and gravel or sandy 
silt (B-1) strata were encountered which extended to depth of from 5.0 
to 7.5 ft., merging gradually into sandy silt or silty sand with numerous 
rock fragments. This latter stratum was interspersed with sandy clay 
seams of limited thickness. 
The lowest soil formation encountered (typically below 15 ft.) 
was a medium dense to very dense silty sand and gravel ,which extended to 
the maximum depths investigated (i.e. 25 ft.). 
WATER TABLE CONDITIONS 
Water level observations made after boring are shown on the 
boring logs. Based on the available information it appears that at the 
time the borings were performed, the hydrostatic water table was at 
approximately 20 ft.' below the present ground surface at all boring 
locations. 
The hydrostatic water table should be anticipated to fluc-
tuate throughout the year depending upon variations in percipitation and 
surface runoff. 
301296 
; C A R I B B E A N 
D R I U I - I N C S E R V I C E S , I N C . 
CDS Job ••'/79512 
Paae ^ 
ANALYSIS AND RECCi-lMENDATiONS 
As described under soil conditions, the upper, near surface 
soils, consisting primarily of silty clay or loose silty sand and are not 
considered competent soils. 
We recommend footing type foundations be used deriving their 
support from either the medium dense silty sand and gravel or sandy silt 
typically encountered at 3 ft. below present ground surface. 
Footings may be designed for a maximum allowable total load 
soil bearing pressure of 3000 p.s.f., when established on the bearing 
soils noted above. If higher allowables are required, footings should 
be established below 5 ft., at which depth an allowable 'total load soil 
bearing pressure of 4000 p.s.f. or higher may be used. 
For footings located on the medium dense silty sand or sandy 
silt at 3.0 ft. (min.) below present ground surface, anticipated settle-
ments should not exceed %". Differential settlements, however, should 
be negligible. 
Due to the nature of the bearing soils, (particularly at the 
location of boring B-1) we strongly recommend that excavations not be 
left open for an extended period of time. Saturation of the sandy silt 
or fine grained sand will affect bearing capacity adversely. If satu-
ration does occur, it is recommended that the soil (saturated) be removed 
to full disturbed depth prior to steel placement and pouring the concrete. 
"No construction problems are anticipated for the smaller 
301297 
; C A R I B B E A N O R I L 1 . I N C S E R V I C E S . I N C . 
• CDS JoD //79512 
Pace 5 
units, but some sloucning of the 53.~i-granular soils may occur in the 
excavations, which may not permit certain foundations to be poured neat. 
Again the longer excavations are left open the more sloughing is to be 
andicipated. 
Site drainage should be given careful attention to insure 
that surface waters are not permitted to stand near or seep into the 
foundation bearing soils. 
This report has been prepared in order to aid in the evalu-
ation of the site soil parameters and to assist the engineer in the 
design of the project. The analysis and recommendations submitted in 
this report are based on data obtained from three (3) soil borings per-
formed at the locations shown on the reference sketch 79512-D. This 
report does not reflect the variations between borings which may not 
become evident until the course of construction. If variations then 
appear evident, it will be necessary for the soil and foundation engineer 
to re-evaluate the recommendations of this report after performing 
on-site observations and noting the effect of such variations on the 
design of the structure. 
301298 
C A R I B B E A N D R I U U I N C S E R V I C E S . I N C . 
# 
SOIL BORING LOCATIONS 
301299 
C A R I B B E A N O R I U U I N C S E R V I C E S . I N C . ; 
^ - 2 
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C A R I B B E A N O R I I . t . l N C S E R V I C E S . I N C . ; 
301300 
SOIL BORINGS 
301301 
; C A R 1 B B E A N D R I U U I N C S E R V I C E S . I N C . 
•. O W N C R 
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COOPER LABS, INC. 
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A R C H I T E C T - E N G I N E E R 
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BORING STARTED 
4 / 1 7 / 7 9 
WL 
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CARIBBEAN DRILLING SERVICES. INC. 
SOIL A N D F O U \ D A T l O H CONSULTANTS 
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COOPER LA3S, INC. 
i-OG o r p O s . N c s „ i . -
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PLANT EXPANSION 
A R C H I T E C T - E N C i N C E R 
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CARIBBEAN DRILLING SERMCES, INC. 
SOIL A N D F O U N D A T I O N 
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301303 
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COuPER LABS, INC, 
L O G 
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B O R I N G 
N U M B E R 
B-3 
. P R O J E C T 
N A M E 
PLANT EXPANSION 
A R C H I T E C T - E N G I N E E R 
GENERAL ENGINEERING, INC. 
I S I T E 
L O C A T I O N 
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CARIBBEAN DRILLLNG SERMCES. INC. 
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N U M B E R 
B-3 
PROJECT 
N A M E 
PLANT EXPANSION 
A R C H I T E C T - E N G I N E E R 
GENERAL .ENGINEERING, INC. 
S I T E 
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4 / 1 7 / 7 9 
CARIBBEAN DRILLLNG SERMCES. INC. 
SOIL A N D FOUNDATION 
CONSULTANTS 
WL 2 0 . 0 ' - A . B . 
RIG 
4 5 - C 
FOREMAN 
KDE 
APPROVED BYJMQ CDS JOB N O . 
7 9 5 1 2 
a i . : l 
301305 
"^ 
SUBSURFACE INVESTIGATION 
PROPOSED FIREWATER TANK 
COOPER LABORATORIES PLANT 
FREDERIKSTED, ST. CROIX 
U.S. VIRGIN ISLANDS 
301306 
ICARIBSCAN DRILLING SERVICES. INC. 
r 
n 
SOIL REPORT 
SUBSURFACE INVESTIGATION - PROPOSED COOPER 
LABORATORIES PLANT EXPANSION, ESTATE BETHLEHEM 
ST. CROIX, U . S . V . l . 
L 
• 
• 
. 
J 
301307 
J Caribbean 
Drilling 
Services 
INCORPORATED 
Pnon« 809-773-6162 
EnglnMrIng Analyili ^ Rtoorti 
— 
Construction Quality Control 
lniD«ctlon 
— 
Ttsting 
— 
D««lgn 
Address Reply To: 
P.O.BOX 4S, KINSSHILL 
ST. CROIX, U.S. VIRGIN ISL. OOiSO 
Cooper Laboratories Inc. 
Frederiksted, St. Croix 
U.S. Virgin Islands 
Reference; 
Dear Sirs: 
Subsurface Investigation 
Proposed Firewater Tank 
Cooper Laboratories Plant 
Frederiksted, St. Croix 
August 19, 1980 
CDS Job No. 81501 
We are submitting herewith, our engineering report on 
the subsurface investigation for the above project. 
Based on the information obtained from the soil borings 
and laboratory test data, it appears that adequate support for 
the proposed tank may be obtained vdthin a reasonable depth at 
the proposed site. Specific recommendations are discussed in 
detail in the body of the report. 
Should you have any questions with regard to this report, 
please do not hesitate to contact us. 
Very truly yours, 
CARIBSEA5%?K,LING SERVJCK, INC. 
301308 
S O I L 
R E P O R T 
SUBSURFACE I.N-VESTIGATION FOR THE PROPOSED FIREWATER TAN'K 
COOPER LABORATORIES PLA.Vr, FREDERIKSTED, ST. CROIX, U.S.V.l. 
CDS Job No. SlSOl 
August 19, 1980 
INTRODUCTION 
The subsurface investigation for the Proposed Firewater Tank to be 
located at the Cooper Laboratories Plant in Frederiksted, St. Croix, U.S. 
Virgin Islands, has been completed. A total of three C2) soil borings were 
performed and the results of these borings together with a location diagram 
are included with this report. 
It is our understanding that the Proposed Tank will be approxima-
tely 57.0 ft. in diameter and approximately 58.0 ft. high. The tank is 
contemplated as a Firewater Reserve and is designed with a tank ring on a • 
compacted and treated fill. Foundation requirements stipulate a bearing 
capacity of approximately 2,000 psf with minimal settlement. Finished 
grade has not been established at this time but is expected to be slightly 
higher than existing plant grade, for ease in piping. 
The purpose of this report is to describe the soil conditions as 
encountered in the borings, to analyze the field and laboratory data and 
to submit recommendations regarding feasible foundation depths for the 
project requirements. 
SUBSURFACE INVESTIGATION PROCEDURES 
The soil borings were performed with a trailer-mounted drilling 
rig equipped with a hydraulic head used in the drilling and sampling ope-
rations, the boreholes were advanced using continuous flight augers and 
301309 
' C A R i a a E A N DRILLING SERVICES. INC. 
CDS Job No. 51301 
Page 2 
representative samples were obtained by means of split-barrel samplers in 
accordance with ASTM Specification D-1S86. 
In the split-barrel sampling procedure, standard penetration re-
sistance values (blows per foot of a 140 lb, hammer falling 50 in. on a 
2 in. O.D. split-barrel sampler were obtained). These resistance values 
(SPT) are an indication of the relative density of the soils in place. 
All soil samples obtained in the field were sealed and forwarded 
to the laboratory for further examination and testing. 
LABORATORY TESTING PROGRAM 
Due to the nature of the soils encountered, a limited laboratory 
testing program was implemented. The samples were carefully examined and 
re-classified and the natural moisture content of representative portions 
was determined. The results of all laboratory tests are plotted graphi-
cally opposite the corresponding samples on the boring logs. 
Careful boring logs were kept in the field where the soil samples 
were classified in accordance with the Unified Soil Classification System 
(USCS). At the completion of the testing program, the samples were again 
examined and the field classifications revised, where necessary. 
SOIL CONDITIONS 
The specific soil conditions at each boring location are detailed 
on the pertinent boring log. Typically, a medium dense browTi sandy silt, 
approximately 2.0 ft. in total thickness, blankets the site. This stratxjm 
is in a loose to medium dense state. 
301310 
;CARIBaCAN DRILLINQ SERVICES. INC.^ 
- \ 
CDS Job No. 81501 
Page 5 
# 
Below this surface veneer, medium dense light brown clayey silts 
or sandy clayey silts were encountered which extended to depths ranging 
from 5.0 ft. at boring B-5, to a maximum of 8.0 ft. at boring B-2. 
The clayey silts in turn are underlain by tough to very tough 
silty sandy clays which continue to the bottom of the boring B-1, and to 
approximately 12.0 ft. in boring B-5. Silty clays are absent in boring 
B-2 and the clayey silts previously mentioned extend to approxiaately 
15.0 ft. 
The lowest soil formation at borings B-2 and B-5, was a dense 
silty sand with varying percentages of gravel which continued to the maximum 
depth investigated (15.0 ft.). 
Typically, below the surface veneer, density and strength increase 
with depth and moisture content decreases significantly below 7.0 ft. 
WATER TABLE CONDITIONS 
Water level observations made after boring are shown on the boring 
logs. Based on the available information, it appears that the hydrostatic 
water table was below the maximum depths investigated. 
The hydrostatic water table should be anticipated to fluctuate 
throughout the year depending upon variations in precipitation and surface 
runoff. 
Due to the possibility of occasional silty sand seams or gravel 
seams within the various formations, a perched water table may occur at 
the site during certain parts of the year. This condition would become 
evident during the time of construction. 
301311 
; CARIBBEAN DRILLING SERVICES. INC.: 
# 
CDS-Job No. 81-501 
Page 4 
A.NALYSIS AND RECOMMENDATIONS 
Based on an analysis of the soil profile and the results of the 
laboratory tests, we recommend that the site be excavated to approximately 
el. 102, and the footing for the tank ring be excavated further to el. 101. 
For footings so located, we recommend an allowable total load soil bearing 
pressure of 2,000 psf. 
Anticipated settlement for this load criteria should not exceed 
%". Differential settlements are not expected to exceed V . For the in-
terior of the tank we recommend select backfill, preferably quarry screen-
ings, between el; 102 and el. 105.5, be used. All backfill should be 
placed in 8 in. lifts Qoose thickness) and compacted "to a minimum of 93% 
of the maximum density as determined by ASTM Specification D-1557. 
We also recommend that the upper 6 in. consist of either oiled 
salt free sand or preferably oiled quarry screenings to preserve the inte-
frity of the tank bottom steel (i.e. reduce moisture migration and oxida-
tion to the bottom plates). 
GE?}ERAL RECOMMENDATIONS 
It should be noted that the proposed bearing soils are moisture 
sensitive. We therefore recommend that excavations not be left open for 
any extended period to minimize the possibility of saturation or overdrying. 
If saturation of the bearing soils should occur, it will be nece-
ssary to remove the disturbed soil to full depth prior to pouring the 
concrete or backfilling within the tank ring. This precaution is necessary 
in order to prevent unduly high differential settlements upon imposition of 
load. 
301312 
' CARIBBEAN DRILLING SERVICES. INC. 
CDS Job No. 81501 
Page 5 
Due to the presence of silty clays and clayey silts relatively 
close to the bottom of the foundation system, it is imperative that mois-
ture migration to the foundation elements be minimized. This may be accom-
plished by sloping the site away from the tank in all directions. Further, 
we suggest paving an annulus around the tank ring with asphaltic concrete 
so that sheetwash from the tank sides will not penetrate the ring founda-
tions or create erosion gullies. A 10.0 ft. annulus should be adequate. 
Needless to say, positive drainage away from the tank pad area to avoid 
local ponding is absolutely essential. 
Additionally, we recommend that the.excavation and backfill 
i 
operations be inspected by a qualified soil technician to verify that the 
proper bearing soil has been reached and to insure that the compaction re-
quirements are met. The technician should perform in-situ density tests 
and the necessary proctor tests to establish compliance with these speci-
fications. 
This report has been prepared in order to aid in the evaluation 
of the foundation soil parameters of this site and to assist in the design 
of this project. In the event that any changes in the design or location 
of the tank pad. , as outlined in this report are planned, the conclusions 
and recommendations contained in this report shall not be considered 
valid unless the changes are reviewed and conclusions of this report modi-
fied or approved in writing by the soil and foundation engineer. 
301313 
' C A R I B B E A N O R I U L I N C S E R V I C E S . I N C . 
SOIL BORING LOCATIONS 
301314 
[ C A R I B B E A N D R I L L I N G S E R V I C E S . I N C . 
-m 
301315 
S O I L 
B O R I N G S 
3 0 1 3 1 6 
-:?3 
; CARIBBEAN DRILLING S F R V l ' ' ^ S 
I N r 
OWNER-
COOPER 'LABORATORIES 
PROJECT NAME 
PROPOSED FIREWATER TANK 
L O G O F B O R I N G 
N U M B E R 
B-1 
A R C H I T E C T - E N G I N E E R 
S I T E L O C A T I O N 
FREDERIKSTED, ST. CROIX, U.S.V.l. 
0 
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D E S C R I P T I O N O F M A T E R I A L 
SURFACE ELEVATION 108.7 
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SANDY CLAYEY SILT, Light Brown to 
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(^^L) 
W L 
WS OR W D 
W L 
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A C R 
BORING STARTED 
7 / 2 1 / 8 0 
BORING COMPLETED 
7/21/80 
CARIBBEAN DRILLING SERVICES, INC. 
SOIL A N D FOUNDATION CONSULTANTS 
WL 
NONE - A J . 
RIC45-C 
FOREMAN 
KDE 
APPROVED B"|JMC( CDS JO^B NO._31501 
"3 01317 
OWNER 
COOPER LABORATORIES 
LOG o r BORING NUMBER 
B-2 
PROJECT NAME 
PROPOSED FIREWATER TANK 
ARCHITECT-ENGINEER 
SITE LOCATION 
FREDERIKSTED, ST. CROIX, U . S . V . l , 
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trace gravel 
CLAYEY SILT W/ LIMESTONE FRAGMENTS, 
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BORING STARTED 
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I 
CARIBBEAN DRILLING SERVICES, ENC. 
SOIL AND FOUNDATION CONSULTANTS 
_ . — 4 C 
n 
301318 
OWNER 
COOPER LABORATORIES 
L O G O F B O R I N G 
N U M B E R 
P R O J E C T N A M E 
PROPOSED FIREWATER TANK 
B-5 
A R C H I T E C T - E N G I N E E R 
S I T E L O C A T I O N 
FREDERIKSTED, ST. CROIX, U . S . V . l , 
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CLAYEY SILT - SOME SAND, Brown, 
Medium Dense (ML-CL) 
SS LD 
PA 
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SILTY SAND - SOME GRAVEL, Brown, 
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7 / 2 1 / 8 0 
| 
CARIBBEAN DRILLING SERVICES, INC. 
B O R I N G C O M P L E T E D 
7 / 2 1 / 8 0 
' 
SOIL AND FOUNDATION CONSULTANTS 
301319 
. 1 ^ . 1 % - — / ? \ 
1 
-
• 
Appendbc G 
Report Concerning Small Quantity Generator Status of Island Chemical 
\WORK\24231\02\WORKPLAN.REP 
HARDING LAWSON ASSOCIATES 
301320 
IVnO • 
KKSK£S UK. 
19 COPEUVND RD.. DENVILLE. NEW JERSEY 07834 
(201)366-6256 
May 7, 1985 
Mr. Robert Harris 
U.S.E.P.A. 
Region II 
Room 1000 
26 Federal Plaza 
New York, NY 10007 
Reference: Island Chemical Co., St. Croix, U.S.V.l. 
Dear Mr. Harris: 
Enclosed is inforination concerning the manifesting of hazardous 
material at Island Chemical Co. when operations ceased and prior 
to its,sale by Berlex to Virgin Island Chemical Co. Included are 
eight (8) manifests. 
In addition/ there is an explanation as to why activities at the 
facility would classify it as a small generator. 
We are anticipating a meeting in the immediate future with USEPA 
staff members to discuss this project. 
If you have any questions, call me at 201-366-6256. 
Very truly yours, 
ENVIRO-SCIENCES, INC. 
Alan L. Kyles, Ph.D. 
Vice President 
ALK/po 
(AK-8531) 
Enclosure 
cc: Mr. Robert Milos 
Mr. Frank Curtis 
Ray Willis, Ph.D, 
301321 
REPORT CONCERNING SMALL QUANTITY 
GENERATOR STATUS OF ISLAND CHEMICAL 
The Island Chemical Company (ICC) was incorporated in 
Delaware on July 21, 1978. All of the shares were then owned by 
Cooper Laboratories, Inc. ICC stock has never been publicly 
traded on any exchange. 
The land currently under consideration, comprised of 
three acres more or less and situated at St. Croix, U.S.V.l. 
(the "leasehold") is owned by Charles H. Steffey, Inc. On May 1, 
1969 Steffey leased the property to Houston Chemical Industries, 
Inc. Houston Chemical assigned the lease to Caribe Chemical Co., 
i 
Inc. (subsequently known as Pierrel America, Inc.) on March 20, 
1972. 
On June 30, 1978 Pierrel America assigned the ground 
lease to Cooper Laboratories, Inc. On October 30, 1979 Cooper 
Laboratories assigned the lease to its subsidiary, ICC. On 
November 1, 1979 Cooper Laboratories sold all of the stock of ICC 
to Berlex Laboratories, Inc. (then known as ASAG Pharmaceuticals, 
Inc.) 
Prior to the acquisition of the leasehold by Cooper 
Laboratories, it is believed the prior owners used the site to 
manufacture phenacetin and ethoxyquin. Shortly before Berlex 
- 1 -
301322 
m 
acquired Island Chemical, and with it the leasehold and 
improvements, the facility was being used by Cooper to perfect a 
four-step process licensed frora a French company to convert 
quinine, a relatively inexpensive compound, to its dextrorotary 
isomer quinidine, a far more expensive product. Cooper halted 
its work on the French process in mid-1979. Quinidine is the 
active ingredient ' in Berlex's product QUINAGLUTE* (quinidine 
gluconate) DURA-TABS* (sustained release tablets). 
After the acquisition of the facility in late 1979, ICC 
began preparation for the use of a quinidine process being 
developed by a West German concern. A single pilot batch was run 
with the French process, but the resulting product was not pure 
enough. It was not until October 198O that sufficient planning 
and research had been done on the German process to warrant full 
staffing and personnel training at the St. Croix facility. It 
was thus not until the end of I98O that production of pilot size, 
batches was begun. In addition, after that time the plant also 
was used to reclaim quinidine from rejected lots of final 
product. 
From the end of 198O until the end of I982 the 
St. Croix plant continued to experience production problems 
related to the purity and yield of the product and only during 
the last few months of 1982 were anything "more, than pilot batches 
produced. Early in 1982, Berlex made a strategic decision that 
- 2 -
301323 
its backward integrating of the supply of quinidine was ill-
advised since it caused Berlex to enter the chemical processing 
business with which it did not possess enough technical 
expertise. Consequently, the plant was permanently closed at the 
end of 1982. During its period of ownership, the plant was 
required only to convert quinine to quinidine or reclaim 
quinidine from final product. In both of these processes, 
toluene was used. In addition, quanitities of pyridine were used 
in the French process. 
Two laboratories were present at the St. Croix 
facility. An analytical laboratory was maintained to test raw 
materials, and to conduct in-process and' final product testing. 
A process laboratory was also present at the site for product 
development functions, primarily the small scalfe duplication (1-5 
liter quantities) of steps in the process to work out problems 
and test improvements. 
Toluene. The German process in use for the conversion 
of quinine to quindine involved neutralization, oxidation, and 
reduction. At several points of the process, toluene was used. 
This toluene was recovered at every step. The entire amount 
recovered in every case was stored and reused when the process 
was run the next time. 
The same is true for the process used to recover 
quinidine from finished product. The toluene used in the process 
was recovered and reused when the process was run again. 
- 3 -
301324 
Thus, the approximately 28,600 gallons of toluene on 
the site during ICC's use of the facility constantly was used in 
the two processes. At the time of the shut-down of the plant in 
December of 1982 by ICC, there was ho further useful purpose for 
this material and it was manifested (see attached manifests IC-01 
through IC-06) and shipped to Inland Chemical of Puerto Rico, 
Inc. of Manati, Puerto Rico, where it was burned. 
Pyridine. Pyridine was used only in the French 
process, which was run only once by ICC. In addition, extremely 
small quantities of pyridine were on the ICC site for use as'a 
reagent in the analytical and process laboratories. 
Unfortunately, some of this material found its way down a sink 
drain in the laboratory, giving rise to the pollution described 
under point 4 on page 2 of the Addendum of Progess Report 
submitted by Enviro-Sciences, Inc. As you can see from the 
extent of the contamination described in this report, only small 
quantities were involved. 
Xylene. At the time ICC acquired the St. Croix site, 
approximately 6,900 gallons of xylene mixed with p-phenetidine 
was present. This substance was a raw material used by a former 
owner. It was at no time used by ICC. After the plant shut-
down, it was shipped to Philipp Brothers Chemcials, Inc. in New 
York for sale. The sale unfortunately was not consummated and 
since no other purchaser could be found, the material was 
- 4 -
301325 
thereafter manifested as a hazardous waste and shipped to Inland 
Chemcial in Puerto Rico for burning. See manifests IC07 and IC08 
attached. 
Other Chemicals. As noted above, ICC maintained 
analytical and process laboratories on the site. Small 
quantities of laboratory chemicals were present in each. These 
included toluene; methyl chloride; alcohols, alkaloys and acids; 
benzophenone; and Dibah. These chemicals were for laboratory use 
only and were in containers.of the pint, quart, liter and gallon 
sizes frequently seen in the laboratory. Only very small 
quantities would be used at a time in laboratory procedures, 
e.g., a half pint or less at a time. 
Conclusion. Thus, as you can see from the foregoing, 
during the period of approximately two years when ICC operated 
the St.Croix site, the only wastes regularly generated were those 
stemming from the process and analtical laboratories. These 
would total no more than a few gallons or so a quarter. Thus, 
ICC was a' small quantity generator during this period. 
- 5 -
301326 
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T W T M a r STORAGE OR OISTOSAI f AUITY BMlUTWN 0 ^ ANY OIFf E«NC£S BflWtEN NUNIFEST ANO SHIPMENT OR LISTING Of RUSONS 
m A i O O U n s m O N OF REJECTED MATIRUIS 
301327 
t tTOMGf OR OlSPONSAl f ACUIIT SIGNATURE "Upon m u j i xipiciion. 
I r M U t r • * * • eoniimi «l Dia tk«mt<n conlaim onh iiu d n o i o i i v O" il>s mimleii 
•0 dJiatOMKie Actt4 on tnu (o«in" 
HANOUNG 
METXQO 
t>^/"^-V • y . 
0 » n 
RECEIVED 
kl cai> «< xtaiincr o< ipij iatn,tii„rf o i l Ilu Eim/onminljl OuaMf 9o«o |t09l 
nS-U92 
DOCUMENT N O . - ^ J , 
P n 
HAZARDOUS WASTE MANIFEST 
OQCUMEffT NO. 
P. K 
Chemical Cocroanv• Incorporated 
PHOMt 
(809) 
778-??nr 
c a r p 
n n F . r a r p 
aprhlphgn^, Cr. r r n i - r 
11. <; . V i - r f ^ n 
T . l . n ^ . 
IRnRNO.I 
T r a i l e r Marine Tranaport Corporation 
PHOM 
(809) 721-1313 
sm AooKss 
l a l a Grande, Puerto Rico 
TMNSraRTlR NO.2 
Tranaporte Diaz 
PHOFC 
(809) 792-7999 
s n AOORtSS 
Zona Portuaria, Puerto Nuevo, San Juan, Puerto Rico 
TKUTMENT. STORAGE OR 
OiSPOSAt fTSO) FACIUTY 
I n l a n d 
C h e m i c a l 
o f P . R . , I n c , 
PHONE 
(809) 85A-1090 
STTE AOORESS 
Km. 5 1 , Highway *2, Hanati, Puerto i i c o 
EPA 
-IMl. 
tlllMlil^LiLlillii! 
0 M. 
ilu 
1 P I R I D I 9 I 8 , 0 , 6 | A , A , 5 I 7 
L :R|D|9|8|0|5|2|6|8|3 
P ' R I D 10 | 9 | 0 | 3 l 9 i9l7 l l 
f 
MORE THAN TWO TRANSPORTERS ARE TO BE UTXKED. F U OUT T « FOUOWING AS A^PROfWn 
1 
1 
THIS FORM IS NO. 
Of A TOTAl Of 
THE fIRST MANIFEST OOCUVEtfT NO. IS. 
PROPER US OOT 
SHIPPING NAME 
P. R. 
^.^ 1° .2 . 
US OOT 
KA2AR0CUSS 
UN 
NUMBER 
fORM 
K T 
OUANTTH 
UMTS 
COtfTAINERS 
NO. 
TTPE 
Eia 
Itk 
KA2 
£001 
EQS/i 
WASTE 
I 
TOLUENE RQ 
Flara. Liquid 
1294 
a q 51 
:ai 
I I I 
1 I I 
I 
I I 
k. u o u 
U Ll-
U U L^ 
U Li_ 
UL. 
U L_ 
SPEDAl HANOUNG INSTRUCTIONS I.NCIUOING CONTAINER tXE.MPTlON l i t lOENTlflCATION Of AOOITIONAl WASTES INCIUOEO IN SHIPMENT OF A N0NHAi4RO0USNATURE WHICH 
DO NOT HAVE TO BE MANIFESTED) 
GE NCRATOfT S CE RTIFICATIOtI: Tta a u n r t i t f Uu lAc U o t nanod n i t B i a t i « i piopcrtr d a u i t i o l i a i a t b t i . n a r t i d ind labtUtd M a i n propn u n a u o n tot iiim«on<non K u i a o q 
te D M •vpliuUo i i g u l i i o u ol K M O n a m n t n i l Tiansponnioo. U.S. EPA n d iKi CanvnonmNh ol PR. Tht w i s t i d t u r i b i d a b n i w i n conv^rud lo thi T i a n u c n v luniid. The 
Tif Mffltni. Slo'>9e or Onoosil f i o i i r t c m md will i c t i p t tht shipfflini ef h u vdous w n t t . and has 3 vsJid ptrnui to do u . I ctnilr thtt thi lofcqotnf is Tut »nd cocrta ta i M best elrnr 
knoMfftdgt^ 
G E K U T O R S SIGNATURE 
r^-T-rVw^ T i l 
Tnu 
Preaident 
OATE SMPPtO 
1 11 11 I 71 Q I 
I fll •>{ 
UU." 
I j i f " 
'JS " 
EXTECTED ARRVAl OAH 
^ 
ANSPORTER NO. I SIGNATURE T o iln ttst oVu^ kntMritdqt tht antfnis ol tht 
sh«intra I h>v« sccepMtftoi irsrfcson cnlorms with Iht diioipiisfl on this mamltsl." 
TJUNS?ORTER NO. 1 
VEHICU 
c r v T T 
10. NO. 
^ ^ ^ " 
I ? ! " " ^^nl^^l ii oi 
OATE RECEIVEO 
1/ 1/ I 
\^Y^\ 
l£ 
MO 
OAT 
TEAR A I THIS PERFORATION 
PART B 
CEN 
EPA 
10 a 
VI TiT^i oiRinifeisnini 
TRANSPORTER NO t SIGNATURE 1 u n i N l h « I h n t nol i i n p n i d M h o t m t i t r u l l Y 
Jdtttd Iht tonunis ol lh"» Ihiomnil • 
OATE OEIIVEREO 
TRANSPORTER NO 2 SIGNATURE "To iht Ptsi ol my knmliOqt Iht nnitnis ol Iht 
thvpmtnt I havt acctplcd foi liansoon conlofms w>ih ir>« dciciiption on ihii miniltsi." 
IRANSPORTER NO 2 
VEHICIE 
10 KO 
I I I I 
I ' 
I I 
OATE RECEIVEO 
I I I I I I L 
T U N S f ORTER NO 2 .^ir.NATURF n ;;nit> i V i U t x ' . ' r t txnpirid »<n oc n t i n i i l l r 
i ^ t r i d Iht contttits ol Ihl, ihioiMni " 
«n 4fr" 
TRUTVENT STORAGE OR OISPOSAI f ACSITY INOICATION Of ANT OlfFERENCES BETWEEN MANIFEST ANOSHIPtmENI OR LISTING Of REASONS 
FOR ANO DISPOSITION OF REJECTED 
MATERUIS 
TRATMENT STORAGE OR OlSPONSAl f ACIIITT SIGNATURE Uoon t i U H nsoitlion 
t ctnihr I h n tht u n i t n i i ol ihii ih«mtni eonloini wiih tht dciaiotiofl on ihit msniltsi 
B u o l Ihdsi OocieDsncifS nolld on this term" 
In c j i t ol tffltrgincy or ipi.l >mmediitilT c**! 'ht EnvMonmenial Quilirr Soiid 18091 
!)2Ma92 
301328 
DOCUMENT NO 
HANOUNG 
METHOO 
DATE RECEIVEO 
L-L-l 
L , ^ 
L 
P R. 
- y 
y 
E / ^ V I R O N M E W f A L QUALITY O O A n o 
O^ZARDOUa WASTE rjANirJ^T 
OOCUM£>(T NO. 
P.R. 
y-'—i 
1^>'\ "taynyi" liXvr^-ft'HeJ 
PHONE 
L.-.;:, 
vi.llfl ti'i" 
• 
'• 
• ' ^ t . .. 
I i-iiuiiE 
.< Ariiia.':<; 
.-.•niiini).-ICJ 
TnJfic 
y---rvV) 
!•- AIMIRESS 
_•_. r . ; r r - . i ' l r ^ r n - V - ' n . ':-.:z. .V--:, 
li.l.Ml.l'NI. SlUIMGC OR 
'•••••""-•' OS--I FACIUTY 
) . - v - . ^ , i 
o ; , , . . . , v . . ; 
r ' 
'• V 
I. 
..Ml Aiiiiws; 
mm. 
(•- ' ' ."-•-Tr-^-> 
' \ ,1:.--rl. ^u 
EPA 
•.:nm ^y^M• r\vu IIIANSCORTERS A K TO BE UTIQID. fm OUT nn FOUOWIHC AS APPROIIAJE 
' 
' — OF A TOTAl Of — 1 — THE FIRST MANIFEST OUCUMENT NO. IS. 
1111$: luiVA IS no • 
P.R. 
>U llll. 
LLLLLinillULLxLL 
.Mr iy-lo.Ki._L.; 
.'.JLi;
iJidxd!jJL_L_l:.J..J;.L.! 
• f - l i t i j ? ,1-; L-J.. J ^ i r J .
I" 
lit 
!• 
rr.iirtR US COT 
SlliniNU NAAU 
us OOT 
HA2AR0aASS 
'A.-:. T,-;-iu.LL 
UN 
NUMOER 
FOfiM 
NET 
OUANTTTf 
.,L..Ld 
l l l l 
I I 
l l l l 
t. ) .1 I 
UWIS 
J i . 
zhrrZ. 
CONTAIWHS 
^0. 
Li_.J 
TTPt 
L J 
L L J 
I 
I 
I 
I 
LJ 
ZZ 
II-.: 
IIM 
I r;:it 
U 
I!l0-
•i:i.v. 
1_L 
L.L 
LLiiU.lL 
LJ ILI ill 
. I > <»l K>\' .'\ii"<- Q S i m c n O N S MaUOWG CONTAINER EXEMTTKM )li. DENTiriCATKM Of AEIOmOHAl WASTES HauOCD M SMPMEKT Of ANOmAZAfnoti':>l«I<)::i 7/:r 
•11 ---.m HJ\=. TO Bt MAWfESTEOl 
' 
;• ii;.iuii • I" liTlFiCMION: Ihs a t» nnitir Uu ihi aten uiwd Kmuvii ait pio^itilr dssilnA UKIIUCU, ouakid andlabettd aid « i n pii>9« conamai ka i.-T>s,i.i Jil^ >.. ..m.. 
i;». Mvlirt Jc rrwiUiom »J tarn P«»«>iien »l TrxspaubK US. EPA m i INt Camnonttitli el f l l The watt d e o i M itiart m n tamnffi w tkt Titwi-:.* i.in>ii T 
-ini.'ni. Sii*'<r" (laroidftoHqaa an^ «4i ecupt the leieHeni e^liaiydanw.isJt. Mti lias i valid pamit la dese. l o i t i ^ lliai ih#> fortyMiqisinManitfanttM'iiHr h"-*"i> 
».Mr«ion'.;siuvMius£ 
THU 
• .'iSnJRTt-'i NO 1 SlGNATUff "T« » • fc««l •* trt ta—UP^t Dw t M t n o tl Iht TRANSTORTER Na t 
VEHKIE 
«. NO. 
.•; 
OATE SMlfED 
4 y y y y y 
) 1 1 V 1 -1 1 1 
•• - 1 •.' -• 1 . 
/xncTio inaii.i. n« 
LJ_J 
l.L.i 
OArEiaci:yin 
1.J-' I. L.l 
' MO 
|..i 
HAR AT TWS PEItfOKAIlUN 
:y-k-. %y---^ 
•/-
.!IT ••! 
GEN 
EPA 
DJ» L J_LJ_L-UI-.I 
••..••.tnjKIIHKO. I 
: - 
.1 Ih:: |..nlrTirt SHNATimE iaryiVi>*'ii>*n'*"'*'*"^.<'<***M<su')r 
\ 
.1 ,.„.''^^/^^,<^-7/kz,:-''..y\,.t .„-.y ylky.-y. 
\ IH :.'.rOn'l R NO 2 SONATUK ~7« Kw kwt ti mt >i«i«ii^. I M wntMs tl Iht 
j •>,),iw«l Liw t r t i > i t d l a r t n > a p « i E B ^ a s ; ± ± : t = ; ; ^ a I k i s s a « l t s l ' 
TRANSTOHtER NO. 2 
vtwaE 
B NO. 
I I I I I I I I 
DATE Ot','•.•»:> ;i 
L L J 
L •• 
OAII 
ir.iii.' I 
L-l_) I..I. 
«X1 
.I;'. 
I \t.y4snm\.*. n i BEUTUK •\^f*t kii i kM m U>«B«d « M « wda>u*r 
k^kk 
ri(.\ W « i SIOMfi M g e r a t M ^ ^ a i n W C t T n IF MtTOFFERCNas I H M i N UMVESTAM SIPMEirT W U T K OF l
U
^ 
rv, 
301329 
TRAiMEin siuHAg OH annmi^ twam awuiat -u>.» tamd t-tieom 
t:«<«t fce-.t dBcinawn «»<•< «* » • > » • ' 
•_ 
l l t « d (tOSI 
" 
C/n 
Mfl'iOO 
5^/ ».' 
S*TF Kcimo 
J^_ilfe 
tWCUMEKT M. 
_ P. H 
i.*E 
A^PilORNAME 
^ i . : ' 
...; ciio-iiciti Co., i f w . 
UUCUMlNi N U . 
PHONE 
(I.U9) 7711-2201) 
P sm AOORESS 
1. 
:<: 13 'J Cctuto flc'ihlchcn, St. Croix, U.S. Vir.nin Irjlcndj 
IIUNjrORIIR NO 1 
r, - l . l - ''..rinn Trmqiort Cnrjinrntlnn 
PHONE 
(!;<iy) 721-1313 
SITE AOORISS 
TRANSPORIER NO } 
1, 
Lo ':;i;iz 
PHONE 
(•JU7) 792-7999 
SITE AOORISS 
/... 
;• M-Lui^rtn, Puerto Nuavo, S:in Ju.jn, Fuorln \\\ca 
TRUTMENT. STORAGE OR 
oisPOSAUTSoiFACIUTY I n l . - n d Clim.i.lcal o f P . H . , I n c . 
PHONE 
(i;;j9) nw-iii90 
SITE AOORESS 
.. . y., lll.MU.iy J 2, M-nncitl, Puorto Rico 
f 
R. 
ir 
'3 
EPA 
0 
mi 
V,I,D,9,a,Q,C,,!.,l,n,;, 
p,n,D,9,Q,n,6,i,A,3,/, 
P|R,D,9,U,0,5,:;,--,,:'.,^ 
p,R,i),n,9,n,3,9,y,7,i, 
IF MORE THAN TWO TRANSPORTERS ARE TO BE UTUIZED. f U OUT THE fOUOWlNG AS APPROPIATE 
THi^ (npM IS nn 
nf A TOTAl O f — J — T H F FiH<n MANiFFrrnnriiurifTiin is 
P R 
I | 
C , 
0 | 
3 ) 
i 
i 
PROPER US OOT 
SHIPPING NAME 
,Ti:>T-..-v:: . . : 
2 
3 
4 
5 
6 
SPECUl HANOUNG INSTRUCTIONS INClUOING C 
00 NOT HAVE TO BE MANIFESTED) 
US OOT 
HAZARD ClASS 
Flcin. Llc^iitl 
UN 
NUMBER 
1294 
FORM 
L 
• 
Mr 
QUANTITY 
lA|7lfi|3 
UWTS 
Ccil, 
CCNTAJNERS 
no. 
TYPE 
1 11 illtX 
I.Jil, 
I n II J 
! 1 
: 1 1 
1 . . 
1 
I 1,1 
L J . 
IdB-
iPA 
KAi 
cirtf 
Li 
EQB/EPA 
WASH h 
In.', 
!- 1 1 
I I 
L. 1 ! 1 
.
1
1 
M i l 
}NTAINER EXEMPTION r i L DE.NTIFCATKIN Of AOOmONAl WASTES INCIUOEO IN SHIPMENT Of A NONHAZARDOUS NATUKE WHICH 
I 
GENERATOR'S CERTIFICATION: This a to unilY tha ih< aboti namtd aaiinals u t piopirtr dassilitd. disoibtd. inarttd and labtlltd and > i n propv onoiuen io> i r n p o n a i a n x u r o i n g 
le Iht applicaMt rtqulaiions ol tht Oiavimtnt ef Trarupontfton U . l E?A and tht Cemaicrwtahh of P.R Tht w m a dtsnihtd a^ovf w t r t conijfntd le dit TiamoonB eamtd. Tht 
Trtaimtnt Sieragt er Oisoosal f acilbr can and will accept ilM shipottm ef haiirdous wasia. and has a vafid ptfmii te do sa. I canifr thai i h t fort^oir^ is n a *^d csnta le ibt best of mr 
inawliiliit 
GENERAIOirS SIGMATURt '. - .-. 
. 
; / 
•, / • f V ' 
' , 
; 
Z 
•Je3:tjnQ H . l u c h v l t ] 
^ 
TlTlE 
P r c j i d c n t 
DATE SHIPPED 
CUII L ^ dJZJ 
*HJ 
D A Y 
\-\ 
ex?ECTIO JUWVAL DAT! 
1 ^ 
q.if' c 
TRANSPORTER NO 1 SIGNATURE "Te the btsi el H Y kKMi<ti«9t the o n i m s el the 
sJiiprntnl t li>ie Kceplcd lor liarissert anlerms with Ihe dtsoplion on iSs maniltst." 
TRANSPORTER ND. 1 
«Hn:u 
SCXU 
P. l3 l l i n r> lO 13 
DATE RECEIVED 
llLJ Liil 
MO 
DAY 
TEAR AT THIS PERfORATION 
yz-zs// 5c-
_ = PART B 
y 
/ k 
GEN 
EPA 
IDS 
|v ll 0 |9 h3 0 n 6 1 0 
IRi';;?ORT'-^IC ' S;GNt:uRE "Icini>y i(iail>ijyr^int»rn:t't4.<?ihorm>itiijilY 
Witrrd the cuflienil o' !hil i n i o m t n i ' 
k
^
—
' 
^ . f ^ - 
7 i -i . '. 
• • y y ' ' • / / .f/1<. 
rS )(o. 2 ^z^L 
' \ j k A ^ 
^ . 
TRANSPORTER NO 2 SIGNATURE "In iht b t i t ol my knowlidjt ihi camtnii ol i « ^ 
shifpmcnl I h^ve .ccipicd lor iraniporl conlorms wilhihe desuioiion en this manilesi 
TRAHSPORTtfi/o. 2 
VEHICU 
10 NO 
I ' I 1 I t ) I 
OATE RECEIVEO 
I I 1 l _ L J 
TRA.'JSPOflrrn NO 7S'CNAruPE t eini^y thai I na-/c not lamot'cd •..rftor 
ffijitnallT 
alltfcd Ihr Lunlenl, ol Ihn shipment ' 
I 
I 
I I 
; 
L _ l 
IKJATiiJJJT STGSiC; S" SISrOSAl fACniTY INDICATION 0? ANY DKfESENCtS BETWEEN MANIFEST ANO SHIPMENT OR USTING Of REASONS 
FOR t n u OiSPOSIIinN Of REJECTED MAIERIAIS 
HA.MUlitJC 
H'll'U.'O 
:5 
TRATMCWr ::onACE Ofl O I S P O N S I L U C a i l t S I C W A T U W -Ueon m u x .Aiptction. 
I ctnity rhat iht contents ol ttiii thipmim conlofm wnh th« dtiuipitononiht] nuntlisi 
i « t i m ilioie dtNd'iuncni ftontj Oft thn •»!(«" 
-'• Ci'.t ul c 
M \r" < •ituitftit.iifiv LJM int EnvKonmrniii GuixiT n m i j lUDOl 
DOCUMENT H ( y p : < i 3 
p fl 
301330 
H A Z A R D O U S WASTE 
M A N I F E S T 
nnciiMEKi NO 
PR 
IC W 
TOI NAM 
land Chemical f n , , liu:. 
Mlii/.l 
(Om) 770-2200 
AOCWSS 
E s t a t e 13n Estutt- Bcthlehefn, St. Cniix, U.S. Vinjin Inlunth 
IPA 
o 
IC 
|V|I|D|9,n,n,6,5|1 (1 
iiuNSPfwnR itl) I 
T r a i l e r Marine Trunnport Corporation 
IH'IM 
(ni)9) 721 1313 
sill APimi.sr. 
I3ln GrantlR, Piu|£to Rico 
1 rnnriportr Dia.'. 
[a\Y)) 7')2-7'.>99 
s;ii i.MRt.^S 
'loiMi Portuaria, Puerto Nuevo, San Juan, Puerto Rico 
i K i i r
~ 
••,:( l•^Cf i.ii 
ij'.i•?!»:•'•••• "-citi:' Inland Chemical of P.R. , Inc. 
i-ll/i:.' 
. 
(009) 034-1090 
Km. ' ' 1 , Highway SI, Manati, Puerto Pico 
JP.R,0,9,0.0,6,^4,5 
P|R|D,9,0[0,5|2|6,I1 
P|R,D|0,9,0|3|9,9,7 
n i i i lii.'iM l i ?.•! 
•.;l IIL-.:..^.|il i - a t l ! M H Uif.lZlO, U l OUl IHE 101llii\.«'.i AS A l T l i ' T U l ! 
1 
.. _ 1 
l-l l lOIAl 01 
TW l.'RIT MAMILSI DilCl.'Mi:,! NO IS 
r R 
II |C 1° 1^ I J 
L 
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US OOT 
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riam. Lic;uiri 
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^ \ 
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301331 
v . - , : ' . u i r • 1 
1./ : ' . ' H I ' ' 
* . i i ' . • : • . » .HirJ r-* ' • • • _ • ' , , , . , _ ^ , _ ^ 
- . ^ — _ _ 
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Ih 'kh 
m 
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A; 
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aVRATOIIM 
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^ 
BnAOoxu 
n**d_«n»-iwt-io 
t i ' A O I C 
M A N I F E S T 
OOCUMJKT NO. 
aVRATOIKAMf 
l a l a n d Chemical Co., 
I n c . 
P fl IC 05 
PNOMI 
(809) 778-2200 
on Aooxu 
Estate 130, Estate Bethlehem, St. C r o i x , U.S. V i r g i n 
Islands 
TUNsmmRao.i 
T r a i l e r Marine Transport 
Corporation 
P1<IINf 
(809) 721-1313 
snt Aoonss 
lala Grande, Puerto Rico 
IRANSPORIIR NO.2 
Tranaporte Diaz 
P1IIINI 
(009) 792-7999 
SmAOMCSS 
Zona Portuaria, Puerto Nuevo, San Juan, Puerto Rico 
TREATMENT. STORAGE OR 
, 
DisnSAi(TSDifAoun Inland Chemical or P.R., 
Inc. 
riiUNE 
(n09) 0 54-1090 
Sin AOORESS 
Km. 5 1 , Highway i 2, M a n a t i , Puerto Rico 
f MORE THAN TWO TRANSPORTIKS A K TQ K UTUZEO. I U OUT T K (OUOWMS AS AnROPUU 
" A 
0 
HO 
| V | I | D | 9 | 8 ,0,6,5,1 Q, 
| P | R l O i 9 i a , 0 , 6 , a . 4 , 5 
ILU 
| P | R | D | 9 , f l , 0 , 5 , 2 | 6 , 8 , 
| P | R | D | 0 | 9 i O , 3 i 9 , 9 , 7 , 
THIS fORM IS NO-
1 
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SHIPPJNG NAME 
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T W f S S T UAJWEST DOCUMENT NO IS 
P.R. 
II 
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US DOT 
HAZARD CUiS 
Flam. L i c u i d 
UN 
NUMBER 
1294 
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so NOT HAVt TO EE MANIiESIEOI 
CJ Nl RAlOfi i CE Rllf ICATIOri l>«s a te ctnih, tha >he tbcwt T»ai«td main«s ar i eroptilr cijtsilitd tir-i niirH mjikeii jnd labcUtd i i m . . . « i - . i , . : , i i»i.i..« i.., :i..r.p.ii.d.oi xiuromij 
to IIM appliciblt.rtpulatioru el Iht Otearuntnt ol Tiartspodairtn. U.S EPA and the Connmwtalih ol I' R Tlir wjsir dnnibcd jtic.-e .^-.tp iiirr.4')i.r.(i -t* ii. - ii-.i-.fl:.-.ti ivencd Iht 
TitauMni. Sioiajeer Disposal I acUtti u n a « d » 4 acttpi ihe shipiitM i l h j / i b a j s want, aidhas j \ J i d | i n i i „ i i u do le I cRiilt ih.i it-- lunKri'iilis n w c o i t u ' i t i i i o i h i l . n i t t i T . r 
Uawltdpt 
GEkERATOfTS SIGNA 
Jerome tf7^Luc>wig 
TTUNSt^RTlR Nfr-1 SICNAIURE H e UM b t i i el r r biewltd9e the csntars t l the 
•Aipmeei Ihakf x c i p i c d br Brupon c o n b m i wkh ihe desof lioa ta ;as luriiltsL' 
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President 
OAiE sini-pin 
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TRANSPORTER NO I 
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^ ^ ^ 
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PART B 
r.iN 
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V| I [ D | 9 | B | 0 | 6 | 5 | 1 | 0 | 
TMNSPORHR NO I SIGNATURE 1 
ahtrvd Iht cviltnis el Ihii 
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TRANSPORTER NO } SIGNATURE l i Ott b u t al n r k m r i t d ^ the c a i n i s t l n t 
l^ipqnicnl I ha.a acceplad tor trtRs^en cartoms wifit the desstptiort e« ?«s c»*nil*^L'' 
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TWATUENT STORAGE ORBIS?DSAi F A n m fCCATION Of ANT OJflHNCES BETWEEN MANIfEST ANOSHIRMENI OR USIINC 01 Kl AS11N5 
F M ANO DISPOSITION Of REJECTED 
UAHRUIS 
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L 
IRAIMENI STORAGE OR D1S?3NSAI lACJinr SICNAIURI "Uoon r u a .mppciion. 
I candy that dit o n i i M i ol ihu ih^mtni (onljim with iht descupiioi en that mjii.iit, 
t i t t e l llioit d'lcrcttancnt neic^ tn Ais term' 
In cast el imfipffnry or ipij ..-mfilia*«>r (III Ih. |n*"«»imeni,l [Vj»J.r, ^•....l , M I " 
l i ' i 199? 
M.MtOUNG 
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UOCllMfKI NU 
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IC U6 
«NIUT0«NAM« 
. 
. 
_ 
I s l a n d Chemical C o , , I n c . 
SIIE AC0MS3 
E s t a t e 13Q, Estate Bethlehem, St. C r o i x , U.S. 
TIlANSMmiXN0.1 
T r a i l e r Marine Transport 
Corporation 
VtlllM 
(niv) 
7711-22(10 
V i n ] i n 
Islands 
1 PHIINI 
|(,009) 721-1313 
I STE AOORESS 
1 I s l a Grunde, Puerto Rico 
TRANSPORTER NQ 2 
1 T r a n s p o r t e Diaz 
riil;M 
i(fin9 
1 SIK AOOMSS 
Zona P o r t u a r i a , Puerto Nuevo, San J u a n , Puerto Rice 
TlttATMEJfT. STORAGE OR 
- „ 
„ 
. 
1 oiswsAirsoif*cwrr I h l v > d Chemical o f P.R., I n c . 
.myji')!..... 
3 
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854-1090 
sm AOORESS 
Km. 5 1 , Highway # 2 , M a n a t i , Puerto Rico 
11' ^ 
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Iitainitni. Sierat;t or Otspdsal f a c ^ on and wtU xctpt the ihjpei«« ef h^adous w^itt. and Kai j».4i;i ti-.n'r.i in ao in i ct^iiK ih.j :IIF •... ..^i^i., n irnr jn.: r..irrn:«'-' t t v <.i :., 
CIWRAIORS S I G N A T U I « W ' ^ ' ) Y V » U . / 7 I 
/Jerome H. Ludwig 
(^ 
iini 
Preaident 
IIAII a'liTiii 
1RANSP0RUR NO ) SfCNATURE Te the k«st o< en trpite»,i xu eeiinis e< the 
Oi^ntv I hart accepted lor uans^art csrilorma weft tht desaipi«ii ee i ^ mamiul.*' 
TRANSPORIlH Nil I 
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IfUNSPORTER NO 1 SIC NATURE T emitr I 
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IRANSrORIER NO 2 SIGNATURE Te ihi hesi ol e^ bioiidt^ Die c^timti s( tht 
ahippeiiri I h m acCKiitd lor trmqen cdxteira rMi the »aa«lr9i at d u Ranfwt." 
lUNSPORTER NO 2 SIGNATURE 1 tariit t u l I kare u l i m ^ w t l a a m a a e r i ^ 
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1 
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VEHIQE 
10 NO 
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E OR AND DISTOSJllON Of REJECTED VUTIRUIS 
Z ^ i Z Z 
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TRAIMENT STORAGE OR OlSPONSAl fAOKTT StCNAIURE "U»a> M a * telaediin. 
Iltiiilf ihei the nnienii oliliiiih«mtfno3nloi>nw<<Kihetaa^iaianlhiitienjleit 
iitipi ihoai diicitpenoti neiid en lAis I o n ' 
In c u t ol fmrigtncr ff i p i j inunidult^r tall Iht E/v.iionmmlii Ok«L/T Aoara iCCJ. 
72i 1197 
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I aland Che»a. 
- t ^ 
- c T ^ OOCUMEjttNO. 
PR. IC 07 
(809) 778-2200 
Eatate 13Q , Estate Bethlehem, St. Croix, U.S.Virgin Islands 
Triilor Marine,Tranaport Corporation 
PHONE 
(009) 721-1313 
SItifiONU 
,, 
Isla Gr^ide, Puerto Rico 
IP» 
0 NO 
V|1|D|9|8,0,6,5| 
|P,R|Di 9,8,0,6,4, 
I H A N S M M I R M J 
Transporte Diaz 
pmiNi 
(U()9) 792-7999 
Slit Aoocn 
, : , 
I..,. 
Zona Portuaria, Puerto Nuevo', San Juan, Puerto Rico 
P|R|D|9|8|0|5|2|, 
TRuiMin. SToua OR 
- | 
Drtyoau.(Ttci fAOJTr Inland Chemical of P.R., Inc. 
"^^009) 054-1090 
tm*oo«a , • |- . ' 
Km. 51, Highway. # 2, Manati,:Puerto Rico 
P,R,0|0,9,0, 3|9,' 
I MORE TMAN nvO T M N S P O n i J B i K TO S U T l u a , H I OUT TW fOUOWNE AS APfflOPIAIE 
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00 NOT HAVE TO K MANffESTlOJ 
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l i i a i m t n i . Siaa^t oi Dopee J f i e * H o « a<d wi« ace w t the i l i r a n e l t a t a d o i a want, and t u t a <aii4 peiiwt te de sa I ceiitt that thi inr^joinqtssueindcancuieiiiebeMi 
inowttdje 
• 
I 
I 
• 
GIWRATOITS SIGNATURE 
Jerome H, LucVig 
TlUE 
President 
IKANSPORTER NO I SIGNATURE T e m t ten el n r k n a t e ^ Ble caaiaMi el I N 
.i!4<iiitni lha%r i K i p i t d I a uausencsnlDiira wentht d i s s v i a a eaOBBanilesL" 
OAIE SHIPHU 
kULMk^ 
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19|2|8i2n |9i0i 
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E«tit« 13Q'| Eatite Bethlehem. St. C roix, U.S.Vinjin IslamJ;-. 
Trailer Marine Trahaport 
Corporatic 
TlWJ) 
721-1313 
BTt lOONSi 
, 
! 
lala Grande', Puerto Rico 
IMANSrORTER NO 2 
Tranaporte Diaz 
nii'.ii 
(iu!M) in-Trj'.i 
JITt AOOMSS 
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Zona Portuiatia, Puerto Nuevo, San Juan, Puerto lUim 
TRIAIWW. n o M W M 
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oorosAtnai>*a"TT Inland'Chefflical of P.R., Inc. 
m AOORin 
1 , 1 : " 
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Km. 51.'Highway: t\:2, Hanati,; Puerto Rico 
PllUfll 
IU!II 
(Ofl')) 11 54-109(1 
r u n « .THW T W TKMsrainiK M C ro • 
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t i i a i n t n i S t a a ^ v O i t p e t i t r i E i i i ^ a i a W a d l accept the iKV'aan e f U i a dais w a i t , a i d h i i a.J>.i|i.iin.i m i i e i o l i n n t i 'ii.i iii.. I>«i.ij<v<j<i our . o d i i - i i i i i i H i c t i M i d n . 
If*wttd9d 
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JeroBB H. Luciwiq 
TlUE 
iiAir jjnniii 
President 
I h ^ 
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IliillSPORirR W 
I SIGKATURE T e Ita k»»l el «ij krawlad^ tfie e o t c n a ol ih« 
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iMAtuiKT STORAGE OR o a r a « 
I OR tJtO DISriiSTXM Of KJICTU 
IRANSPURtill Ml 
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• 
Appendix H 
May 17, 1983 RCRA Inspection Form 
\VVORK\24231\02\WORKPLAN.REP 
HARDING LAWSON ASSOCIATES 
^0133^ 
-±.>. 6^^— ^ s 
RCRA INSPECTION FORM 
I 
a . 
Report Prepared For: 
Generator 
Transporter 
HVJM (TSD) F a c i l i t y 
Copy of Report Sent t o t h e F a c i l i t y 
Z'w k 7 
IZZJ 
C J 
F a c i l i t y 
Information 
Name! 
Address 
EPA iD#: 1/rp 7 ? r o / 5 7 M S ^ -
Date of I n s p e c t i o n : 
t ' ^ . " ' ^ ^ ' / ^ '4^ A * ^ ^ ^ 
f-
4 ^ 
-d, 
P a r t i c i o a t i n a 
Personnel 
*A Personne. 511 KZ%efryZu^../.^^c,^f',. Co.cy.s. 
Dyy^ ^ D ^ Z S ^ 
Facility Personnel: y ^ ^ . y^/Qm^Z.^ u . 
y / ^ y ' ^ ^ A 
• 
Report Prepared by (Name) : /1 . \ / k C^"/^ /r 
Agency: 
C^6ykp//)^y^^/D ^ ^ 
/ J ^ L 
Telephone Numb«r: 
^ K l Z ^ 
- T ^ - ^ ' ^ 
^T^O 
Jefom« H. Ludwvj. Ph.D. 
fratiaant 
JslafKl Chtfnical Co., lf>c 
P.O. Bo« 6733 
OiriitMfMlad, St. C'Oix 
U.S. Virqin I t l j n d i 00820 
(8091 778-2200 
V\ 
AUc B. Smith 
Plant Erigirve*< 
liland Ch«mic«l Co.. Inc. 
P O . Boee733 
C h r i i t x n i l t d . St. C'On 
U.S. V i r f i n i m r y j i 00120 
IBOfi) 778-2200 
s.be.«.«y c( eej?t§x 
''^o rcZ^ykaJlfi/U. 
V V t v M . N . J. 07470 
( 2 0 1 I 6 W - * 1 0 0 
SubdidU fY Of BgJUjLliX 
CaiiM Knolli. NJ 07927 
(201) &40.a700 
301337 
-C-
l3 there reason to believe that the facility has hazardous waste on-
site? 
a. If yes, what leads you to believe it is hazardous waste? 
Check appropriate boxes: 
/ / Company admits that its waste is hazardous during the inspec-
tion. 
/ / Company admitted the waste is hazardous in its RCRA notifica-
tion and/or Part A Permit Application. 
/ / The waste material is listed in the 'regulations as a hazardous 
waste from a non-specific source (261.31). 
/ /. The waste material is listed in the regulations' as a hazardous 
waste from a specific source (261.32). 
/ / The material or product is listed in the regulations as a dis-
carded commercial chemical product (261.33). 
/ / Testing has shown characteristics of ignitability, corrosivity, 
reactivity or extraction procedure toxicity, or has revealed 
hazardous constituents (please attach analysis report). 
/ / Company is unsure but there is reason to believe that waste 
materials are hazardous. (Explain). 
301338 
1 
V 
-A-
Susaarr of Flncdinsza 
Ui 
o 
tjJ 
Ui 
vo 
^:?^ 
Facility Deacripcion and Operaeiong 
nZ<Z^r^ J rI^^:.y.:[P..ySTQrr^ 
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(^^•^Wf 
vlcles chac result in ctie generacion 6Z lUitH-S^Ms^ 
( & . 
^ ^ . - r ± 
Ic^jfe.-::^ -^ y A. k^^y^—y<L. 
(i 
HOT FOR RELEASE TO CDMP.\trf. PROTECTED INFROHAIION 
-C-
Sueaaarv, Conclugiona ^nci Racotanendations 
Z. 
/^^^r- JAAy^-tkkZ~lT7Zt——77nP. 
\ 
•, 
NOT FOR RELE.\SE TO COMP.\NY. PROTECTED 
INFROHAIION 
- C -
Susxjar'i', Concluaiona and Reconmendations 
. ^^>M '-X'--^-----<f^,^^* f i 
^ 
Z 
yyZt^^-kg 
cLmty/ , ^ - ( ^ ^ y i ^ 
lXaJ_£. 
9hrA * 
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.^-••.—,-<:.-.T.^. 
Pump" ' ^ 
re 
ISO 
100 KVA 
Cer.cr.Ttor 
Dryer 
Building' 
, , Cooling 
Tower 
U.S.V.l. 
Guard IIQU.SC 
"'•^^^-*^l 
Reverse Osmosis 
Chlorine 
^
^ 
,.,^Stnrai;c 
350 KVA 
Cone r.l tor 
Glaas Plant 
• Stainless Steel 
Plant • 
Hot Air y 
. 
Drying Roon 
^itainlcsa Steel 
Storaso Tanks 
:!•"••; 
i^P-£S>«Hng 
i, •'•''' 
• Tower>><."- ' 
: 
Utility 
Building 
I . - 
.;..•'S 
iiJ.:""; 
" ": 
Paved Parkin;;/Rond Arna 
M-
unch Uocra — 
roiaing Roora 
Storage 
Shipping; 
: '•••' Aro.T 
Finishing 
Area 
Office 
AriM 
Ljbi)rJCory 
Arra 
Warehouse 
Area 
Truck Dock 
-Truck Dock 
I 
• I 
I
.•
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I ' l 
IJccure 
Storage 
Area 
:-. I 
301342 
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Tank Fam 
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-1-
GENERATOR INSPECTION CHEC.XLIST 
\ 
40 CTR 262 Subpart A ~ General 
YES 
}K) 
N/A 
262.H - Hasardoua Waaea Determination 
1) Old t.ha generator test Its waste to deterraln* 
whether 
It Is hazardous? 
Is the waste hazardous? 
2) Is the generator detenalning thht Its waste 
erhihlts a hazardous waste characteristic(s) 
based on its knowledge of the naterial(s) or 
processes used? 
40 CFR 262 Subpart B - The Manifest 
- - K 
Has hazardous waste b««n shipped off-site since 
November 19, 19607 
If yes, approxiaately how many shipoents, off-site, 
have bi«en aade and describe the approximate size of 
an average shipment made on a nonthly basis.. If fa-
cility i>Na saAlI quantity generator, please" explain. 
Llity ^»^* saAlI quantity generator, please explain. 
^^ . - / 
^ / 
262.21 Does each Rajiifett (or representative sample] 
have the following information? Please circle 
the aissinq elements. 
- a manifest docoaent nuaUser? 
- t h e generators name, mailing address, telephone 
nuaber and I.D. Nusiber? 
- the transporters naste and EPA I.D. Nuaber? 
- the naae, address -and EPA I.O. Number of the desig-
nated facility? 
-. a description of the wastes (DOT) 
- the total quantity of each hazardous waste by units 
of weight or volume, and the type and number of con-
tainers as loaded into or onto the transport vehicle? 
- a certification that the materials are properly 
classified, described, paclcage, marXed and labeled, 
and are In proper condittion for transportation 
under regulations of the DOT and EPA? 
(obtain a copy of the incomplete manifests] 
vaa&.3i.n a t^upy oc 
ci 
5/7-^ 
CUJJ-5^ f^^jk 
k 
301343 
I 
• ^ 
40 CFR 252 - Subpart 0 - Recordkeeping and Reoortlno YES 
NO 
N/A 
262.40 Has the generatoraaintalned facility records 
since November 19, 19807 (manifest, exception 
report and waste analysis) 
262.42 Has the generator received signed copies 
(frcm the TSD facility) of all the manifests 
for waste shipped off-site more than 35 days 
ago? 
If not, have Exception Reports been submitted 
to EPA covering any of these shipments made 
aore than 45 days ago? 
40 CFR 262 - Subpart C - Pretransportation Require-
ments 
262.30 Before transporting or offering hazardous 
-33 
waste for transportion off-site does the 
generator: 
1) Pac)cage the waste in accordance with appli-
cable DOT regulations (i.e., 49 CFR Parts 
173, 178 ( 179) 
2) Label each package according to DOT i i . . ^ . ; 
49 CFR 172) 
3) Mark each package according to DOT (i.c-., 
CFR 172) 
4) Mark each container of 110 gallons or less 
with the words "HAZARDOUS WASTE - FEDERAL 
LAW PROHIBITS I.MPROPER DISPOSAL. IF FOUND, 
CONTACT THE NEAREST POLICE OR PUBLIC SAFETY 
AUTHORITY OR THE U.S. EPA', and Include the 
generators naae, address and manifest docu-
ment nuaber. 
(i.e., 49 CFR 172.304) 
262.34 Accumulation Time 
1] How ia waste accumulated on-site? 
/ 
/ 
Containers 
/ 
7 Tanks 
/ 
/ 
SurfaoB iitpsundnents (carplete SV*5" checJclist) 
/ 
7 
Piles (cotpleto SS*T ciiecklist) 
2) I s w a s t e accumulated for more than 90 d a y s ? 
If y e s , complete SVfl-lF c h e c k l i s t . 
3) Is each c o n t a i n e r c l e a r l y d a t e d wit.h each 
p e r i o d of a c c u m u l a t i o n so as to be 
v i s i b l e 
for 
i n s p e c t i o n ? 
4) Is eac.i c o n t a i n e r c r tank marked or 
l a b e l e d 
w i t h the words "HAZARDOUS WASTE" or i n 
c o n -
p i i a n c e with t h e DOT l a b e l i n g r e q u i r e m e n t s ? 
STOP HERE IF-THE HAZARDOUS WASTE .MGT FACILITY (TSD) CHECKLIST IS 
FILLED CUT 
301344 
-<fflkj<:s t e^kzi 
•,-3-
i / i y C ^ ^ s S L r ^ 
262.34 - Short Ter:n Accumulation Standards 
(For generators who accumulate waste i.i tanks or 
containers for 90 days or less) . 
40 CFR 265 - Suboart I Containers 
YES NO 
N/A 
265.170 - What type of containers are used for storage. 
Describe the size, type and quantity and 
nature of waste (e.g., 12 fifty-five gallon 
druau of waste acetone). 
265.171 - Do the containers appear to be in good condi-
tion, not in danger of leaking? 
If not, please describe the type, condition 
and nuaber of leaking or corroded containers. 
Be detailed and specific. 
265.172 - Axe hazardous waste stored in containers made 
of compatible awiterials? 
. 
If not, please explain. 
265.173(a) - Ara all containers closed except those in 
use? 
• 
i^ . 
, 
265.173(b) - Do containers appear to be properly opened, 
handled or stored in a manner which will 
minimize the risk of the container ruptu-
ring or leaking? 
265.174 - Is tha storage area inspected at least weekly? 
265.176 - Are containers holding ignltable and reactive 
waste located at least 50 feet (15 meters) 
away frca the facility's property line? 
265.177 - Ara incompatible wastes stored separate froa 
each other? 
40 CFR 265 Subpart J - Tanks 
265.190 1) What ara t.ha approximate nuaiber and size of 
tanks containing hazardous waste? 
2) Identify the waste traatad/storad in each 
tank. 
265.192 - General Operating Requirements 
1) Are the tanks maintained so that there is 
no evidence of past, present, or risk of 
futura leaks? 
If no, please explain 
301345 
l i ) • 
b 
YES SO 
N/A 
2) Are there leaking tanks? 
3) Ara all hazardous wastes or treataent rea-
' gents being placed in tanks compatible with 
the tank material so that there is not dan-
ger of ruptures, corrosion, leaks or other 
failures? 
4) Do uncovered tanks hava at least 2 feet of 
freeboard or an adequate containment struc-
ture? 
5) If waste is continuously fed into a tank, 
is the tank equipped with a means to stop 
the inflow from the tank? 
e.g. by^ss system to a sandby tank 
265.194 - Inspections 
1) Is the tahk(s) inspected each operating day 
for: 
a) discharge control equipment 
b) aonitoring equipment ; 
c) laval of waste in tan)c 
2) Ara tha tanks and surrounding areas (e.g., 
dike) inspected weekly for laaks, cncro-
sion or other failures? 
265.198 
3) Ara there underground tanks? 
If yas, how many and can they be entered 
for inspection? 
- Are ignltable or reactive wastes stored in a 
manner which protects there from a source of 
ignition or reaction? 
If no, please explain. 
265.199 - Does it appear that incompatible wastes are 
being stored separate from each other? 
265.16 - Personnel Training 
1) Have facility personnel successfully com-
pleted a program of classroom instruction 
or on-the-job training within 6 months of 
having been employed? 
If ve:^, have facility personnel taken part 
in an annual review of training? 
'
• 
301346 
\ 
\ 
YES 
ao 
N/A 
2) Is there written documentation of the 
following: 
-job t i t l e for each position at the 
f a c i l i t y 
r e l a t e d to hazardous waste management and 
the naae of the esiployee f i l l i n g each job? 
-type and aaount of t r a i n i n g to be given to 
personnel in jobs related to hazardous 
wasra management? 
- a c t u a l training or experience received by 
personnel? 
3) Are training records kept on a l l employees 
for a t l e a s t 3 years? 
40 CFR 265 - Suboart C - Preparedness and Prevention -
265.32 Does the f a c i l i t y cooply with preparedness and 
prevention raquiraaents including" maintaining: 
-an i n t e r n a l coaoiunlcations or:alann system? 
-a telephone or other device to siJmaon 
emergency assistance from local a u t h o r i t i e s ? 
- p o r t a b l e fira aquipswnt? 
-water at adequate volume and pressure to 
supply watar bose streams, foam producing 
equipaent, e t c . 
265.33 Is equipeaent tasted and maintained? 
265.34 Is t h e r e inmediate access to comraunications or 
alara systems during handling of hazardous waste? 
265.35 Adequate aisle spaca? 
If no, please explain storage pattern. 
In your opinion, do the types of waste on-site 
require all of the above procedures, or are some not 
needed: 
Explain. 
301347 
-6-
ai 
YES NO 
N/A 
40 CFR 26S - Suboart D - Contingency Plan and Emergency 
Procedures 
Does the facility have a written contingency plan 
for emergency procedures designed to deal wtch 
fires, explosions or any unplanned release of ha-
zardous waste? 
1) Does tha plan describe arrangements made 
with tha local authorities? 
2) Has the contingency plan been submitted 
to the local authorities? 
3) Does tha plan list naaes, addresses and 
phone nuabers of Emergency Coordinators? 
4) Does the plan have a list of what emer-
gency aquipiant is'available? 
5) Is there a provision for evacuating, fa-
cility personnel? 
' 
6) Was there an awergency coordinator 
present or on cal:at 
-f-
301348 
Appendix I 
Waste Classification Analyses and Disposal Profiles 
\WORK\24231\02\WORKPLAN.REP 
HARDING LAWSON ASSOCIATES 
301349 
Laboratories, Inc. 
Subsidiary ol Schering AG, West Germany 
REPORT APPROVAL FORM 
TITLE OF REPORT: Analysis of Material from Bulk Storage Tanks 
17, #8, #9 and 113, Island Chemical Company, St. Croix, Vircir. Isla.nc£ 
DEPARTMENT/TESTING FACILITY: 
M e d i c i n a l 
C h e m i s t r y 
STUDY NUMBER(S): 
DATE OF REPORT: 
November 
1 0 , 
19S2 
REPORT PREPARED BY: 
D a n i e l 
S z e t o 
SUBMITTED BY: 
APPROVED BY. 
APPROVED BY: 
RECEIVED BY 
•2. •y^^^-^ -^zt^o^r y/. 
cy^' 
Study Director/Mortitor 
. ^ ; y / / ' / A 
^ ^ 
^ 
Departmeni.^Di rector. 
Corji'.' V i c ^ President, R t D 
..yik^</H 
Vice P r e s i d e n t , R ^ ( 
T 
D Admin. 
BERLEX REPORT NUMBER: 
5^/6 7 
DATE: ^ ' / / / r ' / i A ' ^ 
DAT: 
/-' 
DATE : 
c . 
< I I 
DAT ,. ////c/^2^ 
REPORT DISTRIBUTION: 
R t. D ADMINISTRATION/ARCHIVE 
( O r i g i n a l ) 
/ 
M e d i c i n a l 
C h e m i s t r y 
(Org ina t i n g 
Deot.) 
^ 
' Operations Department 
_3 
Island Chemical Co., 
I n c . 
301350 
770 East Hanover Avenue, Cedar Knotls. New Jersey 07927 
(201) 540-8700 
Telex 13635'! 
BERLEX LABORATORIES INC 
RESEARCH REPORT 
jY) CHEMISTRY 
Q 
PHARMACOLOGY 
[n PHARMACEUTICAL DEVELOP, 
DEPT. REPORT NO. 
DATE: 
BERLEX REPORT NO. 
fp/6 7 
PAGE 
OF 1 
PAGES 5 
CHARACTERISTIC 
BIOLOGICAL EFFEC1 
TITLE OF REPORT: 
Analysis of Material from Bulk Storage Tanks 
#7, 18, 19 and 113, Island Chemical Company, 
St. Croix, Virgin Islands 
KEYWORDS (3 t o 5) : 
Storage Tank Analysis. Island Chemical, 
chemical composition 
PROTOCOL NO. 
GROUP/SECTION: 
Medicinal Chemistry Department 
Analytical Chemistry Section 
STUDIES WERE 
CONDUCTED 
FROM: 
TO: 
10/25/82 
11/02/82 
EXPERIMENTS CONDUCTED BY: 
J. Traina, E. Nisperos, M. Johnson and D. Szetc 
AUTHOR 
5IGNATURE: 
y^AzAy 
SECTION HEAD 
SIGNATURE: 
-zyf^^ 
COMPOUNDS STUDIED 
CK NO.: 
GENERIC NAME: 
Toluene, xylene, 
p-phenetidine, 
9-fluor-
enone 
FOR.".JLATIDf.' NO. 
PURPOSE OF STUDY: 
To determine the composition and identify the 
contents of material from bulk storage tanks 
in St. Croix. 
301351 
SUM.HARY AND SIGNIFICANCE 
DEPT. REPORT NO, 
PAGE 
OF 2 
PAGES 5 
Material from bulk storage tanks in St. Croix were 
fractionated by simple vacuum distillations. Fractions 
and residues were identified by NMR and IR. The results 
are as follows: 
Tank «7 
Tank S8 
Tank US 
Tank ^13 
xylene mixture 
p-phenetidine 
toluene 
9-fluorenone 
p-phenetidine 
p-phenetidine 
ca. 14% 
ca. 
80% 
c c . 
29% 
c a . 50% 
ca. 
95% 
ca. 
95% 
-2-
301352 
Analysis of Material from Bulk Storage 
Tanks #7, S8, S9 and S13, Island Chemical Company, 
St. Croix, Virgin Islands 
All four samples Tank S7, 18, #9 and #13 were received 
in 10 ml screw cap vials. These samples were analyzed as 
described below and the results are summarized in Ta'z-ls.- :, 
I I and I I I . 
Tank 17 
This sample was analyzed by semi-micro distillation. 
Two volatile fractions collected at the ranges of 75-100°C 
and 100''C-120°C were both identified by NMR and IR as mixed 
xylene. The residue was also identified by NMR and IR as 
p-phenetidine. 
Tank #8 
This sample was analyzed by semi-micro distillation. 
Two volatile fractions collected at the ranges of 75-100''C 
and 100-120''C were both identified by NMR and IR as toluene. 
The residue was analyzed by NMR and IR. The spectral data 
indicated that the residue was mainly composed of 9-fluorenone. 
Tank #9 
No volatile fraction distilled from the sample when 
heated. The sample was fractionated by semi-micro vacuum 
distillation. Practically 1 fraction was obtained by vacuum 
distillation. The fraction and a small amount of material 
left in the distilling flask were identified by NMR and IR 
as p-phenetidine. 
Tank #13 
No volatile fraction distilled from the sample when 
heated. The sample was fractionated by semi-micro vacuu.Ti 
distillation. Practically 1 fraction was obtained by vacuum 
distillation-. The fraction and a small amount of material 
left in the distilling flask were identified as ;-pheneticine 
by NMR and IR. 
-3-
301353 
Tcbl-: 1: 
Comoosition and P h v s i c a l Aooearance of 
Samoles 
Composition 
#7 
xylene mixture 
ca. 14% 
p-phenetidine 
ca. 80%* 
Tanks 
»8 
#9 
113 
toluene 
ca. 39% 
9-fluorenone 
ca. 50%* 
p-phenetidine p-phenetidine 
ca. 95%* 
cz'. 95%* 
Physical 
Appearance 
slightly 
heavy; 
black 
liquid 
slightly 
heavy; 
black 
liquid 
slightly 
heavy; 
black 
liquid 
slightly 
heavy; 
black 
licuid 
Total Nitrogen 
Content (by 
Galbraith Lab.) 
7.56% 
1 . 8 3 % 
9 . 4 9 % 
9.54% 
T o t a l 
C h l o r i n e 
C o n t e n t 
(by 
k>raith 
Lab.) 
m 
C-...orinated 
hydrocarbon 
content (by 
Beilstein test) 
0 . 0 8 8 % 
Not 
d e t e c t a b l e 
(N.D.) 
0.081% 
N.D. 
0.24% 
N . D . 
0.24% 
• E s t i m a t e d by NMR. 
- 4 -
301354 
Identification and Pronerties of Volatiles 
Tanks 
# 
17 
#8 
#9 
=1 
Boiling Point 
Mixed xylenes 
Toluene 
volatile 
Lit. 137-140°C 
Lit. 110°C 
Flash point 
xylene 
Toluene 
Lit. 17°C(o-) 
Lit. 4.4°C 
Lit. 25°C(/n-&p-) 
Identification 
NMR, IR 
NMR, IR 
Identification and Prooerties of Non-Volatiies 
Tanks 
l l 
ii 
il 
=13 
Boiling point 
p-phenetidine 
9-fluorenone 
p-phenetidine 
:-pheneticir 
non-volatile 
Lit. 250''C 
Lit. 342°C 
95°C (O.OSmmHc) 
95-105°C 
(760mmHg) 
Lit. 250''C 
(0.05.T.mHc) 
(760mmHg) 
Lit. 250°C 
(7 60mm.Hg) 
I d e n t i f i c a t i o n 
NMR, 
IR 
NMR, IR 
NMR, IR 
NM?., 
I." 
- 5 - 
301355 
- t 
t^wao 
19 COPELAND RD. DENVILLE! NEW JERSEY 07834 
(201)366-6256 
August 15, 1985 
Mr. Austin Moorehead 
Department of Conservation and Cultural Affairs 
Division of Natural Resources Management 
14F Building 111 
Water Gut Homes 
Christiansted, St. Croir, U.S.V.l. 00820 
Dear Mr. Moorehead: 
As per our telephone conversation on August 9/ Enviro-Sciences, 
Inc. is requesting perinission to dispose- of contaminated materials 
on St. Croix. The materials are on the Island Chemical Company 
site (now known as Virgin Island Chemical Company) and have been 
collected and stored in drums" or will be collected for disposal. 
The collection and clean up of these materials has been described 
previously in documents submitted to your office. 
The location and description of materials are as follows: 
Location 
Type 
Amount 
Major 
Contaminents 
1) Drain line 
2) Dryer (soil 
collected 
from a spill) 
Soil 
Soil 
Water 
18, 55 gal. 
drums 
14, 55 gal. 
drums 
2, 55 gal. 
drums 
Toluene, see 
Data Sheets 1 & 2 
Toluene, see 
Data Sheets 3-5 
The Data Sheets are inclusive of a four week drying 
period. 
Note that toluene concentrations decreased 
from 4000 ppm to 1.5 ppm during this time interval. 
Drying continued for an additional week after the 
last sampling period. 
3) Process Pit 
Sludge 
2,000 gals. 
Toluene, zinc, see 
Data Sheets 7-11 
4) Process Pit 
Water 
6,-000 gals.-
Data Sheets 12-17 
301356 
We would appreciate your timely review of this request and a 
determination as to the disposal location of each item listed 
above. I will contact you next week as to your progress. If you 
have any question, please call me collect at 919/499-5182. 
Very truly yours, 
ENVIRO-SCIENCES,. INC. 
^ . ^ z ^ ^ 
"^ ' (7 
Alan L. Kyles, PhD. 
Vice President 
AK/po (AK-85225) 
cc: Mr. Greg Rhymers 
Dept. Conservation & Cultural Affairs 
P.O. Box 4399 
St. Thomas, D.S.V.I. 00801 
301357 
INDUSTRIAL 
CORROSION 
MANAGErvlENT 
INCORPORATED 
IIS2 RQUre 10. RANDOLPH. NEW JERSEY 07869 
•201-584-03:0 
CLIENT: ENVIRO SCIENCES, INC 
SAMPLE SOURCE: 
ICC (BERLEIQ, PROJECT 
Data Sheet I 
NJDEP Certified Drinking Wacer/ 
Wascewacer Lahoratory ID i^l^llS 
REPORT DATE: 
August 15.1985 
LAB II 
42882 
SAMPLE ID: Drain Line ^1 
SAMPLE DATE: 
6/7/85 
SAMPLED BY: 
A. Kvles 
SOIL SAMPLE 
LABORATORY ANALYSIS 
REPORT 
AT LAB DATE: 
6/1S/85 
Identification of Black Soil; 
Parameter 
Benzene 
Toluene 
Ethylbenzene 
M-Xylene 
Q,P-Xylene 
Resul 
0-
c 
10 
233 
0. 
0. 
0. 
25 
33 
27 
Sample has "Toluene like" or solvent odor. 
Lf^'rCS'0'-'N ?£^\KS 
R.T. 6.89 ac 40 mg/kg 
R.T.30.81 -c 2 mg/kg 
All results reported in mg/kg. 
We thank you for this opportunity to serve you- If you have any quescions, 
please do noc hesitate co call. 
INDUSTRIAL CORROSION MANAGEMENT, V.:C. 
m. 
jmg 
• 1 
Edwin Tichenor 
Vice President 
n = L e s s Than 
301358 
Ui 
o 
l-» 
Ui 
Ul 
vo 
f a ] 
1 ^ INDUSTRIAL 
if 
CLIENT; 
ENVIRO SCIENCE - ICC (Berlex) 
^Jlil 
CORROSION 
MANAGEMENT 
INCORPORATED 
SOIL SAMPLE 
NJDEP Certlticci Urinking Waier/w<i:>iuw<iLcr 
Laboratory (0 #14116 
REPORT DATE; July 31. 1985 
LAB #_12M1 
•SAMPLE. ID; 
Drain Line 112 
•SAMPLE DATE: 
6/7/85 
SAMPLED BY: 
A. Kylea 
VOLATILE ORGANICS BY PURGE AND TRAP 
By CC 
BTX/HEADSPACE 
AT LAB DATE; 
6/18/85 
CHLOROMETHANE 
• 
BROMOMETHANE 
• 
VINYL CHLORIDE 
• 
CHLOROETHANE 
• 
METHYLENE CHLORIDE 
ACETONE 
- 
• 
1,1-DICHLOROETHYLENE -
1,1-DICHLOROETHANE **-
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER -• 
1,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE -
BROMODICHLOROMETHANE -
I.2-61CHLOROPROPANE — 
Compounds detected In parts per million (milligrams/kilograms) dry weight basis 
X 
X 
1,240 
*rC-l,3-DICHL0R0PR0PENE 
't-l,3-DICHLOROPROPENE 
~ 
TCE (TRICHLOROETHYLENE) 
X 
rl,I,2-TRICHLOROETHANE 
'DIBROMOCHLOROMETHANE '"" 
~ 
68 
10 
BENZENE 
• 
DIISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER • 
BROMOFORM 
I,1,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE -
TOLUENE 
CHLOROBENZENE 
ETHYLBENZENE 
M-XYLENE 
• 
*f O-XYLENE 
5.600 
^Compounds co-elute (could be either material). 
LT-Less Than, GT-Greater Than 
dwb-Dry Weight Basis. 
X-Not Detected 
P-XYLENE 
AATetrahydrofuran ( Phosgene also elute at this 
point. Numerical results are calculated for 
I,]-Dlchloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of:_ 
_Unknown peaks detected (retention tIme,estImated amount): Xylenes 
18; ]0 unknown hydrocarbon peaka ranging 
from 2 to 10 mR/kg. 
_J 
NOTE;Compound Identification is based upon retention time matches with specific known standards. Confirmation 
of analysis using GC/MS Is required to positively Identify any material and/or amount detected. 
I NDUSIiUAt:i:ORR0S ION^ 
win TTcheKor, Vice PresJ^rrrt--
n 
rt 
rti 
r t 
N) 
o 
Ui 
o 
Pi 
irtuubiHlAU 
CORROSION 
MANAGEMEhfT 
INCORPORATED 
t u ; ROUIE lO.IWMOOLtN. WW jCMSfYOrui MI-U4.0U0 
CLIENT; 
ENVIRO SCIENCE 
ICC (Berlex) 
SOIL SAMPLE 
• 
'- 
1 
i 
• 
» 
• 
''• 
HJDEP Certified Drinking Water/Wast ,^^«r 
Laboratory 10 ||i«li6 
REPORT DATE:_ 
LAB # 
42889 
July 31.1985 
SAMPLE ID: 
Dryer 
•SAMPLE DATE; 
6/14/85 
SAMPLED BY: 
A. Kylea 
VOLATILE ORGANICS BY PURGE AND TRAP 
By GC 
BTX/HEADSPACE 
_AT LAB DATE; 
6/18/85 
CHLOROMETHANE 
• 
BROMOMETHANE 
• 
VINYL CHLORIDE 
• 
CHLOROETHANE 
• 
HETHYLENE CHLORIDE 
ACETONE 
- — 
1,1-DICHLOROETHYLENE -
1,1-DICHLOROETHANE **-
t-I, 2-DICHLOROETHYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER -
1,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE — 
BROMODICHLOROMETHANE --
1,2-DICHLOROPROPANE 
— 
Compounds detected In parts per million (milligrams/kilograms) dry weight basis. 
TCE (TRICHLOROETHYLENE) 
X 
jkfC-l,3-DICHLOROPROPENE 
't-l.3-DICHLOROPROPENE 
M 
1,1,2-TRiCHLOROETHANE 
X 
4.0 
340 
4.2 
'^Compounds co-elute (could be either material). 
LT-Less Than, GT-Greater Than 
dwb-Dry Weight Basis. 
X-Not Detected 
'DIBROMOCHLOROMETHANE 
BENZENE 
DIISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER 
BROMOFORM 
1,1,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE 
TOLUENE 
CHLOROBENZENE 
ETHYLBENZENE 
-
' M-XYLENE 
-
*rO-XYLENE 
P-XYLEME 
**Tetrahydrofuran ( Phosgene also elute at this 
point. Numerical results are calculated for 
I,1-DlchIoroethane only. 
X • 
X 
X 
6.6 
X 
X 
X 
X 
X 
4.000 
X 
16.1 
17.7 
15.1 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of; 1 mg/kR dwb. 
Unknown peaks detected (retention tIme,estImated amount): 
NOTE:Compound identification Is based upon retention time matches with specific known standards. 
Confirmation 
of analysis using GC/MS Is required to positively Identify any material and/or amount detected. 
INDUSJ 
win Tlchefior, Vice Presf^trrt--
rf 
It 
rt 
JDUSTRIAL 
CORROSION 
MANAGEMENT 
L ' J I I I INCORPORATED 
111} ROOK 10. tUtUDCLfii. WW JCRSEr 07Mt 
20l-Si4.O]}0 
NJDEP Certified Drinking Water/Wastewatf 
Laboratory ID #1M16 
REPORT DATE:_ 
LAB a 43747 
August 15.1985 
CLIENT; EKVIRO SCIENCES,INC. - ICC (BERLEX) PROJECT 
SAMPLE DATE; 
7/1/85 
SAMPLED BY: 
Enviro Sciences 
SAMPLE ID: Dryer 
AT LAB DATE; 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CHROMATOGRAPHY/HEADSPACE 
7/11/85 
Compounds detected In parts per million (mi 11tgrams/kllograms) dry weight basis 
CHLOROMETHANE-
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
HETHYLENE CHLORIDE — -
ACETONE 
],1-DICHLOROETHYLENE -
1,1-DICHLOROETHANE ** • 
t-l,2-DICHLOROETHYLENE 
X 
X 
CHLOROFORM 
• 
1 ,2-DICHLOROETHANE 
- -
t-BUTYL METHYL ETHER -
1 ,1,1-TRICHLOROETHANE 
CARBON TETRACHLORIDE -
BROMODICHLOROMETHANE -
1,2-DICHLOROPROPANE 
c-r,-3-DICHLOROPR0PENE 
t-l,3-DICHL0R0PR0PENE"' 
TCE (TRICHLOROETHYLENE) 
- -
1,1,2-TRICHLOROETHANE 
DIBROMOCHLOROMETHANE 
BENZENE 
DIISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER -
BROMOFORM 
1,1,2,2-TETRACHLOROETHANE • 
PCE ( TETRACHLOROETHYLENE) 
TOLUENE - 
-
CHLOROBENZENE 
• 
ETHYLBEHZENE — 
• 
X 
SLM 
'••Compounds co-elute (could be either material). 
LT-Less Than 
dwb-Dry Weight Basis. 
GT-Greater Than X-Not Detected 
**Tetrahydrofuran & Phosgene also elute at this 
point. Numerical results are caluclated for 
1 ,1-DichIorocthane only. 
o 
M 
Ui 
a\ 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 
mg/kg dwb. 
rt 
(t 
rt 
JJ 
Unknown peaks detected (retention time, estimated amount) 
numerous other liydrocnrbon peaks, 0.02 to 0.1 mg/kg 
NOTE; Compound Identification Is based upon, retentIon time 
matches with specific known standards. Confirmation 
of analysis using GC/HS Is required to positively 
£y/ 
identify any material and/or amount detected. 
INDUSTRIAL CORROSION MGMT.,INC, 
iwin Tichenor, Vice President 
I i'i I 
INDUSTRIAL 
JORROSION 
MANAGEMENT 
INCORPORATED 
iisiMxm IC. RAMoam. wwjdisfYorui 
toi-iu-oao 
NJDEP Certified Drinking Water/Wastewat 
Laboratory ID tl\h\\(> 
REPORT DATE;_ 
LAB # 
43752 
August 15.1985 
CLIENT; ENVIRO SCIENCES,INC. - ICC (BERLEX) PROJECT 
SAMPLE ID: 
Dryer 
SAMPLE DATE: 
7/1/85 
SAMPLED BY: 
Enviro Sciences 
AT LAB DATE: 
7/11/85 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CHROMATOGRAPHY/HEADSPACE 
Compounds detected In parts per million (milligrams/kilograms) dry weight basis 
CHLOROMETHANE—-
BROMOMETHANE 
VINYL CHLORIDE 
• 
CHLOROETHANE 
• 
HETHYLENE CHLORIDE — • 
ACETONE 
• 
1,1-DICHLOROETHYLENE -
1,1-DICHLOROETHANE ** • 
t-I,2-DICHLOROETHYLENE 
CHLOROFORM 
X 
X 
JLH 
1,2-DICHLOROPROPANE - — 
^rc-1,3-DICHLOROPROPENE 
't-l ,3-DICHLOROPROPENE" 
TCE (TRICHLOROETHYLENE) 
. , 1,1,2-TRICHLOROETHANE 
'DIBROMOCHLOROMETHANE 
" " 
X 
1,2-DICHLOROETHANE —• 
t-BUTYL METHYL ETHER • 
1,1,1-TRICHLOROETHANE 
CARBON TETRACHLORIDE -
BROMODICHLOROMETHANE -
X 
X 
BENZENE 
DIISOPROPYL ETHER — 
2-CHLOROETHYLVINYL ETHER -
BROMOFORM 
1,1,2,2-TETRACHLOROETHANE 
PCE ( TETRACHLOROETHYLENE) 
TOLUENE 
• 
CHLOROBENZENE 
• 
ETHYLBENZENE 
•Ixi 
'•'Compounds co-elute (could be either material). 
LT-Less Than 
dwb-Dry Weight Basis. 
GT-Greater Than X-Not Detected 
**Tetrahydrofuran i Phosgene also elute at this 
point. Numerical results are caluclated for 
1,1-Dlchloroethane only. 
u> 
o 
oji X 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 
mg/kg dwb. 
Unknown peaks detected (retention time, estimated amount) 34.07 3 15 mg/kg 
NOTE: Compound Identification Is based upon, retentIon time 
matches with specific known standards. Conflrmatlori 
of analysis using GC/HS Is required to positively 
^ j / 
identify any material and/or amount detected. 
INDUSTRIAL CORROSION HGHT.,INC, 
win Tichenor, Vice President 
n 
(u 
rt>
rt 
* 
I 
iU 
\i 
^ ^ 
i 
i 
I, 
I 
.•JDUSTRIAL 
CORROSION 
MANAGEMENT 
L'J I J I INCORPORATED 
CL I ENT; ENVIRO SCIENCES. INC. - ICC (BERLEX) PROJECT 
SAMPLE DATE; 
7/17/R5 
SAMPLED BY; 
Enviro Sciences 
NJDEP Certified Drinking Water/Wastewat 
Laboratory ID #11(116 
REPORT DATE: 
LAB i 
44629 
August 15.1985 
SAMPLE ID; 
Dryer 
AT LAB DATE: 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CHROMATOGRAPHY / HEADSPACE 
7/25/85 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis 
CHLOROMETHANE 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
• 
METHYLENE CHLORIDE —-• 
ACETONE 
• 
1,l-DiCHLOROETHYLENE -
1,1-DICHLOROETHANE ** • 
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER -
1,1,1-TRICHLOROETHANE -
CARBON-TETRACHLORIDE — 
BROMODICHLOROMETHANE — 
X 
X 
1,2-DICHLOROPROPANE 
— 
- 
X^ 
^rC-1,3-DICHLOROPROPENE 
't-i,3-DICHLOROPROPENE 
— 
TCE (TRICHLOROETHYLENE) 
X 
1.2 
^r1,1,2-TRICHLOROETHANE 
'DIBROHOCHLOROMETHANE 
— ~ 
X 
X 
BENZENE 
-
DIISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER -
BROMOFORM 
1,1,2,2-TETRACHLOROETHANE 
PCE ( TETRACHLOROETHYLENE) 
TOLUENE 
CHLOROBENZENE 
• 
ETHYLBENZENE 
• 
0.07 
0.36 
'•'Compounds co-elute (could be either material). 
LT-Less Than 
dwb-Dry Weight Basis. 
GT-Greater Than X-Not Detected 
**Tetrahydrofuran & Phosgene also elute at this 
point. Numerical results are caluclated for 
1,1-Oichloroethane only. 
Ui 
o 
Ui 
o^ 
CO 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 
mg/kg dwb. 
Unknown peaks detected (retention time, estimated amount) niimeroug other hydrocarbon peaks 0.01 to 1 mp/kg 
NOTE: Compound Identification is based upon retention time 
matches with specific known standards. Confirmation 
of analysis using GC/MS is required to positively 
£j/ 
identify any material and/or amount detected. 
INDUSTRIAL CORROSION MGMT.,INC 
rt 
Itl 
f t 
^ 
fn Tichenor, Vice President 
INDUSTRIAL 
CORROSION sI^L 
MANAGEMENT 
INCORPORATED 
1152 ROUTE 10. RANOOtPH. NEW JERSEY 07869 
201-5^-0330 
CL I E N T : 
EKVIRO 
S C I E N C E S 
, 
NJDEP C e r t i f i e d Drinking Water/ 
Wastewater Laboratory ID # m i l 6 
REPORT DATE: 
Julv 3 1 , 198.S 
LAB i 
42886 & 42887~C0MP0SITE 
SAMPLE SOURCE:. 
SAMPLE DATE: 6/14/85 
ICC (Berlex) 
SAMPLED BY: 
A.Kyles 
AT LAB DATE; 
6/18/85 
PRIORITY POLLUTANT VOLATILE ORGANICS + AO 
by 
GC/HS + 15 PEAKS 
Parameter 
a c r o l e i n * 
a c r y l o n i t r i l e * 
benzene 
bromoform 
carbon t e t r a c h l o r i d e 
chlorobenzene 
chlorodibromomethane 
chlorethane 
2-chloroethylvlnyl 
e t h e r 
chloroform 
— 
dIchlorobromomethane 
- - - • 
1,l-dlch1oroethane 
1,2-dlchloroethane 
1,1-dIchloroethylene 
Result 
X 
Parameter 
Result 
X 
22SL 
X 
1,2-dichloropropane 
1,3-dichloropropylene 
ethylbenzene 
methyl bromide 
methyl chloride 
methylene chloride 
1,1 ,2.,2-tetrachloroethane -
tetrachloroethylene 
toluene — • 
: 
1,2-trans-dlchloro«ithylene 
1 , 1 , 1 - t r i c h l o r o e t h a n e 
1 , 1 , 2 - t r i c h l o r o e t h a n e 
t r i c h l o r o e t h y l e n e 
vinyl chloride 
Results reported in mg/lcg (ppn), dry weight basis. 
•Detection Lii»it 
LT-Less than 
X=Not detected 
100 ppm 
OTHER COMPOUNDS DETECTED 
APPROXIMATE CONCENTRATIONS 
125 
1.560 
X 
benzyl acetate 
22 
1430 
l-chloro-2-iaethyl benzene 
40 
chloromethyl benzene 
ET/jmg 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
dwlnVTichen&r- 
v-- 
/ 
EdwlnVTichent 
Vice President 
301364 
l1 
, , J I INDUSTRIAL 
y ,! I 
CORROSION 
P l ' j 
MANAGEMENT 
9 1 I I INCORPORATED 
OUTE 10. RAMDOIPH, NEW JERSEY 07869 
201 •5ft4-0330 
11£NT; 
ENVIRO SCIENCE 
NJDEP Certified Drinking Water/ 
Wastewater Laboratory ID #1^116 
•il 
REPORT DATFrJuly 3 1 . 1985 
LAB I 
42886 & 42887 COMPOSITE 
SOIL SAliPLE 
AMPLE SOURCE: 
ICC (Berlex) 
AMPLE DATE:fi/14/8S 
SAMPLED BY: A. Kvles 
.AT LAB DATF.; 6/18/8S 
PESTICIDE S PCB EXTRACTABLES 
PRIORITY POLLUTANTS -K AO 
• by GC/MS 
arameter 
Result . 
Idrin 
• 
LT 2-
-BHC 
- — 
LT 2 
-BHC — 
- 
LT 2 
-BHC 
- 
- LT 2 
-BHC 
^- LT 2 
hlordane 
LT 12 
,i»'-DDD 
— 
LT 3 
,^-DDE 
LT 3 
ODX 
LT 3 
'drln 
LT 3 
iiaosulfan I 
' 
LT 3 
ndosulfan II 
LT 3 
ndosulfan Sulfate 
.- 
— 
LT 3 
ndrin 
LT 3 
:ndrin Aldehyde 
LT 3 
eptachlor 
LT 3 
eptachlor Epoxide 
LT 3 
oxaphene 
• 
LT 12 
'CB-10'16 
LT 45 
'CB-1221 
^ 
- 
LT 45 
CB-1232 
—
- 
T.T 45 
'C8-12'»2 
- 
— 
T.T 45 
'CB-I2A8 
- 
T.T 45 
'CB-1254 
- 
- 
- 
T.T 45 
'CB-1260 
- 
LT 45 
vll r e s u l t s are reported In mg/kg (ppm), dry weight b a s i s . 
INDUSTRIAL 
CORROSION 
M G M T . , I N C . 
EdwiH^ T i c n ^ o r 
^ - 
7» 
iT^mg 
Vi-ce P r e s i d e n t 
/(jJZ) 
r - L e s s 
Than 
<-Not 
D e t e c t e d 
3 0 1 3 6 5 
3 
U 
•J 
u 
Data Sheet 11 
^1 
INDUSTRIAL 
CORROSION 
SOIL SAMPLE 
MANAGEMENT 
INCORPORATED 
NJDEP Certified Drinking Water 
Wjsiewater Laboratory 10 lUllS 
REPORT DATE: j u W 31. 1985 
LAB » 42886 & 42887 Coouosite 
US? ROUll IU. RANOOiPH. N£W XRSIT 0;il69 
?QI ^ 4 0 l\(l 
CLIENT 
ENVIRO SCIENCES 
SAMPLE SOURCE: ICC (Berlex) 
SAMPLE DATE: 6/14/85 
<;&MPI cn BY: A. Kvles 
AT LAB DATE:6/18/85 
-'"'^^ 
PRIORITY POLLUTANTS-f 40 
TOXIC POLLUTANTS: Metals, Cyanide and Total Phenols 
PARAMETER 
Total Antimony -
Total Arsenic — 
Total Beryllium 
Total Cadmium --
Total Chromium -
Total Copper — 
Total Lead 
;-• 
Total Mercury — 
Total Nickel — 
Total Selenium • 
Total Silver --
Total Thai 1ium 
Total Zinc 
RESULT 
T,T 118 
40.0 
LT 2.87 
22.8 
592 
327s 
688 
2.73 
134. 
LT 
1^08 
LT 7^48 
LT 66.2 
3,594 
Total Cyanide 
Total Phenol • 
A4.44 
^ 0 1 
A M results are reported in mg/kg (ppm)',' dry weight basis.. 
We thank you for this opportunity to serve you. If you have any questions, please 
do not hesitate to call. 
Very truly yours, 
INDUSTRIAL CORROSION MGMT.,1HC. 
ET/jm<3 
LT-Less 
Than 
X-Not 
Detected 
Edwin" TicheWor 
Vice 
President 
301366 
aw 
# 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Certified Drinking Water/ 
Wastewater Laboratory ID HlkWS 
REPORT DATE: August 15.1985 
LAB # 44418 
1152 ROUTE 10. RANDOLPH. NEW JERSEY 07869 
201-584-0330 
CLIENT: ENVIRO SCIENCES. INC. 
SAMPLE SOURCE: ICC (BERLEX) PROJECT 
SAMPLE ID; St.Cro-tx 
SAMPLE DATE: -W«^WHW»- 
SAMPLED BY: 
Al Kyles 
.AT LAB DATF- 7/22/85 
WATER 
Parameter 
PRIORITY POLLUTANT VOLATILE ORGANICS 
by GC/MS 
acrolein* 
acryloni t r i l e * 
benzene 
: 
bromoform 
carbon tetrachloride 
chlorobenzene 
chlorodibromomethane 
chlorethane 
2-chloroethylvinyl 
ether 
chloroform 
dichlorobromomethane 
I ,l-dichloroethane 
1,2-dlchloroethane 
1 ,1-dichloroethylene 
Result 
X 
0.04 
_X 
X 
X 
X 
X 
Parameter 
Result 
X 
X 
X 
X 
X 
X 
1 ,2-dichloropropane 
I,3-dichloropropylene 
ethylbenzene 
methyl bromide 
methyl chloride 
methylene chloride 
1,1,2,2-tetrachloroethane -
tetrachloroethylene 
toluene 
^ 
1,2-trans-dichloroethylene 
I,1,1-trichloroethane 
I,1,2-trichloroethane 
trichloroethylene 
vinyl chloride 
Results reported in mg/l (ppm). Detection limit 0.001 mg/l (ppm). 
•Detection Limit: Q.l mz/1 
Q.3S 
JL 
ET/jmg 
INDUSTRIAL CORROSION 
MGMT.,INC. 
Edw i n 
T i c h e n o r 
V i c e P r e s i den t 
LT=Less Than 
X=Not Detected 
//"A 
'yyyr 
/z^-^ 
301367 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
. ' - o c r 
^ci t i 1 . CO Ul I nn, I ng wa cer/Was t e w a t e r 
(^(^ 
L a b o r a t o r y 
ID #li»116 
Data Sheet 13 
REPORT DATE: 
August 15.1985 
LAB if 
^^^18 
1152 ROUTE 10, RANOOLPH. NEW JERSEY 07869 
201-544.0330 
CL I FNT: 
FNVTT^n «;rTFNrES. TNC. 
ICC(BERLEX) 
SAMPLE SOURCE:_ 
SAMPLE DATF; TinVnnT.nw 
SAMPLED BY: 
St. Croix 
Al Kvles 
AT LAB DATE: 
/yy/a'atyyr'ji'S'^ 
WATER 
PESTICIDE & PCB EXTRACTABLES 
PRIORITY POLLUTANTS 
bv GC/HS 
Parameter 
Result 
Aldrin 
• 
LT 0.01 
a-BHC 
LT 0.01 
b-BHC 
LT 0.01 
d-BHC 
LT 0.01 
g-BHC 
- 
- 
— 
- 
:- 
LT 0.01 
Chlordane 
• 
LT 0.02 
A,if'-DDD 
7 
LT 0.01 
1»,I»'-0DE 
— 
LT.O.-Ol 
^,if'-DDT 
LT 0.01 
Dieldrin — 
r 
'• 
LT 0.01 
Endosulfan I 
LT 0.01 
Endosulfan 11 
• 
LT 0.01 
Endosulfan Sulfate 
: 
LT 0.01 
Endrin 
LT 0.01 
Endrin Aldehyde 
LT 0.01 
Heptachl or 
LT 0.01 
Heptachlor Epoxide 
LT 0.01 
Toxaphene 
LT 0.02 
PCB-1016 
LT 0.01 
PCS-1221 
LT 0.01 
PCB-1 232 
r 
LT 0.01 
PCB-12A2 
LT 0.01 
PCB-12^8 
LT 0.01 
PCB-1 25A 
LT 0.01 
PCB-1260 
LT 0.01 
All r e s u l t s reported in mg/l (ppm). 
INDUSTRIAL CJUUlgSI 
/-o ,-• 
Edwin Tichenor 
ET/jmg 
Vice President 
LT=Less than 
X=Not detected 
7/22/85 
M G M T . , I N C 
301368 
m 
hUSTRIAL 
'RROSION 
MAHAGEMEFfT 
INCXtRPORATED 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID #IA116 
n i l R O i n i IO.IUMX)LrH.N£WJEJa{r07Mt 
»n-S»4-01)0 
REPORT DATE:. 
LAB # 
August 15,1985 
44418 
CLIENTL 
ENVIRO SCIENCES, INC, 
SAMPLE S O U R C E L -
.SAMPLE DATE: 
-^xnkxuiUfi^ 
ICC (BERLEX) PROJECT 
/yjZ'^yyi^jir^ 
SAMPLED BY: 
Al 
BASE/NEUTRAL 
Parameter 
Result 
acenaphthene 
X 
acenaphthylene 
X 
anthracene 
X 
benzidine 
X 
benzo(a)anthracene 
X 
ben2o(a)pyrene 
X 
3,^i-benzof luoranthene 
X 
ben2o(ghl)perylene 
X 
ben2o(k)fluoranthene 
X 
bls(2-chloroethoxy)methane 
• 
X 
bls(2-chloroethyl)ether 
X 
bis(2-chlorolsopropyl)ether 
X 
bis(2rethylhexyl)phthalate 
X 
^i-bromophenyl phenyl ether 
X 
butylbenzyl phthalate 
X 
2-chloronaphthalene 
X 
4-chlorophenyl phenyl ether — 
X 
chrysene 
X 
dIben2o(a,h)anthracene 
X 
1 ,2-dichlorobenzene 
X 
I ,3-dlchlorobenzene 
X 
to'I,^-dichlorobenzene 
X 
<=> 3,3-dichlorobenzldlne -- 
- 
X 
^ None of the above Priority Pollutonts detected 
vo 
**Other compounds see Addendum I 
LT-Less Than 
X-Not Detected 
FT/Imo 
SAMPLE ID; ST. Croix 
Kylea 
AT LAB DATE; 
7/22/65 
EXTRACTABLES PRIORITY POLLUTANTS 
t?Y 
GC/MS 
Parameter 
diethyl.phthalate 
dimethyl phthalate 
dl-n-butyl phthalate 
; 
2,^l-dini trotoluene 
; 
--
2,6-dinitrotoluene 
dl-n-octyl phthalate 
I,2-diphenylhydra2ine (as azobenzene) 
fluoranthene 
. 
fluorene 
hexachlorobenzene 
hexachlorobutadiene 
hexachlorocyclopentadiene 
hexachloroethane 
indeno(l,2,3-cd)pyrene 
Isophorone 
naphthalene 
nitrobenzene 
N-nitrosodimethy lamine 
N-nItrosodi-n-propyI amine 
N-nltrosodiphenyl amine 
phenanthrene 
pyrene 
1,2,'•-trichlorobenzene 
at a sensitivity level of 0.03,mg/l (ppm) 
INDUSTRIAL CORROSION MAIjAGEHENT, INC. 
' ••'' 
C " 
c T " : ^y. 
Edwin Tichenor 
Vice President 
Result 
rt 
(0 
(t) 
rt 
^i'l i 
NJDEP Certified Drinking Water/ 
Wastewater Laboratory ID #14116 
REPORT DATE: Augiist 15,1985 
LAB # 44418 
CLIENT: 
ENVIRO SCIENCES, INC. 
SAMPLE SOURCE: 
ICC (Berlex) 
SAMPLE ID: St. Croix 
SAMPLE DATE: uatereirtr SAMPLED BY:_ 
y9A^yy9/'J-' 
Al. Kvles 
AT LAB DATE: 
1I22I%5 
BASE/NEUTRAL EXTRACTABLES PRIORITY POLLUTANTS 
ADDENDUM I 
OTHER COMPOUNDS DETECTED 
by GC/MS 
Parameter 
benzaldehyde 
Result 
3.0 
chloromethyl benzene 
benzene methanol — — 
phenyl acetate 
diphenyl methane — — 
0.3 
24.0 
26.0 
0.4 
0.4 
l-l'-[oxybis(methylene]bis benzene 
All results are reported in mg/l (ppm). 
We thank you for this opportunity to serve you. If you have any questions, 
please do not hesitate to call. 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
ET/jmg 
end. 
LT=Less Than 
Edwin TicK'enor 
Vice President 
3 0 1 3 7 0 
^m. 
# 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROOTE 10. RAHOOLPH. NEW JERSEY 07869 
201-584-0330 
NJDEP Certified Drinking Water/ 
Wastewater Laboratory ID #U116 
REPORT DATE: 
August 15.1985 
LAB # 
44418 
CLIENT: 
ENVIRO SCIENCES. INC. 
SAMPLE SOURCE 
ICC (BERLEX) PROJECT 
ST. Croix 
SAMPLE DATE: 
uukiiuwu' SAMPLED BY: Al Kvles 
/9j:ycy/9fr^ 
AT LAB DATE: 
ACID EXTRACTABLES 
PRIORITY POLLUTANTS bv GC/HS 
7(171^^ 
WATER 
Ji 
Parameter 
2-chlorophenol 
2-nitrophenol 
phenol 
Result 
2,4-dimethyIphenol 
2,'l-dlchlorophenol 
2,'»,6-trichlorophenol --• 
pentachlorophenol 
2,^-dinitrophenol 
4 , 6 - d I n I t r o - o - c r e s o l 
'•-nitrophenol 
4-chloro-3 methyl 
phenol 
X 
X 
X 
None of the above P r i o r i t y P o l l u t a n t s detected a t a s e n s i t i v i t y l e v e l of 0.01 mg/l (p
OTHER PEAKS DETECTED: 
benzoic a c i d (§ 3 mg/l 
INDUSTRIAL 
CORROSION 
MGMT.,INC 
ET:jmg 
LT=Less Than 
X»Not Detected 
Edw i n T i cheiio r 
V i c e p r e s i d e n t 
*** 
3 0 1 3 7 1 
^ 
Data Sheet 17 
Cfc 
T i l 
I 
I 
INDUSTRIAL 
NJDEP Certified Drinking Water 
U 
. I j 
CORROSION 
Wostewater Laboratory ID ^1M16 
. P I I 
MANAGEMENT 
REPORT DATE: A,,^,,,^ is.igRs 
L'J I I 1 INCORPORATED 
^AB » 44418 
IS? ROUli 10. RANOOlPH. N[W JERSEY 07»69 
201 58< O.IV) 
r-LIFNT; 
ENVIRO SCIENCES INC. 
SAMPLE SOURCE: ICC (BERLEX) PROJECT 
SAMPLE ID: St. Croix 
SAMPLE DATE: 
.unlma<rf=* <;AHPI Fn BY: Al Kyles 
. AT LAB DATE: 
7/22/85 
PRIORITY POLLUTANTS 
WATER SAMPLE 
TOXIC POLLUTANTS: Metals, Cyanide and Total Phenols 
PARAMETER 
RESULT 
Total Antimony 
LT 0.016 
Total Arsenic 
LT fa.005 
Total Beryllium 
• 
LT &.013 
Total Cadmium 
'-— 
0.003 
Total Chromium 
'• 
0.027 
Total Copper 
; 
0.153 
Total Lead ---. 
n.O'n 
Total Mercury 
n.001 
Z 
Total Nickel — 
0.080 
Total Selenium 
'• 
T.T 0.005 
Total Silver- 
0.008 
Total Thallium --' 
o.o29 
Total Zinc 
•_ 
4.85 
Total Cyanide 
0.053 
Total Phenol 
0.161 
All results are reported In mg/l (ppm). 
We thank you for this opportunity to serve you. If you have any questions, please 
do not hesitate to call. 
Very truly yours, 
INDUSTRIAL CORROSION MGMT.,INC. 
Edwin Tichenor 
ET/jm<3 
Vice President 
LT=Less Than 
X=Not Detected 
301372 
CHAIN OP CUSTODY RECORD 
19 COPtLANO RO.. DENVIUi NCW JERSET 07O4 
Inatallation: 
ICC (Berlex) 
Survey No .: 
V 
a 
B 
tz c 
to 2 
Station Location 
Analysis 
S a a p l e r s : 
( S i g n a t u r e ) 
Date 
Time 
Sample Type 
Comp 
Gra b 
BT 
Ui 
V 
c 
u-l ..-I 
o <0 
u 
• c 
o o 
2 U 
Drain Line 
A / A ^ S ' I 
Toluene 
6/8/85 
2 
3 
4 
5 
6 
^y2tSv'>-
Identify the contents of^the black soil 
sample.] 
Uboratory Pit 
^ 5 cP<F3 
Pyridiw 
6/14/85 
Laboratory Pit-duplicate ^ ^ « ^ V VOA k ^ 
6/14/85 
Time limit may have expired, if so do not run.] 
Z?57?3 
Pit-duplicate (liquid) Priority Pollutantb 6/14/85 
^,3,Pf-i.\ 
combine and 
4iAJl 
Pit-Interface(liquid/slidgeTN 
^un 
6/14/85 
Pit-sludge 
"K priority 
''^ pollutants 6/14/85 /P^^o 
X 
One container has a white lump, segregate it and anc 
lyze for quinid .ne.] 
U 
Drver 
i k k ^ ' ^^ ^^^^^ 
Toluene 
Relinquished by: (Sign.) 
6/14/85 
Relinquished by: (Sign.) 
Received 
JyJLy A 
(Sign.) Date/Time 
Received by: (Sign.) Date/Time 
Relinquished by: (Sign.) 
Received by: (Sign.) 
Relinquished by:/-6Sign.) 
Dispatched by: (Sl/^n.) 
Date/Time 
Rec'd by Laboratory 
for field analysis 
( S i g n . ) 
Date/Time 
y 
vytfs /:x!/.r 
Date/Tim^[Rec'd for 
Laboratory 
by: 
Date/Time 
Method of 
Shipment: 
Express Air Freight 
O 
301373 
LAB NO. 42885 
Pit duplicate (liquid) Priority Pollutants +40 
(Process Pit) 
Samples not analyzed because sample volume too small. 
301374 
cnwio • foaKu VK. 
CHAIN OP CUSTODY RECORD 
I i O0«I>«0 TO.. DCNVIUX N€W JEBSEY 0T»4 
I n s t a l l a t i o n : /CC (^/f&€yftA 
Survey No.: 
a 
a 
nj 
C 
tn a 
y > ^ ^ 
Station Location 
^ 
/y^ytf/^ 
/fia^ifr-e-' 
ykt;^ Tzr /^JZ fe^-"^ 
<,yy!y/iyj/.ry 
^ a 
^- 
>l/. 
Samplers: (Signature) 
date 
Time 
Sample Type 
Liomp .( Cirao 
/iyycy 
A/iyti.y 
y^.-f^yayrj 
/ / ^ ^ ^ 
/J^y.y 
\ 
BT 
u 
V 
a 
o m 
u 
• c 
o o 
V 
/ 
y 
^
^ 
ky/^'-. 'tL 
.-y-. 
-^ 2 
^/^yA^ 
yv-iztiT*.<.. 
/yt^y 
\ 
/ 
Relinquished by: (Sign.) 
y^:^,y^rzyy-y 
Relinquished (^y: (Sign.) 
Received by: (Sign.) Date/Time 
HhLLzZzzdzi^yii=zir^''y-' y'^l'"^ '^''^• 
Relinquished by: ^Stgn.) 
Relinquished by: (Sign.) 
Dispatched by: (Sign.) 
Received/by: (Sign.) Date/Time 
Received by: (Sign.) Date/Time 
Rec'd by Laboratory 
for field analyais 
(Sign.) 
Date/Time 
Date/Time 
Method of Ship|aen£_^ 
ky 
yA , 
• 
-
j
^ 
5 / 
Rec'd for Laboratory 
by: 
Date/Time 
301375 
•WHO tM KttncMS WKm 
CHAII OF CUSTODY RBCOID 
ItCOraAMO n o . O e M U X NCW J ^ K T 07B« 
Instaiiacion: 
Survsy No.: 
ZZiiL. 
Ol • 
« ci 
j - ^ 4 6 3 1 
S t a t i o n Location 
Saaplars: 
( S i f n a t u r a ) 
7)/ev<^ ( T a ' / ^ ^ 
yA^-S'/S / y k ' J ^ m y f ^ J 
AA^zyyy^, 
Data 
"T:^—7 
/
^ Vy/eyry /ali^/Sf^yX T ^ ^ ^ 
7^^ru^ '^ ^SM^Zy 
ZA'' "IT 
y/ 
\ 
y\yar' /=^4t^/3 yyi^rrc y^y=y^yi-.^ r^yTT/^cxy 
^/ 
/VSU) <^^y^£^. /Ce./i^frPiyzj) y < ^ c y y h ^ \ 
Rfl^inquishad by:, (Si^n.) 
-
• 
Ra/linquiahad by: 
(Signj/) 
Ralinquiahad by: (Sign.) 
Ralinquiahad by: (Sign.) 
^ 
< ^ 
1 
Racalvad by: (Sign.) 
Racalvad by: flSign.) 
Data/Tiaa 
Data/Tima 
Racalvad by: (Sign.) pata/Tiaa 
Dispatched by: (Sign.) 
Data/Tiaa 
Rac'd by Laboratory 
for field analyaia 
(Sign.) 
Rac'd for Laboratory 
by: 
Data/Tiaa 
Data/Tiaa 
Method of Shipaent: 
cSyZ^y<iaA <kiU^ /^Zi^^i^ 
301376 
m 
CHAIl OF CUSTODY RBCOID 
It cofCUMO w}< ocMvaii. 
amn 
Installation: y ^ ^ 
^
^ 
Survay No.: 
a 
• 
<« d 
Vi 
Station Locatioa 
Saaplars: (SIgnatura) 
Data 
T/ 
Til 
Saapla Typ< 
UoapTF^TrTB" 
—a-
a 
o m 
w 
• a 
o o 
o z 
rj:t.2> 
fSi./ 
I ^ 
^gd-^ /y^t^^ya»^, i 
y ^ ^ 
( ^ l ^ a Z 2 ^ ^^<»a^, 
7y^4^i^'Aa/. 
T 
/ I 
^ • ^ ( f y ^ 
<^-'^^A^ 
>r 
\ 
^ 
\ 
^ 
R ^ i n o u i s h e d by: 
( S i g n . ) 
Racalvad by: 
( S i g n . ) 
RacaiVad by :(jT5ign. ) 
D a t a / T i a a 
Raiinquishad by: 
( S i g n . ) 
Relinquished by: 
( S i g n . ) 
Data/Tiaa 
Received by: (Sign.) Data/Tiaa 
Ralinquiahad by: (Sign.) 
Diapatched by: (Sign.) 
Data/Tiaa 
Rac'd by Laboratory 
for f i e l d 
a n a l y a i s 
(Sign.) 
Daca/Tlaa 
Rac'd for 
Laboratory 
by: 
Data/Tiaa 
Method of Shipaant: 
( Z ^ 
C ^ a ^ j * ^ / 4 l ^ k ^ 
301377 
CHAII OF CUSTODY RECORD 
It COfOMO MX. OOMUI. MCW JCMCr ortM 
Installation: _72r(L ! ^ ^ 1 ^ 
u-yy. 
Survay No.: 
Saaplars: 
( S I g n a t u r a ) 
'•4^/g 
03 
Station Location 
Data 
/^/f/^/Ay yi^^-^z^/^^/zz -f <^o 
y^^<^:^i*^ y ^ ^ /^yL^ckk 
Tiaa 
Saapla Typa 
(Joap.t'<>rao 
/^jS^y/^ '^t2-^o 
T 
Relinquished by: (Sign.) 
u 
fi 
144 tr^ 
O « 
• fl 
o o 
2 U 
^ c 
^ 
Relinquiahad by: (Sign.) 
/ 
Kaiinquishad by: (Sign.) 
Racalvad by: (Sign.) 
(ZZi. L • — L J ej>y—U^.-~yit..y-L. 
Data/Tiaa 
l i s 2 
J - I S 
Received by: ciSign.) Data/Tiaa 
Received by: (Sign.) Data/Tiaa 
Ralinquiahad by: (Sign.) 
Diapatched by: (Sign.) 
Data/Tiaa 
Rac'd by Laboratory 
for f i e l d 
a n a l y s i s 
( S i g n . ) 
Data/Tiaa 
Rac'd for Laboratory [Data/Tiaa 
b y : 
Method of S h i p a a n t : 
^ 
' 
y ^ (£yeyy^ ^^^y^r^ 
301378 
- • * » 
£nv«io 
19 COPELAND RD.. DENVILLE. NEW JERSEY 07834 
(201) 365-5256 
iOBKiSVK, 
32 EAST 39 STREET. NEW YORK. NEW YORK 10016 
(212) 697-9450 
November 15, 1985 
Mr. Carl Becnell 
G. A. Becnell, Customs Brokers 
150 Marine S t r e e t 
Lake Charles, Louisiana 70601 
Dear Mr. Becnell: 
As per a telephone request from Mr. Frank Curtis of Berlex L a b o r a t o r i e s , I n c . , 
I am sending the enclosed laboratory a n a l y t i c a l sheets which d e s c r i b e the chemical 
contents of hazardous wastes which o r i g i n a t e d in St. Croix, USVI. 
I t i s my 
understanding t h a t U. S. Customs w i l l not r e l e a s e .the material for shippment 
to Chemical Waste Management, I n c . i n Alabama xmtil they know the contents 
of the shippment. 
•• 
Below i s a l i s t i n g of data sheets and to which drums they are a p p l i c a b l e . 
DATA SHEETS 
1 and 2 
3 - 6 
7 - 11 
1 2 - 1 7 
* 
CHEM. WASTE 
MANIFEST NO. 
ALA D 48604 
ALA E 68803 
ALA D 48603 
ALA D 48602 
ALA E 68804 
MATERIAL 
Soil 
Soil 
Sludge 
Water 
Pieces of 
Metal Dnrni.s 
NO. OF DRUMS 
24 
15 
45 
94 
14 
* Pieces of washed drums which contained materials in items 1 and 2 above, 
I t r u s t . t h a t this information will suffice for release of the material. 
If you 
have any questions, contact me at 919/499-5182 or 201/366-6256. 
Very truly yours, 
Alan L. Kyles, 4hD. 
Vice President 
enclosures 
301379 
S & W 
WASTE, INC. 
15 JACOBUSAVE. . SOUTH KEARNY. NJ. 07032. 
(201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
APPROVAL 
COOE 
TECHNICIAL 
REP. INITIALS 
. GENERAL INFORMATION 
ZZ^l'-lo-'^l 
JENERATOR NAME 
~/^SC'5>ff£ 
C Z ^ f f f r f / i ^ C ^ / Z 
^ i " 7 ^ 7 ? r > ^ 
GENERATOR EPA LD. NO. '^O 9 P a ^ r y a ( ? r -
ADDRESS, 
[Sx:^ ^'7'PS 
Cyy^.ys/7?^jrz£ _ Jr-. /Z-^yr-^. tyJ^Zf 
C c f Z o 
TECHNICIAL CONTACT 
^ ' ^ • ^ ^ 
/ Z ^ t U ^ k c ^ t - ' y / ^ 
/g.A'CiMy) 
/ASTE NAME 
/4y^^i^^ ^U^tZ Zpyyo yTy^j:, 
TITLE. 
V ^ 
PHONE ^<r.<^dy<g'-^-^"C" 
PROCESS GENERATING WASTE. 
zy—r—*^— 
B. PHYSICAL CHARACTERISTICS OF WASTE 
PHYSICAL STATE @ 7 0 " F J ° ° ° " 
yyfr<.,y3 
Z SOLID 
V-'Q'J'O 
I C / L 
C SEMI-SOLID D POWDER 
«t. LIOUID 
%H20 
COLOR 
r'ORGANIC 
^INORGANIC 
C CHLORINATED 
ORGANIC 
BTU VALUE PER G A L . 
"b C L _ 
BS4W_ 
Ob ASH. 
% S 
LAYERS 
a MULTI LAYERED 
G BI-LAYERED 
^ S I N G L E PHASED 
TOC. 
COO. 
% S C L : 
y y m ^ 
PH: 
DO-2 
D 2.1-4 
C 4.1-6.9 
C 7 
• 7.1-10 
G 10.1-12.5 
G>12.5 
G E X A C T _ 
• N/A 
v.-t^*^ 
SPECIFIC 
GRAVITY 
I <-8 
: J-.9 
: .5-.95 
: .95-1.0 
: 1.0-1.1 
C 1.1-1.24 
C 1.25-1.4 
G 1.5-1.7 
C>1.7 
G EXACT.£L 7S/9 
• FUVSH 
• POINT 
GCF) 
GCC 
QOC 
CEXACT. 
Q<90 
• <100 
a 100-140 
• 140-200 
n <2oo 
VISCCSiTY (Centipoise) 
g l - l O O 
G 100-1000 
C 1000-10000 
G >iaooo 
C EXACT 
C. CHEMICALCOMPOSITION(MUSTTOTALioo%) % 
-rr-
D. 
Ag 
As 
Ba 
Cd 
Cf 
Cu 
OTHER. 
METALS V. 
C TOTAL 
ZZE. 
yjfi 
AJy. 
y/z 
G EP TOX 
Hg 
Ni 
Pb 
Se 
2n 
Te 
y 
F. HAZARDOUS CHARACTERISTICS: 
TOXICITY RATINGS 
INHALATION 
DERMAL 
ORAI 
C 
EXPLOSIVE 
G WATER REACTIVE 
C MSDS ATTACHED 
NFPA RATING 
yt/c^c' 
q. 
PYROPHORIC 
G SHOCK SENSITIVE 
G. MANIFEST INFORMATION 
PROPER DOT SHIPPING NAME / ^ " ^ ^ ^ i t ^ u J . y y y ^ Z ^ yZi^^ey.r, / t / g ' : 
DOT HAZARD CLASS _ 
UN/NA NO. y ' Z ^ 
(^yeyu-^ 
^yy^ 
EPA/STATE WASTE TYPE _ 
EPA/STATE HAZARD CODE. 
A)€kp/ 
ydAdL 
XJA. 
y^y/i 
yy/l 
y//> 
JilAL 
E. 
G 
G 
G 
G 
G 
G 
G 
G 
G 
OTHER COMPONENTS 
PCB'S* 
PESTICIDES/HERBICIDES* 
CYANIDE OR CYANIDE PRODUCING . 
SULFIDE OR SULFIDE PRODUCING . 
PHENOLICS J 
RADIOACTIVE 
INFECTIOUS "1 
y/yd 
'2K. 
y/yf 
y y y ! 
y < ^ 
y/i^ 
ELEMENTAL METALS*_ 
OTHER. 
,^M^ 
•ATTACHED DISCLAIMERS MUST BE SIGNED 
k M 
H. SHIPPING INFORMATION 
G BULK LIQUID 
G BULK SOLID 
>g DRUMS 
COTrlE 
SHIPPING FREQUENCY: 
nUANTlTY 
/ 
Y.'=.r\. 
PER. 
I. SPECIAL HANDLING INFORMATION/COMMENTS: 
I HEREBY CERTIFY THAT ALL INFORMATIl 
ARE REPRESENTATIVE OF THE WASTE. 
SUBMrrTHD ABOVE AND ALL ATTACHMENTS ARE COMPLETE ANO ACCURAT 
DATE 
TITLE 
SAMPLES SUBMITTED 
301380 
GENERATOR'S SIGNATURE 
Polychlorinated Biphenyl (PCB) Warranty 
This disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
. 
;B'S are used in this disclaimer to refer to any chemical substances and combinations of substan-
Jjes that contain 50 ppm orgreater of PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shali 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who 
knowingly or willfully Ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
hereby warral^ts that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability 
resulting from the breach of this warranty. 
DATED; 
BY:. 
WITNESS: 
Herbicide/Pesticide Warranty 
l^i^^rNtv^ CorrA(r Pr^ roX^tfershy warrants that material transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greater than 0.001% when measured in eSch container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. Z£S=L?^Z^ Qj^^r^iCRp.^ GSl ~iOC. 
nAT.n. 3 - 3 ^ ^ 
RV. VcUk iVAyy^ 
^e.c\tii^.j 
WITNESS; 
yy^2fy<-'^•^:P\ y \ yyy^tZ^-
Aluminum and Reactive Metal Warranty 
k - ^ z y N ^ 
OyZ^^i(^':'^CQ:)^^Z>zZ./L hereby warrants that material offered to S&W Waste, Inc. 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powderor pigment and hereby agrees to idemnify andholdS&WWaste, Inc. harmless 
^rom any costs, damages, or other liability resulting from breach of this warmnty. 
~ . v ^ 
xsLf^Ai^ ctt^t^MusL co,y^k 
..... '^-^'-^^ 
..-.k^rkAJkL-^ 
<^^yjCy 
WITNESS; 
301381 
TABLE 1.4 
30870-0705 
EITVISOSCIEHCSS 
Sajnple Identification: ALAB 64570 
FC3 Isomer 
Result 
.-E • .U 
FC3 1016 
<0.20 
PC3 1221 
<0.20 
PCB 1232 
PCB 1242 
PCB 1248 
PCB 1254 
PCB 1260 
<0.20 
<0. 
<0. 
<0, 
<0 
20 
,20 
.20 
.20 
301382 
YWC. INC. • 200 Mcnrce Turnpike • Monroe. Connecticut 06468 • (203) 261-4458 
"INDUSTRIAL '^-
. CORROSION 
.MANAGEMENT 
INCORPORATED 
NJDEP,.Cercified Dri.-.kins Vacar/ 
...Wascewacer LabqricWy..IDi^ 
14116 
'•.REPORT :,DATE; j ^ ^ j ^ T T ^ _/-7_c 5 5 
1152 ROurt 10. RANOOLPH. NfiV JERSEY 07869 
iOl-584-0330 
CLIENT: E>TVIRO SCIENCES -.. Island Cheaical Proiecc 
SAMPLE SOURCE: SamDle ')3' 
SAMPLE DATE: February g5.--19S6 SAMPLED BY: \_ Kvles 
_AT LAB ..DATE: ^ria-zr. 7. 193 6 
LABORATORY ANALYSIS 
REPORT 
Parameter 
**Pecroleuzi Evdrocarfaon — 
Result 
220"' 
' tug./lXppia) 
We chank you for chis opporrunicy to'ser-/e you.' If you have any questio.r.s-',''please. 
do noc hesicaca co call. 
Sincerely, 
•-•-
INDUSTRIAL-.CORROSION .MAKAGIiHENT',-, 1NC%' 
" 
yky 
lichard S. /Levijie 
Presiden 
RSL: dlh 
LT=iess Chan 
**This cesc employs arialycical mechodology which can-give false posicive readings. •SimpI 
scaced, chis cesc is .measuring che Carbon-Hydrogen linkaga ia...-.c.tganic molkcuies.;- Wiile 
Pecroleum Hydrocarbons mosc cercainly possess chis link, a-^nujabar of organic molecules 
^(H'.imus, Lignin ecc.) noc considered pecroleum based, also p_os.sess it as wellv Therefora 
in order Co more correcdy confirm a high reading, iC is suggesced chac a GG run ba 
additionally performed. 
The above Tocal Pecroleum Hydrocarbon con•cehc^acion•^ffl!ay'•^_QOC^•reJ5Ee•sen 
cRf-r 
hydrocarbon value'as ."ihdicaced by an incerference at-.;.i745 cm-1.'' 
301383 
/ } t ^ ^ 6 ¥1/0 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Carcified Drinking Wacer/Vastavace: 
Laboracory IDi^ 14116 
REPORT DATE; April 14. 1986 
_ ^ ^ 
LAB H 52956 
1152 ROUTE 10. RANOOLPH, NEW JERSEY 07869 
201-534.0330 
CLIENT: ENVIRO SCIENCES - Island Chemical Proiecc 
SAMPLE SOURCE: Samnle il2 
SA:-I?LE DATE: Februarv »28, 19S6 TAKEN BY: A. Kvles AT LAB DATE: 
LABORATORY ANALYSIS 
REPORT 
PARAMETER 
.RESULT 
Flashpoint 
GT 95"C boiled 'I 95'C 
Specific Gravity ~ 
.0.9319 
pH(uni.ts) 
7 . 44 
If you should have any questions, please do not hesitate co call. 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
I 
Richard S. Zervtn 
Presidenc 
RSL:dlh 
GT=Greacer Than 
301384 
y^y.yit^ciyy7a 
S & W WASTE, INC. 
115 JACOBUS AVE. . SOUTH KEARNY. N.J. 07032. 
(201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
APPROVAL 
CODE 
TECHNICIAL 
REP. INITIALS 
I.A. GENERAL INFORMATION 
C
^ 
GENERATOR K.AMP 
J ^ C ^ ^ 
ZPyr<^^iI^ <^ 
k - S ^ 
'juL'*^ I c y . , 
'/^-^7 
ADDRESS. 
^ ^ ! ^ C^y^ kyyy.ys/r7^^^zz> 
Jr. ZZw-^ 
c/S'lZT 
ergfzo 
GENERATOR EPA LD. N Q . / ^ ' . ^ '^Z^ZTyp-y.T-
TECHNICIAL CONTACT 
»VASTE NAME_ 
- / 
y < . V t * ' 
y^ /f^-^ko 
cyvif/£yJCi»*'ti--
ftt*^ti-'jk 
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TITLE, V/^" 
PROCESS GENERATING WASTE. 
yXAcTTT^ 
PHON E 
^ c y j i 6 - f = : z S X 
B. PHYSICAL CHARACTERISTICS OF WASTE 
PHYSICAL STATE «> 70°F 
C SOLID 
' ^ I Q U I D 
C SEMI-SOLID C POWDEH 
% LIQUID 
% H20 
ODOR 
\^^ 
COLOR 
AA{£u>>ryy /P*r 
ORGANIC 
INORGANIC 
: CHLORINATED 
ORGANIC 
BTU VALUE PER GAI 
«<. CL. 
9SiW_ 
«(>ASH. 
% S . 
LAYERS 
a MULTl LAYERED 
^ii'BI-LAYERED 
D SINGLE PHASED 
; TOC. 
I COD. 
•>. SOLIDS 
• t / g ^ ^ -
PH: 
CO-2 
C 7.1-10 
C 2.1-4 
C 10.1-12.5 
C 4.1-6.9 
0 1 2 . 5 
C7 
C EXACT _ 
C N/A 
^. / / 
SPECIFIC 
GRAVITY 
: <.S 
: .a-.9 
: .9-.95 
; .95-1.0 
: ;.o-i.i 
G 1.1-1.24 
G 1.25-1.4 
C 1.5-1.7 
G >1.7 
G EXACT. / : 0 & 
D FLASH 
C POINT 
acc 
DOC 
GEXACT. 
D <90 
C <100 
C 100-140 
D 140.200 
O <200 
'(iSCOSmr (Cemiooiiei 
G 10O-1000 
G 1000-10000 
G > 10.000 
G EXACT 
CHEMICAL COMPOSITION (MUSTTOTAL100%) % 
/Atysy^/Tcy/yz. Z3,L 
y7.£> 
y/. yuAy/TZZ. 
F. HAZARDOUS CHARACTERISTICS: 
TOXICITY RATINGS 
INHALATION 
DERMAL 
ORAL 
G EXPLOSIVE 
• 
WATER REACTIVE 
C MSDS ATTACHED 
y//? 
NFPA RATING 
D 
PYROPHORIC 
C SHOCK SENSITIVE 
G. MANIFEST INFORMATION^ 
PROPER DOT SHIPPING NAMF //2^7*:0C^.i:r 
C ' ^ / Z / . J C W / C 
D. METALS 
Ag 
As 
Ba 
Cd 
Cr 
Cu 
G TOTAL 
Zy/yZ 
y j y ) 
yZTT 
y y / l 
OTHER. 
C EP TOX 
Hg 
Ni 
Pb 
Se 
Zn_ 
Te 
/v'/f 
^z^yL 
y / / : 
y ^ / l . 
DOT HAZARD CLASS 
C / ^ L y ^ - ^ 
UN/NA NO. 
y V y ^ - 
9 r f ^ 
EPA/STATE WASTE TYPE 
EPA/STATE HAZARD CODE. 
<P=^^ 
/ A £ r < i - / . 
.A. 
H. SHIPPING INFORMATION 
G BULK LIQUID 
O BULK SOLID 
7:$)RUMS 
"OTHER 
SHIPPING FREQUENCY: 
QUANTITY 
/ 
PER Ji2L£i:_ 
^ 
E. 
G 
G 
G 
G 
G 
G 
G 
G 
G 
OTHER COMPONENTS 
PCB'S' 
/ / ^ 
PESTICIDES/HERBICIDES*. 
yZiC 
CYANIDE OR CYANIDE PRODUCING 
y ^ ' ^ 
SULFIDE OR SULFIDE PRODUCING 
/ ^ ^ 
PHENOLICS 
/ Z A Z 
RADIOACTIVE 
INFECTIOUS 
yyyi_ 
ELEMENTAL METALS^ 
OTHER. 
y ^ 
•ATTACHED DISCLAIMERS >*US1 8£ SIGNED 
yz>^ 
I. SPECIALHANDLING INFORMATION/COMMENTS: 
J . 
I HEHEBY CERTIFY THAT ALL INFORMATION SUBMITTED ABOVE AND AL'L ATTACHMENTS ABE COMPLETE AND ACCURATE. ANO THAT ALL S-»MPLES SUBMlTTcD 
ARE REPRESENTATIVE OF THE WASTE. 
DATE 
CyQ.zj] 
TITLE 
GENERATORS SIGNATURE 
'^^ZL-f-
301385 
Polychlorinated Biphenyl (PCB) Warranty 
""Ms disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
JB's are used in this disclaimer to refer to any chemical substances and combinations of substan-
ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shali 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, inc. to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
hereby warrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability 
resulting from the breach of this warranty. 
DATED: 
: 
BY: 
WITNESS: 
Herbicide/Pesticide Warranty 
jSurrivi?) ^rtn^.lrpn_r^^ -J^^iMnereby warrants that material transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greater than 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. 
X^'\J^ZiZ> CH^HlC/'tL. Q.C^~i^<Z. 
DATED:. 3-3i-n 
sr.Vs:LXSkiAn 
^^^\?xr--n 
WITNESS:. 
Y?/y^ykky^'-k 
Aluminum and Reactive Metal Warranty 
^Si\z?yZ^C^AAM\'{Z^ ClCl^f^cL 
hereby warrants that material offered to S&W Waste, Inc 
for transportation, treatment and/or disposal does not contain elementa! aluminum ot reactive 
metal paste, powderorpigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmles.< 
Vom any costs, damages, or other liability resulting from breach of this warranty. 
y:^J^-/^j^^ 
— ^ v ' z 
301386 
DATED: 
WITNESS 
m 
TABLE 1.3 
30870-0705 
MYTROSCIENCBS 
Sample Identification: ALAE 64869 
PCB Isomer 
Resiilt. -g'K:? 
PCB 1016 
<3.0 
PCB 1221 
<3.0 
PCB 1232 
'3.0 
PCB 1242 
' 
<3.0 
PCB 1248 
<3.0 
PCB 1254 
<3.0 
PGB 1260 
<3.0 
301387 
YWC. INC. • 200 Monroe Turnpike • Monroe. Connecticut 06^8 • (203) 261-4453 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROUTE 10. RANDOLPH, NEW JERSEY 07869 
201-;34-0320 
J 
August 13, 1986 
Mr. Al Kyles 
ENVIRO SCIENCES INC. 
610 we: 
Main Street 
Rockavay, NJ 07866 
RE: 
Island Chemical Project - Flashpoincs 
Dear Mr. Kyles: 
Upon your request three samples fron Island Chemical( Sanple data: 2/2S/86) have 
been reanalyzed for Flashpoint using a Pensky-Martens Closed Tester. Saapla v5 
(Labv 52958) and Sanple •t'V-s.bi.- 52960) were composited and analvzed on .V. 
1986. 
The conoosita boiled a- 98°C. The 
:us; 
il results reportad(Re:;or: cata: 
March 7, 1936) were Sample =5 - 40°C duplicate 41°C and Sample it 7 - 45'c. Sample 
Y5 and iH were originally analyzed separately. There was insufficient samoie 
remaining to reanalyze sample i'S and -17 individually. 
Sample H i l a h i f 52957) was also reanalyzed on August 7, 1986., The original Flash-
point reported for this saaale was 50''C. The reanalysis resulted in a flashpoint 
of 5^'C. 
We do not feel that the results of these reanalyses are as reliable as possible since 
the samples have been held for over five months from the date of collection. As 
stated in the method erroneously high flashpoints may be obtained due to loss of 
volatile material. These saaples were-n^ox stored in volatile organic bottles and 
therefore volatiles may have been lost. We are also unsure as to the correctness • 
of compositing hazardous waste for analysis. Enclosed please find a page from the 
NJDE? Field Procedures Manual, November 1985, cautioning against this practice. I 
have also enclosed a copy of the procedure for determining flashpoint by Pensky-
Martens Closed Tester. 
If you have any further questions, please do not hesitate to call. 
Sincerely, 
INDUSTRD^ CORROSION MANAGEMENT, INC. 
Susan Richardson 
Quality Assurance Coordinator 
SR:dls 
enclosures 
301388 
yii.A^€<S61 
STATE CERTIFIED DRINKING WATER/WASTEWATER LABORATORY I.D. #14116 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROUTE 10. RANOOLPH. NEW j£J?SEir 07859 
201-584.0320 
NJDE? Certified Drinking Wacer/ 
Wastewater Laboratory ID-/ Uli6 
REPORT DATE: .a,nril U . 198c 
LAB Q 
52957 
CLIENT: ENVIRO SCIENCES - Island Chemical Proiect 
SAMPLE SOURCE: Samnle •f^-
SAMPLE DATE: February 2S. 1956 SAMPLED BY: A. Kvlas 
AT LAB DATE: \t^~.--
1936 
LABORATORY ANALYSIS 
REPORT 
Parameter 
**Petroleum Evdrocarfaon 
Result 
176.000 
mg/l(ppm) 
We chank you for chis oppo: 
do not hesitate to call. . 
to serve you. If you have any questions, please 
j 
Sincerely, 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
..,,, ,,zyy 
Lcnard S./LaviXe 
ichard S.A. 
resident/ 
RSL:dlh 
LT=less Chan 
**This test employs analytical mechodology which can give false positive readings. Simp' 
stated, this test is measuring the Carbon-Sydrogen linkage in organic molecules. While 
Petroleum Hydrocarbons most certainly possess this link, a number of organic molecules 
(Humus, Lignin etc.) noc considered petroleum based, also possess it as well. Therefore 
in order to more correctly confirm a high reading, it is suggested that a GC run be 
additionally performed. 
The above Tocal Petroleum Hydrocarbon concentration may noc represenc crue peer 
hydrocarbon value as indicated by an interference at 1745 cm-1. 
301389 
,cyi'^6<'f^'^ 
INDUSTRIAL . 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROUTE 10. RANOOLPH. NFiV JERSEY 07869 
201-534-0230 
NJDEP Certified Drinking Wacer/Vastewaca-
Laboratory IDi? 14116 
REPORT DATE: April 14, 1986 
LAB ? 52957 
CLIENT: ENTIRO SCIENCES - Island Chemical Proiect 
SAMPLE SOLTICE: Samnle fM 
SA>£PLE DATE: Februarv 28, 1986 TAKEN BY: A. kvles AT LAB DATE: March 7, l = i 
LABORATORY ANALYSIS 
REPORT • 
PARAMETER 
RESULT 
Flashooin; 
50' 
Specific Gravity 
1. 0565 
pH(units) 
• 
6.81 
If you should have any questions, please do not hesitate to call. 
INDUSTRIAL COI^ROSION MANAGEMENT, INC. 
[/v^y---e^ 
President 
RSL:dlh 
301390 
.^cyiei"/*''' 
S & W WASTE, INC. 
1 5 JACOBUS AVE. . SOUTH KEARNY, N.J. 07032. 
(201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
APPROVAL 
CODE 
TECHNICIAL 
REP. INITIALS 
GENERATOR EPA I.D. NO. V / C 
^ t f ^ ^ ^ - / ^ 3 r -
/GsTfZ. (^"^"^.^ 
k'yy/?/srr:i*fj7^, J r - 
dyie<^ , / / n Z T 
c c p z . 0 
GENERAL INFORMATION 
'.ENERATOR NAMP 
JlTctT^^? k k y y ^ / C a c k J ' ( / , 
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y i ^ 
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ADDRESS-
TPrHNiriAi r.nNTAP.T 
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TiTi P 
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ASTE N A M E . 
P R O C E S S GENERATING W A S T E . y'^<r?f^ 
PHONE . ^ ^ J z k t l l k ^ ^ ^ 
B. PHYSICAL CHARACTERISTICS OF WASTE 
'HYSICAL STATE » TCFi °°°"y<^/'<Lp 
: SOLID 
^ L I Q U I D 
C SEMI-SOLID 3 POWDER 
"b LIQUID 
. H 2 0 _ 
o/<.^ 
j ' ^ O S G A N l C 
I 
J ~ INORGA.NIC 
COLOR 
"Z CHLORINATED 
ORGANIC 
BTU VALUE PER GAL 
• • > * • 
• • • - ' 
_ ^ 
% C L _ 
BS4W_ 
""b ASH. 
% S . 
LAYERS 
C MULTI LAYERED 
•:; BI-LAYERED 
2<SiNGLE PHASED 
] TCC 
i COO 
I 
i a^ SOLIDS Vt'-Ty<g" 
pH: 
• 0-2 
G 7.1-10 
C N/A 
C 2.1-4 
G 10.1-12.5 
G 4.1-6.9 
0 1 2 . 5 
^ 
. y 
C 7 
G EXACT 
ZZZZ— 
SPECIFIC 
GRAVITY 
:• <.3 
; .5-.3 
: .9-.95 
: .95-1.0 
: 1.0-1.1 
C 1.1-1.24 
G 1.25-1.4 
G 1.5-1.7 
= >'-7 
/ . e r ' 
G EXACT _ 1 _ _ I _ _ 
D FLASH 
G POINT 
CCF) 
• CC • 
• OC 
• EXACT. 
• <90 
• 
<100 
C 100-140 
G 140-200 
G <200 
9/'<^ 
iN(lSyOSrrY (CentiDoise) 
^ 1 - 1 0 0 
G 100-1000 
G 100O-10000 
G > 10.000 
G EXACT 
C. CHEMICALCOMPOSIT10N(MUSTTOTALioo%) 
% 
zR. 
/ : & : ^ i y M * - ^ 
/4c/y.yr^-y 
< ^ o . ( j ^ : , 0 / 
D. METALS 
Ag 
y
^ 
As 
Ba 
Cd 
Cr 
yZA. 
Cu 
^ Z : 
D TOTAL 
zz>y 
~zzyr 
y//^ 
O T H E R . 
A/y; 
C EP TOX 
H g . 
N i . 
P b . 
S e . 
Z n . 
T e . 
AJ^ 
y y y ; 
y j y . 
~/yyr 
yyyi 
yZZZ 
F. HAZARDOUS CHARACTERISTICS: 
TOXICITY RATINGS 
• 
INHALATION 
D F R M A l 
ORAL 
G 
EXPLOSIVE 
G WATER REACTIVE 
C 
M S D S ATTACHED 
yA/f--
NFPA RATING 
G 
P Y R O P H O R I C 
D 
S H O C K SENSITIVE 
G. MANIFEST INFORMATION 
PROPER DOT SHIPPING NAME ^r.A.cAt«^ oAy^T^ yZca/cyi/y 
DOT HAZARD CLASS _ 
UN/NA NO. 
yJy} 
OyCyff-€' 
^yA^ 
EPA/STATE WASTE TYPE 
_ 
EPAySTATE HAZARD C O D E . 
^ Z ^ - ' 
t Z y y t z f y 
H. SHIPPING INFORMATION 
C 3 U L K L I Q U I D 
C B U L K S O L I D 
" ^ D R U M S 
G O T H E R 
SHIPPING FREQUENCY: 
QUANTITY 
S r ^ j ? 
ER 
g*^cy 
E. 
G 
0 
C 
Q 
G 
G 
G 
n 
OTHER COMPONENTS 
PCB'S* 
PESTICIDES/HERBICIDES* 
CYANIDE OR CYANIDE P R O D U C I N G . 
SULFIDE OR SULFIDE P R O D U C I N G _ 
P H E N O L I C S 
RADIOACTIVE 
INFECTIOUS 
y y ^ 
yZAT 
y/r 
/ j y t 
E L E M E N T A L M E T A L S * . 
O T H E R . 
•-ZA4-
yyy^ 
vTTACHED DISCLAIMERS MUST BE SIGNED 
I. SPECIALHANDLING INFORMATION/COMMENTS: 
I HEREBY CERTIFY THAT ALL INFOF^^lOflON SUBMIfTEp|ABOVE 
ARE REPRESENTATIVE OF THE WAS 
• 3 - I b ^ ^ T 
DR^OriON SUBMIfTEplABOVE AN» ALL ATTACHMENTS ARE COMPLETE 
ALL ATTACHMENTS ARE COMPLETE AND ACCURATE. AND THAT ALL SAMP'.ES SUBMlTTcD 
DATE 
TITLE 
GENERATOR'S SIGNATURE 
301391 
Poiychiorinated Biphenyl (PCB) Warranty 
•' '-^ disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
_ 3's are used in this disclaimerto refer to any chemical substances and combinations of substan-
:es that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
in a process which contains less than 50 ppm PC3 because of any dilution; again, these.latter shall 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
hereby warrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability 
resulting from the breach of this warranty. 
DATED: 
EY: 
WITNESS; 
Herbicide/Pesticide Warranty 
T^Lf^^JD r'-tfcl'^-lC/>?P^ca.'DK4ifirphy warrants that material transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greater than 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. ^jiSL-fVJi^C n^.tC^'tV- OJC aTfXl 
DATED:. 
V/ITNESS: 
Aluminum and Reactive Metal Warranty 
" I ^ V , < V ^ rngTAiTftu ( ^ . A>f3T . 
hereby warrants that material offered to S&W Waste, Inc. 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powderorpigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless 
''om any costs, damages, or other liability resulting from breach of this warranty. 
— ^ 
:P3U.VJO ctKwMC/?u06\<^^c 
DATED:_?±il^3 
PV- ^ . . W . ^ C
^ 
WITNESS: 
301392 
TAHLB 1.0 
30S70-0705 
ENVTROSCIENCES 
Samule Identification: KARB 64980 
PCB Isomer 
P.es'a.1' 
PCB 1016 
<0.20 
PCB 1221 
<G.20 
PCB 1232 
<0.20 
PCB 1242 
. 
<0.20 
PCB 1248 
' 
<0.20 
PCB 1254 
<G.20 
PCB 1260 
<0.20 
301393 
YWC. INC. • 200 Monroe TL^npske • Monroe. Connecticut 06d6& • (203) 261-'U58 
p' 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
.1152 ROUTE 10. RANOOLPH. NEW JERSEY 07863 
201-534^330 
August 13, 1986 
Mr. Al Kyles 
ENVIRO SCIOCES INC. 
610 West Main Screec ..... 
Rocks.way, NJ 07866 
RE: 
Island Chemical Project - Flashpoinrs 
Dear Hr. Kyles: 
Upon your request three saaples from Island ChemicaK Sanple date: 2/2S/86) have 
been reanalyzed for Flashpoint using a Pensky-Martens Closed Tester. Sancie ?5 
(Lab/f 52958) and Sample i-7(Lab# 52960) were composited and analyzed on Aurust 7, 
1986. 
The composite boiled at 9S°C. The original results reported(Re::ort date: 
March 7, 1986) were Sanple -75 - '^O'C. duplicate 41°C and Samule -f 7 - ^'s'C 
ianaie 
115 and 
were origina 
si 
LVZ: 
setjar; :eiv. There was insufficient sansle 
remaining to reanalyze sanple ^5 and 117 individually.-
Sample ill4(lab# 52957) was also reanalyzed on August 7, 1986. The original Flash-
point reported for this sasrole was 50'C. The reanalysis resulted in a fashpoint 
or 54°C. 
We do not feel that che results of these reanalyses ara as reliable as possible sines 
the samples have been held for over five months from the dace of collection. As 
stated in Che method erroneously high flashpoints may be obtained due co loss of 
volacile material. These sanples were"."n'ar stored in volatile organic bottles and 
therefore volatiles may have been lost. We are also unsure as'to the correctness 
of compositing hazardous waste for analysis. Enclosed please find a page fron the 
NJDE? Field Procedures Manual, November 1985, cautioning against this practice. I 
have also enclosed a copy of the procedure for determining flashpoint by Pensky-
Martens Closed Tester. 
If you have any further questions, please do not hesitate to call. 
Sincerely, 
INDUSTRIAL CORROSION M.'^AGEMZNT, I N C . 
y 
SR:dls 
enclosures 
Susan Richardson 
Quality Assurance Coordinator 
301394 
STATE CERTIRED DRINKING WATE.R/WASTEV/ATER LABORATORY I.D. S14115 
/*^yiyzcc^9S^0 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Certified Drinking Wacer/Wastavate: 
Laboratory ID# 14116 
REPORT .DATE: .^oril 14. 1986 
LAB H 52960 
1152 ROUTE 10. RANDOLPH. NEW JERSEY 07£o5 
201-584-;3330 
CLIENT: ENVIRO SCIENCES - Island Chenical Project 
SAMPLE SOURCE: Samole -fH 
SAMPLE DAIE: Februarv .28, 1986 lAKZM SY: A. Kvles AT LAB DATE: March 
?86 
LABORATORY ANALYSIS 
REPORT 
PARAMETER 
RESULT 
F l a s h p o i n t 
S p e c i f i c 
Gravi 
p H ( u n i t s ) 
45°C 
1.0836 
5.05 
If you should have any questions, please do not hesitate to call. 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
RSL;dlh 
glchard S. I^vWe 
President r 
y»l y,yci.4'/i^ 
301395 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROUTE 10. RANDOLPH. NEW JERSEY 07865 
201-534.0330 
NJDE? Certified Drinking Wacar/Wastevate: 
Laboracory IDi* 14116 
REPORT DATE; April 14. 1986 
LAB# 52958 
CLIENT: ENVIRO SCIENCES - Island Chenical Proiect 
SAMPLE SOURCE; Samnle •'/5 
SAMPLE DATE: Februarv JS, 19S6 TAKEN BY: A. Kvles AT LAB DATE: March 
LABORATORY ANALYSIS 
REPORT 
PARAMETER 
RESULT 
Flashpoint 
Specific Gravit; 
pHCunits) 
^0°C 
1.0206 
4.51 
— 1 U V .-ur; 
If you should have any questions, please' do noc hesicace to call. 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
V ^ 
' / y j y ^ y - - ^ 
RSL:dlh 
Richard S. LfevThe 
Presidenc 
/ 
301396 
y y ^ ^ £ 6<tl<' 
..INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROUTE IQ. RANOOLPH. NEW JERSEY 07863 
201-584-01-0 
NJDE? C e r c i f i e d Drinking Water/ 
Wastewater Laboracory IDi/ 14116 
REPORT DATE; A p r i l 14. joRf, 
LA3 i 
52953 
CLIENT; ENVIRO SCIENCES - Island Chenical Proiect 
SAMPLE SOURCE: Sample •?5 
SAMJ'LE DATE: February 28. 1986 SAMPLED BY; A. Kvles 
AT LAB DATE: ^'=-
LABORATORY ANALYSIS 
REPORT 
Parameter 
**Pecroleum Evdrocarbon 
Result 
LT 5 
mg/l(ppm) 
We chank you for this opportunity to serve you. If you have any questions, please 
do noc hesicace co call. 
Sincerely, 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
lichard S. /Levi^e 
Presidenc k 
RSL;dlh 
LT»less than 
**This Cesc employs analytical mechodology which can give false positive readings. Sinp 
stated, chis cesc is measuring che Carbon-Hydrogen linkage in organic molecules. While 
Pecroleum Hydrocarbons mosc certainly possess chis link, a number of organic molecules 
(Humus, Lignin ecc.) noc considered pecroleum based, also possess ic as well. Therefore 
in order to more correctly confirm a high reading, ic is suggesced chac a GC run be 
addicionally performed. 
The above Tocal Pecroleum Hydrocarbon concentration may noc represenc crue peer 
hydrocarbon value as indicated by an interference at 1745 cm-i. 
301397 
^ y j / l . e ' 6 ^<lfO 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP C e r c i f i e d Drinking Water/ 
Wascewacer Laboracory ID') 14116 
RZPORT DATE; 
April 14. 1986 
L ^ 
^ 
52960 
1152 ROUTE 10. RANOOLPH, NEW JERSEY 07869 
201-584.0330 
CLIENT; prVIRO SCIENCES - Island Chenical Proiect 
SAMPLE SOURCE; Samole ••?7 
SAMPLE DATE: February 28. Icge SAMPLED 3Y: 
A. Kvles 
_AT LAB DATE: Manr. 7. 19S5 
LABORATORY ANALYSIS 
REPORT 
Paramecer 
**Pecroleun Hydrocarbon 
Resulc 
100 
ng/1(ppm) 
We chank you for chis opportunicy to serve you. If you have any questions, please 
do not hesitate to call.. 
• 
" 
Sincerely, 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
Aichard 
S./Levi^e 
President 
RSL; dlh 
LT-less than 
**This Cesc employs analycical mechodology which can give false posicive readings. Simpi 
scaced, chis cesc is measuring che Carbon-Hydrogen linkage in organic molecules. While 
Pecroleum Hydrocarbons mosc cercainly possess chis link, a number of organic nolecules 
(Humus, Lignin etc.) not considered pecroleum based, also possess ic as well. Therefore,
in order Co more correcdy confirm a high reading, it is suggested that a GC run be 
additionally performed. 
The above Total Petroleian Hydrocarbon concentration may not represenc crue peer 
hydrocarbon value as indicaced by an incerference at 1745 cn~l-. 
301398 
^ ^ A : ^ £ < ' 7 y ^ 
^INDUSTRIAL ••^•-
JCORROSION 
1 MANAGEMENT 
INCORPORATED 
.^^- 1152 ROUTE JO, RANDOLPH. NEW JERSEY 07869 
r01-5M-033O 
CLIENT; EN\'IRO SCIENCES - Island Ihemical Proiect 
NJDEP Certified Drinking Water/ 
Wastewater Laboratory ID# 14116 
REPORT DATE; Apr-;i 14, iofl<^ 
LAB } 
59ot;6 
y ' ^ " -t 
^ 
SAMPLE SOURCE: Samole il3 
SAMPLE DATE; February 18.- 1986 SAMPLED BY: A. Kvles 
AT LAB DATE; March 7. 1986 
LABORATORY ANALYSIS 
RZPORT 
Parameter 
**Petroleum Evdrocarbon 
Resulc 
22£L 
mg/l(ppm) 
We chank you for chis opporcunicy to serve you. If you have any quescions, please 
do noc hesicace to call. 
Sincerely, 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
iichard 
S./L 
P r e s i d e n c / 
evi;(e 
RSL: dlh 
LT-less Chan 
**This Cesc employs analycical mechodology which can give false posicive readings. Simp.' 
stated, chis cesc is measuring che Carbon-Hydrogen linkage in organic nolecules. While 
Pecroleum Hydrocarbons mosc cercainly possess chis link, a number of organic nolecules 
(Humus, Lignin ecc.) noc considered pecroleum based, also possess iC as veil. Therefore 
in order co more correcdy confirm a high reading, iC is suggesced chac a GC run be 
additionally performed. 
. 
. 
The above Tocal Pecroleum Hydrocarbon concentration may noc represenc true peer 
hydrocarbon value as indicaced by an incerference ac 1745 ca-1. 
301399 
/o^ytT^ ¥!/o 
^ 
S & W WASTE, INC. 
115 JACCBUS AVE. . SOUTH KEARNY. N.J. 07032. 
(201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
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A P O R O V A L 
COOE 
TECHNICIAL 
REP. INITIALS 
. GENERAL INFORMATION 
CA^'^'/DSI 
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D MSDS ATTACH ED 
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ARE REPRESENTATIVE OF THE WASTE. 
y \ 
TITLE 
DATE 
BMITTED ABOVE AND ALL AHACMMENTS ARE COMPLETE AND ACCURATE. AND THAT ALL.£AMP 
ily€^^' AAy.iA.kLI 
GENERATOR'S SIGNATURE 
THZZZZ 
301400 
Polychlorinated Biphenyl (PCB) Warranty 
•^his disclaimer is to all persons v/ho generate and dispose of chemical waste. The terms PCB and 
r'CB's are used in this disclaimerto refer to any chemical substances and combinations of substan-
ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct 
in a process which contains less than 50 ppm PCB because of any dilution; again, these lattershall 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc. to receive PCB'a Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
Ooyy 
/.^ 
A -. ,. 
f Z 
\'z:xz^-r-'-r=r:r^=^/ 
hereby warrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability 
resulting from the breach of this warranty. 
J ^ L f ^ O 
CthiA^ UZb-^ Qyj J I M <=-
DATED:. 
g - ( / - ^ ? 
.v ^ y V ^ C k f M - - QeeyJuP^ 
WITNESS: 
( ^ y ^ ^ ^ 
Herbicide/Pesticide Warranty 
hereby warrants that material transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greater than 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. X ' - ^ L P ^ ^ Cff-^O^^^^TV ^ ^ ^ 
^ ^ ' 
DATED: 
wn..... 
k^^<ky^/^yzCy 
Aluminum and Reactive Metal Warranty 
^ 
hereby warrants that material offered to S&W Waste, Inc 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless 
from any costs, damages, or other liability resulting from breach of this warranty. ^ ^ 
DATED: 
' S ^ ^ I S l 
BY: ^ j ^ rJA^/i/K/V-^ ^ U ^ A s J ^ ^ 
wnt^F'^.- 
/ ^ k ^ . * < J ^ y ^ c ^ L y ^ 
301401 
S & W 
WASTfc, INC. 
15 JACOBUSAVE. . SOUTH KEARNY. N.J. 07032. (201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
CODE 
TECHNICIAL 
REP. INITIALS 
GENERAL INFORMATION 
_ 
GENERATOR M A I ^ P 
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•ATTACHED DISCLAIMERS MUST BE SIGNED 
F. HAZARDOUS CHARACTERISTICS: 
TOXICITY RATINGS 
INHALATION 
DERMAL 
ORAL 
D 
EXPLOSIVE 
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WATER REACTIVE 
O MSDS ATTACHED 
NFPA RATING 
y / C y ^ ^ 
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S H O C K S E N S m v E 
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DOT HAZARD CLASS, 
UN/NA NQ. 
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EPA/STATE WASTE T Y P E . 
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^ C X ^ Z -
- / -
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C BULK LIQUID 
G BULK SOLID 
X ' D R U M S 
SHIPPING FREQUENCY: 
QUANTITY 
y7y6^A~r*:C^ £fyjy 
O O T H E R 
5 
PER,i!25£*-' 
I. SPEplALHANDLING INFORMATION/COMMENTS: 
y y ^ < ^ : 
k/y^jy/^ i^/t^^t;^ ^/=- / ^ rr<L. /7/iyo 
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I HEREBY CERTIFY THAT A.LL INFORMATION SUBMITTED ABOVE AND ALL ATTACHMENTS ARE COMPLETE ANO ACCURATE. AND 
ARE REPRESENTATIVE 0= THE WASTE. 
A>'ID-3 7 
DATE 
czy,y-. 
TITLE 
GENERATOR'S SIGNATURE 
lAT ALL SAMPLES SUBMITTED 
301402 
Polychlorinated Biphenyl (PCB) Warranty 
T 
- disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
F-^^B's are used in this disclaimer to refer to any chemical substances and combinations of substan-
ces that contain 50 ppm org reater of PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
in a process which contains less than 50 ppm PCB because of any dilution; again, these lattershall 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlavi^ul for S&W Waste, Inc to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
" 4 ^ ^ ^ ^ 
-^—^^'^£r^S 
hereby warrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc harmless from any costs^ damages or other liability 
resulting from the breach of this wan-anty. 
XSLl*rAJD CtrtC^'-<^/'^~>- CO ZP^^ 
3-f(-S? 
RY- ^ S k A r v y - 
^ c y j - ^ 
wiTNF.';.^- /z2iz^^y^^zk^iyu/ 
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Herbicide/Pesticide Warranty 
KZ y A i • -y 1 . " ^ 
hereby warrants that material transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greater than 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. JTx-^A-IAJO QtPiyA^CATi C ^ Z ^ <^ 
DATED:. 
DATED: 
WITNESS: 
Aluminum and Reactive Metal Warranty 
? £ ^ 
hereby warrants that material offered to S&W Waste, Inc. 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powderorpigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless 
'•om any costs, damages, or other liability resulting fr©ffl±)reach^fihisw^n^i;^^ ^ ^ 
_ . 
DATED:_Ojl/_|2i2 
. 
Ry. I ^ W ^ j 
C L ( ^ I V \ 
, Scg^^-/^ 
WITNESS: 
c^ty^'^^^..rr<. 
y \ <yU 
^ 
301403 
S & W 
WASTE, 
INC. 
115 JACOBUSAVE. . SOUTH KEARNY. N.J. 07032. (201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
GE NERATOR NAME 
J
^
g
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APPROVAL 
CODE 
TECHNICIAL 
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A. GENERAL INFORMATION 
ADDRESS 
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GENERATOR EPA I.D. NO. fAZ^^JlZ^J/.y'^ 
TECHNICIAL CONTACT 
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WASTE MAK.c 
/ y ^ - ^ j y ^ ^ 
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0 £ f ^ 
TITLE. yp 
PROCESS GENERATING WASTE 
yZy^/fy/Chc^rrj 
PHONE ^ / / W - g . ^ 
B. PHYSICAL CHARACTERISTICS OF WASTE 
PHYSICAL STATE @ TCF! 
^ S O L I D 
12 LIQUID 
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% LIOUID 
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F. HAZARDOUS CHARACTERISTICS: 
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D MSDS ATTACHED 
yj/^ 
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QUANTITY. 
COTHER 
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OTHER. 
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ZZM. 
I. SPECIALHANDUNG INFORMATION/COMMENTS: 
y ^ y a o u t y ^ ^ . y t y y / Z : y ^ 
y ^ ^ y i y ^ ^ y 7 y y j y ^ < . y y y A i ^ 
1 HEREBY CERTIFY THAT ALL INFORMATION 
ARE REPRESENTATIVE OF THE WASTE. 
DATE 
lACHMENTS ARE COMPLETE AND ACCURATE. AJ<D THAT AU. fAMPl.ES SUBMITTED 
/ 
C^^.iA. 
TITLE 
GENERATOR'S SIGNATURE 
301404 
Polychlorinated Biphenyl (PCB) Warranty 
is disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
rCB's are used in this disclaimerto refertoany chemical substancesand combinations of substan-
ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
in a process which contains less than 50 ppm PCB because of any dilution; again, these lattershall 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils,* heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
PtQsecution. 
o,o-x 
_ 
y k r > , Av^.O^r^TT^lO^ (^<) -P^J"^ 
ireby warrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability 
resulting from the breach of this warranty. 
JkS\.f\^k) C^'^A^Ur^ (ZO or/^o. 
DATED:. 
3->(-^V 
PY- \^\od^(3J^fhy^rSey^^i{^^y 
WITN 
i Z ^ ^ ^ 
_ 
Herbicide/Pesticide Warranty 
17_1-^•ll y z . --fz. 
Kr=^ L'-rr-r-TT': v:::rT 
hereby warrants that material transferred by it to S&W Waste, Inc. 
fortransportation, treatment and/or disposal is not contaminated by herbicide/pesticide ata level 
greaterthan 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc harmless from any costs, damages or 
other liability resulting from the breach of this warranty. 
jpTS {.^f\T>ZO> C ti^r^C^rh^Cl U 
DATED: 
^ - )/-^7- 
py. ^l>vtC|/alAv— iQzc^Jz-^^ 
WITNESS: /M^^k^jy 
^Aluminum and Reactive Metal Warranty 
\ 
\^^^—^ 
.^-P-TTSI^* 
hereby warrants that material offered to S&W Waste, Inc. 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, I nc. harmless 
-om any costs, damages, or other liability resulting fronoLbreach of this warranty., ^ . 
n yr. T 
yU.^f\/y^y) ol^^^^j^icn- ^ 
y 
^ ' \ i - y 
._ ... ^i^^ciMy— ^^o^ 
DATgP- 
; 
„ 
. 
^ 
WITNESS: _ 
301405 
:^i'i 
PRIORITY POLLUTANT VOLATILE ORGANIC ANALYSIS 
LABORATORY ID IU116 
LAB # 
5295^ 
CLIENT: ENVIRO .SCIENCES-I.siand Chemir::! V-ni 
SAMPLE SOURCE Sample n 
... .-..-:. 
ec; 
GC/MS Method 624* 
Tier II Deliverables 
PARAMETER 
Chloromethane 
Bromomethane 
-• 
Vinyl Chloride 
• 
Chloroethane 
Hethylene Chloride 
1 ,1-Dichloroethene 
1 ,1 -Dichloroethane 
Trans-l ,2-Dichloroethene 
• 
Chloroform 
1,2-Dichloroethane 
1 ,1 ,1-Trichloroethane 
Carbon Tetrachloride 
Bromodichloromethane 
1,2-Dichloropropane 
• 
--
Trans-1,3-Dichloropropene 
Trichloroethene 
Di bromochloromethane 
1,1 ,2-Trichloroethane 
Benzene — 
cis-1", 3-Dichloropropene — 
2-Chloroethyl vinyl ether 
Bromoform 
Tetrachloroethene 
1,1 ,2 ,2-Tetrachloroethane 
Toluene 
• 
Chlorobenzene 
Ethyl benzene 
Total Xylenes 
*Dichlorobenzenes noc analyzed under chis mechod. 
RESULT 
ug/l 
u 
u 
u 
u 
u 
u 
u 
u 
8.2B 
U 
U 
U 
U 
U 
u • 
" 
i 
u 
u 
u 
u 
u 
u 
u 
u 
3.900B 
U 
6. 7J 
U 
HtiHOD 
BLANK 
ug/l 
u 
u 
u 
u 
7 = ' 
U 
u 
u 
".8 J 
U 
U 
U 
U 
IT 
U 
u 
u 
D 
2.0J 
U 
D 
U 
U 
U 
^.9J 
U 
U 
HDL 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
• 10 
10 
10 
Analyzed by GC/MS Method 625. 
y<is^^</iyf 
301406 
INDUSTRIAL 
-
CORROSION 
^MANAGEMENT 
INCORPORATED 
NJDEP Certified Drinking Wacer/Vascewac« 
Laboracory IDtf 14116 
REPORT DATE: April 16. 1986 
LAB i 
5295A 
.1152 ROUTE 10. RANOOLPH. NEW JERSEY 07869 
201-584.0330 
CLlENT: ENVIRO SCIENCES - Island Chemical Project 
SAMPLE SOURCE: Samnle #1 
SAMPLE DATE: February 28... 1986 TAKEN BY: A. Kvles AT LAB DATE: M.arch 7, 19S6 
LABORATORY ANALYSIS 
RZPORT 
PARAMETER 
RESULT 
Benzoohenone 
Neat Benzoohenone 
If you should have any questions, please do not hesitate,to call. 
INDUSTRIAL CORROSION MANAGEMENT, INC, 
Ritf^ard S. L^v 
President 
RSL:dlh 
y<^£(.4s^i' 
301407 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Certified Drinking Water/wasravace: 
Laboracory IDif 14116 
. .... ' 
RZPORT DATE: April 14. 19^6 
LAB 9 52954 
.1152 ROUTE 10. RANOOLPH. NEW JERSEY 07869 
201-584-0330 
CLIENT:-ENVIRO SCIENCES - Island Chemical Project 
SAMPLE SOURCE: Samole #1 
SAMPLE DATE: Februarv.28, 1986 TAKEN BY: A. Kyles AT LAB DATE: M.arch 7. 1986 
LABORATORY ANALYSIS 
REPORT 
P.ARAMETER 
Ignitability 
Specific Gravity 
— 
pH(units) 
RESULT 
Ignites without persistent burr 
21.97 
8.06 
ng 
If you should have any questions, please do not hesitate co call. 
INDUSTRIAL CORROSION MJ^AGEMZNT, INC. 
lichard S 
President 
RSL:dlh 
301408 
ynyc'n^/i!' 
S & W WASTE, INC. 
115 JACOBUSAVE. . SOUTH KEARNY, N.J. 07032. 
(201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
APPROVAL 
COOE 
TECHNICIAL 
REP. INITIALS 
GENERAL INFORMATION 
C£iZ)^-lo-'Sn 
GENERATOR NAME - / ^ S ^ " ^ ^ Cyr<*ff''e/i£.. C t J ^ ^ 
i 
id"^'/ 
GENERATOR EPA LD. NO. Y'^/Z 9P(/>&r/a<?r 
ADDRESS 
^fcg? (Z77S- 
<Zyyy.ysr>?y*jTZD _ J r - . ^ ^ ^ , ^ y j l j ^ 
C o / ^ o 
MuuMtsa 
' — ^ ~ :^_ - 
^ 
/ 
: •- 
^ i — r : 
TECHNICIAL CONTACT 
/
^ 
A Z . A t S l - ^ Jc^cy/c^ J c ^ ^ ^ c ^ 
. y 
. 
^ y - y - y • • 
. . 
WASTE NAME, 
Af^y^^^y-*"!^ 
^ t y c * ! " ^ 
yZptyye 
. ^ / C S - ' 
— — i — 
— 
TITLE. vr 
PROCESS GENERATING WASTE 
/ZZ-Z'^Ki'^i^ ^
^ Z ) a 
PHONP ^ C / / ^ 6 - < Z : ' 
B, PHYSICAL CHARACTERISTICS OF WASTE 
PHYSICAL STATE @ 70"F 
C SOLID 
"^LIQUID 
• SEMI-SOLID C POWDER 
t LIQUID 
%H2D 
ODOR y ^ , t . ^ 
C/y.. 
COLOR 
G'ORGANIC 
^INORGANIC 
n CHLORINATED 
ORGANIC 
BTU VALUE PER GAL. 
% CL_ 
BS4W. 
%ASH. 
% S, 
LAYERS 
D MULTI LAYERED 
D BI-LAYERED 
"^SINGLE PHASED 
TOC. 
COD. 
•H. SOUPS y y r n ^ 
pH: 
• 0-2 
D 7.1-10 
n N/A 
D 2.1-4 
D 10.1-12.5 
D 4.1-6.9 
D>12.5 
^ ^ ^ f i , 
0 7 
n C5rArT 
' • ~ ^ 
• EXACT. 
SPECIFIC 
GRAVITY 
C <.8 
D J-.9 
0 5 5 
D .95-1.0 
• 1.0-1.1 
• 1.1-1.24 
D 1.25-1.4 
D 13-1.7 
D>1.7 
• EXACT. c. 9S/9 
OFLASH 
G POINT 
am 
OCC 
• OC 
G EXACT. 
• <90 
• <100 
G 1OO-140 
O 140-200 
"D <200 
.VlSCOSmr (Centipois 
S'l-ioo 
• 100-1000 
• 1000-10000 
• >iaooo 
C EXACT 
C H E M I C A L C O M P O S m O N (MUSTTOTAL 100%) % 
y ^ 
• ^ 7 ^ ^ 
D. METALS 
Ag 
As 
A ^ 
' 
D TOTAL 
y 
./Ay^ 
Ba 
C(j 
Cr 
Cu 
OTHER. 
yA/\ 
y A y 
ZML 
JiAL 
D EPTOX 
Hg. 
Ni yyy^ 
Pb 
r / A 
Se 
/ / f l . 
2n y y / l 
TP yyy^ 
E. 
D 
D 
D 
a 
D 
D 
D 
D 
D 
OTHER COMPONENTS 
PCB'S* 
' 
PESTICIDES/HERBICIDES* _ _ _ _ _ 
CYANIDE OR CYANIDE PRODUCING . 
SULFIDE OR SULFIDE PRODUCING _ 
PHENOLICS 
^ 
RADIOACTIVE 
INFECTIOUS 
\ZK. 
Z^Z 
yK. 
A ^ 
y A 
ELEMENTAL METALS*_ 
OTHER. 
yK. 
•ATTACHED DISCLAIMERS MUST BE SIGNED 
AJA^ 
F. HAZARDOUS CHARACTERISTICS: 
TOXICITY RATINGS 
INHALATION 
DERMAL 
ORAL 
. D EXPLOSIVE 
D WATER REACTIVE 
• 
MSDS ATTACHED 
NFPA RATING 
y ^ O T l / E ' 
D 
PYROPHORIC 
D SHOCK SENSITIVE 
G. 
M A N I F E S T I N F O R M A T I O N 
j . j . 
PROPER DOT SHIPPING NAME / ^ l ^ - ^ ^ g ^ A y / y x . A/t:cy,r, Ay 
DOT HAZARD CLASS _ 
UN/NA NO y'AA-
< p / ^ y ~ ^ 
WJ? 
EPA/STATE WASTE TYPE. 
EPA/STATE HAZARD CODE. 
"25^Z 
_y_ 
H. SHIPPING INFORMATION 
D8ULKL/0UID 
DBULKSOLID 
"JXDRUMS 
SHIPPING FREQUENCY: 
QUANTITY 
DOTHER 
/ 
p g R c-*<y^— 
I. SPECIAL HANDUNG INFORMATION/COMMENTS: 
I HEREBY CERTIFY THAT ALL INFORMATIl 
ARE REPRESENTATIVE OF THE WASTE. 
DATE 
L ATTACHMENTS ARE COMPLETE ANO ACCURAT, 
SAMPLES SUBMITTED 
TITLE 
GENERATOR'S SIGNATURE 
301409 
Poiychiorinated Biphenyi (PCB) Warranty 
•^his disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
CB's are used in this disclaimerto refer to any chemical substances and combinations of substan-
ces that contain 50 ppm orgreater of PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
in a process which contains less than 50 ppm PCB because of any dilution; again, these lattershall 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
hereby warrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability 
resulting from the breach of this warranty. 
DATED: 
BY: 
WITNESS:. 
Herbicide/Pesticide Warranty 
T ^ r V s i T ^ Ccmv.(r(TL rPi:<.tferehy warrants that material transferred by it to S&W Waste, Inc. 
fortransportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greaterthan 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. 
' X ^ L N Z } ) (Zd^Q^iZRp.^ ( j l ~fOC. 
3-5^^^ 
. . . ^ U [LlZy,.t 
DATED:. 
WITNESS: 
Aluminum and Reactive Metal Warranty 
J - S l j f V J ^ C[inZ)\(C(^ CfpyTy^C hereby warrants that material offered to S&W Waste, Inc. 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powder or pigmentandherebyagreestoidemnify and holdS&WWaste, Inc. harmless 
*''om any costs, damages, or other liability resulting from breach of this warranty. 
_ ^^ 
xsLf^isit^ ctt^Hcrj^ co,/-roc 
DATED: _ i l _ _ _ 
" 
nv 
^ r A x J i 
A u U ^ T ^ 
Ak^yy^ze:^^ 
WITNESS: 
301410 
TABLE 1.4 
30870-0705 
ENVISOSCIHNCBS 
Saaple Identification: ALAE 64S70 
PCB Isomer 
Res--ilt. v.^.^': 
PCB 1016 
<0.20 
PCB 1221 
" 
<0.20 
PCB 1232 
<0.20 
PCB 1242 
, 
<0.20 
PCB 1248 
' 
<0.20 
PCB 1254 
<0.20 
PCB 1260 
<0.20 
301411 
YWC. INC. • 200 Monroe Turnpike • Monroe. Connecticut 06468 • (203) 261-iU58 
S & W WASTE, INC. 
115 JACOBUSAVE. . SOUTH KEARNY. N.J. 07032. (201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
APPROVAL 
CODE 
TECHNICIAL 
REP. INITIALS 
A. GENERAL INFORMATION 
C/kyl) ^ - - A d S "> 
GENERATOR K..MC 
Z Z I c ^ ^ 
k ^ ^ ^ ^ i ^ ^ J S ^ - 
J ^ ^ j ) 
_ 
^ 
GENERATOR EPA I.D. UO.lA'J> ' ^ f i ^ T / a ? ^ 
ADDRESS 
^^ZSK^ (Z'y'yi^ ky^y^S/T^^J^^^ , J r . (Zk^-yy 
(y^KT 
jfofZO 
TECHNICIAL CONTACT 
A Z ^ - ^ ^ 
^ 
/ ^ - ^ / ^ t - ^ > / C > ^ g ^ - - ^ 
WASTE NAME 
A f 4 . T y . y f ^ ^ u T s y ' ^ 
A k ' s V / P ( A / c f ^ 
TITLE. VA' 
PHONE _ £ C y ^ 6 2 5 ^ r X 
PROCESS GENERATING WASTE 
y l ^ i T T i ^ 
B. PHYSICAL CHARACTERISTICS OF WASTE 
PHYSICAL STATE @ 7 0 T 
D SOLID 
' ^ I Q U I D 
a SEMI-SOLID 
D POWDER 
% LIQUID 
%H20 
ODOR 
,y>fy<~o 
COLOR 
^ORGANIC 
D INORGANIC 
D CHLORINATED 
ORGANIC 
BTU VALUE PER GAI 
(/yy:/<C/.An<.nr) 
% CL_ 
BS4W_ 
%ASH, 
% S . 
LAYERS 
a MULTI LAYERED 
X'BI-1-AYERED 
D SINGLE PHASED 
TOC. 
COO. 
<»> SOUDS 
y y < ' ^ < - ' 
pH: 
nO-2 
D 7.1-10 
D N/A 
D 2.1-4 
C 10.1-12.5 
• 4.1-6.9 
0 1 2 . 5 
. 
p , 
D 7 
n P Y a r r 
G - ' ' 
SPECIFIC 
GRAVITY 
n <.8 
• .fl-.9 
• .9-.95 
D .95-1.0 
D 1.0-1.1 
D 1.1-1.24 
• 1.25-1.4 
D 1.5-1.7 
0 1 . 7 
D EXACT_ y. e 6 
D FLASH 
• POINT 
• CF) 
DCC 
• OC 
• EXACT. 
• <90 
• <100 
• 100-140 
• 140-200 
• <200 
yiSCOSmr (Centipoise) 
X'-ioo 
C 100-1000 
G 1000:10000 
OI'OOOO 
C EXACT 
C. CHEMICAL COMPOSITION (MUSTTOTAL 100%) % 
AA/cZAac/^rL O r L 
y 7 . 6 
~Z7ZZkJ. 
/Zi/'ATT^ 
F2tf^ 
D. 
Ag 
As 
Ba 
Cd 
Cr 
Cu 
OTHER. 
METALS 
n TOTAL 
A m — 
yZ/Z 
y j A 
yZTT 
yZ/iZ^ 
: ^ 
ZUTT 
D EPTOX 
Hg 
Ni 
Pb 
. Se 
Zn 
Te 
Ai/A 
^/K. 
y y y 
y/£-
yjA. 
A ^ 
F. HAZARDOUS CHARACTERISTICS: 
TOXICITY RATINGS 
INHALATION 
DERMAL 
ORAL 
D EXPLOSIVE 
D WATER REACTIVE 
Q MSDS ATTACHED 
yA//? 
NFPA RATING 
D 
PYROPHORIC 
D SHOCK SENSITIVE 
G. MANIFEST INFORMATION 
PROPER DOT SHIPPING NAME AA?'- :7/:ocu:. c','=-/rz yucw/c 
DOT HAZARD CLASS 
C / ^ y f f - ^ 
UN/NA NO. 
y A y : - 
9 / ^ ^ ? 
EPA/STATE WASTE TYPE 
EPA/STATE HAZARD CODE. 
tPeSay 
2 h r ^ / . 
/ 
; ^ = ^ 
H. SHIPPING INFORMATION 
D BULK LIQUID 
DBULKSOLID 
)g^RUMS 
G OTHER 
SHIPPING FREOUENCY: 
QUANTITY _ _ _ Z _ _ 
PER _£21«£-
E. 
a 
D 
D 
D 
D 
D 
D 
D 
D 
OTHER COMPONENTS 
PCB'S* 
A t ^ 
PESTICIDES/HERBICIDES* 
yV/' 
CYANIDE OR CYANIDE PRODUCING 
yV/! 
SULFIDE OR SULFIDE PRODUCING 
AJA 
PHENOLICS 
y / A 
RADIOACTIVE. 
INFECTIOUS _ 
yyy7_ 
yzz^ 
ELEMENTAL METALS*_ 
OTHER. 
y A 
•ATTACHED DISCLAIMERS MUST BE SIGMED 
yZA_ 
I. SPECIALHANDUNG INFORMATION/COMMENTS: 
I HEREBY CERTIFY THAT ALL INFORMATION SUBMITTED ABOVE ANO ALL ATTACHMENTS ARE COMPLETE ANO ACCURATE. ANO THAT ALL SAMPLES SUBMITTED 
ARE REPRESENTATIVE OF THE WASTE. 
DATE 
TITLE 
GENERATOR'S SIGNATURE 
301412 
Poiychiorinated Biplienyi (PCB) Warranty 
"^his disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
r'CB's are used in this disclaimerto referto any chemical substances and combinations of substan-
ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct 
in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shall 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
hereby warrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability 
resulting from the breach of this warranty. 
DATED: 
: 
BY: 
WITNESS: 
Herbicide/Pesticide Warranty 
J^'yU'ZZi CrXa^.i/fryr:^ .Z^j^&rehy warrants that material transferred by it to S&W Waste, Inc. 
fortransportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greaterthan 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. XSij^iMT^ C t r t ^ l C / " ^ CO ~<uC. 
DATED:. 3-3i-n 
,.-.^sk±lkA: 
• ^ r . \ g W ^ 
y^.yyyAC 
WITNESS:. 
'' yj^y/T^^- y \ y ( , y ^ - ^ y 
Aiuminum and Reactive IVIetal Warranty 
'^ZAyyFZ^ C^pA\f{Z\^ ^ . T / I ^ k 
hereby warrants that material offered to S&W Waste, Inc. 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powderorpigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless 
from any costs, damages, or other liability resulting from breach of this warranty. 
XSLAMIi CH©n[C/^ co.^rf^c 
3-^'-^^ 
, 
BY:J^eki-Ly^ 
DATED 
WITNESS: . y^A^^AAZy 
301413 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Cercified Drinking Wacer/Vasteuace: 
Laboracory IDif 14116 
. __* 
REPORT DAIE: April U , 1986 
LAB H 52956 
1152 ROUTE 10. RANOOLPH. NEW JERSEY 07863 
201-584-0330 
CLlENT: ENVIRO SCIENCES - Island Cheaical Projecc 
SAMPLE SOURCE: Sample #3 
S.\MPLE DATE: Februarv «£8, 1986 T.^CZN BY: A. Kvles AT LAB DATE: March 7, 19 = 6 
LABORATORY ANALYSIS 
RZPORT 
PARA-^TER 
Flashpoinc 
Specific Gravicy 
pH(unics) 
RESULT 
GT 95'C boiled @ 95°C 
0.9319 
7.i4 
If you should have any quescions, please do noc hesicace Co call. 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
RSL:dlh 
GT=Greacer Than 
Richard S. Ee'v^ne 
Presidenc 
301414 
yfy-y<s- 6 i y 7 a 
TABLE 1.3 
30870-0705 
ENVHtOSCIBNCBS 
SaaiJle Identification: ALAE 64869 
PCB Isomer 
R e sill t. mff.^ll? 
PCB 1016 
PCB 1221 
PCB 1232 
PCB 1242 
PCB 1248 
PCB 1254 
PCB 1260 
3.0 
3.0 
3.0 
3.0 
3.0 
3.0 
3.0 
301415 
YWC INC. • 200 Monroe Turnpike • Monroe. Connecticut 06^8 • (203) 261-A^S 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
J 
1152 ROUTE 10, RANDOLPH. NEW JERSEY 07869 
201 •584-0330 
Augusc 13, 1986 
Mr. Al Kyles 
ENVIRO SCIENCES INC. 
610 Wesc Main Screec ...... . 
Rockaway, NJ 07866 
RE: 
Island Chemical Project - Flashpoincs 
Dear Mr. Kyles: 
Upon your requesc chree sa:=?les from Island ChemicaK Sample dace: 2/28/86) have 
been reanalyzed for Flashpoint using a Pensky-Martens Closed Tester. Sanpls ?5 
(Labi? 52958) and Sample a'7(Lab-? 52960) were composited and analyzed on August 7, 
1986. 
The composite boiled at SZ'C. 
The original results reported(Report date: 
March 7, 1986) were Sample #5 - 40°C duplicace ^ T C and Sample H 7 - Zs'C. Sa-iple 
#5 and v7 were originally analyzed separacely. There was insufficienc sample 
remaining Co reanalyze sample S5 and S7 individually.• 
Sample jf4(labi? 52957) was also reanalyzed on August 7, 1986. The original Flash-
poinc reported for this sasple was 50''C. The reanalysis resulced in a flashpoinc 
of 54''C. 
We do not feel that the resulcs of these reanalyses are as reliable as possible since 
the samples-have been held for over five monchs from che dace of collection. As 
stated in the mechod erroneously high flashpoincs may be obtained due Co loss of 
volacile material. These samples were:n-Dr stored in volatile organic bottles and 
therefore volatiles may have been lost. We are also unsure as to the correctness 
of compositing hazardous waste for analysis. Enclosed please find a page from the 
NJDE? Field Procedures Manual, November 1985, caucioning against this practice. I 
have also enclosed a copy of the procedure for decermining flashpoint by Pensky-
Martens Closed Tester. 
If you have any further-questions, please do not hesitate to call. 
Sincerely, 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
Susan Richardson 
Quality Assurance Coordinator 
SR:dls 
enclosures 
301416 
.y}4y^6¥tf67 
STATE CERTIFIED DRINKING WATER/V/ASTEWATER LABORATORY I.D. #14116 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Certified Drinking Water/ 
Wastewater Laboracory ID/ U116 
RZPORT DATE; April 14. 1936 
LAB 3 
5 29=' 
1152 ROUIE 10. RANOOLPH, NEW j£j?SEY 07869 
201-584-0330 
CLIENT: ENVIRO SCIFJiCES - Island Chemical Proiect 
SAMPLE SOURCE; Sample .U-• 
SAMPLE DATE: Februarv 28. 1986 SAMPLED BY: A. Kvles 
_AT LAB DATE: y.ar:h 7. 10R6 
LABORATORY ANALYSIS 
REPORT 
Paramete: 
**Pecroleum Hydrocarbon 
Result 
176.000 
mg/l(ppm) 
We thank you for this opportunicy to serve you.- If you have any quescions, please 
do not hesitate to call. 
Sincerely, 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
^/:^^!^^^uc^ 
lichard S./Levi;<e 
Presidenc 
RSL:dlh 
LT-less than 
. A m i 
**This test employs analytical mechodology which can give false posicive readings. Simply 
stated, this test is measuring che Carbon-Hydrogen linkage in organic molecules. While 
Petroleum Hydrocarbons most certainly possess chis link, a number of organic molecules 
(Humus, Lignin ecc.) not considered petroleum based, also possess it as well. Therefore, 
in order to aore correctly confirm a high reading, ic is suggested that a GC ran be 
additionally performed. 
^The above Total Petroleum Hydrocarbon concentration may noc represenc crue pecrol 
hydrocarbon value as indicated by an incerference at 1745 ca-1. 
301417 
yftiyi ^e<tf6'L. 
INDUSTRIAL _ 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Certified Drinking Wacer/Vastewace: 
Laboratory ID# 14116 
REPORT DATE': April 14. 1986 
LAB # 52957 
1152 ROUTE 10. RANOOLPH. NHW JERSEY 07869 
201-584^0330 
CLIENT: ENVIRO SCIENCES - Island Chemical Project 
SAMPLE SOURCE: Sample #4 
SA.MPLE DATE: Februarv 28, 1986 TAKEN BY: A. kvles AT LAB DATE: March 7, I9S6 
LABORATORY ANALYSIS 
REPORT 
PARAMETER 
Flashpoint 
Specific Gravity 
pH(units) 
RESULT 
50°C 
1.0565 
6.81 
If you should have any quescions, please do not hesicace Co call. 
INDUSTRIAL CORROSION M.'^AGEMINT, INC. 
Xichard S./lV-fine 
Presidenc' 
RSL:dlh 
301418 
,i<./)£<iii*''i 
, 
S & W WASTE, INC. 
115 JACOBUS AVE. . SOUTH KEARNY. N.J. 07032. 
(201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
APPROVAL 
CODE 
TECHNICIAL 
REP. INITIALS 
I. GENERAL INFORMATION 
GENERATOR MAI^F 
y S C / h ^ klYy^/Cec/Jy^ ( j 
ADDRESS 
^ : : e ^ g 7 ? S 
(Zyy/?/jrr:>afj7ZD , J r 
ZUr*^ 
. 
GENERATOR EPA LD. NO. A/£_£.£^L^uZyC?T 
TECHNICIAL CONTACT 
WASTE NAME. 
y^Lz*f yZ. /AZyzu^ Cky/iy/yjc JiayyueA 
TITLE 
//fyTygyuti.^ 
Z^MifZ^ >c/g^.ie y y c ^ ^ -
V/> 
PROCESS GENERATING WASTE 
A y < Z 7 y ^ 
PHONE ,^£AZ^£zLk^^^^ 
B. PHYSICAL CHARACTERISTICS OF WASTE 
PHYSICAL STATE @ 70°F 
• SOLID 
^LIQUID 
n SEMI-SOLID C POWDER 
% LIQUID 
%H20 
ODOR 'yrfycy> 
I'V'ORGANIC 
i 
J :: INORGANIC 
COLOR 
C/<i^y~.//Sy^<v^<^t^ 
D CHLORINATED 
ORGANIC 
BTU VALUE PER GAL 
G 
U^/t/^a*<-
««> CL_ 
BS4W_ 
%ASH. 
;X 
•fcS . 
LAYERS 
0 MULTI LAYERED 
D BI-LAYERED 
JSlSINGLE PHASED 
TOC. 
COD. 
'>*! SOLIDS yiZ^Ty^ 
pH: 
co-2 
D 7.1-10 
C 2.1-4 
•10.1-12.5 
• 4.1-6.9 
• > 1 2 J 
• 7 
• EXACT 
• N/A 
<'7 
SPECIFIC 
GRAVITY 
• -ca 
D .a-.g 
• .9-.95 
• .95-1.0 
• 1.0-1.1 
• 1.1-1.24 
• 1.25-1.4 
a 1.5-1.7 
n FXArT 
^ 
• FLASH 
• POINT 
DCF) 
• CC • 
• OC 
• EXACT_ 
• <90 
• <100 
• 100-140 
• 140-200 
• <200 
9/'<: 
\ ^ p O S m r (Centipois*) 
^ 1 - 1 0 0 
C 100-1000 
• 1000-10000 
• >iaooo 
• EXACT 
CHEMICAL COMPOSITION (MUSTTOTAL IOO%) % 
'y-t^:&iruyiy^ 
/yyc/^u:=^ 
< r o . o t T O / 
D. 
Ag. 
As. 
Ba. 
Cd. 
Cr_ 
Cu. 
METALS 
D TOTAL 
W/Z 
'TJTT 
y/A 
~yJAZ 
OTHER. 
y/y. 
D EP TOX 
Hg 
Nl 
Pb 
Se 
Zn 
Te 
yJA 
y y A 
y j y ; 
yyyr 
yUA 
AZK. 
E. 
D 
a 
D 
Q 
D 
D 
D 
D 
G 
OTHER COMPONENTS 
PCB'S* 
PESTICIDES/HERBICIDES* 
CYANIDE OR CYANIDE PRODUCING. 
SULFIDE OR SULFIDE PRODUCING _ 
PHENOLICS 
. 
RADIOACTIVE 
INFECTIOUS _ 
yZAT 
~^Z 
Z^HL 
.AyA 
ELEMENTAL METALS'_ 
OTHER. 
Z^/1 
yyA 
•ATTACHED DISCLAJMEHS MUST BE SIGNED 
F. HAZARDOUS CHARACTERISTICS: 
TOXICITY RATINGS 
INHALATION 
DERMAL 
ORAL 
D EXPLOSIVE 
D WATER REACTIVE 
D MSDS ATTACHED 
y/// 
NFPA RATING 
D 
PYROPHORIC 
a 
SHOCK SENSITIVE 
G. MANIFEST INFORMATION 
- J y. 
PROPER DOT SHIPPING NAME ^ r y u A ^ ^ ^ (Z/yyT^ y Z y S i y r o / i / u ^ 
DOT HAZARD CLASS _ 
UN/NA NO. 
y^AA 
o y y f / ' € ' 
^y,r? 
EPA/STATE WASTE TYPE 
. Z c ^ V ^ 
EPA/STATE HAZARD nODF 
^ W v 
yL. 
H. SHIPPING INFORMATION 
D BULK LIQUID 
DBULKSOLID " ^ DRUMS 
G OTHER 
SHIPPING FREQUENCY: 
QUANTITY 
- ^ ^ 
P=R 
C-fc^ 
I. SPECIALHANDUNG 
INFORMATION/COMMENTS: 
I HEREBY CERTinr TMAT AtL INFOI 
ARE REPflESENTATlVE OF THE WAS' 
•3~-|D''^7 
DATE 
3RI|0»T10N SUBMlfTEBlABOVE ANA AU. ATTACHMENTS ABE COMPLETE 
^^^^fci y^ 
' T I T L E 
I 
GENERATOR'S SIGNA' 
AND ACCURATE. AND THAT ALL SAMP_ES SUBMITTED 
301419 
Polychlorinated Biphenyl (PCB) Warranty 
is disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
JB's are used in this disclaimerto referto any chemical substances and combinations of substan-
ces that contain 50 ppm orgreater of PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shall 
be includec as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships-PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
hereby warrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability 
resulting from the breach of this warranty. 
DATED: 
BY:. 
WITNESS: 
Herbicide/Pesticide Warranty 
T S L I ^ V J ^ C^^^'^'lCf^^CQilXZherehy warrants that material transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greater than 0.001% when measured in each container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. 3:su/VOi>CCiO^.(C'^t\_ 0D<. X•^Xl. 
DATED: 
I ' ^ J - ^ 
BY: i 4 4 v . A f k ai'Tr 
WITNESS: 
Aluminum and Reactive Metal Warranty 
" T ^ \ . N ^ r.m^Ai/^ftV- (^. X A ^ . 
hereby warrants that material offered to S&W Waste, Inc. 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless 
^^om any costs, damages, or other liability resulting from breach of this warranty. 
— y 
DATED:_llill^3 
. 
BY: J ^ c W K ^ ^ ^ f c ; ! 
WITNESS: 
301420 
TABLE 1.0 
30870-0705 
ENVIROSCIENCES 
SajnT3le Identification: MARE 64980 
PC3 Isomer 
PCB 1016 
PCB 1221 
PCB 1232 
PCB 1242 
PCB 1248 
PCB 1254 
PCB 1260 
Result. ug./L 
<0.20 
<0.20 
<0.20 
<0.20 . 
<0.20 
<0.20 
<0.20 
301421 
YWC. INC. • 200 Monroe Turnpike • Monroe. Connecticut 06^66 • (203) 261-4.458 
G' 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROUTE 10. RANOOLPH. NEW JERSEY 07869 
:01-5S4.0330 
Augusc 13, 1986 
Mr. Al Kyles 
ENVIRO SCIENCES INC. 
610 Wesc Main Screec ...... 
Rockaway, NJ 07866 
RE: , Isiand CheTsical Pro j ecc - Flashpoincs 
Dear Mr. Kyles: 
Upon your requesc chree samples from Island ChemicaK Sample dace: 2/28/86) have 
been reanalyzed for Flashpoinc using a Pensky-Marcens Closed Tescer. Sanple r5 
(Lab// 52958) and Sample #7(Lab# 52960) vere composiced and analyzed on Augusc 7, 
1986. The composice boiled ac 98°C. The original resulcs re?orced(Reporc dace: 
March 7, 1986) were Sample #5 - AO'C duplicace UVC and Sample il 7 - A5'C. Sample 
i;5 and #7 were originally analyzed separacely.' There was insufficienc sample 
remaining Co reanalyze, sample #5 and #7 individually. 
j 
(. : 
Sample i^4(labi? 52957) was also reanalyzed on Augusc 7, 1986. The original Flash-
poinc reporced for chis sairole was 50*C. The reanalysis resulced in a flashsainc 
of 54'C. 
- 
' 
We do noc feel chac che resulcs of chese reanalyses are as reliable as possible since 
Che samples have been held for over five monchs from che date of colleccion. As 
seated in che mechod erroneously high flashpoincs may be obtained due to loss of 
volacile material. These samples were:ntj£ stored in volatile organic bottles and 
therefore volatiles may have been lost. We are also unsure as to the correctness 
of compositing hazardous wasce for analysis. Enclosed please find a page from the 
NJDEP Field Procedures Manual, November 1985, caucioning against this practice. I 
have also enclosed a copy of the procedure for decermining flashpoinc by Pensky-
Marcens Closed Tester. 
If you have any further questions, please do not hesitate to call. 
Sincerely, 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
Susan Richardson 
Quality Assurance Coordinacor 
SR:dls 
( • ! 
enclosures 
STATE CERTIFIED DRINKING WATER/WASTEV/ATER LABORATORY I.D. #14116 
y*f/l/ZCCHf9S^ 
301422 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Certified Drinking Wacer/Vascewace: 
Laboracory ID# 14116 
RZPORT DATE; April 14,, 1986 
LAB S 5296G 
1152 ROUTE 10. RANDOLPH. NEW JERSEY 07869 
201-584-0330 
CLIENT: ENVIRO SCIENCES - Island Chemical Projecc 
SAMPLE SOURCE: Samnle #7 
SAMPLE DATE: February.28. 1986 TAKEN BY: A. Kvles AT LAB DATE: March 7. 1985 
LABORATORY ANALYSIS 
REPORT 
PARAliETER 
RESULT 
Flashpoinc 
Specific Gravicy 
pH(units) 
45°C 
1.0836 
5.05 
If you should have any questions, please do not hesitate to call. 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
RSL:dlh 
Tchard S. Lk^ 
resident 
^ i 
/ j A * : ^ 
vTAe 
301423 
yafyty rt> 4 . ^ i ^ 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Certified Drinking Wacer/Vascevace-
Laboratory ID? 14116 
REPORT DATE: April 14, 1986 
LAB? 52958 
1152 ROUTE 10. RANOOLPH. NEW JERSEY 07869 
201-584.0330 
CLIENT: ENVIRO SCIENCES - Island Chemical Proiecc 
SAMPLE SOURCE: Sample #5 
SA.MPLE DATE: Februarv JJ8, 1986 TAKEN BY: A. Kvles AT LAB DATE: March 7, 15S6 
LABORATORY ANALYSIS 
REPORT 
PARAMETER 
RESULT 
•CS 
Flashpoint 
40°C 
41*0(dup) 
Specific Gravicy 
1.0206 
pH(units) 
— 
4.51 
If you should have any quescions, please do not hesitate to call. 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
RSL:dlh 
Richard S 
President A 
301424 
^ A C C 6<-'Jt'' 
INDUSTRIAL ---
CORROSION 
-
MANAGEMENT 
INCORPORATED 
1152 ROUTE iO. RANOOLPH. NE"W JERSEY 07869 
201-584-O330 
NJDEP Cercified Drinking Wacer/ 
Wastewater Laboracory LD# 14116 
REPORT DATE: April 14. 1035 
LAB i 52958 
CLIENT: ENVIRO SCIENCES - Island Chemical Proiect 
SAMPLE SOURCE: Sample J?5 
SAMPLE DATE: February 28. 1986 SAMPLED BY: A. Kvles 
_AT LAB DATE: Msr:h 7. 1986 
LABORATORY ANALYSIS 
REPORT 
Paramecer 
**Pecroleum Hydrocarbon 
Resulc 
LT 5 
mg/l(ppm) 
We thank you for this opportunicy to serve youl If you have any quescions, please 
do not hesicace to call. 
Sincerely, 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
lichard S./leviXe 
Presidenc 
RSL:dlh 
LT"less than 
**This test employs analytical methodology which can give false positive readings. Simply 
scaced, this test is measuring the Carbon-Hydrogen linkage in organic molecules. While 
Pecrcleum Hydrocarbons mosc cercainly possess chis link, a number of organic molecules 
(Humus, Lignin etc.) not considered petroleum based, also possess it as well. Therefore, 
in order to more correctly confirm a high reading, it is suggested that a GC run be 
additionally performed. 
^The above Total Petroleim Hydrocarbon concentration may not represent crue pecrol 
hydrocarbon value as indicaced by an interference at 1745 cm-l. 
301425 
^ y t / c e " G^flfO 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Cercified Drinking Water/ 
Wascewacer Laboracory IDt 14116 
REPORT DATE: Anrll 14. 1986 
LAB S 
52960 
1152 ROUTE 10. RANOOLPH. NEW JERSEY 07869 
201-584-0330 
CLIENT: ENVIRO SCIENCES - Island Chemical Proiect 
SAMPLE SOURCE: Sample 47 
SAMPLE DATE: February^ 28. 1986 SAMPLED BY: 
A. Kvles 
AT LAB DATE: Mar:h 7. I9{ 
LABORATORY ANALYSIS 
REPORT 
Parameter 
**Pecroleum Hydrocarbon 
Resulc 
100 
mg/l(ppm) 
We thank you for this opportunity to serve you'. If you have any questions, please 
do not hesitate to call. 
Sincerely, 
INDUSP.IAL CORROSION MANAGEMENT, INC. 
Aichard S./ievi;(e 
Presidenc J 
RSL: dlh 
LT-less than 
**This test employs analytical mechodology which can give false positive readings. Simpl: 
stated, this test is measuring the Carbon-Hydrogen linkage in organic molecules. While 
Petroleum Hydrocarbons most certainly possess this link, a number of organic nolecules 
(Humus, Lignin etc.) not considered pecroleum based, al.«?o possess ic as well- Therefore, 
in order to more correctly confirm a high reading, it is suggested that a GC run be 
additionally performed. 
The above Total Petroleum Hydrocarbon concentration may not represenc true pecro 
hydrocarbon value as indicated by an interference at 1745 cm-1. 
301426 
/ n y i j i t y 6 < ' J f ° 
S & W WASTE, INC. 
115 JACOBUSAVE. . SOUTH KEARNY, N.J. 07032. 
(201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
APPROVAL 
CODE 
TECHNICIAL 
REP. INITIALS 
.. GENERAL INFORMATION 
^4^^^ 
"/O'^'^y/ 
GENERATOR NAME. -2^^^^^^ y^fyTfyCS,, d>, 
ADDRESS. 
^ ^ 
GENERATOR EPA LD. NO. \ZZ^_2if^Syo^r~ 
yis!:*i' (s-A?S 
k k y l y j / f ^ T ^ ^ 
S r 
<Z/Zyr.Ay 
/ / S V / 
g t e ^ ^ o 
TECHNICIAL rnNiT^rT 
y ^ ' > ^ / • 
/ ^ ^ » g ^ / ' C f y r r - e 
J O U ^ U C A ) 
WASTE NAME 
/>^.e<<Zy<^ <:yyyy:7ZZ J
^
/ 
y ^ < ^ ^ 
TITLE. 
vy 
P H O N F - ^ g / A ^ ^ - g - Z J - Z . 
PROCESS GENERATING WASTE. 
/yyryy^ADu/yy 
B. PHYSICAL CHARACTERISTICS OF WASTE 
PHYSICAL STATE © 7 0 T 
^ S O U I D 
C; LIQUID 
D SEMI-SOLID 
O POWDER 
to LIOUID 
'><.H20 
ODOR y j f ^ C t O 
. 
/ ^ . ^ C y c 
'^ORGANIC 
C INORGANIC 
COLOR 
2 < i , S U ^ 
• 
CHLORINATED 
ORGANIC 
BTU VALUE PER GAI 
( / y . f K / / C U ^ 
«*> C L _ 
BS«W_ 
% A S H . 
% S . 
LAYERS 
/ ( / / 
C MULTI LAYERED 
G BI-LAYERED 
• SINGLE PHASED 
TOC. 
COD, 
y/y? 
<K) SOLIDS. 
pH: 
DO-2 
D 7.1-10 
D 2.1-4 
D 10.1-12.5 
D 4.1-6.9 
0 1 2 . 5 
D 7 
O EXACT _ 
D N/A 
SPECIFIC 
GRAVITY 
~ J-.9 
D .9-.95 
2.95-1.0 
O 1.0-1.1 
D 1.1-1.24 
a 1.25-1.4 
D l i - 1 . 7 
• >1.7 
< . - t t ' y 
O EXACT _ £ £ : L i _ 
D FLASH 
n POINT 
DTF) 
D C C 
D O C 
DEXACT. 
D < 9 C 
D < 1 0 0 
D 100-140 
D 140-200 
X y t 2 0 0 
VISCOSnY (CentiooiM) 
C 1-100 
C lOC^lOOO 
• 
1000-10000 
o i a o o o 
j r , y 
C S X A C T ^ y Z Z L 
C H E M I C A L C O M P O S I T I O N (MUSTTOTAL ioo%) 
% 
j ^ * * Zcy'Af£/^<^tL, 
\ 
<JtO 
yZ/^^v^yr ZL^ 
•:y/y^A:<^£ey ^ / 
2 - 7 ^ ^ „ A \ 
D . 
M E T A L S 
nTOTAL 
Ag 
y A A 
A^ 
yy/: 
Ba 
Cd 
Cr 
Cu 
OTHER. 
yy/i 
yyy: 
y / A 
a E P T O X 
Hg. 
A M 
Ni. 
Pb 
'Zn 
^ A 
T P 
/ t A 
yi/A 
OTHER COMPONENTS 
PCB'S* 
A / / . 
PESTICIDES/HERBICIDES*. 
E, 
D 
D 
D 
D 
a 
D 
a 
D ELEMENTAL METALS*_ 
D OTHER. 
.^J/L 
y / A 
y l ^ 
CYANIDE OR CYANIDE PRODUCING . 
SULFIDE OR SULFIDE PRODUCING . 
PHENOLICS 
^ 
y/A... 
RADIOACTIVE 
INFECTIOUS 
A/A 
y Z / ^ 
.yi^iSL 
y / A 
•ATTACHEO DISCUUMERS MUST BE SIGNED 
F. HAZARDOUS CHARACTERISTICS: 
TOXICITY RATINGS 
INHALATION 
DERMAL 
ORAL 
n 
EXPLOSIVE 
a WATER REACTIVE 
G MSDS ATTACHED 
y A 
NFPA RATING 
D 
PYROPHORIC 
D 
S H O C K 
SENSITIVE 
G. MANIFEST INFORMATION 
PROPER DOT SHIPPING NAME y-/,7MCe.fii, c U y i 
Z r A . / 
y y ^ 
DOT HAZARD CLASS 
^ S ^ ^ 
UN/NA NO 
/ i A / f ~ 9ycP7 
EPA/STATE WASTE TYPE 
EPA/STATE HAZARD CODE. 
^-^Sf 
y 
H. SHIPPING INFORMATION 
D BULK LIQUID 
CBULKSOLID 
X^DRUMS 
C OTHER. 
SHIPPING FREOUENCY: 
QUANTITY__Z___ 
PER. OT..£y. 
I. SPECIALHANDLING 
INFORMATION/COMMENTS: 
/^^^^^gy^jyofTcz. ^cytcAJy^yjiy^ yuyZ'.j^Ayft^f^tfcy.y 
Jay>s^ gty*^ y;^y*<'^ yJAJJy^ 
^yyATyf 
1 HEREBY CEHTIFY TMAT A1.L INFORMATION^ 
ARE REPRESENTATIVE OF THE WASTE. 
[JBMITTED ABOVE ANO ALL ATTACHMENTS ARE COMPLETE AND ACCURA' 
. 1 - / ^ - ^ ^ 
TITLE 
^Sm^Me^U. 
SAMPLES SUBMITTED 
301427 
GENERATORS SIGNATURE 
Polychlorinated Biphenyl (PCB) Warranty 
"• 's disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
^B's are used in this disclaimer to referto anychemical substances and combinations of substan-
ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shall 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
hereby warrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability 
resulting from the breach of this warranty. 
DATED: 
BY:. 
WITNESS:. 
Herbicide/Pesticide Warranty 
ySW^-ZQ C'rtQH(C(H^^^X^^:C• hereby warrants that material transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greaterthan 0.001% when measured in each containerorvessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. J ^ L / W V > CHQ^AVC/^ CO ~«CC. 
o...o:yyn 
,.. ^^L.irUrrl 
wiTNF«;s 
/ y ^ . i < y ^ y k y / j ^ ^ 
Aluminum and Reactive Metal Warranty 
I L ^ L N J O rt^GtVj^f? Q2i.1Z\AX 
hereby warrants that material offered to S&W Waste, Inc. 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless 
^rom any costs, damages, or other liability resulting from breach of this warranty. _ ,^ 
^ 
/
a 
:c:^LAjo-^ (;^^g^^(;^ <J5 rKiC 
DATED: 
; 
BY:. 
WITNESS: 
/ y ^ / ^ ^ - A k y k Z ^ y y 
^ 
t y 
301428 
TABLE 1.2 
30870-0705 
E2TVIR0 SCIENCES 
Sample Identification: ALAS 64867 
PCB Isomer 
. Result • rif.'S? 
FC3 1016 
PCB 1221 
PCB 1232 
PCB 1242 
PCB 124S 
PCB 1254 
PCB 1260 
1.0 
1.0 
1.0 
1.0 
1.0 
1.0 
1.0 
301429 
YWC. INC. • 200 Monroe Turnpike • Monroe, Connecticut 06468 • (203) 261-4458 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Cercified Drinking Wacer.'Vascevace: 
Laboracory IDi* 141L6 
REPORT DATE: April 14, 1986 
LAB il 52954 
1152 .lOUTt 10. R;>NOOLPH. NCtV llRSey Q78£: 
:Ql-5a4.0330 
CLIENT: ENVIRO SCIENCES - Island Chenical Proiecc 
SA^[?LE SOURCE: SamDle in 
SA>f?LE D.-i.TE: Februarv.28, 19 = 5 T.-.KEN 3Y: .-i.. KvLes .J.T L.^3 DATE: March 
LA30R.iT0RY ANALYSIS 
REPORT 
P.A-RA-METER 
Ignicabilliy -
Specific Grav: 
pH(uniC3) 
RESULT 
ISS wichouc persis; 
21.97 
8f06 
If you should have any quescions, please do noc hesicace co call. 
INDUSTRIAL CORROSION MANAGE^IE:rr, INC. 
lichard S. /Le^J^ne 
Presidenc/ 
RSL:dlh 
301430 
/ l y t i i ' f / ' i ' 
••.•••• PRIORITY POLLUTANT VOLATILE ORGANIC ANALYSIS '— 
f.'^ 
J 
I 
LABORATORY ID /14116 
••"•' 
••••'-
' 
• 
• 
LAB # 52955 
" - 
" " ' " 
M 
CLIENT: E N V I R O '^rT-vrES - I^I.T^H r>.o,. 
SAMPLE SOURCE Sa~ple ^2 
- 
•-' 
GC/MS Method 624* 
Tier II Deliverables 
PARAMETER 
Chloromethane 
Bromomethane 
Vinyl Chloride 
--"-"- 
'• 
— 
Chloroethane 
Methylene Chloride 
1,1-Dichloroethene 
1 ,1-Dichloroethane 
Trans-1,2-Dichloroethene 
Chloroform 
1 ,2-Dichloroethane 
1 ,1 ,1-Trichloroethane 
Carbon Tetrachloride 
Bromodichloromethane 
1 ,2-Oichloropropane 
- -
Trans-1,3-Dichloropropene 
Trichloroethene 
: 
; — — 
Dibromochloromethane 
1,1,2-Trichloroethane 
Benzene 
cis-V,3-Dichloropropene 
2-Chloroethylvinyl ether 
Bromoform 
Tetrachl oroethene 
1,1,2 ,2-Tetrachloroethane 
Toluene 
Chlorobenzene 
Ethyl benzene 
Total Xylenes 
*Dichlorobenzenes noc analyzed under this method. Analyzed by GC/MS Method 625, 
RESULT 
ug/kg 
u 
u 
u 
u 
7.SB 
U 
U 
U 
U 
u 
u 
u 
U 
u 
U 
U 
u 
3. OB 
U 
U 
U 
U 
U 
U 
U 
u 
1.295 
HETriOD 
BLANK 
ug/kg 
IT 
u 
u 
7.5 J 
U 
u 
u 
7. 8J 
U 
U 
U 
U 
u 
u 
u 
u 
u 
2.0J 
u 
u 
u 
u ' 
u 
t.9J 
U 
U 
U 
MDL 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
301431 
/ic^<^ 6t/-^7 
• 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Certified Drinking Vacer/Vastevace: 
Laboracory ID^ 14116 
REPORT DATE: April 16. 1966 
LAS S 52955 
1152 ROUTE 10. RANOOLPH. NEW JERSEY 07863 
201-584.0330 
CLIENT: ENVIRO SCIENCES - Island Cheaical Proiect 
SAiMPLE SOURCE: Samole HI 
SAMPLE DATE: Februarv 28, 1986 TAKEN BY: A. Kvles AT LAB DATE: March 7, 155: 
LABORATORY ANALYSIS 
REPORT 
P.ARAMETER 
Z Paraphenetidene 
RESULT 
None Found 
FINDINGS: Seac benzophenone 
If you should have any questions, please do not hesicace to call. 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
Rfchard S 
President 
RSL:dlh 
/qcy ^^f^-(''7 
301432 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDE? Certified Drinking Vater/Vasteva-a-
Laboracory ID# 14116 
REPORT DATE: April 14, 1986 
LAB i 52955 
1152 ROUTE 10. RANOOLPH. NEW JERSEY 07563 
201-584.0330 
CLIENT: ENVIRO SCIENCES - Island Cheaical Proiect 
SAMPLE SOURCE: Sample 02 
SA.MPLE DATE: Februarv 28.--1986 TA-KEN BY: A. Kvles AT LAB DATE: March 7, 19S5 
LABORATORY ANALYSIS 
REPORT 
PARA.METER 
Ignitability 
Specific Gravity 
pH(units) 
RESULT 
Ignites without persistent burning 
- ' 
32.47 
7.38 
If you should have any quescions, please do noc hesitate to call. 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
RSL:dlh 
Presidenc 
y ^ C A ^ i i - f f i y -. 
301433 
S&W 
WASTE, INC. 
115 JACOBUS AVE. . SOUTH KEARNY. N.J. 07032. 
(201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
APO^OVAL 
CODS 
TECHNICIAL 
REP. INITIALS 
\. 
GENERAL INFOmwiATION 
C^"?])^^'! 
GENERATOR M A U C 
- Z - ^ ? ^ ^ 
C r T . y n ' K A / , d ) k
j y . \ 
l " " 
•-) 
GENERATOR EPA I.D. N n k / Z 9 / ^ T r c ? ' . 
. p n c r Q . ; 
2 s c Z ' < ^ ^ - ^ ^ ( T U y ^ r / T S x ^ J / ^ 
J r " C y ^ ^ : , 
C / J V / 
u^ACTPNiAMP 
AZka<>u/fuy..~ 
AyysJTZ:, /y&cy^c ' A I A ^ 
t:^or2.o 
TITLE __ / P 
PHONF ^C//:£6-GZZ 
PROCESS GENERATING WASTE. 
yye*-*^£-^ 
B. PHYSICAL CHARACTERISTICS OF WASTE 
PHYSICAL STATE @ 70'Fj 
3 SOLID 
^ L I Q U I D 
| 
C SEMI-SOLID G POWDER 
% LIOUID 
<><JH20 
ODOR 
/ c i y i a * . m j t ^ 
COLOR 
y < j i 
pg'ORGANlC 
] 3 INORGANIC 
n CHLORINATED 
ORGANIC 
BTU VALUE PER G A L . 
c y ^ y : y t f * ^ r * i 
«b CL _ 
BS«W_ 
" B A S H . 
9i>S. 
LAYERS 
Q MULTI LAYERED 
G BI-LAYERED 
" ^ S I N G L E PHASED 
TOC, 
COD. 
ifc SOLIDS 
y y r y y - c 
pH: 
CO-2 
D 7.1-10 
C 2.1-4 
D 10.1-12.5 
0 4.1-6.9 0 1 2 . 5 
C 7 
D EXACT _ 
D N/A 
^z2Z. 
SPECIFIC 
GRAVITY 
D < J 
C.8-.9 
C .9-.95 
D.95-1.0 
D 1.0-1.1 
O 1.1-1.24 
D 1^5-1.4 
D li-1.7 
0 > 1 . 7 
D EXACT_ y-ce' 
• FLASH 
D < 9 0 
C POINT 
• <100 
G f F ) 
C 100-140 
G CC 
D 140-200 
D O C 
G EXACT: 
. • g . < 2 0 Q p 
T v r 
yiSCOSmr (Ceniicxjise) 
^ 1 - 1 0 0 
C 10O-100O 
C 1000-10000 
. Oiaooo 
c EXACT 
CHEMICAL COMPOSITION (MUSTTOTAL 100%) % 
/ S c ^ y ^ u ^ I y ^ e 7 ? y ^ ^ e y y y v c , 
^ J ^ 
t7 
y / , i y / 
D y y * f f ; 7 r / < L . 
/ c z y / j y f - c ^ 
^ O - v e ^ / 
D. METALS 
C TOTAL 
yyA 
As 
Ba 
r.fl 
Cr 
r.u 
y / f i 
yyA 
y y A 
y / A 
y / A 
DEPTOX 
Hg 
y y A 
Nil 
y y / : 
Ph 
^
^ 
SP 
Ayy; 
7n 
y y A 
Te. 
y / / ^ 
- / - r -
F. HAZARDOUS CHARACTERISTICS: 
TOXICITY RATINGS 
INHALATION 
DERMAL 
ORAL • 
O EXPLOSIVE 
D WATER REACTIVE 
D MSDS ATTACHED 
NFPA RATING 
y ^ c y y ^ 
• 
PYROPHORIC 
D SHOCK SENSITIVE 
G. MANIFEST INFORMATION 
. 
PROPER D O T S H I P P I N G NAMP 
A A i i y u , / e t x / 
/ ' y y - J T ^ / C y f T e y / ' i y y ^ f 
DOT HAZARD C L A S S . 
UN/NA NO. 
y / y ^ 
O/Cy^e 
9yf? 
EPA/STATE WASTE TYPE 
EPA/STATE HAZARD CODE. 
AA2.Za 
y 
H. SHIPPING INFORMATION 
D BULK LIQUID 
DBULKSOLID ' ^ D R U M S 
D OTHER. 
SHIPPING FREQUENCY: 
QUANTITY 
/ _ 
PER jr>«ct— 
OTHFR 
Ai/A 
E. OTHER COMPONENTS 
n PCB'S* 
n 
PP=;Tir.inF';/HPPRirinF.'?» 
a CYANIDE OR CYANIDE PRODUCING. 
D SULFIDE OR SULFIDE PRODUCING 
n 
PHFNni in.<? 
n 
RAniOArrivF 
n 
iNFPCTir)u.<i 
n Fl FMFNTAI MFTAl 5?* 
n 
OTHFR . 
yJA 
y j A 
y y / : 
y/A 
y / A 
yyA 
y / A 
y/A 
y A 
•ATTACHED DISCLAIMERS MUST BE SIGNED 
I. SPECIALHANDUNG INFORMATION/COMMENTS: 
I HEHEBV CERTIFY THAT ALL INFORMATION SUBMITTED ABOVE AND AU. A 
ARE REPRESENTATIVE OF THE WASTE. 
3-/0_<i-7 
DATE 
ARE COMPLETE AND ACCURATE. AND 
cy€.y 
TITLE 
GENERATORS SIGNATURE 
SUBMITTED 
301434 
# 
Polychlorinated Biphenyl (PCB) Warranty 
"^his disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
JB's are used in this disclaimer to referto anychemical substances and combinations of substan-
ces that contah 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shall 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc to receive PCB's, Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
hereby warrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability 
resulting from the breach of this warranty. 
DATED: 
BY: 
WITNESS: 
Herbicide/Pesticide Warranty 
XSvPn^'^ cw^f^^c^r^ CC\ ITi^hprehy warrants that material transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greater than 0.001 % when measured in each container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc harmless from any costs, damages or 
other liability resulting from the breach of this warranty. Zil^\^f\tZi'i> C HH$I"Ai r/?rL ce). ITkOc. 
HATPn- 3 - ^ l - F f 
RY- \ ^ ( / y , . ,~k CUgVv^' 
• 
y y y y 
WITNESS: 
,zZ%-^.^yzZjy 
A 
Aluminum and Reactive Metal Warranty 
TSl^^tvv^ LAAy^\^J\\ c^ ; X K I C I 
hereby warrants that material offered to S&W Waste, Inc. 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless 
from any costs, damages, or other liability resulting from breach of this warranty. 
3-31-H 
,, yzAxCkv^ 
WITNESS: 
301435 
^ 
-
• 
w 
TASLE 
1.1 
30870-0705 
EJTTISOSCIENCSS 
Sample I d e n t i f i c a t i o n : 
MARS 64981 
PC3 I s o m e r 
R e s u l t . 
-^i^/L 
PCB 1016 
<0.20 
?C3 1221 
<0.20 
PCB 1232 
. <0.2Q 
PCB 1242. 
. 
«0.20 
PCB 1248 
<0.20 
PCB 1254 
<0.20 
PCB 1260 
<0.20 
301436 
YWC INC • 200 Monroe Turnpike • Monroe. Connecticut 06468 • (203) 261-^^3 
INDUSTRIAL 
^ ^ ^ ^ certified Drinking Wacer/Vascevace-
^ ^ ^ _ 
, ^ 
Laboracory JUtf K116 
CORROSION 
MANAGEMENT 
"^'^^^ DATE: Aoni K . 1986 
INCORPORATED 
LAS ^ 52959 
1152 ROUTE 10. RANDOLPH. NEW JERSEY 07S53 
201-53*^330 
CLIENT: ENVIRO SCIENCES - Island Cheaical Proiect 
SAMPLE SOURCE: Samole #6 
SA.^?LE DATE: Februarv ^S. 1986 TAKEN 3Y: A. Kvles AT LAB DATE: March 7, 19£6 
LABORATORY ANALYSIS 
REPORT 
PARA-^IIR 
RESULT 
Paraphenetidene 
~ Not Present 
Findings: 
chloroaethyl benzene 
benzene nechananuime, n,n-dimethyl 
If you should have any quescions, please do noc hesicace co call. 
DTDUSTRIAL CORROSION M.\NAGZXENT, I^'C. 
Richards. Livr^e 
Presidenc / 
^/ik^"-^ 
RSL:dlh 
.-/^^n 
3 01437 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROUTE 10. RANDOLPH. NEW JERSEY 07SS3 
201-58i-0230 
NJDE? Certified Drinking Water/Wastevat. 
Laboracory ID? 14116 
REPORT DATE: April U . 1986 
LAB S 52959 
CLIENT: ENVIRO SCIENCES - Island Chenical Proiect 
SAMPLE SOURCE: Samnle US 
SA.MPLE DATE: Februarv iS,..1986 TAKEN BY: A. KvLes AT LAB DATE: March 7, I9E6 
LABORATORY ANALYSIS 
REPORT 
PARAMETER 
RESULT 
m 
. Flashpoint 
gT'C boiled 3 97'C 
Specific Gravicy 
1.0809 
pH (units) 
— 
6:71 
If you should have any quescions, please do not hesicace Co call. 
INDUSIXIAL CORROSION MANAGEMENT. INC. 
y^ 
RSL:dlh 
301438 
y ^ y y t T ^ t Z y T / 
S & W WASTE, IN 
CODE 
1 5 JACOBUS AVE. . SOUTH KEARNY. N.J. 07032. (201) 344-4004| 
TECHMCIAL 
GENERATORS WASTE MATERIAL PROFILE SHEET 
"^^'^'^'^^^ 
GENERAL INFORMATION 
/ l ^ ^ ^ - 7 4 ^ 7 
GENERATOR NAMP 
yAh--?^/) Cy/^y?f/c:^ 
Cy k : ^ y . 
/ . , / , ( ] 
GENERATOR EPA LD. NO. / y ^ ^foes'yo^r-
^^^, ^ . . y 
. /I yzz. zkkzz. ^ 
ADDRESS. 
<A^Z^.^./Zy/ys/yzy^jrc/:. Jr- Ckk'^ 
0(Z\T ^ o / ^ 
TECHNICIAL rnvTArT 
/ ^ ^ / Z y c U t - / ^ ^ r / y / t y i J : ^ ^ ] 
TITLE. 
y / 
PHONE j ^ £ v ^ £ £ - i Z . r ; ^ 
.'ASTE NAME. 
PROCESS GENERATING WASTE . 
y / c 
'(T^/C-
B. PHYSICAL CHARACTERISTICS QF WASTE 
LAYERS 
y A ^ 
C MULTI LAYERED 
Q BI-LAYERED 
D SINGLE PHASED 
=HYSICAL STATE @ 70'F 
sfSOLIO 
C LIQUID 
Z SEMI-SOLID G POWDER 
^ LIOUID 
5«H20 
ODOR 
y y o y i y t ^ " 
Z ORGANIC 
JClNORGANIC 
COLOR 
y y A 
: CHLORINATED 
ORGANIC 
BTU VALUE PER GAL 
V Cl 
y y A 
^ % 
R?J.VJ 
<feASH 
yZAZ 
TOC. 
COD. 
% SOLIDS. 
DH: 
0 0-2 
C 7.1-10 
C i 1 - 4 
C 10.1-12.5 
C 4.1-6.9 
0 1 2 . 5 
D 7 
a EXACT _ 
> N/A 
SPECIFIC 
GRAvmr 
c.a-.9 
C .9-.9S 
C.95-1.0 
D 1.>1.1 
C 1.1-1.24 
S . 1.25-1.4 
C l i - 1 . 7 
C>1.7 
• 
EXACT. 
a FLASH 
O POINT 
DCF) 
DCC 
C O C 
CEXACT. 
n<90 
o <100 
Q 100-140 
C 140-200 
VlSCOSiTY (CenliDOise) 
C 1-100 
D 100-1000 
G 1000-10000 
D > 10.000 
y y A -
C EXACT _ r Z ^ 
% 
CHEMICALCOMPOSmON (MUSTTOTAL 100%) % 
A ^ r r L . mheyiyyf yZ/A/cer y<<Ltni^AA 
7 o 
y^^:^^<.ga^fr^<L^ 
S O 
o.cyxy 
F. HAZARDOUS CHARACTERISTICS: 
TOXICITY RATINGS 
INHALATION 
DERMAL 
ORAL 
C EXPLOSIVE 
a WATER REACTIVE 
D MSDS ATTACHED 
NFPA RATING 
y/(>u^ 
D PYROPHORIC 
a 
SHOCK SENSITIVE 
D, 
Ag 
As 
Ba 
Cd 
Cr 
Cu 
O T H E R . 
METALj^ 
C TOTAL 
vW 
y A 
XML 
y y ^ 
y/A 
DEPTOX 
Hg 
Ni 
Pb 
Se 
Zn 
Te 
y . « 
ZZA^ 
yC*±_ 
y/y: 
y/A 
y y 
G. MANIFEST INFORMATION 
y _t 
/ 
• 
PROPCRDnT.«;HippiNiRNAMFyi^^>i.iyA> /yAy^/i- 
J ^ ' A y / c L 
DOT HA2ARD CLASS 
€ A A ' - ^ 
UN/NA NO. 
y ^ A f 
9 y J ' 9 
EPA/STATE WASTE TYPE 
EPA/'STATE HAZARD C O D E . 
. ^ 2 2 ^ 
H. SHIPPING INFORMATION 
C BULK LIOUID 
C B U L K S O L I D 
^ 
DRUMS 
SHIPPING FREQUENCY: 
QUANTITY 
y7A'ZyZL €>// 
/ 
COTHER. 
PER. g r ^ - g ^ 
E. 
D 
C • 
a 
n 
c 
D 
n 
D 
OTHER COMPONENTS 
PCB'S* 
y / / 
PESTICIDES/HERBICIDES' 
y ^ ^ 
cyANioe OR CYANIDE PRODUCING 
y / A 
SULFIDE OR SULFIDE PRonnCiNn 
yJiC 
PHENOLICS 
y-'A 
RADIOACTIVE. 
INFECTIOUS _ 
y/A 
y.'A 
ELEMENTAL M E T A L S * . 
O T H E R . 
y/A 
•*TTACHED DISCLAIMERS MUST BE SIGNED 
yZA_ 
y 
I. SPECIALHANDUNG INFORMATION/COMMENTS: 
yj/^'fCc,: /Z^c/SZZ, /k^ccaeZ, 2)^M^y^y<cy 
^ ^ ^ • f ^ 
^ ^ - ^ 
yCiyiC^y<L y2y.y;A.,y:r^y y Z Z y Z ^ 
l 7 ^ 'y^y.^Xy^<Z 
ZZ^Z/^'AI^T^, 
^ 
yitii 
I HEBESY CERTIFY THAT ALL INFORMATION SUBMITTED ABOVE AN^ 
ARE REPRESEhTTATIVE OF THE WASTE. 
DATE 
TTACMMENTS ARE COMPLETE ANO ACCURATE, A N D T H A V A L L SAMPLES SUBMITTED 
kZ^t ,Z 
^^<t 
301439 
TITLE 
GENERATOR'S SIGNATURE 
Polychlorinated Biphenyl (PCB) Warranty 
•^'-'is disclaimer is to ail persons who generate and dispose of chemical waste. The terms PCB and 
>B's are used in this disclaimer to refer to any chemical substances and combinations of substan-
ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shali 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
I_S>LfVJT^ r VrQNA(.(l^ CohPrPhy warrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or^ther liability 
resulting from the breach of this warranty. 
' X ^ L ^ ' Z O 
Ctt^f^^rTL. C o -HNC^ 
DATED: ^-(i-y 
. 
^.^.Ckak 
WITNESS 
Herbicide/Pesticide Warranty 
X S L \ ^ 0 i i k ^ ' M d ' ^ (L^l^^ffirPhy warrants that material transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greater than 0.001 % when measured in each container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmlessfrom any costs, damages or 
other liability resulting from the breach of this warranty. JTS t f-rAJZ) C f p ^ C l ^ L CO. ZZ.^^ 
DATED: _ . 5 l l h l 3 _ _ _ 
— 
RY- ^ I.LpJ^^- , 1 
e ^ ^ S ^ 
^ ^ i r c / 
. . y 
WITNESS: yZy^^iiy^A^ X T 'Z^yC 
Aluminum and Reactive Metal Warranty 
T S l f l \ ] r ) r , H t M / C f a _ 
C J ^ 
TVVJC. hereby warrants that material offered to S&W Waste, Inc. 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless 
*-om any costs, damages, ot other liability resulting from breach of this warranty, 
r.^ 
^_ 
1-^^ 
• • BY: "S . ClllLrw-1 \e.f.Ml--V 
DATED: 
--^ 
_ 
WITNESS: 
301440 
1 15 JACOBUS AVE. . 
SOUTH KEARNY, N.J. 0 7 0 3 2 . 
(201) 344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
CODE 
TECHNICIAL 
REP. INITIALS 
\ . GENERAL INFORMATION 
k^lA} 
^"^0-^7 
GENERATOR NAME -ASCC^c C ^ ^ ^ ^ t ^ c Z ^ o . ( \ f U ,i . i ^ - r J 
GENERATOR EPA LD. NO./^i:^ 
'PA^S'yp^ 
ADDRESS 
^ ° A : '^<^y^S, 
ZZyyy^yyrySfy.f/ZD . J r . CygZy.^, C/SiZZ OcfJLts 
TITLE 
/ y ^ 
PHONF ^y<Ty.^C-<^zS7k 
TECHNICIAL rnNTAr.T 
y Z ^ y y 
'^Z. A Z U S J J z ' ^ y y f i x } - k / i ^ e t k l 
WASTE NAME 
y ^ ^ ^ y j ^ y ^ ^ y ^ y:yy^^^ZZ yZyaeyy/p 
PROCESS GENERATING WASTE . • ^ 
A^Ttzy^A 
ZZAy,^....rojA.., ^ > ^ € i . yZgy^ A^trc3^..m^Zi~ 
J ^ ^ 
y^rTc 
B. PHYSICAL C H A R A C T E R I S T I C S OF W A S T E 
y7c>cyyy.o ZZ. 
• y ^ c i i r ^ y ^ y k 
PHYSICAL STATE @ 70"F 
D SOLID 
C LIOUID 
C SEMI-SOLID C POWDER 
% LIQUID 
% H20 
ODOR 
COLOR 
• ORGANIC 
• INORGANIC 
C CHLORINATED 
ORGANIC 
BTU VALUE PER GA1_. 
% CL_ 
BS«W_ 
%ASH. 
% S . 
LAYERS 
• MULTI LAYERED 
• 
BI-LAYERED 
Q SINGLE PHASED 
I »«i SCLICS . 
TOC. 
COD. 
pH: 
DO-2 
G 7.1-10 
C N/A 
C 2.1-4 
m 0 . 1 - 1 Z 5 
C 4.1-6.9 
0 1 2 . 5 
C 7 
D EXACT 
SPECIFIC 
GRAVITY 
G < J . 
G .8-.9 
G .9-.95 
C.95-1.0 
C 1.0-1.1 
D 1.1-1.24 
a 1.25-1.4 
a 1.5-1.7 
a > i . 7 
D EXACT. 
G FLASH 
D POINT 
GCF) 
GCC 
GOO 
OEXACT. 
Q <90 
C <100 
0 100-140 
D 140-200 
G < 2 0 0 
VISCOSITY (CentiDoise 
G 1-100 
G 100-1000 
G 1000-10000 
O 1 0 . 0 0 0 
C EXACT 
C. C H E M I C A L C O M P O ^ I O N ( M U S T T O T A L 100%) 
% 
D. 
Ag. 
As. 
Ba. 
Cd. 
Cr. 
Cu. 
METALS 
yyy 
n TOTAL 
yyA 
y y y ; 
~yz;y 
yyy; 
y y y 
GEPTOX 
H g . 
y < ^ ^ 
Ni_ 
Pt>, 
sg 
y^yy 
7n 
y < / / r 
• Te 
y , ' A 
y A T 
OTHER. 
Al/L 
E. OTHER COMPONENTS 
y / / P 
a PCB'S* 
D 
D 
D 
D 
D 
a 
a 
D OTHER 
y^'A 
PESTICIDES/HERBICIDES* 
. 
CYANIDE OR CYANIDE PRODUCING. 
SULFIDE OR SULFIDE PRODUCING, 
PHENOLICS 
RADIOACTIVE 
INFECTIOUS 
y/. 
~yZ7S 
ELEMENTAL METALS*_ 
OTHER. 
y ^ 
•ATTACHED DISCLAIMERS MUST BE SIGNED 
F. HAZARDOUS C H A R A C T E R I S T I C S : 
TOXICITY RATINGS 
— 
y , 
NFPA RATING 
INHALATION 
«i<iC 
y^'TT^aetetC 
DERMAL 
2 > ^ y ^ y y h f r 
. 
ORAL 
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D PYROPHORIC 
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D MSDS ATTACHED 
G. M A N I F E S T I N F O R M A T I O N 
. 
PROPER DOT SHIPPING NAME 
Ayf;-z::yU,^^e^ y/yZrATt yZ-cc: 
DOT HAZARD CLASS. 
UN/NA NO 
y > ^ y ? y y ^ y € / J r y . y > j r A 
Ay:yyy:A-C' rSr:^ y/yjA 
EPA/STATE WASTE TYPE 
jAy^JypyiC 
J
^ yZy's. 
EPA/STATO-I lAZARD CODE 
iyy<y<^<ft£j:/'Js^^ 
y/^rlZ] 1 
H. SHIPPING INFORMATION A-7AAtZrccc a.A/. 
C BULK LIQUID 
DBULKSOLID 
X DRUMS 
MOTHER 
SHIPPING FREQUENCY: 
QUANTITY 
^
9 
P F P f*>*c, 
I. S P E C I A L H A N D L I N G I N F O R M A T I O N / C O M M E N T S : 
^ ^ / O g / ' g c y 
y ^ , y , ' ^ 
6<yy77y y^/sayzA**/^ 
C' ^ 
J . 
I HEREBY CERTirr THAT ALL INFORMATION SUBMITTED ABOVE AND ALL ATTACHMENTS ARE COMPLETE ANO ACCURATE. ANO THAT ALL SAMPLES SUBMITTED 
ARE REPflESENTATlVE OF THE WASTE. 
DATE 
TITLE' 
" 
GENERATOR'S SIGNATUR 
301441 
Poiychiorinated Biphenyl (PCB) Warranty 
""^is disclaimer is to all persons who generate and dispose df chemical waste. The terms PCB and 
JB's are used in this disclaimerto referto any chemical substances and combinations of substan-
ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct 
in a process which contains less than 50 ppm PCB because of any dilution; again, these lattershall 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc to receive PCB's. Any generator and/or transporter who 
knowingly or wiiirully ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
J , 5 L f i r A j ^ Ctf^CcfT^C-c^^Vphy warrants that materials transferred by it to S&W Waste. Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc harmless_from any costs, damages or other liability 
resulting from the breach of this warranty. 
4 ^ ^ L r r < ^ ^ 
Cfr=#Tvi(c^r\ (Lo . X J c 
DATED:. ^-"-^7 
Br-.^^Rykd^y^ 
WITNESS:. /
^
^
J
y
^
y
^
^ 
T 
Warranty 
[TStt^rr^o^ C t t P ^ C ^ ^ Cl^TiPrfihy wan-ants that material transferred by it to S&W Waste, Inc 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greater than 0.001% when measured in each containerorvessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc harmless fromjgny costs, damages or 
other liability resulting from the breach of this warranty. X ^ C A ^ ^ 
C t t V ^ ^ ^ ^ H - ^ 
-'^^ < 
DATED: _ 3 _ : i b £ I 
RY- l
^ 
/ 
W l o ^ V - ^ , 
" ^ . ^ y ^ j - ^ ^ y ^ 
y 
WITNESS: 
-
• 
Aluminurn and Reactive Metal Warranty 
T^StfVKjT^ f f - H ^ a r / ^ 
0 5 h J^K^rehv warrants that material offered to S&W Waste, Inc 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless 
'•"om any costs, damages, or other liability resulting from breach of this warranty. 
_ 
^ , 
^ 
A 
DATED: 
WITNESS:. 
'^ ^ ty 
301442 
AZ^^^z^y^ 
S & W WASTE, INC. 
115 JACOBUS AVE. . 
SOUTH KEARNY. N.J. 07032. 
(201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
-
• 
TV-
A P o q o v A L 
C O D E 
TECHNICIAL 
REP. INITIALS 
. GENERAL INFORMATION 
i j A ^ ' ^ - / Q ^ ^ f j 
GENERATOR NAMC 
. Z s z ^ ' y ^ 
kl/</ynyCS<, d s k ^ 
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GENERATOR EPA I.D. NO. ^^<^ ?A-^ryeCr~ 
TPrHNiriAi r.nNTArT 
/•^r>? A - A^Zyg^ AkZfyfy-a J c u t ^ o i j ) 
VASTE NAME 
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j y / y y T e Z 
J p y / / 
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T I T L E . 
y y 
9H0U^'iZZ//l^JLZ^^^ 
PROCESS GENERATING WASTE 
AAr-yryyi!>u/yy 
B. PHYSICAL CHARACTERISTICS OF WASTE 
PHYSICAL STATE @ TOTj ° ° ° " y?/yCy:i . 
XSOLIO 
C LIQUID 
I 
/ Z ^ C y C 
~ SEMI-SOLID a POWDER 
"A^ ORGANIC 
I 
J ~ INORGANIC 
% LIQUID 
«b H20 
COLOR 
2<:2c 
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ORGANIC 
STU VALUE PER GAI 
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y / A 
p H : 
2 0-2 
C 2.1-<» 
C 4.1-6.9 
G 7 
G 7.1-10 
C 10.1-12.5 
0 1 2 . 5 
G EXACT _ 
G N/A 
<r.Sf 
SPECIFIC 
GRAVITY 
G ca 
G .8-.9 
C .9-.95 
G.95-1.0 
G 1.0-1.1 
G 1.1-1.24 
G 1.25-1.4 
a l i - 1 . 7 
C >1.7 
G EXACT. ^^.^7 
G FLASH 
G POINT 
GCn 
GCC 
G O C 
G EXACT. 
D <90 
O <100 
G 100-140 
C 14O-20O 
S > 2 0 0 
VISCOSITY (Centiooise 
G 1-100 
G 100-1000 
G 1000-10000 
G > 10.000 
G EXACT_ 
/ V A 
CHEMICAL COMPOSITION (MUSTTOTAL 100%) % 
y Z / ^ ^ ^ y r zZy 
-y:y:yA^iey J A S-Zry,^/) 
F. HAZARDOUS CHARACTERISTICS: 
TOXICITY RATINGS 
INHALATION 
D E R M A L 
ORAL 
C 
EXPLOSIVE 
G 
WATER REACTIVE 
G 
MSDS ATTACHED 
y A 
NFPA RATING 
D 
PYROPHORIC 
C 
S H O C K SENSITIVE 
D. 
M E T A L S 
C TOTAL 
Ag 
y.'A 
A.. 
y / / : 
Ra 
yy/t 
Cd 
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Cr 
y/A 
Cu 
y/zZL. 
O T H E R . 
A Z ^ 
D EP TOX 
Hg 
A/A 
Nii 
y y A 
Ph 
y</AZ 
.<;«. 
yJ/'A 
7n 
y / A 
Te 
yZAZ 
G. MANIFEST INFORMATION 
PROPER DOT SHIPPING NAME y^Tt^ty:*^. C^A'r<Ai. f y . A yV^-, 
DOT HAZARD CLASS 
y P A y f - ^ " 
UN/NA NO. 
y J A ^ 9 y ( Z ^ 
^ 
EPA/STATE WASTE TYPE 
cy.^S'^ 
EPA/STATE HAZARD CODE 
^ » ^ ~ - ~ ^ 
/ 
H. SHIPPING INFORMATION 
G B U L K L I Q U I D 
C B U L K S O L I D 
X ^ D R U M S 
" O T H E R . 
SHIPPING FREQUENCY: 
QUANTITY 
/ 
P E R . tzyr-y,. 
E. OTHER COMPONENTS 
n 
PCR-s* 
n 
PF.<;TiciOES/HFnRi'~iOP'^ 
G CYANIDE OR CYANIDE PRODUCING 
a 
SULFIDE OR SULFIDE PRODUCING 
n 
PHFNOLICS 
a 
RADIOACTIVF 
n 
INPFCTIOUS 
n 
ELPMFNTAI WFTAI ??• 
G 
O T H P H 
•ATTACHED OISCLAJMEBS MUST BE SIGNED 
y y y 
y y y 
y y y 
y / y ; 
y y y 
y/A 
y y y 
yyy; 
y/yj 
I. SPECIAL HANDLING INFORMATION/COMMENTS: 
y ^ ? . ^ 
/2y*y^ /:AZtyy^ ykyiA/y*/^ 
^yyAAyf 
I MEBEBY CESTIFY THAT ALL INFORMATION 
ABE SEPRESENTATIVE OP THE WASTE. 
BMITTED ABOVE ANO ALC ATTACHMENTS APE COMPLETE ANO ACCURAT 
DXTE 
fntE 
/ye. M : 
NO THAT Ajfl. SAMPLES SUBMITTED 
301443 
GENERATOR'S SIGNATURE 
TABLE 1.2 
30870-0705 
ENVIROSCIENCSS 
Sainple Identification: ALAE 64867 
PCB Isomer 
P.es'clt. rsv-^Kg 
PCS 1016 
<1.0 
PCB 1221 
<1.0 
PCB 1232 
<1.0 
PCB 1242 
- 
ci.O 
PCB 1248 
<1.0 
PCB 1254 
<1.0 
PCS 1260 
<i.O 
301444 
YWC. INC. • 200 Monroe Turr.pike • Monroe. Connecticut 06468 • (203) 261-4^53 
PRIORITY POLLUTANT VOLATILE ORGANIC ANALYSIS T^--
LABORATORY ID #14116 
~ ' —• 
' " 
LAB # 52955 
' 
""""" 
""' 
CLIENT: ENVTRO SCT^MP^C - 1,1^.^^ r:-. 
SAMPLE SOURCE 
Sami^l^ •?? 
' 
• 2 ~ -. • 
GC/MS Method 624* 
Tier I I Deliverables 
PARAMETER 
Chloromethane 
Bromomethane 
Vinyl Chloride 
1 - . . - 
— 
Chloroethane 
Methylene Chloride 
1 .l-Oichloroethene 
1 ,1-Dichloroethane 
Trans-1 ,2-Dichloroethene 
Chloroform 
1 ,2-Dichloroethane 
1 ,1 ,1-Trichloroethane 
Carbon Tetrachloride 
Bromodichloromethane 
1 ,2-Oichloropropane 
' 
Trans-l,3-Dichloropropene 
Trichloroethene 
Di bromochloromethane 
1,1 ,2-Trichloroethane 
Benzene 
cis-T,3-Dichloropropene 
2-Chloroethylvinyl ether 
Bromoform 
Tetrachloroethene 
1,1 ,2 ,2-Tetrachloroethane 
Toluene 
Chlorobenzene 
Ethyl benzene 
Total Xylenes 
*Dichlorobenzenes noc analyzed under chis mechod. 
RESULT 
ug/kg 
u 
u 
tJ 
u 
7.83 
U 
U 
U 
U 
U 
u 
u 
u 
u 
u 
u 
u . 
3. OB 
U 
U 
U 
U 
U 
U 
U 
U 
1.295 
METHOD 
BLANK 
ug/kg 
u 
u 
u 
u 
" . 5 J 
u 
u 
u 
7 . 3 J 
U 
u 
;j 
!j 
IJ. 
U 
u 
u 
u 
2.0 J 
U 
U 
u 
U " 
u 
4.9 J 
U 
U 
U 
MDL 
10 
; n 
: r\ 
. 
-.1 
LO 
10 
LO 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
..- iO 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
Analyzed by GC/MS Mechod 625. 
301445 
/ I C M l f t S f S ^ ' / 
Polychlorinated Biphenyl (PCB) Warranty 
r^^is disclaimer is to all persons who generate and dispose of chemical waste. The terms PCS and 
% 3's are used in this disclaimerto referto any chemica! substances and combinations of substan-
ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct 
.n a process which contains less than 50 ppm PCB because of any dilution; again, these lattershali 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
hereby warrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability 
resulting from the breach of this warranty. 
DATED: 
BY:. 
WITNESS:-. 
Herbicide/Pesticide Warranty 
i^3Li^\C> C^C^.{C{Z^f:^i<jZ • hereby warrants that material transferred by it to S&W Waste, Inc 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greater than 0.001 % when measured in each container or vessel transferred to S&W Waste, I nc, 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. XTSLAIMII^ C ^ ^ M U ; / ^ QQ 
~ K C . 
DATED:. 
WITNESS 
Aluminum and Reactive Metal Warranty 
lXLh^Z^r\ravj(^Z? C'2).lyJZ 
hereby warrants that material offered to S&W Waste, Inc 
for transportation, treatment and/or disposal does not contain elemental aiuminum or reactive 
metal paste, powderorpigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless 
*rom any costs, damages, or other liability resulting from breach of this warranty. _ , _ 
X 5 . L ^ ^ ^ 
C V ^ Q ^ I C ^ C J O . , ^ ^ ^ ^ 
DATED: 
•- 
BY; 
\<~r^;r>A-A \ ^ \ \ J A X J 7 \ — 
, 
WITNESS: 
/ ^ ^ y k y j ^ ^ / A L / . . 
. 
y- y c/ 
301446 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
N J H E ? Cercified Drinking Wacar/Wascevace-
Laboracory ID// 14116 
REPORT DATE: April 16, 1986 
LA3.-? 52955 
.1152 ROUTE 10. RANOOLPH. NEW JERSEY 078S9 
201-534.03;0 
CLIENT: ENVIRO SCIENCES - Island Chenical 
P r o i e c c 
SAMPLE SOURCE: Samole ill 
SANIPLE DATE: Febr'jarv 28, 19S5 T.AKEN BY: A. Kvles 
AT LAB DATE: 
March 7, 1? = = 
LABORATORY .ANALYSIS 
REPORT 
P.AR.iMETER 
RESULT 
7. Paraohenacidene 
None Found 
FINDINGS: 
Neac benzophenone 
If you should have any q u e s c i o n s , p l e a s e do noc h e s i c a c e Co c a l l . 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
Ri^chard S. 
1 / e A ^ 
P r e s i d e 
i S. I/e 
inc 
^ 
RSL:dlh 
# 
301447 
y^cy A-6ffC7 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Carcified Drinking Wacer/Wascavaca-
Laboracory IDi* 14116 
RZPORT DATE: April 14, 19S6 
LAB # 52955 
1152 ROUTE 10. RANOOLPH, NEW JERSEY 07865 
201-3a4-03;o 
CLIENT: ENVIRO SCIENCES - I s l a n d Cheaical 
P r o i e c c 
SAMPLE SOURCE: Samnle if2 
SA2-IPLE DATE: Februarv I S . 1935 
T.iJCEN BV: A. KvLes 
.-^T L.AB DATE: March 7, I = :£ 
LABORATORY .ANALYSIS 
.REPORT 
PASAMETEPv 
Ignicabilicy -
Specific Gravi 
pH(unics) 
Ig^i; 
RESULT 
as wichouc persisce 
•?2.4: 
nc Durr.^ng 
7.38 
If. you should have any quescions, please do noc hesicace co call. 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
''Richard S./LeV{ne 
Presidenc/ 
RSL:dlh 
301448 
y9/y£'<£^'f67 
S & W WASTE, INC. 
; 15 JACOBUS AVE. . SOUTH KEARNY, N.J. 07032. 
(201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
APPROVAL 
C O D E 
TECHNICIAL 
REP. INITIALS 
. GENERAL INFORMATION 
C t^'5'll'^i^'^ 
GENERATOR S.AK.P 
- 2 ^ ? ^ ^ 
k!^yf/ycay. (ZZ> k / y A - t ^ = = i ^ - ^ 
/Sc£Z'(^^'^, C^ytTyy!>rjrZ£ 
J f Zy.y<-t^ 
C/JV/ 
OaT2.0 
GENERATOR EPA LD. NO. YiC^^^2^r7C?:r 
A D D R E S S 
T E C H N I C I A L CONTACT 
y
^
^ 
A 
A Z y c y ^ / t k r ^ y y u i 
t J d J ' * ^ ^ ) 
/ASTE N A M E 
Ay^yiyKy/tyy..' 
A ^ y ^ ' Z e ^ 
Aye>t:yfc 
- y / c ^ 
TITLE. 
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P R O C E S S GENERATING WASTE . _yZA 
P H O N E ^ C ' ' / Z 6 
B. PHYSICAL CHARACTERISTICS OF WASTE 
PHYSICAL STATE ® 70'F 
Z SOLID 
^ L I Q U I D 
Z ScMI-SGLID - POwOc.=^ 
% LlOUlO 
\ H20 
ODOR 
/ c ^ y i O i r Z ^ T ' 
{ " ^ ' O R G A N I C 
3 r j VALUE PER G A L . 
£ j y i f / l ^ y * < - ^ 
COLOR 
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£.0 
- INORGANIC 
Z CHLORINATED 
CRGANIC 
^ CL _ 
B S i W . 
»: ASH . 
">>> S 
LAYERS 
C MULTI LAYERED 
a BI-LAYERED 
^ ^ SINGLE PHASED 
>= SOLIDS y y t T C t L -
PH: 
CO-2 
C 7.1-10 
C Z.l-i 
- 10.1-12.5 
C 4.1-6.9 
3>12.5 
G 7 
Z EXACT _ 
C N/A 
^.7/ 
SPECIrIC 
GRAVITY 
Z <.8 
z .a-.9 
~ .3-.95 
r .95-1.0 
Z 1.0-1.1 
C 1.1-1.24 
Z 1.25-1.4 
Z 1.5-1.7 
z EXACT _ _ i l i r i _ 
a FLASH 
G POINT 
GCF) 
CCC 
GOC 
G EXACT 
Vsco; 
^ 1 - 1 
G 10< 
G 10< 
- G.<20q-5 
_ _ 
G>10.' 
D <90 
G <100 
C 10O140 
G 140-200 
OSITYfCentiooisei 
00 
G 100-1000 
G 1000-lOOCO 
000 
XACT 
J >' 
C. CHEMICAL COMPOSITION (MUSTTOTAL 100«r:) % 
y, 
yco/l^yrfiTTrWc. 
/^ti^^^V'x.g. 
^?^ 
/^c*tftj-^.^ , yrre /?y^y^iy^yv<=. 
Ly 
' 
. ^ ^ 
y t y , y / - 
2 > y y * f ' ^ y i — 
y e z z y - y j y f t 
* ^ 0 . i-^^i^/ 
F. HAZARDOUS CHARACTERISTICS: 
rOXICITY RATINGS 
INHALATION 
DERMAL 
ORAL 
N r r A RATING 
yi/<r7y<t 
C 
EXPLOSIVE 
G WATER REACTIVE 
G 
MSDS ATTACHED 
G 
PYROPHORIC 
G 
S H O C K SENSITIVE 
G. MANIFEST INFORMATION 
PROPER DOT SHIPPING NAME 
AAi^^yty./my 
/ y y ^ y C y T c ' f ' i . 
D. METALS 
C TOTAL 
Ag 
A^A 
A . 
A / / : 
Ba 
''yA 
Cd 
A'A 
Cr 
yyA 
c Z 
^AZZ 
G EP TOX 
HQ 
A J A 
Ni 
y / A 
Ph 
y t / A 
Se. 
A/A 
Zn. 
Te. 
DOT HAZARD C L A S S . 
UN/NA NO. 
y A y -
q y y ^ ' e 
9yA? 
EPA/STATE WASTE T Y P E . 
EPA/STATE HAZARD C O D E . 
Ay^ziZa 
y/A 
y y y ; 
H. SHIPPING INFORMATION 
G BULK LIQUID 
C B U L K S O L I D 
' ^ D R U M S 
G OTHER 
SHIPPING FREQUENCY: 
QUANTITY 
/ 
PER J T ^ i i u 
nTHFP 
A / A 
E. OTHER COMPONENTS 
n 
PCR'S* 
r 
pc=;Tir.inp=;/HPPRirinp.s;« 
G CYANIDE OR CYANIDE PRODUCING _ 
a SULFIDE OR SULFIDE PRODUCING 
n 
PHFNni ir.9 
n 
RAninACTivF 
p 
iNFPrTinn.<:; 
n 
Fl FMFNTAI MFTAI f^* 
n 
OTHFR . 
yJA 
y J A 
y / / : 
y / A 
y A 
yyA 
y/y; 
y/A 
y y 
•ATTACHED OlSCLAlWESS MUST BE SIGNED 
I. SPECIALHANDLING INFORMATION/COMMENTS: 
I HEREBY CEBTirr THAT ALL INFORMATION 
SUSWITTEO ABOVE ANO ALL A H A C H M ^ T S 
ARE COMPLETE ANO ACCURATE. AND 
ARE REPRESENTATIVE OF THE WASTE. 
y - \ 
SUBMIT 
3-/0 -'^1 
u 
-yJLyl ULiclL 
DATE 
TITLE 
GENERATOR'S SIGNATURE 
301449 
Polychlorinated Biphenyl (PCB) Warranty 
This disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
\ 3B's are used in this disclaimer to refer to any chemical substances and combinations of substan-
'jes that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shali 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
: 
hereby warrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc. harmless from any costs, damages or other liability 
resulting from the breach of this warranty. 
DATED; 
BY: 
WITNESS:-
Herbicide/Pesticide Warranty 
Cb'v.Pnv'^ C K ^ A i c A ^ CC- j : i ' < hereby warrants that material transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greater than 0.001 % when measured in each container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. X S t P V ^ I ^ C'i^-'$r/\icnrt. ce). ^vOc. 
DATED: T^-^i-r^ 
R v ^ ( ^ . .:iCUi:^Ow-
WITNESS 
Aluminum and Reactive iVietal Warranty 
TSt^^'v^ cHv^vtrr^ r^ , X K \ C , 
hereby warrants that material offered to S&W-Waste, Inc. 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless 
from any costs, damages, or other liability resulting from breach of this warranty. 
3 - B ' - " 
.• ... ^rk\ 
CK 
DATED: 
BY: __ 
WITNESS:. 
301450 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDE? Certified Drinking Vacar/Wastevaca-
Laboratory IDi? 14115 
RZPORT DATE: April 14. 1986 
LAS il 52959 
1152 ROUTE 10. .RANDOLPH. NfW JERSEY 07Se9 
2Ql:a4-0:30 
CIIZNT: ZNVIROSCIENCES - Island Chenical Proiect 
SA>SLE SOURCE: Saiapie =?6 
S.^-LPLZ D.-^TZ: Februarv ^ S . 1936 T-AiCZN 3Y: A. Kvles AT L.\3 DATZ: March :. . r z -
LABORATORY ANALYSIS 
REPORT 
P.AR.iJ>!ZTZ; 
RZSUIT 
ParaDcenetidena 
' 
Xoc Present 
Findings: 
chloronethyl benzene 
benzene cethananuiae, n,n-dinethyl 
If you should have any questions, please do not hesitate to call. 
INDUSTR.IAL CORROSION Mi^AGEMINT, INC. 
Rfchard S. Livi^^e 
President 
/ 
h/f/yj/^^-^ 
RSL:dlh 
301451 
y y A r^cHlSl 
?C3 Isomer 
PCB 1254 
PC3 1260 
TABLB 1.1 
30870-0705 
MYIHgSCIENCES 
Samnle Identification: HARE 64981 
PCB 1016 
<0.2G 
PCB 1221 
<0.20 
PCB 1232 
PCB 1242 
PCB 1248 
<0. 
<0. 
<0, 
<0 
<0 
20 
,20 
.20 
.20 
.20 
301452 
YWC, INC. • 200 Monroe Turnpike • Monroe. Connecticut 06468 • (203) 261-4458 
'"ill 
it i'i 
INDUSTRIAL -
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDE? Cartified Drinking Water/Wastevate: 
Laboratory IDi/ 14116 
RZPORT DATE: April 14. 1986 
LAB if 52959 
1152 ROUTE 10. RANOOLPH. NEW JERSEY 07863 
201-534.0330 
CLIZNT: ENTIRO SCIZNCZS - I s l a n d Chenical 
P r o i e c t 
SA.MPLE SOURCE: Samole f?6 
S.A>:PLZ D . \ I Z : Februarv I S , .19 = 6 
T.AKZ^; 5Y: A. Kvles 
.AT L.A3 DATZ: 
LABORATORY ANALYSIS 
RZPORT 
P.ASAMZTZP. 
Flashpoint 
Specific Gravity 
pH(units) 
RESULT 
97°C boiled (3 97'C 
1.0809 
6.71 
If you should have any questions, please do not hesitate to call. 
INDU^TRLAL CORROSION M.ANAGZMINT, INC. 
Richard S. Lerrt. 
President 
/ 
RSL:dlh 
301453 
y t ^ y y y ^ - z y T / 
S & W 
W A b T t , 
I N O , 
CODS 
5 JACOBUS AVE. . SOUTH KEARNY. N.J. 07032. (201)344-4004; 
TECHNICIAL 
GENERATORS WASTE MATERIAL PROFILE SHEET i "^"^ '^'^'^^s 
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TITLE 
GENERATOR'S SIGNATURE 
301454 
I 
Polychlorinated Biphenyl (PCB) Warranty 
^ ^ ^ ' ~ ' s disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
' • • 
yB's are used in this disclaimerto referto any chemical substances and combinations of substan-
- 
jes that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shali 
* 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
- 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who 
-* 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
I S L H T P ' O C k i ^ y ^CfV^ COfiereby warrants that materials transferred by it to S&W Waste. Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability 
resulting from the breach of this warranty. 
IX5>uAJ^•vp C r r O ^ ^ r p - (Z/Z -^^v'C 
DATED: 
-^ 
WITNESS:. 
Herbicide/Pesticide Warranty 
-LSL \ V J C ) ('y^Al(iZ^ d^ir\ih'k'rphy warrants that material transferred by it to S&W Waste, Inc. 
fortransportation, treatment and/or disposal is not contaminated by herbicide/pesticide ata level 
greater than 0.001 % when measured in each container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. X S t f ^ r V / D Crh^VNA.^/^ ^ CO.ZZ'J^ 
DATED: _ _ ^ 1 [ / Z i 1 _ _ 
PY- 
^ 
/,(/i_r7 I T V — r i ^ ^ V . - J - ^ 
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WITNESS: y^^^y^y^yy^^ztyA. 
Aluminum and Reactive Metal Warranty 
r ^ l f V O n r h t O M ^ C i ^ U 
C J ^ 
TVVJC. hereby warrants that material offered to S&W Waste, inc. 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powderorpigmentandherebyagreestoidemnifyandholdS&WWaste, Inc. harmless 
•
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V V M O I C J 
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115 JACOBUS AVE. . SOUTH KEARNY, N.J. 07032. 
(201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
TECHNICIAL 
REP. INITIALS 
A, GENERAL INFORMATION 
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ARE REPRESENTATIVE OF THE WASTE. 
DATE 
f..Mj(it[l yzy.i.x) 
TITLE 
GENERATOR'S SIGNATURE 
301456 
Polychlorinated Biphenyl (PCB) Warranty 
T<- is disclaimer is to all persons who generate and dispose of chemical waste. The terms PCS and 
.B's are used in this disclaimerto refer to any chemical substances and combinations of substan-
jes that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct 
in a process which contains less than 50 ppm PCB because of any dilution; again, these lattershali 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
J,5LrTAJV) Ctt'Qi'^CcnrvCx4TF>Veby v/arrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
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agrees to idemnify and hold S&W Waste, Inc. harmless_from any costs, damages or other liability 
resulting from the breach of this warranty. 
f ^ i f\fA ^ 
Crt^TM-fC/^TV Co X-u'v 
DATED:. ^ - ^^-^7 
RV. ^ . rki^irw—- ,<Uz^sjJr^ 
V/ITNESS .' y^^^y^jy 
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Herbicide/Pesticide Warranty 
T S L I V N A : ) C-iitl^fxC ( ^ ^ e ^ i i p r f i h y warrants that material transferred by it to S&W Waste, Inc. 
fortransportation, treatment and/or disposal is not contaminatec j y herbicide/pesticide at a level 
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L ' t f \ / v \ f f ^ 0 ^ S ^ < ^ 
DATED: 
3-11-^7 
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V/ITNESS: 
Aluminum and Reactive Metal Warranty 
J S ^ f W T ) 
rH-T-V^Kf/^ 
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for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless 
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^ 
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V/ITNESS 
301457 
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- . D r u m Type 
j m Nu'mter 
Generator 
Harard Class 
D R U M INVENTORY 
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D R U M INVENTORY 
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DRUM INVENTORY 
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D R U M INVENTORY 
Pac 
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j m Nu'm.ber 
Generator 
Hazard Class 
D R U M INVENTORY 
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WPS S 
Date 
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I WASTE 
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301466 
DRUM INVENTORY 
Page 
/__ cf 
-. Drum Type 
j m Nulnber 
Generator 
Hazard Class 
SzT-r-jk, /7/A Zy/fy/ yZrJs: 
1 
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Generator 
Hazard Class 
CRUM INVENTORY 
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301468 
— Drum Type 
j m Numoer 
Hazard Class 
D R U M INVE.NTQRY 
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K/A'f^L 
Generator 
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301469 
;. Drum Type 
j m Nu'mber 
Generator 
Hazard Class 
CRUM INVENTORY 
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WFS ^ 
Data 
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:, Drum Type 
j m Nulnber 
Hazard Class 
D R U M I N V E N T O R Y 
yy-Cy^y. J k Z j L 
A7A/A7^^^y / / k i . ^ ^ • 
enerator 
— 
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9 
WPS ^ 
Date 
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^—:. Drum Type 
l ^ k 
j m Nulnber 
Generator 
Hazard Class 
DRUM INVENTORY 
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-.Drum Type 
_ j m Nu'mber 
Generator 
Hazard Class 
CRUM INVENTORY 
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DRUM INVENTORY 
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S & W WASTE, INC. 
15 J A C C B U S AVE. . 
SOUTH KEARNY. N.J. 0 7 0 3 2 . 
( 2 0 1 ) 3 4 4 - 4 0 0 4 
GENERATORS WASTE MATERIAL PROFILE SHEET 
APPROVAL 
COOE 
TECHNICIAL 
REP. INITIALS 
GENERAL INFORMATION 
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RADIOACTIVE 
INFECTIOUS 
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DATE 
TITLE 
GENERATOR'S SIGNATURE 
"^"7 
301476 
Polychlorinated Biphenyl (PCB) Warranty 
This disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
PCB's are used in this disclaimerto referto any chemical substances and combinations of substan-
ces that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
in a process which contains less than 50 ppm PCB because of any dilution; again, these lattershall 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
prosecution. 
Vr-yy 
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hereby warrants that materials transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability 
resulting from the breach of this warranty. 
'JZZ^K.i\!\^{Z) 
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DATED: 
WITNESS; 
Herbicide/Pesticide Warranty 
^ ^ A ]yzye>-^c\k^'^^itk^ c^"^^^ 
f kjAI 
hereby warrants that materic 
rial transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greater than 0.001 % when measured in each container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. X ^ l L f V t ^ ^ C t ^ c ^ ^ r l T \ ^H2) ^ ^ 
DATED: ^ - (f-<^^ 
RV- fe^> CLr7,.Wv\^ 
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WITNESS:. k2k^^^y^z/C7 
Aluminum and Reactive Metal Warranty 
^ ' 
^^^^^ '' ~ , ^ M 
hereby warrants that material offered to S&W Waste, Inc 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactiv 
metal paste, powderorpigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmles 
from any costs, damages, or other liability resulting from breach of this warranty. ^ , 
_ 
DATED: 
WITNESS 
301477 
S & W 
WASTE, INC. 
15 JACOBUS AVE. . SOUTH KEARNY, N.J. 07032. 
(201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
APPROVAL 
COOE 
TECHNICIAL 
REP. INITIALS 
GENERAL INFORMATION 
'.ENERATOR NAUC 
/ k s ^ ^ y i kk'£y*'^CS^ < ^ . / ^ C m / ' ^ ) 
ADDRESS, ^^TH ^ 7 7 S 
yy-yyAi-yrttm^sy-y f r . Cyyry: 
/ y j i ' ^ 
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GENERATOR EPA I.D. NO. AZ/l££0^yZyC9s 
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TECHNICIAL CONTACT 
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ASTE NAME 
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PHONE 
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OTHER COMPONENTS 
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PHENOLICS 
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ARE REPRESENTATIVE OF THE WASTE 
DATE 
TITLE 
GENERATOR'S SIGNATURE 
301478 
Polychlorinated Biphenyl (PCB) Warranty 
• disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
d's are used in this disclaimer to referto any chemical substances and combinations of substan-
^.JS that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
..1 a process which contains less than 50 ppm PCB because of any dilution; again, these latter shali 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
mited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
..uids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
t is unlawful for S&W Waste, Inc. to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
!:°^^^H!^^^LAvO CrP^yn ^ Co -
hereby warrants that materials transferred by it to S&W Waste. Inc, 
'or transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc harmless from any costs, damages or other liability 
-esulting from the breach of this warranty. 
XSL/VAJHi CtKA^^C}^^ CO -^Vw 
DATED: _ 2 J 1 [ 1 I 1 ? 
RY- l < . r [ \ ^ l ? W - 
"S^fi 
WITNESS: A 
/kyk^y py^yZi::j. 
^ J (/ 
^ 
Herbicide/Pesticide Warranty 
hereby warrants that material transferred by it to S&W Waste, Inc. 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greater than 0.001 % when measured in each container or vessel transferred to S&W Waste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. _j> -^/^yy} r ^i^C^M. ^CPrx. C^"" I^NJ ^ 
DATED: 
y 
WITNESS: 
y^yyi^^y^ykry / \ y / y . 
Aluminum and Reactive Metal Warranty 
hereby warrants that material offered to S&W Waste, Inc. 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metalpaste, powder or pigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless 
>m any costs, damages, or other liability resulting fr©ffl±)reacly3f t h i s w | ^ 
O ' " ' o 
WITNESS:. 
301479 
S & W 
WASTE, 
INC. 
115 JACOBUS AVE. . SOUTH KEARNY, N.J. 07032. 
(201)344-4004 
GENERATORS WASTE MATERIAL PROFILE SHEET 
APPROVAL 
CODE 
TECHNICIAL 
REP. INITIALS 
GENERAL INFORMATION 
O^-^^/o - ^ 7 
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GENERATOR NAME 
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y-^aZZZutyyy:i^y:y^iy^ 
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I HEBEBY CERTIFY THAT ALL INFORMATION 
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SUBMITTED 
ABE HEPSESENTATIVE OF THE WASTE 
/
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/ ^ . / / 
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^ 
DATE 
C-y. I AA 
TITLE 
GENERATOR'S SIGNATURE 
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301480 
Polychlorinated Biphenyl (PCB) Warranty 
's disclaimer is to all persons who generate and dispose of chemical waste. The terms PCB and 
^B's are used in this disclaimer to refer to any chemical substances and combinations of substan-
"Les that contain 50 ppm orgreaterof PCB's as defined in 40 CFR 761.3 (s), including any byproduct, 
in a process which contains less than 50 ppm PCB because of any dilution; again, these latter shali 
be included as PCB and PCB's. Substances that are regulated by this rule include, but are not 
limited to, dielectric fluids, contaminated solvents, oils, waste oils, heat transfer fluids, hydraulic 
fluids, paints, sludges, slurries, dredge spoils, soils, materials contaminated as a result of spills, and 
other chemical substances or combination of substances, including impurities and byproducts. 
It is unlawful for S&W Waste. Inc. to receive PCB's. Any generator and/or transporter who 
knowingly or willfully ships PCB's to our facility will be subject to civil penalties or criminal 
prasecution. 
trrr-r^ 
hereby warrants that materials transferred by it to S&W Waste. Inc. 
for transportation, treatment and/or disposal is not contaminated by polychlorinated biphenyl 
(PCB) at a level greater than 40 ppm when measured in each container or vessel, and hereby 
agrees to idemnify and hold S&W Waste, Inc harmlessjrom any costs, damages or other liability 
resulting from the breach of this warranty. 
Jr-5LlV^'0 C ^ Q A K U 1 \ ^ CO nr(^<. 
DATED: 
3-)l-SV 
=Y. 
fii^CU'/>v^.S^^;k^^^ 
WITNESS:. 
^^1*/ 
EHJerbicide/PesticBde Warranty 
- p 
^ • ^ ' y . ^ 
y, 
- A 
fy=^-. -"^^ ^ z - '^-^^ 
hereby warrants that material transferred by it to S&W Waste. Inc. 
for transportation, treatment and/or disposal is not contaminated by herbicide/pesticide at a level 
greaterthan 0.001% when measured in each containerorvessel transferred to S&WWaste, Inc., 
and hereby agrees to indemnify and hold S&W Waste, Inc. harmless from any costs, damages or 
other liability resulting from the breach of this warranty. 
^ S i^fYtZ'O C t-pe^ C C n-\-C (J 
DATED: 
^- j y ^ ^ 
„v. ^ V r ^ d ^ ^ l ^ y — /CecAjJs-
WITNESS: 
/ ^ < < k y y ^ ^ ^ y ^ € y 
Aluminum and Reactive Metal Warranty 
^ 
^ II r ' 
* 
^ 
^~~ l \ 
\ k - ~ y ^ ,^^^=-nc_tJ^ 
hereby warrants that material offered to S&W Waste, Inc. 
for transportation, treatment and/or disposal does not contain elemental aluminum or reactive 
metal paste, powderorpigment and hereby agrees to idemnify and hold S&W Waste, Inc. harmless 
-im any costs, damages, or other liability resulting frornJoreach of tbis warranty ^ ^ 
,T^^ J-^^: 
DATED: _ ^ : l L ! l l i 
^ BY: 
^ ^ 
U^CM, 
WITNESS: 
y Z ^ ^ ^ p ^ y c ^ ^ i z k L y 
/ 
(/....... 
301481 
PRIORITY POLLUTANT VOLATILE ORGANIC ANALYSIS 
LABORATORY ID I U U 6 
LAB # 
5295^ 
• - - • 
CLIENT: ENVIRO SCTgNCES-Islar.d Cherj^'cal 
P r s i e t 
SAMPLE S O U R C E s a r i D l e l l 
-• ---.-:. 
GC/MS Method 
6 2 4 * 
Tier II Deliverables 
PARAMETER 
Chloromethane 
Bromomethane 
. 
Vinyl Chloride 
-- — 
Chloroethane 
Methylene Chloride 
1,1-Oichloroethene 
1 ,1-Dichloroethane 
Trans-1 ,2-Dichloroethene 
•— 
Chloroform ; 
1 ,2-Oichloroethane 
1 ,1 ,1-Trichloroethane 
Carbon Tetrachloride 
Bromodichloromethane 
: 
1 ,2-Oichloropropane 
Trans-1,3-Oichloropropene 
Trichloroethene 
Dibromochloromethane 
1 ,1 ,2-Trichloroethane 
• 
Benzene — 
• 
cis-T,3-Dichloropropene 
2-Chloroethyl vinyl ether 
Bromoform 
Tetrachloroethene 
1,1 ,2 ,2-Tetrachloroethane 
— 
Toluene 
Chlorobenzene 
: 
Ethyl benzene 
Total Xylenes 
*Dichloroben2enes noc analy2ed under chis mechod. 
RESULT 
ug/l 
u 
IJ 
u 
u 
u 
u 
u 
u 
8 . 2 3 
u 
u 
u 
L' 
U 
u 
u 
u 
u 
u 
u 
u 
u 
u 
3 . 9 0 0 B 
U 
6 . 7 J 
U 
METHOD 
BLANK 
u g / l 
u 
IT 
u 
u 
u 
u 
7 . S J 
IT 
u 
u 
u 
r: 
U 
U 
U 
U 
2.0J 
u 
u 
u 
u 
u 
i . 9 J 
U 
u 
u 
MDL 
I n 
! n 
i n 
10 
10 
10 
LO 
LO 
LO 
10 
10 
LO 
10 
10 
10 
10 
10 
- 
1 0 
10 
10 
10 
10 
10 
10 
• 10 
10 
10 
10 
Analyzed by GC/MS Mechod 625, 
301482 
X^CV-JVJ:'^ 
INDUSTRIAL 
-
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDE? Certified Drinking Vacer/Vascevate-
Laboracory ID-:/ 14116 
RZPORT DATE: April 16. 1986 
LAB H 52954 
.1152 ROUTE 10. .RANDOLPH. NfW JERSEY O/HSi 
ZCl-SSi^ljO 
CLIZNT: ENVIRO SCIENCES - Island Chenical Proiecc 
SAMPLE SOURCE: Samole 5*1 
SA>C?LE DATE: Februarv 2S,.19S6 TAKEN BY: A. Kvles AT LAS DATE: March 7. L9=: 
LA30RAT0RY ANALYSIS 
REPORT 
PARAMETER. 
RESULT 
Ben2c::h£r.cr.a 
Neac Benrochancr.e 
If you should have any quescions, please do not hesicace t o call. 
INDUSTRIAL CORROSION M.^AGEMZNT, INC. 
Richard S. L 
Presidenc 
RSL:dlh 
y/<^.C6'/S^,f 
301483 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROUIE 10. RANOOLPH. NEW JERSEY 07865 
2Q1-S84<1320 
NJDEP Cercified Drinking Vacar.'Vastavace-
Laboracory IDrf 14116 
REPORT DATE: April 14, 1986 
LAB il 52954 
CLIENT: ENVIRO SCIENCES - Island Chemical Proiecc 
SAMPLE SOURCE: Sample ill 
SA-^dE D.klZ: Februarv.28, 15H5 TAKEN 3Y: A. Kvles 
.Kl L.\3 DATE: y.a: 
LABORATORY ANALYSIS 
REPORT 
P.ARAMETER 
Ignicabilicy 
Specific Gravicy 
pHCunics) 
RESULT 
,Igr.iC5s wichouc persisc=r.c burni: 
21.97 
8; 06 
If you should have any quescions, please do noc hesicace co call. 
INDUSTRIAL CORROSION MANAGZMEin, INC. 
RSL:dlh 
lichard S. /Lev^tne 
P r e s i d e n c / 
301484 
ycyt'C'j/iS' 
Appendix J 
Disposal Manifests 
\WORK\24231\02 \WORKPLAN.REP 
HARDING LAWSON ASSOCIATES 
301485 
nAZ.A,iuuub WASTL MANlPtb" 1 
^ y ^ 
(As Recuired By The Alabama Department of Environmental Wanagement) 
•••Jfc« bnnt or TVO*. 
I f o r m aesigned for usm on e/it» ^J2-0itcnj tyo9>Mf,ttf ; 
•: 
U M I F O R M 
H A Z A R D O U S 
W A S T E M A N I F E S T 
/ ' / - ^ i f - g . g . ^ ^ r ^ / • tf^^ • i H T ^ ^ y i ^ ' ^ i 
vjffnoraior & t%atT\a ana .N^anin; Acores& 
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G«oeraiors 
Pnnne i 
Z < ' Z 
) 
^ 9 < i . ^ - < y 0 3 
foem Aooroit9< 
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2. Pa«* I 
ATiACHMI}.. 
K ,7-7777 
01 
X 
F a c a r al 
T r a i l e r Nu=ber 
.=::M.- 251880 
> ^ S u i * 
M a n t a A 
Document 
Numcw 
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d m n m r a i o t a 
10 
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O'yy^^yiC's TyZocxyiyG. « r.€3yccyz, 
T y i B * t f / > o y r - , 
y ' y r C 
6. 
US EPA 10 Numoar 
C S u i « . . T i 
s 10 
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••» .PT«n« 
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i 
vomoanv 
>^am« 
yyiey</yt., yr.i'yyttyy r.*9yi£yKX.7~yy/e. 
u s £?A 10 Numoaf 
£. Stat* T r a n a o o n v » IO 
uasignaiaa 
racmry 
HMtrta anc Siia 
Aocras^ 
C H E M I C A L W A S T E . M A . N A G E M E N T . I N C . 
E.Tieile Faciiiry 
A l a o a m a HiyivAay 17 at M i l e M a r k e r 163 
Emelle. A l a o a m a 2 5 - i 5 9 
\ ^ i ^ ' D 
'. 9 ' - f f l a l A i r f l « I J ^ 7 
-C I F. Trarv«oon*ri 
PTxx»« 
107 
US EPA 10 Numo«r 
I A, 
L| 
0. 
0, Ol 0 , 6 I 2 I 2i 4 , 6 I 4 
C S u t a 
f a o i t r y t 
lO 
M. FaciuTY 1 
^ i o r m 
205/652-9721 
11. US OOT Oascriotior\ llneiutiin^ Prepar Sliioomg Nan-im. Maja/a CUia. anc ID ftv/ncarl 
12. Containars I 
No. 
I TvOB ' 
13. 
Total 
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9 ^ ^ ^ 3 
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CAAeyt^y^tmty 
I 
I 
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r 
15. Soociai nanoiing 
insiructions ana Aaojiionai 
irTo/mation 
K.. Hanoling Cooes tor Wasias u s e e Aoovo 
/z^i 
3. doociai 
nanoiing 
insiructions ana Aaoitionai 
irTo/mation 
/ 
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^ 
/ / c . J ^ y > c M ^ y ^ ^ i c ^ 2 i y y < m / . yfAuy^y^ ^ ^ - ^ - ^ 5 ^ ^ 
/yy^,y>yoyi ^ ^ ^ 
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1 6. G c . N E R A T O R ' S C c A T l F I C A T t O N : i nereoy caciara tr^ai tna'caniants oi mis ccnsignmeni are tully and accurately aescrioec aoove sv 
prooar snioomg n a m * ana ara cla»i<i»a. oacxec. m a r i a d . ano laeeiaa. ana ara m ail r a u e c u in prooar conoition lor iransoon Sv n i f rrway 
accordir>g to aoplicaoie iniarnational and national govemmant refutations. 
Unless I am a small auanriTy generator w n o Kas deen examotea Sy statute or regulation Irom ine Suty to make i 
waste m m i m i ^ j n o n 
cenification 
unasr Saciion 30C2(&) of RCHA. I also cenify tnai I nav« a program in place to raouca tne volume and IOXICMY ol waste genarateo *.o ine oegraa I 
ttata determined to ba economically 
practieaol* and I nave selected tne mctnoo of treatment, storage, or oisoosal currently avaiiasie to me 
w m c n 
m:nTmiras tne oresent and futura threat to h u m a n neartn and tne environment 
Print»a/7yt3ed 
N a m * 
1/ 1 yced 
f<am« 
^
^ 
A:. pZy/M 
Signaiufj 
^ ^ c A ^ < : ^ i ^ 
M o m n 
Oar 
''«« 
/ t O i / a \ f f i . 
T 
17.Transoon«r 
1 Acxnowi»agem«ni 
ot R*caiof 
of 
Matariais 
O^Neale s xransporc Inc. 
Signaiura 
(1- m . /CU;, 
*^ u t^ ? ^ ' 
Mont/1 
Oar 
yat 
1 II nlir? te t 
O 
IS.Transoonar 
2 Acx/^owiaagamant 
ot 
Recaiot 
ot 
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(^r>»tad/Typed 
Nama 
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kykkyZc/fyy. 
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y y y 
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i 
y 
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T 
20.Facility Owner 
or Ooaraior: Canilication ol recaict ol na^ardous materials covered Oy this mavTiast V^ceot as noiec m nam 
19. 
Pr:m«Q/Typ«i N a m a ^ 
• 
A h y A ^ / A r > y ^ P c - ^ 
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-pPczcAuAyy/zl.^ 
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EPAFt«ng7oo-22(R«.*.8B)Pr.vH.ui«iitK)n.1 oDMiaia. 
STATE OF A L A B A M A (Mus/Acccmpanv Shipment) 
y///' 
- ) , . ' ^ 
• ' 
. 
301486 
u 
UNIFORM HAZARDOUS 
i 
» ; . v j e n e r j i o r j '.,5 £.-A iC . \ o . 
M a n i i a s i 
O o c u m a m No 
f o r m A o o " - e a 
C M S MO : C X > lyto-i 
E i o . ' n 7 i i 
A y /) 9 S o 6 s ' / o 9 s -
WASTEMANIF^-^T-
(ContinuaTioc/SheeT) 
2 3 . G e n e r a t o r s Njmv.- 
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N - i r i h p 
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T r a n s p o n a r 
V.omoany 
N a m a 
• . . . r a g e 
Za/Z, 
i n i o r m a i i o n .n m e s.-.acea aress 
IS 
n o l 
r s Q u i r e d 
Oy 
P o c a r j i 
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iZc'cyyc-Cye. 
yy^^yy^uyyzy: 
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' f o n t p n 
I ' l m n a n v 
N a m a 
"is. 
u s EPA 10 N u m o e r 
y e a <? g o ff O S 9 7 7 
L. S l a i e 
M a n i l e s i 
D o c u m e n t 
N u m o a r 
CWMA 
^ 4 - ^ ^ ^ / :-:-. 
M . ^ t t i s 
G a n a r a i o r s lO 
"" 
!— 
U S EPA 10 N u m o e r 
N. S l a i o 
T r a n t o o n a r s 
i U 
0 . T r a n t o o n a r s. P n o n a 
P. Scaia 
T i o n s o o a e r s 
10 
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s 
^ " o n a ~ T p _ i, 7 Q r o / t Q 
28. U S D O T D e s c r i p t i o n ( I n d u l g i n g P r o p e r S h i c p i n ^ N a m e . H a z a r d Class, a n d ID Humberl^ 
. i S . i - o n t a i n a r s 
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\4* . i ^ ^ * Ay( 77"^ 
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a. 
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o« 
Raceiot 
o l 
M a t e r i a l s 
34. T r a n i o o n a f " ^ 
A c x n o w i a o g a m e m 
or 
H a c a i o t 
of 
M a t a n a l i 
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T/Stl/^T /T) klcz/^oAjy^lATk^Tr^^. 
1/0-1 C^ 1^ 
3 5 . OiacrapanCY i n d i c a t i o n S p « c a 
3 0 1 4 8 7 
n/MA. tUUU^WAb 1L MANiFEST 
(As Required By The Alabama Depanment of Environmental Management) 
• a sa onnt or rvDa. 
t f c r m emsiqnati for usa on alira f t 2-oitcftl tYoe.mrner.1 
f a r m Aoortitietl Q M B Na. 20<X-C.iCJ Eioitfs 7 . J ; 
UINJIFORM H A Z A R D O U S 
W A S T E M A N I F E S T 
i. 
vjtfherator s Same ano .Vtamnc 
Aooress 
SscSMP Cy^y/CSc day>ryffy/ty 
3'ffo yrt^y/irysu) ^oSa 
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aiyyj'yyt^, ^.Ciiy--A,Ljej/ty c**» *u 
4. 
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Phona ( • Z - ^ / ) £ 9 < i - t X / O O 
I. uanarator s uS cPA 10 No. 
Manilas! 
^^^^^/>'7.g; o i£ I r- /: oy^i^f^i^^o*^ 
2. Page I 
ol Z , 
Intormation .n ir.a $.-iac«c 
i r e i s 
'» 
n o t r a q u i r a o Sy f e o o r a i 
(aw. 
Trailer Number 
I^ZLZ 680365 
A . State Mamlftsi Ooeumant 
fnimcar 
cvvnviA_24303 2 
Q. Stata Ganaraior $ 10 
3^ 
transooner 1 Company 
Name 
QZA/£^<-ff ryyycjiyyye- .--t-«3 rf.sycj:y.. 
r/iS-uU y>oxr~ - ^ y / c . 
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C S u t a 
Trantoonar s lO 
\ / ^ ^ . / S . ' . £ > \ 9 ' . S \ a \ ^ \ P ' t ^ \ £ ' \ 7 ' 9 i 0. Transooner » Pnona 
.ransoonar 4. company 
Name 
r/iV/cc/i. y^yayAyif y^z^jj-rya^rjj'yyi. 
6. 
uS cPA lO Numoer 
l-^'/^'^)! ? i ^ l <:>.6^<3.\ <£.:£'\ 7 ' 9 
E. S U i a Traruooner s 10 
P. Trartsconer s Phone < - / y : f f . , , ' i r — \ 
i / i > -
•- • " * 
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/ t~. I.J 
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uasignaied racmry Name ano ^ i i e Address 
C H E . M I C A L W A S T E M A N A G E . M E N T . I N C . 
Emelle Faciiiry 
A l a o a m a Hi9nvvav 17 at Mile M a r k e r 1 6 3 
Emelle. Alacjama 35-^59 
10. 
US EPA 10 Numoer 
Al L. D. Ol Ol Ol 6 I 2 I 2i 4 I 6 I 4 
G. State Facility s lO 
K. Faciirtv s Phone 
205/652-S721 
1 1 . u s OOT Description (Including Propar Sfiipping Name. Hazard Class, and ID Humoar) 
/y^-By/yz/yffcyj /yy^'^/z A/^cyy/y yycs(7-oca,f»i: p/S^^zu/e) 
12. Containers 
No. 
I Tvpa 
13. 
Total 
Ouaniirv 
Unit 1 
W i / V c i 
Wasts No. 
oyty^-e' yyy9A,/7 
C^•^/^.l Profile N u m o e r ^
.
^
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I 
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AdcitKxiai Descriptions tor Matenais Usied 
AOcva 
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k / / 6 ' y ^ ' ^ c y - ' ^ ^ ^ r ^ T i ^ ^ O y i ' C y ^ ^ 0 ^ t P . y / / 3 y j y P a < Z / f ' ^ ; ^ ^ ' U ^ ^ 
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K. Handling Cooes tor Wastes u s e s Asova 
15. Spvoat 
nananng 
instruciions ana Aocitionai 
irformation 
/Ac,. ^^^^jKPi* U P U J .yyiy^<^ ^yi<.^j^y^usCy ^•*'iA^^^Pj^iy^m 
t u ^ ^ 
Ceyjy>fy? 
i . y 
16. 
GE.NERATOR'S C E R T I F I C A T I O N : 1 nereov declare mat tne cements ot tnis consignment are tuily ano accurately oescrioeo aoove oy 
prooar snipping name and are classified, packed, marred, and laoeied. and are in all resoaas in proper condttion for i r a n s o o n oy hignway 
according to aoolicaole intemational and national govemmertt regulations. 
Unless I am a small quantity generator w n o has been exempted by statute or regulation Irom the dury to make a waste m i n i m i i j t i c n 
cenification 
under Section 30021b) ol RCRA. I also cenihy that 1 have a program in piaee to reduce the volume and toxicity of waste generated to tne degree I 
hava determined to Ba economically pracricaole and I have seieaed the method of treatment, storage, or disposal currently availasie :o me wnicn 
m m i m i i e s tna oresent and future threat to h u m a n health and the environment. 
V 
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Montn 
Day 
Year 
IS.Transoortar 2 Acxnowieagamen^ of Recaiot OT Materials 
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f T T A T P 
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UNIFORM HAZARDOUS 
-* 
WASTE MANIFEST 
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21.vjcnerator i uS c?* 
No. 
/tannest 
Document No 
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fai^.f. A eo'o»»a QMS So :ooo OJ.-.4 E.c..-^ 7 : • 
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N 
:PA Form 8700-22A (3-84) 
STATE OF ALABAMA (Must Accomoanv Shioment) 
301489 
UrvJIFOBIV. HAZARDOUS 
hAZAr^!JUUS"WASTL i/iAf^iPEST 
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v u a i a onnt or type.. 
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WASTE MANIFEST 
Mailing 
1. Ganaraior s uS EPA iC No. 
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prooer sniooing n a m * and mr^ classifi«0. oacxati. rrarxac. »r\C taDaiad. and are m all resoecrs in prooor condtiion (or iransoon Dy n i g n w i y 
according to applicaole international and national gov«fnmcnt ragulations. 
Unlasa I am a small a u a m i i y ganaraior 
w h o has &««n exemoieo by statuia or regulation from tne duty (o maka a waste minimization 
cenification 
under Saction 300Z[b) of RCAA. I also canity tnat I have a program m place to reduca the volume and toxicity of waste generated to tne degree I 
have determined to be economically practicaPle a r ^ t f\m>f% selected tne metnod of treatment, storage, or disposal currently avaitasie to me 
w m c n 
minimiies tne oresent and future tnreat to h u m a n neatirx and trie tnvtronmeni. 
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Prinied/Typwd 
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Norron C.M. Burt 
Signature 
m. /d-o^tt yH. 
Montn 
Day 
Year 
11 ! 0 11 I 7 18 ' = 
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S T A T E OF A L A B A M A 
(A\ust A c o D m w j w ^ShiRfSrW^^ 
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301490 
.11 Of rvoe 
I f o r m c t f u a n e d ' o r use o n gtite (1 2 o * t c n ) t v o e w n t e r I 
UNIFORM HAZARDOUS 
WASTE MANIFEST 
(ContinuaTJon Sheet) 
A . . u o n f r a ; o r i .^5 £ r A i J .No. 
M a n i l e s i " 
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Mtfnrn Oay 
1 /.LI .^ 
301491 
1 
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A Form a700-22A (3-84) 
C;TATP D P A» A R A M A f M i . ^ A^ 
cu:...— 
• 
Appendix K 
ESI February 7, 1986 Letter to USEPA Regarding Waste Disposal 
\W0RK\2 4231\02\WORKPLAN.REP 
HARDING LAWSON ASSOCIATES 
301492 
'^^'ij 
5CI&KE5 inc. 
19 COPELAND RD., DENVILLE. NEW JE.RSEY 07834 
(201)365-5256 
February 7, 19 8 6 
Mr. Conrad Simon 
USEPA Region II 
26 Federal Plaza 
New York, N.Y. 10007 
Dear Mr. Simon: 
Enviro-Sciences, Inc. (ESI) has completed the proposed 
scope of work for on site cleanup of the Island Chemical 
Company (Berlex) facility in St. Croix, U.S: Virgin Islands. 
The cleanup program and methodology were presented to Mr; 
Robert Harris of your office in December, 1984 and ammended 
in a subsequent report dated April 4,1985. 
Briefly, the cleanup involved decontamination at several 
locations. These are: 
i 
1) soil around above ground storage tanks - Toluene; 
':Z 
2) soil around a concrete pad - Toluene; 
3) soil along a collapsed drain line - Toluene, Heavy 
Metals; 
4) water and sludge in a process pit - Toluene, Heavy 
Metals, Benzyl Acetate; and 
5) soil in a laboratory waste pit - Pyridine. 
All materials from the first four (4) locations listed above 
were containerized in proper 55-gallon steel drums, manifested 
and shipped as hazardous wastes to Chemical Waste Management, 
Inc. (CWM) Emelle, Alabama. CWM acknowledged receipt of 
these materials for disposal. 
The laboratory waste pit soil was treated on site to decrease 
pyridine contamination level from above 1000 ppm to less than 
2 ppm. ESI considers this level of contamination to be.below 
levels which would require any additional cleanup efforts. 
301493 
February 7, 1986 
Page -2-
The collapse of the drain line and subsequent analysis 
of soil has initiated the need to conduct additional 
sampling off-site in the "cut" or dry creekbed. ESI 
will undertake this sampling program immediately to 
ascertain the presence of contamination and, if present, 
concentration levels. 
We would appreciate any comments relating to our cleanup 
program at the Island Chemical Company site. 
You may contact me cr Mr. Irving Cohen at (201) 366.-6256, 
Very truly yours, 
ENVIRO-SCIENCES, INC. 
Alan L. Kyles, Ph.D, 
Vice President 
ALK/ak 
cc: Robert Milos 
Frank Curtis 
301494 
Appendix L 
USEPA Pollution Reports 
\WORK\24231\02\WORKPLAN.REP 
HARDING LAWSON ASSOCIATES 
301495 
4 / 
I 
# 
U.S. EKVIRONKENTAL PROTECTION AGENCY 
POLLUTION REPORT 
. y 
Region II 
Response and Prevention Branch 
Edison, New Jersey 08837 
(201) 548-8730 - Comnercial.and FTS 
24 Hour Emergency 
DATE: February 8, 1989 
TO: W. Muszynski, EPA 
S. Luftig, EPA 
R. Salkie, EPA 
M. Randol, EPA 
G. Pavlou, EPA 
ERD, WH-548B 
(E-Mail) 
B. Sprague, EPA 
G. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, DPNR 
LEPC 
TAT 
POLREP NO: 
INCIDENT/SITE NO, 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
One (1) 
N/A 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VI CHEM) 
St. Croix, US Virgin Islands 
800 Lab Chemicals, 400 Drums, 22 Tamks 
Groundwater, Caribbean Sea 
1. 
SITUATION; 
A. The Virgin Island Chemical Company (VICHEM) site is 
located on the Island's south side. The site is situated on 
Route 66, approximately 0.5 miles due north of the Alexander 
Hamilton Airport. The site covers approximately 3.5 acres 
and is bordered to the north by an intermittent stream that 
originates on the north side of the Island and discharges 
into the Caribbean Sea. 
A nmnber of residences and industries are located as 
close as one-tenth of a mile from the site. In addition, 
several well fields are located in the vicinity of the site. 
The St. Croix prison is located 1/4 mile downwind froa the 
site. DPNR stated it would be very difficult to evacuate 
prisoners in the event of a chemical fire at the site. 
B. The site consists of a main warehouse building including 
offices, the reactor, centrifuge and maintenance buildings 
and fourteen above ground tanks. Living on-site adjacent to 
the main warehouse building are anywhere from 15 to 25 guard 
dogs housed in individual kennels. 
Also living on-site is the kennel operator, Kate Wesp. 
A house trailer is located on the concrete surface near the 
301496 
loading dock. It is also apparent that Wesp uses the 
restroom facilities and kitchen area in the main building as 
living quarters. 
.*-
C. Presently occupying the site is the company VIAG Fuels, 
Inc. VIAG utilizes some office space in the main building 
and also has ethanol stored in four of the aboveground 
tanks. The principals of the firm plan to begin an alcohol 
dehydration project on-site in the near future. 
D. The 3.5 acre site is owned by Charles H. Steffey, Inc. 
On May 1, 1969 Steffey leased the property to Houston 
Chemical Industries, Inc. Houston Chemical assigned the 
lease to Caribe Chemical Company, Inc., (subsequently )cnown 
as Pierrel America, Inc.) on March 20, 1972. 
On June, 1978, Pierrel America assigned the ground lease 
to Cooper Laboratories, Inc. (Cooper). On October 30, 1979 
Cooper Laboratories assigned the lease to its subsidiary, 
Island Chemical Company (ICC). On November 1, 1979, Cooper 
Laboratories sold all of the stock of ICC to the 
predecessor of Berlex Laboratories, Inc. (Berlex) . .. On 
September 14, 1984, ICC sold its assets to Virgin Island" :-
Chemical Company (VICHEM). 
This background information has been supplied by the 
Virgin Islands Department of Planning and Natural Resources 
(DPNR). 
E. Limited PRP (Berlex) site clean-up and soil excavation 
has taken place in the recent past under a RCRA enforcement 
action. Berlex is currently finalizing a scope of work for 
a remedial investigation/feasibility study addressing soil 
and groundwater contamination. 
2. 
ACTION TAKEN: 
A. On Tuesday, January 31, 1989, the U.S. EPA Response and 
Prevention Branch conducted a Preliminary Assessment and 
Removal Evaluation at the VICHEM site. This action is in 
reply to a request from George Pavlou, Associate Director 
Enforcement Programs dated 1/23/89. 
B. This preliminary assessment vas coordinated with and 
observed by DPNR personnel. DPNR's primary concerns with 
this site are the threat of fire/explosion, and the threat 
(or actual) migration of spilled materials to the 
surrounding coil and groundwater. 
C. The initial entry into the main warehouse building vas 
made at 0930 hrs. on January 31, 1989. All safety 
procedures were followed for a level "B" entry in a hot 
climate. Air monitoring was conducted with OVA, HNU, CGI, 
Radiation Detector, HCN Monitox, H2S Monitox and pyridine 
301497 
Draeg.er tubes. All air monitoring readings were equivalent 
to background (taken off-site), except for in room 5 of the 
drum warehouse which showed ambient conditions 1 unit above 
background on the OVA. All further entries were made in 
level " C . 
D. Three areas were delineated based upon the type of 
material located in each of these areas are: 
A. The laboratory (main building). 
B. The drum storage warehouse (main isuilding). 
C. The grounds outside the building including the 
reactor and centrifuge. 
Each of these areas will be described below. 
1. Laboratory 
813 containers of laboratory reagents and unJcnown 
liquid and solid material are located in^this area. 
Some of the more dangerous items of note'are as 
follows: 
'vr: 
^^^' 
'kkr--
» 
,• ^-, -
a. Sodium metal (2 _boxes). Water reactive. 
b. Ethyl Ether (6 cans). Potential explosive. 
c. Diisobutyl aluminum hydride (4 lecture 
bottles). Spontaneously combusts in air. 
d. Potassium cyanide (2 bottles).. Poisonous. 
Stored.near acids, potential for release of 
hydrogen cyanide gas. -f^ 
,,^, 
e. Phosphorous pentoxide (1 bottle). Reactive. 
f. Sodium hydride (1 bottle). Water reactive. 
g. Two flammable storage cabinets containing 
various materials and un)cno%ms. • 
h. Two office type storage cabinets. One cabinet 
has spilled material on the top shelf which 
has dripped downward to mix with other 
chemicals. 
Many other chemicals exist in the laboratory; as veil 
as many containers vith unlcnovn materials. All the 
chemicals vhich had dates are at least five years old. 
2. Drum Storage Warehouse 
In-the main varehouse are located approximately 400 
drvims, of these, 211 are green painted dmms vhich have 
the vords ETHYL ALCOHOL stenciled on the lid. The 
condition of the ethyl alcohol drums vary from fairly 
sound to extremely deteriorated. Some of the drums 
consist of only a rusted shell with gaping corroded 
holes. A rough estimate shovs that 100 are empty and 
100 contain material. This material may be some type 
of sludge. Other materials found are as follows: 
301498 
a. 
Laboratory unknowns (75 c o n t a i n e r s l e s s than 1 M 
gal.) 
b. 
Methanol (5 x 55 g a l . ) 
c. Glacial acetic acid (13 x 55 gal.) 
d. Benzyl acetate (21 x 55 gal.) 
e. Toluene (8 x 55 gal.) 
f. Antifreeze/glycol (20 x 55 gal.) 
g. Benzyl chloride (28 x 55 gal.) 
h. Salicilic acid (27 fiber drums) 
i. Methyl isobutyl carbinol (12 x 55 gal.) 
j. Sodium hydroxide (12 x 55 gal.) 
k. iJulging drum, unmarked (1) 
1. Drums in which some type of reaction has taken 
place, lid popped off (2) 
m. Drums of known and unknown material, 
n. Paint (97 x 5 gal. - 21 x 1 gal.) 
o. Cylinder chlorine (1 poor condition). 
p. Cylinder hydrogen chloride (Ideteriorated 
condition). 
g. One dnim of sulfonic acid, broken and 
leaking its contents, 
r. A cistern with PVC pipe leading to a pumping 
system outside the building. 
3. Outside Grounds 
An inspection of the reactor and centrifuge and 
maintenance buildings revealed various production 
materials including lubridating oils; propane; oxygen 
and acetylene cylinders; filter media; ethanol; 
assorted paints and some sodium hexa-meta phosphate.. 
Some of the oil drums are leaking. 
Scattered aro\2nd the facility are eight stainless steel 
tanks with quantities of unJcnown liquid varying from 
empty to three quarters full. A large storage tank is 
on site along with numerous pressure and reaction 
vessels. Fourteen large green storage taxoks are also 
on-site." Ten are planned to be used in the alcohol 
dehydration project. Four of the ten are full of 
ethanol. The other six are empty. The remaining four 
not being used are empty and unsound. 
E. The Governors office Department of Fire Services was 
contacted to assess local chemical fire control 
capabilities. Three fire companies are located on the 
island with the nearest to the site being Grove Place. All 
firefighting personnel are equipped with SCBA, however, 
only some have had formalized chemical hazard training. A 
limited amount of foam capability is available. 
301499 
3. 
FUTURE PLANS AND RECQMKENDATIONS: 
A. The USEPA CERCLA Enforcement Program is actively 
pursuing PRP involvement in a site clean-up and drum 
removal. 
B. An action memo and disposal plan will be drafted by this 
branch in the event the PRP's fail to act promptly. 
FURTHER 
POLRZPS 
FINAL POLREP. 
FORTHCOMING X SUBMITTED BY. 
DbuglaS R. Kodama, 
OSC ' ' 
Response and 
Prevention Branch 
DATE RELEASED ^ ^ gjl'^g'l. 
301500 
> 
I 
U.S. ENVIRONMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
DATE: June 7, 1989 
Region II 
TO: 
Response and Prevention Branch 
Edison, New Jersey 08837 
(201) 548-8730 - Commercial and FTS 
24 Hour Emergency 
w. 
s. 
R. 
M. 
G. 
Muszyns 
Luftig, 
Salkie, 
Randol, 
Pavlou, 
ki, EPA 
EPA 
EPA . 
EPA 
EPA 
ERD,- WH-548B 
- • 
B. 
8. 
P. 
A. 
(E-Ma 
Sprague 
Zachos, 
Gelaber 
Smith, 
LEPC 
TAT 
il) 
, EPA 
EPA 
t, EPA 
DPNR':. 
POLREP NO.: 
Two (2) 
INCIDENT/SITE NO.: N/A 
POLLUTANT: 
Lab chemicals, Alcohols, Solvents, Acids 
CLASSIFICATION: 
Major 
SOURCE: 
Virgin Island Chemical Company (VIChem) 
LOCATION: 
St. Croix, U.S. Virgin Islands 
AMOUNT: 
800 Lab Chemicals, 400 Drums, 22 Tanks 
WATER BODY: 
Groundwater, Caribbean Sea 
1. 
SITUATION: 
A. Same as previous polrep. Site conditions have not 
significantly changed. 
2. 
ACTION TAKEN; 
A. OSC discusses contents of Notice Letters with ORC and 
Enforcement Programs. On March 13, 1989 Notice Letters were 
issued to the following Potentially Responsible Parties (PRPs): 
Berlex Laboratories, Island Chemical Company, CHS Holding 
Company (land owner). Virgin Island Chemical Company, and VIAG 
Fuels. 
B. March 30, OSC receives copies of Notice Letter replies 
from Berlex, VIChem and VIAG Fuels. None of the PRP's are 
willing to conduct or finance a CERCLA response. OSC informed 
verbally that Region II will conduct a removal action at this 
site and that an Administrative Order may not be issued to the 
PRPs. 
301501 
C. April 5, OSC contacts D. Weston of VIAG Fuels and 
requests him to inform Enforcement Programs of VIAG's intended 
use of ethanol, paints and water treatment chemicals, thus 
averting the need for EPA to dispose of these materials. 
D. OSC drafts memo to Enforcement Programs concerning 
enforcement issues which must be addressed prior to an EPA 
removal action. Issues include material owned or planned for 
purchase by VIAG and temporarily evacuating VIAG and St. Croix 
Security Kennels (SCSK). Memo issued April 20, 1989. 
E. Draft Action Memorandum prepared and distributed for 
comment on May 17, 1989. Comments due June 2. 
F. OSC contacts Fred Schubert, .President..of. VIChem and 
receives verbal permission for access to the site during the 
week of May 22, 1989. Mr. Schubert was not aware that there 
were hydrogen chloride and chlorine cyliners on-site and knew 
nothing about the cans of ether stored in the labs. Mr. Schubert 
informed the OSC that he is making plans to repair the warehouse. 
G. OSC discusses proprosed removal action with 
representatives from" DPNR on May 22. Discuss possibility of 
having DPNR order VIAG and SCSK to leave the site during on-site 
removal activities and monitoring the site prior to EPA's 
mobilization to the site. OSC will write a formal' request for 
DPNR to carry out these tasks. 
H. May 23, 1989, OSC discusses with Lt. Steve Hanewich, the 
possibility of using the US Coast Guard HazMat unit in San Juan 
for technical and contractor oversight assistance during the 
removal. USCG will need a Memorandum of Understanding (MOU) for 
reimbursemewnt of lodging/per diem and disposable personnel 
protective gear, 
I. OSC briefs the Caribbean Regional Response Team on 
EPA's proposed removal action at VIChem. FEMA recommends that 
during on-site treatment activities or a fire at the facility 
that the nearby prison not be evacuated. 
J. OSC visits VIChem with OH Materials Project Manager on 
May 25, 1989 to review site conditions and discuss proposed 
clean up activities for the site. Conditions within the labs 
remains the same. Drums within the warehouse have been restaged 
in an orderly fashion however they are not staged by 
compatibility groups. The warehouse floor has been swept clean 
and the leaking drum of sulfamic acid has been overpacked, 
according to VIChem's President, however this drum was not 
located. One drum labeled "skin cleaner" was leaking. 
According to D. Weston of VIAG, the company remains inactive 
and is having trouble getting ethanol from Europe. Within the 
tank farm., the first four tanks contain ethanol and the fifth 
tank contains diesel fuel. The red tank truck contains water 
• •" 
...A 
301502 
VIAG has had water from the on-site well analyzed and 
determined that it was free of contamination and suitable for 
their treatment process. OSC inquired if chloroform was included 
in these analyses, Mr. Weston was not sure. 
K. May 26, 1989, OSC meets with Winston Turnbull, Director 
for VI Fire Services and Kirk Grybowski, Director for VI 
Emergency Management Services and briefed them on EPA's proposed 
removal action. Grybowski recommended meeting with the St. 
Croix hospital administrator and EMS's Deputy Director on St. 
Croix to discuss EPA's on-site decontamination procedures since 
neither the hospital or EMS is prepared to receive contaminated 
personnel. 
L. May 30, OSC receives copies of letters from VIChem (thru 
Enforcement Programs) stating that " VIChem is prepared to make 
its best effort to undertake the clean-up at the site" and "As 
you know, I feel the clean up needed at the site is quite 
manageable...". This contradicts VIChem's reply to the Notice 
Letter in which VIChem stated "...I have to indicate for the 
record that Virgin Island Chemical Company has no funds with 
which to have any required work carried out and has no staff to 
perform such work," ' 
M. OSC coordinates with Enforcement Programs and is 
informed that ORC and NY/CC will meet on June 1 to develop an 
enforcement strategy. 
N. June 2, 1989, OSC has received comments on draft action 
memo from AD-REPP and at his suggestion will include^resampling 
of wells contaminated with chloroform in the scope of work for 
this removal. 
• 
3. 
FUTURE PLANS AND RECOMMENDATIONS: 
A. OSC will investigate the possibility of developing a 
MOU with USCG for MSO-San Juan HazMat assistance during the 
removal action. 
B. OSC will request ATSDR to notify and inform the St. 
Croix hospital and EMS of EPA's proposed activities and 
decontamination procedures which will be available. 
C. OSC will prepare notification procedures and a 
contingency plan for the prison at Golden Grove. 
D. OSC will develop CAMEO plume models for various weather 
conditions and air release scenarios. 
301503 
E. OSC will formally request DPNR to monitor the site 
prior to EPA's mobilization, investigate the possibility of DPNR 
ordering SCSK and VIAG off-site during EPA's removal action, and 
request a list of appropriate agencies and politicians to notify 
concerning the proposed removal action. 
FINAL POLREP 
FURTHER 
POLREPS 
FORTHCOMI N G " ^ 
SUBM ITTED BY 
Douglass R. Kodama 
OSC 
Response and 
Prevention Branch 
DATE RELEASED -X^7\q^ 
# 
301504 
U . S . 
ENVIRONMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
Region 11 
Response and Prevention Branch 
Edison, New Jersey 08837 
(20i) 548-8730 - Commercial and FTS 
24 Hour Emergency 
DATE: August 8, 1989 
TO: W. Muszynski, EPA 
5. Luftig, EPA 
R. Salkie, EPA 
M. Randol, EPA 
6. Pavlou, EPA 
ERD, WH-548B 
(E-Mail) 
B. Sprague, EPA 
6. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
LEPC 
TAT 
Three (3) 
N/A 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, USVI 
800 Lab Chemicals, 400 Drums, 22 Tanks 
Groundwater, Caribbean Sea 
POLREP NO.: 
INCIDENT/SITE NO. 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
1. 
SITUATION 
A. 
Same as p r e v i o u s 
P O L R E P S . 
S i t e c o n d i t i o n s 
have n o t 
s i g n i f i c a n t l y 
changed. 
2. 
ACTION TAKEN 
A. 
June 14, 1989, conference cal1 conducted between ORC, 
NYCCB, OSC and F. Schubert (owner of VIChem). Mr. Schubert 
explained that he will not be able to finance a clean-up at the 
facility. EPA informed him that due to the significant hazards 
presented by the site. Region II is prepared to conduct a 
removal action and remove the chemicals from .the facility. 
EPA informed Mr. Schubert that he will have approximately 
one month to contact facilities which may be interested in 
buying some of the materials on-site. EPA will send him a 
Letter OT Intent form to be used during these recycling efforts. 
Mr. Schubert had no objection to EPA removing all chemicals 
from the site and further stated that he would not be obstructive 
to EPA • s, cleanup. 
• 
B. 
301505 
July IB, 1989, Action Memorandum finalized and sent to NY 
office for concurrence and approval. 
DSC received a copy of a letter from Mr. Schubert to NYCCB, 
stating that he has a potential buyer for the site and requesting 
EPA to hold off on the removal action. OSC coordinated with 
NYCCB on this matter. 
C. 
July 25, 1989, Chief RPB coordinated with ORC on potential 
sale of VIChem. 
D. 
August 1, 1989, receive fax from NYCCB concerning VIAG's 
request to start operation shortly and install a water treatment 
unit for their ethanol dehydration operation. 
E. 
August 4, 1989, conference call conducted with OSC, ORC, 
NYCCB and F. Schubert. The potential sale of VIChem has fallen 
through and it appears doubtful that a sale with other potential 
buyers will occur. Mr. Schubert assured EPA that all prospective 
buyers of VIChem Are aware of EPA's interest in having the site 
cleaned-up. ORC informed Mr. Schubert that EPA will proceed 
with our plans for a Superfund clean up, EPA will send him an 
access agreement form for his signature and wanted to be sure 
that all prospective buyers have received copies of the March 
13, 1989 Notice Letter to VIChem. 
F. 
August 8, 1989, Consent for Access to Property form sent by 
ORC to F. Schubert. Acting Regional Administrator approves 
Action Memorandum. 
FUTURE PLANS AND RECOMMENDATIONS: 
A. 
OSC will initiate a Delivery Order for O.H. Materials to 
conduct the site clean up. 
B. 
OSC will inform USVI DPNR about the Action Memorandum 
approval. 
C. 
OSC will coordinate contingency planning meeting for 
appropriate U.S.V.l. public agencies. 
FINAL POLREP 
FURTHER 
POLREPS 
. 
FORTHCOMING X SUBMITTED BY 
Douglas R. Kooama 
On-Scene Coordinator 
Response and 
Prevention Branch 
DATE RELEASED 
301506 
S.yl.7Hg=l. 
../, 
3 . 
U.S. ENVIRONMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
Region II 
Response and Prevention Branch 
Edison, New Jersey 08837 
(201) 548-8730 - Commercial and FTS 
24 Hour Emergency 
DATE: September 8, 1989 
TO: W. Muszynski, EPA 
S. Luftig, EPA 
R. Salkie, EPA 
M. Randol, EPA 
G. Pavlou, EPA 
ERD, WH-54BB 
(E-Mail) 
B. Sprague, EPA 
G. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
LEPC 
TAT 
POLREP NO.: 
SITE NO.: 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
(4) 
Four 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
I 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
BOO Lab Chemicals, 400 Drums, 22 Tanks 
Ground water, Caribbean Sea 
1. 
SITUATION; 
A. 
The Action Memorandum was approved by the Acting Regional 
Administrator on August B, 1989. Site conditions have not 
significantly changed. 
2. 
ACTION TAKEN; 
A. 
August 8, 1989, DSC coordinated Mith ORC concerning language 
in Consent for Access to Property for« to be sent to F. Schubert, 
owner of VIChem and discuss possibility of placing a lien on 
VIChem's property. 
B. 
August 9, 1989, OSC informed of Action Memo approval. 
Receive Site ID No. from PSB, 4V. Delivery Order Number 7445-02-
064. Initiate Procurement Request for •250,000. 
Upon reveiwing and approving the Action Memo, the Acting RA 
revealed several concerns about this removal including 1) 
possible RCRA violations by Berlex, 2) a schedule for tbe 
removal of the 40,000 gallons of ethanol stored on the site, 3) 
additional PRPs and 4) can the site be designated. OSC 
instructed to contact VIAG and determine the schedule for 
removing the ethanol from the site. Other concerns will be 
addressed by other, program offices. 
301507 
' A , 
C. 
August 10, 1989, receive DCN, KE3042 for $250,000. 
D. 
August 25, 1989, OSC contacts VIAG, D. Weston and was 
informed that VIAG intends to buy the 40,000 gallons of ethanol 
from Ethanol Corp. by the third week in September. It will take 
VIAG one day to dehydrate this alcohol and less than one week to 
sell and ship the material off—site to the buyer. By October, 
VIAG expects to be able to purchase ethanol froa Europe and 
start full operation. 
OSC expressed his concern for the safety of VIAG and St. 
Croix Security Kennels personnel (and dogs) while EPA is 
conducting the clean—up at the site and the hazards posed by the 
materials on-site. Mr. Weston shared the same concerns and 
seemed agreeable to vacating the site while EPA is working at 
the site. 
OSC drafts reply addressing Acting RA's concerns regarding 
a schpdul^ l a r the removal of ethanol froa the site and sends it 
to ERRD for a coordinated response to the Acting RA-
E. 
August 29, 1989, John Higgins assigned as alternate OSC for 
the VIChem removal -and D. Kodama to act as his mentor under the 
new Mentoring Program per OSWER Directive h9285.9-6l. 
A. Bosques of the CFO may also assist with this removal. 
Initiate two Procurement Requests for •250,000 and »500,000. 
F. 
August 30, 1989, OSC coordinates with DPNR (B. Rhymer) 
concerning contingency planning Aeeting for VIChem removal. 
DPNR will send out letters to appropriate public agencies and 
schedule the meeting. 
DSC reviews Delivery Order scope of work with Prograa 
Management for the ERCS contractor, O.H. Materials (0<-H1) . OHM 
will be the ERCS contractor for this removal since they are the 
only ERCS contractor to serve the Caribbean. 
G. 
September 5, 1989, Jeff Bodi assigned as Response Manager 
for OHM. 
OSC coordinates with DPNR and informed contingency planning 
meeting scheduled for September 13, at 10 am. St. Croix Fire 
Department, Police Department, Emergency Management Agency, 
Emergency Medical Team, and Department of Justice (Corrections) 
will attend. 
OSC coordinates with ORC concerning access agreement. The 
signed access agreement has not been received from VIChem yet. 
However, ORC contacted Mr. Schubert on August 31 and was informed 
that he will send it to EPA soon. 
3 01508 
H. 
September 6, 1989, OSC receives two additional DCNs. 
4 
KE3069 for •500,000 (9/1/89) and KE3073 for $250,000 (9/6/89). 
This brings the total obligated funds for mitigation contracts 
to $1,000,000. 
OSC develops removal briefing and contingency plan for 
September 13 meeting. 
OSC writes letter to VIAG informing them to proceed with 
removal of paints and that their alcohol dehydration operation 
may proceed as long as it does not interfere with the removal 
action. As for their request to discharge water from thveir 
operation to the adjacent ditch, NYCCB will make this decision. 
I. 
September 7, 1989, OSC initiates a Procurement Request for 
•262,000. This will bring the total obligated funds to 
•1,262,000 which is the mitigation contracting ceiling. 
Discuss Delivery Order with OHM Response Manager. The 
Response Manager and a Chemist will attend the contingency 
planning meeting and visit the site with the OSC. 
J. 
September 8, 1989, OSC distribute's POLREP 3 and sends 
Preliminary Assessment form (EPA Form 2070) to PSB for 
processing. 
.; 
Concerning future plans listed in Polrep 2, time and 
administrative constraints will not allow for development of an 
Inter Agency Agreement with the US C:oast Guard. OSC will 
coordinate with EMT, and if appropriate, the St. Croix hospital 
next week. TAT continues to work on CAMEO plume model for 
possible chlorine and hydrogen chloride release. 
3. 
FUTURE PLANS AND RECOMMENDATIONS: 
A. 
Discuss local response agency concerns at contingency 
planning meeting on September 13. 
B. 
Visit site and develop plan for mobilization with OHM on 
September 13 and 14. 
C. 
Site mobilization tentatively scheduled for September 25 or 
October 2. 
4. 
FINANCIAL ACCOUNTING: 
A. 
Total Project Ceiling Authorized 
•1,840,000 
B. 
Total Funds Authorized for 
Mitigation Contracts as of 8/8/89 
1,262,000 
C. 
Expenditures for Mitigation Contracts 
I.a. Amount Obligated to DCN KE3042 
250,000 
301509 
l.b. Estimated Expenditures as of 9/8/89 
-0-
l.c. Balance Remaining 
250,000 
2.a. Amount Obligated to DCN KE3069 
500,000 
2.b. Estimated Expenditures as of 9/8/89 
-O-
2.C. Remaining Balance 
500,000 
3.a. Amount Obligated to DCN ICE3073 
250,000 
3.b. Estimated Expenditures as of 9/8/89 
-0-
3.C. Remaining Balance 
250,000 
D. 
Unobligated Balance Remaining 
-O— 
E. 
Estimate of Total Expenditures 
to Date for All Mitigation Contracts 
F. 
Other Extramural Costs 
I.a. TAT salary/travel as of 8/8/89 
H. 
Total Expenditures X of S2 Million 
—O-
OX 
I. 
Percentage of Total Project Ceiling 
OX 
FUTURE 
POLREPS 
yy 
F I N A L POLREP 
^FORTHCOM I NG_^i_SUBM I TTED BY 
D o u g l a s O R . 
Kodama, 
O n - S c e n e 
C o o r d i n a t o r 
R e s p o n s e a n d 
P r e v e n t i o n 
B r a n c h 
DATE RELEASED ,Z>eD C^/ O 
l \ ( y K 
301510 
U.S. ENVIPOI^MENTAL PROTECTION AGENCY 
POLLUTION REPORT 
Region II 
Response and Prevention Branch 
Edison, New Jersey 08837 
(201) 548-8730 - Commercial and FTS 
24 Hour Emergency 
DATE: Sept. 29, 1989 
TO: K. Muszynski, EPA 
S. Luftig, EPA 
R. Salkie, EPA 
M. Randol, EPA 
G. Pavlou, EPA 
ERD, WH-548B 
(E-Mail) 
B. Sprague, EPA 
G. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
LEPC 
TAT 
POLREP NO.: 
SITE NO.: 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
Five(5) 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
800 Lab Chemicals, 400 Dmms, 22'Tanks 
Ground water, Caribbean Sea 
1. 
SITUATION: 
A. 
Site was impacted by hurricane "Hugo" from September 17 
through September 19, 1989. 
2. 
ACTION TAKEN: 
A. 
September 12, 1989, OSC and Assistant OSC fly to St. Croix. 
Meet with VIAG, D. Weston. OSC reiterated his concerns for the 
safety of VIAG and St. Croix Security Kennels during site clean-
up. D. Weston affirmed VIAG's agreement to vacate the site while 
EPA is working at the site. 
VIAG also reassured EPA of their plans to process the 
ethanol that is now on-site and ship this material off-site by 
the end of September 1989. This ethanol will remain the property 
of Ethanol Corp. VIAG has an agreement with Ethanol Corp.in 
which VIAG dehydrates ethanol for them. Their plans to commence 
full operation of their alcohol dehydration process were also on 
schedule to occur in October 1989. 
OSC noted the addition of a trailer to the site and VIAG 
responded that it was for removing their paint materials. 
301511 
I 
9 
: # 
B. 
September 13, 1989, the Contingency Planning meetiTig is held 
at the St. Croix VIDPNR offices. The meeting went well with all 
concerned government agencies, except the National Guard, in 
attendance and actively participating. Agreement was reached to 
schedule a subsequent meeting for the following day for the 
purpose of developing a Local Responders site specific 
contingency plan using the Virgin Islands Local Contingency Plan 
as a model. 
C. 
September 13, 1989, the OSC conducts a tour of the site for 
Jeff Bodi (Response Manager) and Jack Herzig (Chemist) of OHM, 
and Jeff Bechtel (TAT). Several items were discussed at 
subsequent meeting. 
OHH agreed to develop waste treataent plan, QA/QC Plan, by 
September 22, 1989. The OSC agreed to coordinate with VIDPNR in 
requesting a waiver of the excise tax which would otherwise be 
levied on the materials OHM is to transport to the site. OSC 
directed OHM to provide daily Progress Reports while on-site, and 
informed OHM that financial data would have to be inputted to 
ROMS. OSC stated his preference for overpacking all drxims to be 
transported for disposal because of the -potential for reactions 
to occur during sea transport of bulked materials. The OSC 
directed OHM to mobilize crew when equipment is received on St. 
Croix. 
OSC wrote up work orders for OHM activities for past two days. 
D. 
September 14, 1989, met with VI Govt, officials at VIDPNR 
offices. Greg Rhymer of VIDPNR distributed a draft site-specific 
Contingency Plan. The Plan was reviewed,•revised for phone 
number corrections, and the final version distributed during the 
meeting. 
E. 
September 14, 1989, OSC met Alan Chardon of St. Croix 
Security Kennels and informed him of risks, prior to and during 
the clean-up, to humans and dogs that would be on-site. Alan 
agreed to drop off dogs prior to daily start-ups and pick up dogs 
after 6 p.m. OSC will write letter acknowledging this agreement 
and requesting contact numbers in the event of problems with the 
dogs. 
F. 
September 14, 1989, VIAG expressed confusion with gaining 
government approval for their intended discharge of 10,000 
gallons/day of wastewater from the reverse osmosis desalinization 
of saline well water, which is part of the alcohol dehydration 
process, to a drainage ditch. After conferring with Marcia 
Taylor of VIDPNR, the Assistant OSC and VIDPNR informed VIAG that 
a NPDES permit issued by VIDPNR would be necessary. VIDPNR 
further advised VIAG that it does not permit discharges to 
drainage ditches and advised VIAG to contact VIDPW for connection 
to the public sewerage system. 
301512 
G. 
September 15, 1989, Assistant OSC drafted excise tax 
exemption letter to be signed by the VIDPNR Commissioner and sent 
to the VI Bureau of Internal Revenue. Greg Rhymer revised draft 
and said he would see to it being typed and signed. 
H. 
OSC letter to U.S. Coast Guard, dated September 12, 1989, 
inforining them that time and administrative constraints would not 
allow the development of an Inter-Agency Agreement for EPA to 
fund USCG involvement but that they will be welcome to observe 
site under USCG funding. 
I. 
September 18, 1989, OSC receives additional DCN, KE3085 for 
$262,00. This brings the total obligated funds for mitigation 
contracts to $1,262,000. 
J. 
Site Safety Plan developed by TAT is insufficient. OSC and 
assistant OSC will develop final plan. 
K. 
September 26, 1989, EPIC aerial photos taken; photos showed 
very little structural damage to VIChem. The roof to the dnim 
warehouse and labs appeared intact. All tanks appeared to be 
unaffected. 
L. 
September 27, 1989 overflight of site was unsuccessful 
because site air space was closed for air traffic control 
reasons. September 28, 1989, Carlos O'Neill and Greg Rhymer 
visited site and the site conditions were assessed ais stable and 
secure. The dogs were alive but some fence damage was noticed. 
VIDPNR agreed with EPA that site is not an emergency and clean-up 
can be postponed until support services are available. 
M. 
October 2, 1989, Assistant OSC spoke with ORC conceming 
status of the Consent for Access to Property for*. F. Schubert, 
owner of VIChem, stated to ORC on August 31, 1989 that he had 
received the form and that he would soon be returning the 
completed form. ORC has not yet received the completed form and 
will again contact Mr. Schubert. Also, Assistant OSC discussed 
possibility of placing liens on Vichem property, and any legal or 
financial ramifications of disaster relief, as a result of 
"Hugo", accruing to VIChem. 
3. 
FUTURE PLANS AND RECOMMENDATIONS: 
A. 
Continue to discuss hurricane impact on site with CFO, 
VIDPNR, OHM, and TAT. 
B. 
Coordinate clean-up operations with VIDPNR and prepare to 
mobilize when basic necessities (i.e., power, vater, and lodging) 
are restored. 
301513 
4. 
FINANCIAL ACCOUNTING: 
A. CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
$1,840,000 
$1,262,000 
$200,000 
B. UNOBLIGATED MITIGATION FUNDS REMAINING 
C. COSTS t BALANCES as of 9/29/89 
DCN 
KE3042 
KZ3069 
KE3073 
KE3085 
Subtotal 
OBLIGATED 
A.MOUNT 
$250,000 
500,000 
250,000 
262,000 
$1,262,000 
Other Costs 
TAT Salary\Travel as of 8/31/89 
EPA Salary\Travel as of 9/22/89 
Estimate of Total 
Expenditures to Date 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
1* 
PERCENTAGE OF $2 MILLION 
1* 
MITIGATION 
1% 
EXPENDED 
AMOUNT 
$7,116 
0 
0 
0 
TAT 
$105,000 
$0 
BALANCE 
$242,884 
500,000 
250,000 
262,000 
$7,116 $1,254,884 
0 
9,306 
$16,422 
EPA 
5% 
TAT 
0% 
FINAL POLREP. 
FUTURE 
POLREPS 
FORTHCOMING. X SUBMITTED BY 
^uglas R. Kl 
% $ - -
^^oT Douglis R. Kodama, 
On-Scene Coordinator 
Response and 
Prevention Branch 
DATE RELEASED Z>P c Z V ^ m ^ r 
2> 1 H O 7 
3 0 1 5 1 4 
U.S. LNVJRQNMENTAL PKOTECTION AGENCY 
POLLU r ION fgtIPORT 
DATE : i>j\^\-^^ V\%\ 
Region 11 
Respon-jc? ^nti Prevention Branch 
Edison, New Jersey 08837 
(201) b4b-8y30 - Commercial and FTS 
24 Hour Emergency 
TO: W. Muszynski, EPA 
5. Luftig, EPA 
R. Salkie, EPA 
M. Randol, EPA 
6. Pavlou, EPA 
E. Schaaf, EPA 
ERD, WH-548B 
(E-Mail) 
B. Sprague, EPA 
G. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
LEPC 
TAT 
POLREP NO.: 
SITE NU.: 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATI UN: 
AMOUNT: 
WATLR DUDY: 
Six (6) 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
800 Lab Chemicals, 400 Drums,'22 Tanks 
Ground water, Caribbean Sea 
1. 
H1 IUAI 1 ON; 
A. 
Site was impacted by hurricane "Hugo" frora September 17 
through September 19, 1989. 
Sc-ijlember 28, 1989, EPA and DPNR visited site and the siti 
condition'^ were assessed as stable and secure. 
2. 
ACnUN TAKEN: 
A. 
October 17, 1989, OSC contacted by Scott Silverlight, 
attorney for potential purchaser of VIChem facility. Potential 
purchaser interested in getting the plant operating in three to 
four months- OSC informed Mr. Silverlight that the EPA removal 
action may take nine months or longer and may be postponed even 
further due to island disruption caused by hurricane Hugo. 
USC al^ao informed Mr. Silverlight of the anticipated costs 
to conduct the clean up, types of materials present at the site, 
and wr)y VJAU and SCSK have been allowed to continue operating at 
the silt*. OSC referrt?d him to Lnforcement Programs concerning 
jnl ur ni.3l J tjii on any subsurlace remi'diation at the site. 
UiJlJ in lormed Enforcement Pro«jrams and Office of Regional 
301515 
':i]i 
Count.el jtjcjut his phone conversation with Mr. Silverlight. 
B. 
U(. tuber 24, 1989, OSC informed that Chief, RPB instructed 
the EHi:s contractor to prepare to mobilize to the site to repair 
the site's, perimeter fence and stabilize the site. 
Under the circumstances of St. Croix's devastated 
infrastructure, OSC has revised the scope of work for this first 
phase to securing the site (fence repair), and if possible, 
sampling, segregating and overpacking drums. Due to concerns 
for worker safety, on-site treatment of reactiwe materials may 
not be corjducted at this time. 
C. 
one coordinated with ERCS contractor, OH Materials, October 
24-27 deciding what equipment and supplies should be mobilized. 
A gaily trailer (food), decon trailer, office trailer (command 
post), equipment t r a i l e r j three generators, bobcat, passenger 
van, pick-u|) truck, microwave communications system, foam fire 
fighting unit and other appropriate response gear Are scheduled 
to be shipped from Elizabeth, NJ on Friday, October 27 and 
arrive in St. Croix on Thursday, November 2. All attempts to 
air lift the above equipment and supplies proved unsuccessful. 
The cost for this mobilization may range from •lOC^OOO to 
•200,000. 
A'j ot October 27, lodging for the ERCS contractor remains 
an unresoved issued 
i 
Due to the fact that the St. Croix hospital is not fully 
operational and outbreaks of typhoid and cholera may occur in 
the near future, OSC has requested an EMT certified Health and 
Safety Officer to monitor and treat the clean up crew as needed. 
D. 
Hei»pcMise Manager Arrives, on St. Croix October 26 with an 
electrician and structural engineer to assess electrical 
generator hook-up needs and structural integrity of the 
buildings. 
Initial entry by ERCS revealed water damage to the office 
Area, liowever no spills were noted in the lab or drum storage 
area. 
E. 
OLtober 26, 1989, OSC receives a copy of a letter sent from 
DPNR Commissioner Smith to the Director of the Virgin Islands 
Interna J Revenue Services dated October 11, 1989 requesting 
waiver- of the Virgin Islands Excise Tax for equipment and 
supplies shipped to St. Croix for EPA's removal action. CJSC 
will inquire as to the status o i IRS's decision. 
3. 
miUHi: PLANS AND RECOMMENDATIONS; 
A. 
OSC will arrive on St. Croix, November 1, 1989 and 
coordinate removal activities. OSC will instruct ERCS to 
mubili2e irew once equipment has A r r i v e d on-island. 
301516 
4• 
FINANCIAL ACCOUNTING: 
A. CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
$1,840,000 
$1,262,000 
$200,000 
B. UNOBLIGATED MITIGATION FUNDS REMAINING 
C. COSTS & BALANCES as of 9/29/89 
DCN 
K23042 
KI3069 
KE3073 
KE3085 
Subtotal 
OBLIGATED 
AMOUNT 
$250,000 
500,000 
250,000 
262,000 
EXPENDED 
>_MOUKT 
$7,116 
0 
0 
0 
TAT 
$105,000 
SO 
BALANCE 
$242,884 
500,000 
250,000 
262,000 
$1,262,000 
Other Costs 
TAT Salary\Travel as of 8/31/89 
EPA Salary\Travel as of 9/22/89 
Estimate of Total 
Expenditures to Date 
$7,11'> $1,2 54,88 4 
0 
9,30C> 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
U 
PERCENTAGE OF $2 MILLION 
MITIGATION 
1% 
$16,42? 
EPA 
5t 
TAT 
0% 
FINAL POLREP 
FUTURE 
POLREPS 
FORTHCOMING / SUBMITTED BY 
k 
fiT^ [/sgAjWsrv 
Kodama, 
On-Scene 
C o o r d i n a t o r 
Response and 
P r e v e n t i o n 
Branch 
301517 
U.S. liriV]hOli«£HTil. DhOTHCTlOH iOHrtCif 
t'UliJilUQtL-iLtlfDiil 
K . . . 
I' -. 
( 'z'. 
l u l l 
i l 
DATB: I Hovcfcibar 8, 
1989 
TO: 
C 
!•..(.' UII.I Prev»5nLio/i bl u>i(.-ii 
1.. How J e r s e y Ooti'jil 
'..•1H-U730 - CtLiiorcihl aiij Vl'^ 
24 Hour Eiior^tana-y 
SivitA.un-Bri«toff, 
BPA 
hw»..yiiuki, SPA 
L u f t i g . KPA 
S a l k i e , BPA 
H a r s h a l l , EPA 
P a v l o u , BPA 
NH-S48B 
B K a i l ) 
, S p r a ^ t , BPA 
G. ZaohoB, BPA 
P . O t l a b t r t , BPA 
A.' S B i t h , 
?IDPIR 
L^PC 
TAT 
¥ . 
S. 
R-
a] 
B 
B 
0 
i'i.l h-ci 
hi'). : 
!•'.:! i.i--TA«'i' • 
(M A.'".:-IFJCATION : 
:",UiilirK. 
J.'.!-"AiTTO.i . 
.••.KMUhT 
W/.TLh luiuY: 
A l c o h o l s , S(.l vtiita, 
Acids 
SoVBl. 
( V ) 
4V 
l.ab 
Cj.t-ljiciil; 
Mao or 
Virgin IjJuJifl C h e n i c a l Coii,'»i;iV (VIChem) 
S t . Crojjf. UO V i r g i n 
Itsle^nde 
600 Lub C l m c i c a l a . 400 Druua, 22 Tank* 
Grojrifl water, Caribbean SJea 
i 
i^liUcJLLnH: 
I . : •iateugB frvi. hurricaiic liLifo wbd uinaV. 
I ' o r t i o n s of 
A 
:; 
1.1. 1 --i icoi.Br feju,B wert> kiiockwd du«f;. 
Ho sp'illfc of 
a a t t r i a l s 
Hill ,l...l.t.-d t o s t o r e , deiiiilto Juoit^-c t o roof of one l a b . 
BRCS 
c-.:;-. rr <u lur (OK Kateciiils) d i r t c t e d 
Lo B o b i l i z b t o K i t e t o 
r e p a i r 
y.i . It. .:•'z.y fojiue, 
tui.l if fu-.s^ il i e , f;ntiple, s t a b i l J ' B 
(ovefp»ck>, 
(ii..i {..11^ I'cilutu 
kjnLoiJ^lb. 
MiQrt TAKKH: 
f. 
t .. 
(ii.i.'btr 3 1 , lOctf. 
OSC Cuiitinuea r e n o v a l ' u ^ b i 1 i z a t i o n 
.11.f.l lull and C'rr.i-fcrt»l i<yi< fron Bdibon 6fflb*r. 
OSC a u t h o r i z « B 
:..:iiir 
lo&dt uf uvoTt'ock druLb, trauxia k i t for • e d i c (EMT 
; i{.!ulUi hi.d S a r r l y O f f i c e r ) , 
c y l i n d e r 
w ^ a i r a c k s , 
and 
. i ..li uf [tbri'.al (.»oH f; >. i- L'HCS: R8Bi>ur._-. Ku.iager, 
F i e l d 
...i ;.iloriiB t.hux, ,.. 
. ./wriii" OCC i I.. • 
. . VTCliCk. Prej.. . 
.c 
tPA ( v e r b a l I. 
1.1'/. *i a c t i o n . 
I l i e 
s t a t u a 
'. I "Y B t i l l 
have 
. but 
t h a t 
• Hi he Mould 
3 0 1 5 1 8 ^ ~ 
" 
. - 
i 
• 
' . ' • V I -
•i>".v'; iuforuor^ thfct h i ] 
fw>Ji- tl ui Itjra (dtinoi., c d i l 7 » 
o f f i c e 
.....I .-,-1 ii-ijuiit t.rttilorb), 
luiboQt, p i c k - u p trv ck unri two 100 KM 
j<;ii,-i .'.K>j & w i l l ar.'ive on Gt 
Cri.ix Novenbor 1 or 
2 . 
,.^.••. Leo kjBij b© . a . - i I t b l e a t 
priuon 
itliin ona uontjh 
OSC t r i l l 
i n s t r u c t 
•rd l i n e a s veXl ua Eicrowave 
.••:.<.' xiifi.."uud .l.b I v >•.*>... 
.1.. 
.li.iTtex u i l n t'lOk. •.>itr.. 
i'i.ri I »• I'l-cp f'honts 'iine;> 
f o r 
i" » ' l . ^ ) j '. 1 o i l . 
!'• 
hi.vjkiber 1. 35)60. 0:3C fj.-io 
t o S t . C r o i x . 
lihCS B o b i l i r e o 
jM.iLi'il crew (ReGponae Hnnt^ur, 
F i e l d C l e r k , 
ajid 
two 
i; 1 Uv. 1. X i o j aiicj) 
i . 1 -
I !- / 
: • 
J 
Mw.ciabor 2, 1W88, OSC teu^oi or i l y Horkfl out of FBMA D i a a s t e r 
.; (Jffice Ar.nex, and cuoriJ iii&tos with DPNR on s t a t u s of 
e x c i a e 
-.'.vi-.r. 
OSC i n f o r t o J 
t.luil. VI I n t b r n a l Revenue 
S a r v i c e 
. .M.; t.lmt ihes wnivftr cf tlit; e x c i s e tax i'« r.pproprimte 
'. !.i.ui:li a tirivute i;t.ntro. l o / i s s h i p p i n g bnd utting » a t © r i B l s . 
^•.^etJJ ut QjJi.roiJr i i» Lo r.-vtu eJid procedui'cs t o 
c l e a r 
i .1 .1 hfid c-vju Ji'i^oii I tJiruLiuli Cu^tOBS. 
; . ^ . ; i 
y , . \ 
_ .; r ». 
f. l l 
'.nforuoJ K K O S i.ubi.-.>..i . octor (Lynan JBri.-li&rs) on-island 
l o g 
on thb inuLul luL ).>«. of sicrovavW cocAunicationii 
. 1. . 
I 
i • . 
k / i > r i 
K-iuU hourn, O^C xir>et.£> wiih Jios-ponae Har\a£«r and on9 
i i j i i h u . 
Three OHH pt-rscnnel a r e stayinji; on S t . Thosaa and 
.i: i..^ Lu S t . Croix. 
T))oy vuria a b l e t o f|ind l o d f i n f f o r ona 
t.rjvian on S t . C r o i x , 
ho>«'.;ver, h o t e l doep n o t hAT9 
ti i.:iLy, p)ioijbt> ur w b t e r . 
Ali four OHM p e r s o n n v l v i l l 
s t a y 
( 
TliuBHis tonigliL ajid c h ^ r t b r p l a n e t o opiuDute bet««*n 
I,-ill 
OSC will ucet DilM bl a i r p o r t a t 1800 h o u r s t o g a t 
1. 
'.I OHM'e s e a r c h for on i s l a n d lodging', r e n t a l Oft7f 
(thajr 
nrttiiitly uhiiii toxj 
atiTM i c e ) and if t r a i l a r B a r r i r e d 
in 
nuuberb l o r t r e i l e r a and s u p p l l a a 
t t 
p p l i u s tirrivud in S t . Croix t o d a f 
a t 
uSC aota 
waybill 
h'.i :.••'(. nrit'i inforued 
su 
Ittj^iTii via Navieras de P u e r t o Kiuo. 
IbJO iiuLirs, DSC ttofetb Cihh a t a i r p o r t 
pr 
I.., :..t 
TlKieaa. 
OHM wat not sl.Je t o 
f i n d ' o n -
r....iul > arti and wafa i n f o r c e J 
thai /lone of 
t h 
:.w,i 1 ;'-... have a r r i v e d 
in the t ^ r t . 
OHM depa 
OB 
0700 
lor t o t b t i r 
f l i g h t 
i s l a n d l o d g i n g or 
i r e i l a r s 
or 
r t s f o r S t . 
T h o s a s . 
. w.-ril i nut ca v« J I (. £nji.^.. ^ ' f i o t i and ^UCS Progri 
'..i bi>() i^; iiii'urt.1.J tl.i.t 
i.M.jlers and; s u p p l i e s a r e due in 
. t.Mturvuv, Hvjvetbcr ^ .-. i O'OO h o u r s . lEdiaon o f f l o e 
has 
I littL it. i./iy bu t..i..;.:i .:... t . £ e t hard jlinH phone hook ups 
re-jjcJt 
K i t e / « 
VI 
V iw i Lb 
b i l l . 
a J i J 
»,r».J by Ms 
Woej' 
{tjpJione CoBPar.y (VITJJtCO). 
1 
3 0 1 5 1 9 
a.t>. i_ with Eate Mest}, t^ite 
r a a i d s n t . 
i h u t Iw,. <<ther hurrlchi.f 
h o s a l e a a 
I 
. r 
pnorln fsre l i v i n g tn r.'.l.' vi*.)i h*>r 
Ofir B " ! ^ '. • ' ' *• <• i.-r..;irj \^Q 
p o n r l b l c t o h i r e .*^Cr>F. f-i':'>c!'. '.]nftn iv gwn-d l}-''''^rr- »,r,,> 
, . . , , . . i j , . _ 
wliilo P.PA/OHM i s o f f - y j t ' ? . 
H?. ^''•vv hnr. hmtZ v ^••'i'lrg 
o)l."with 
her f>srLner, b u t F t i l l 
''-i*: ^.hnrt,,,., Jp thn b<jr {''..-••'-, 
S^** ^.-R? 
roljM-lunt t o havft ETA v.v.o ilm n t t s r k dngn, I'Ut oxp"! "R i rir-d t h a t 
ehn hpn never had n trrsprtns/vsndp.l i s n / r o b b o f y 
prp»-ler, ^i. tho 
B i t e nnd nould voliml.Brrly look a f t r our 
ftquir^"*^* '"""^ rjurrlieg 
ovnr-nijjht. .She f o l t 
< IIM p i t - vni'ld hn rnfr!.*^'"' 
-^'oure. 
D. 
Noveaber 3 , 1999, 0100 h o u r s , OSC iJoes j : ' ^ Mrvinr^r n f r i o p a t 
p o r t and was inforr^H 
thnt. four t r n i l o r r 
a.-rlv^H ->f. TnuBdp.y, 
October 3 1 . 
OSC proceedn t c uStn ^nH rn**?:- T.yrnn DiC'l'"«Tn nn-J TITFJ.CO. 
VITEf.CO i s a b l e to p r o v i d e two " h i r d 
l i n e " conn n d i r.-«n «nd T.yjcnn 
B r o t h e r s w i l l l a y l i n e Ihrnuj^h pprT>'^' »'u< e>"ly '''"• '"'"^ ff 
"oungle" 
in order t o r e a c h 
s i t e . 
OSC Boets with 0H><, r]e>r«? *.hrnri tre.il'-r!- 
' ' • • - • T ! - ^nr^'.t^ns. 
Docon »rid e q u i p n e n t t r o i l e r R ar «< ^.'-nnapcr <-.«*rJ "r "•»•. r- -r * i.i. pjt.o. 
Thf< th«rd t r a i l o r 
( g a i l y ) w i l l nrrW»» rn-r5'«* ' -.r-- • v.-. 
J]i» 
o t f i o r 
t r a i l e r i s cinpiMji pnd unBPConnl.ed f c r . 
"Hard l i n e " phcnpi* i n n t s l l e d i n ' ' working 
^vr '.'.• l.hr 
trrr-"*T »ry n a t u r e of t h e " ' "hard l i n e " hooV up'- ., ''"'^ •;,.--;-'»^-.. <n 
p r o i - ' ^ e ^ 
w i t h 
B i C r o w - v - 
- y r ' n r 
fjin'-'! 
-^n;. th^'T 
\.- •';""' 
-• ] i'- 1.« 
UHH d e p a r t s for fi 
Thorn-: »i 3 9^n h o u r s . 
'^"" ^^ • • ' " : < ' 
lodj!'""^ on S t . Croix fo- 1'-imrrtjw. 
Since o f f i - ' 
' T - . ' ? - - - " . I ^ 
oth^r f»'juipBent and FDpt'lics nrn du*- i n t o p c ' 
'' •' ^''•'•" , -T-'.' 
dnridoi* to B O b i l i r e »<dH''. inni"! RRCr. p"'-7onn''1 
' • - • ' - •»• 
? '!.''"«.n 
up T'":hB, 1 l a b o r e r , 
aixl 1 c a r p e n t e r ) . 
n:'>C a e e t s with D. v-)"ton of VIAG a t a i t q . 
E. 
Hoveaber 4 , IfiPn. o T T^orkr v - t h CEP rn '•••••n-^r' '.,r: VTCSPTI 
p r e s s 
r e l e a s e . 
OHH e l e c t r i c i a n 
e . t ' T p t B t o r^na'-r VJChw*-''- r n - ' e r w t c r . 
Klp»^ir«r power i c in'rr»^ ''.'.^nt fr>' '.'^^icr" nrnr. - ' '• • < Ir*!nr;. 
f"'^' coordln««.er> ^•- " *-MTPI<"'I •-.«J ... ...i^,-i.. 
, 
....-i._„p 
f{ir 
f.-.r.r 
l i n o B 
f o r r ^ r • • - v f , 
p y r t r r 
^'-.'ly trailer r*bc'.' ^^ cite. 
Or.r infoTBed by 0. V^Rfnn cf VT^G thwt r'T«-':*-!r- pcle on-
giiM br-. elctricity m ^ "nly needr n hnok-up. 
V. 
HoveBber 5. JPP9. 0«00 hcurr OHM on-r.. -u" 
I'nloadinS 
of dbn-.n and equipront trnSlers inti» cffirn arr" r^'" builrtitig. 
Field Clerk and Cook depur*. t.n look for additicnn] .T<;r.t«l cars 
and ptock up on food for lunch and liquidr. 
Lyren Prothi^rB on-
BCoii' end at Bicrowpvp r'n»ion (off-Fit.e) vorVfia nr ricrowfivB 
301520 
sysl''«i p r e p a r a t i o n . 
Tl ^ «n «••'-,>wn v- -'..fit.Vnn «;! 
Btojtr ovnod by ?,nT)\'• n.n-- r^uir. P I M ' '.'>'?, i-iT---
fvjl'- 
^i«rit«llnti(M^ - r < ''^ i r 
p v j i ' e M y . 
M 
r t n p s b u i l t for nqi'ipi.-n* 
t r - ' l " - . 
Wotrr 
»-r.^ V-.-* • • c- .''rcn on-
R i t e h y d r a n t t o de.eon. 
"IT*!- u n j l 
ond f J T 
hC'-»- " " ' 
ur -•:• 'J-UB 
wprrhnuoe. 
B l e c t r 3r im' i.'r»P t. iPU"»p in a t t e r i p t r T - r i • p*" cm-hite 
goii-tfitor. 
The vDl<ef»r. r»'f»iilntor 
'"or th? r.H.r 
K"-- ~»^'•'" Jr -"<-
f u n c t i o n i n g p r o p e r l y , 
vnltoRo o.f ci Intifi)? by K'M v u J l ? . 
"'.^•.'•^ 
hourn OSC c o n d u c t s (JV^rfliiiM. of viCbHC Bit*-, 
!.y.-r'. n,.,.tb--v 
Brruiir'f.- for a i r froiphl 
o.<* r.'t:r«^wnve iJinbon e.-' 
•••]•• = r' • r - f 
I 
(i:^C drafts Been fcr rPKP C O O . - T 1 ntf c'«"M" •-",-. p-''»n:--;rr Dnd 
inforiJHtional BoetJMg o-> VTChen pi'-e. 
R-t.j.ir-r'- ...,,.•"»--:e by 
PulJnp, Fire, KMT, DPHP., VITKHA nn-" CM-rccMn:. 
'••'': THqi"?-=*.e 
BBotinG to be Rohodnlt-d HovorH^^r '', «. or "^, i-!'- '-i --^T 3'--^K 
and Mtcbiliration 
jirtivitiBK. 
'C. 
G. 
Hoveaber B, 19Pfi, 9000 b">)r'.i 'JH" np 3-rnr 
-••!» •^--f--,-
BHfot.y B e a t i n g . 
Mirrownve r y n t e u «rriv©E. 
C r r p e r ' 
ropijirjnff 
binl'JJng roof and d r H i r i n n B»?t»»r fm^j rrflirifl 
*-tr,: 
( - - - - t i - . o 
c u n t r n i ) . 
OSC inforrr^^^ •vo l.'-nil*':-; cf rjr-^rr--' 
•' 
I - • .rl or 
Hovnr.bor 2. 
nil** to lack of gen'!r»i'"T'« and nn-i'• t r i r !.y o r i ' - - - - 
--.-•i-':' 
t i r r . 0.<'«C c o n a i d e r a »5 r Tr-i/^ht. n^" • 1 "0 kf :u»- 
-- 
""".* 
l?rr- 
rhonc working r:|..)-mii CB P y . 
'^'^''. d e l i v e r e d r ^ f t 
'••>••' i r f . c r - 
•«••-^c-f "ir" -i"-
Crow u s i n g wee.d oH^^erK t o «^1«»«i- V9g'>1 B t i'•• 
neodiii}' r e p a i r . 
Posponr" Mftnegor v i l l 
nhock - ' [-^r'. t r ^io 
jf 
overi.?»<'k druBS havo nrr'^'ftJ. 
Cook r - p c r t r 
I.'i »''n-.<'..- »-f.5«. t.'.- >fet 
i n t o Pu«»blo groce.ry 
K I O ' " , Grpnd "I'ion s t i l l 
r !-'-«•? 
r-in-p "o 
prnr """•» for g a i l y , r'"r>v ' iiv? f h o r r ^ ^ i 
gri"*! 
r.--
1 
HI'Towave d i s h ref 
-t: on ^ i t c 
nnrl J» t. of ^ •-= < ,- 
. f „ i i , . . _ 
Nor lb vide of fftnoo 
lin' 
- I c o r ^ d -<*' vn^..!.*.! lo:- ' v . • • ' • - - • ' 
'."-Wr 
ContiniT'.ns a i r B o n i t " r i - ^ vM>^ cxr ^ ">• " r - t r r t?"' ''•'•: -'-••••••' -.-
e3".v-'<d readingB Hu-^i'-r 
' ^-o. fir.^.--;r 
r r ^ - ' - . ' ^ - 
' •• 
' " 
-.:' 
r.l •••». •!., drop off b ' ••-•_' ' .' n^' 
r ^ ' 
.r'o.-: 
r-„.;....• 
_. 
. • ,,. 
tr 
' ' ' ' ' T 
ceiJin/? ' ".'' 
"-i ! r p« i • bn ^ II ii7>; 
/ 
•'/^pair of northrr-^ ••"•^ticn of p r T i u i ' ' ' ' r 
f - 
- ' y c-hH-ft 
tetik- 
- v i t i a t e d . 
Kler.f.r 5 ci "ni p l a r v t ) : e j c ? t r i r r . . ' 
•s'j'.'i 
for 
t r u i K r 
c o n n e c t i o n s . 
OFT apprnvcp " w 
froigM 
'•<• T^? kv 
geiT-;: r l o r . 
OSC infnreerl by Edjpon 
t h a t P'^A pr>r • ir.--! v c r k i n g on 
hiirri (•''.>'e daBage sav an »dd t.b.ni Hr'-ifr-^r hnr •• vf'-.r^r-ni'ir 
nnd 
bobchi 
for r e n t . 
0.*iC jrtids e l r c t r i c i m 
to pnrr 
tn 
•••vvire ebout 
thn;.-e ) 1 OBS and check s r r i n l 
niirbpr'- <o Ban :T • ho"'- err. 
Y P A ' H . 
K l t t i t r i n i a n r e p o r t s *hfl< w.Mvirres v.,p.w notinnjy "?-'•'•;« l^r 
edM, 
g e n e r a t o r or b o b c a t . 
3 0 1 5 2 1 
nPC infoTBed t h e t i «-> ifen«*r»it-'- . •pir'k up '•u'-l 
e-vH hnbcnt 
. j - . i l y b«^iiio li.t..l.;d Oil jJiii' in Gan Jyaii today and due to 
.. i:c. Ctoi-j. un WcdiicJ.iu) . 
OSC cancepe a i r l i f t 
of 100 kw 
I. 
Crfiitc 
t r a i l e r 
and ovtrpacka Bay'be a v a i l a b l e 
today 
i ..iw thrciJijb TM? ( s h i p p e r ) . 
' 
.<,....*.bci 
7, 
l&o3. 0:>i; hcc-uiipuuies H. Chpn^f of RPB to WAPA 
.1. wAPA l i u r 
tt.uiM!iviuur 
VlChfii e l e o t r i c p o l e and r e q u e s t s 
..t J h..f>u-\jii. 
Thir. i-ower will bo good For b u i l d i n g 
a i r 
1.1.1.It: Ouly. 
If »!Al'A pu».cr i s o b t a i n e d e l e c t r i c i a n 
w i l l 
: i <!..;.t'v..rtLr :ii 1..JL ioii« LK p r e v e n t fp.re h a z a r d . 
Thia 
-<.- tr.nncil 
I f i.5.jd to t l 6 p down WAPAl power (480) for uae 
; r.s \^:'.y.O). 
nM'h vc.<Ui.i.ts .'rloaring pbtli t o pole BO they 
.. !.i...:k i;. wi.vl ciK;ck t r aiis, f ;> r o t r B . 
|*APA w i l l r e t u r n 
at 
:. . . .'s.. u b 
i ;3 I. 1 iju'i c d . 
•i..:ivi.tti .'>:jt. rur b / 1 2 - y / l 5 and 1 0 / 2 4 - 1 1 / 3 . 
Review 
b.'j'ti. 
Proi-iiiirt a r r i v t s , 
however jfally propane tank* 
11 
<n,| f u l l 
Carpcitit«rt> o o n t i n u e b u i l i i n g 
r e p a i r s ^ 
ii.i 
rouf. 
K l e o t r i n i h i i t-untinues t r a i l e r 
hook-ups. 
.1... c ](-«.. I ic:i .i;i (phrir.c) d«jsob«atd f roe e i t e . 
TAT haa 
b.-^u .i'jL.ii ie.-i t.u work with EPA/TA" on 
h u r r i o a n t 
jriiii2 TAT";. i i r ; , t f u l l 
day on-Bcen» thoy inventory BRCS 
i..J fiji.pl ii;:i cii Ditt;. 
Medio (BMT C e r t i f i e d 
h e a l t h and 
i. .-.J ) u r r i . o i i o n e i t t r . 
ERCS t r y i n g t o d e t e r a i n e how 
hi.;* fa Ili p.'od t o S t . 
C r o i x . 
I 
' 
.••1 IvbJi'wiiwo Ht>^>ri«{er ^-..1 to p o r t t o check on two t r a i l e r s 
i-,v<.rp8:k3 and office- t r a i l e r . 
Overpack t r e i l e r a 
have 
}, .jffit:t, 
L r a i l o r cltiared t h r o u g h Custosa and scheduled 
v»ir,(J 1-v :;ite tusiorruw. 
Mo g e n e r a t o r s , bobo»t or p i o k -
..-. J v,oiiV.iiii.r.-» i.o ». Icwr puth to u t i l i t y p o l e . 
P o r t a John 
. . i - u i L e . 
"iiurd l i n e " ^^hon^s w o r k i n g ' a p o r a d i o a l l y , 
VAPA 
... 
it 
k i l l 
Li.kt^ I.WO L(< tliree weeks t p g e t e l e c t r i c i t y 
t o 
i.tiCJ titrtrLa x:Jebrin^ vi.£utBLion a l o n g , w e s t e r n p o r t i o n of 
i r.,- fuitce neuJiiiiJ 
r e p a i r . 
. i i u i 
\Taot.ti k i t hirivfro : . n - 9 i t e . 
Lab roof 
r e p a i r e d . 
. . 
<AiiU<->r bei.L w h i l e dikft^i'^E 
f e n c e poBt holu, s p a r e auger 
-l.l I'l-oi.:^;. 
:>uil 
id e x t r c L o l y h a r d . 
B x t r e s e l y 
low 
i.k..>U|^ 
«•'r e w . 
h 
H . i 
V. ; 
t 
1 
. • 
,>. . . . A i b v - r 
d , 
. .. i J ia 
t h e r 
,. 
W.ZiL i s 
St 
: ,.. 
.1V 
? \ :^ 
. . . . 1 : be 
. . 
i J * r I L f c - . 
. 
f i t . 
1 
i 
i . I < • K 
: 
b 
u 
iubvr d, 
JbOQ, htiniu ^^..^ale anong oraw i s e x t r e B a l y 
lov. 
i:s t h e r e no u i r c o n d i t i o n i n g a t t h e I s i t e , but t h e h o t e l 
i i s steyiini bnu no a i r c o n d i t i o n i n a and t u r n s off 
i t s 
.iV ?\:^C\ b .iirs tii.d t h r BosquitOBS a r e bad. 
Thia 
ri.-.i. i-f u t i i m d t a l a r i a 
haa acrjfu.ly 
daBponed 
301522 
I 
wit.. J^L-4,.»-.».-.o n li.i li ti t.z. s h i p a i t j . 
t^vusrators, 
.ii> ivuck >%ill M-jt be dockod u n t i l 
1300 houra and 
\ 1. 
I 
»• 
k 
C; 
• • i. 
u^tjiprent u n t i l 
toaorrow 
III . u f ••> 
1.1 urdwr tCi t r y to buoyt crtiw B o r a l e , w i l l 
i n s t r u c t 
Roaponso 
^ -...t.,,!.-. i b n t u f t e r 
tlie fence iw r e p a i r e d otof may have t h e 
r e s t 
...;• 1 i... (liiy off, 
if tlitsy want. 
" u r i i o 
t r t i l r - r 
urrivoB on a i t e . 
Power luger blows engine 
.>-. i. 
•:'afc;^"tl Ifitt .-u3t Jiole. 
OSC c o o r d i n a t o a with C o n t r a c t s 
in 
I-.: r * v . i . ( i i . j 
to cbuii^u pur dicu i.u a c t u a l s i b e i s t b n c a for ERCS. 
/•.... :'.ii:.iMi offict: iz.r E.~.j^;i rit aji.u iri t h i a s a t p e r . 
Lysan 
B r o t h e r s 
i. ••i--ii.j, .:' phc.i;r 
fty_tok. 
LiJ t r;. i 1 o r . 
1 
.it.u.. up t . . i . w\.i.i-j, 
iioii while r e p i i i r i n j 
f e n c e . 
.••1 Xitu.. k,v..uJiJ, I bo no".. <.iitored forward of the s t e a l 
shank 
:. • r...ih b!/oLa. 
ttoJic 
ttdui..jutfjra 
f i r s t 
^id i n j u r e d 
haa had 
:.ji;;i. wltliiii tJiu lt.3t yitiT. 
Clean upjtecJj 
v o l u n t a r i l y 
. 1 . 
11.1 HLi/k 
Pnuues workir>^ s i p o r a d i c a l l j . 
. . i/.iit.u.' 
foncw Jt> rcptiiii:.] and two s t r a n d s of barbed wire 
I . 
;•• t . t i l d d . 
Oiil/ tww clfeaai up t e c h s ( i n c l u d i n g 
i n j u r e d ) 
.:. . . u 
1.1. tukw afttjri.ijon 
off. 
.:,•' ,-ii:k:> up voltage- re^iuliitor for a i t o jgen&rhtor. 
1500 
iu jij:<t i^ci.tiini ill t c I ' o r t . 
B l e q t r i c i a i i 
f i n d s 
i i i..;t 
rcCult»'_-..r i:. broko.i a j sJiipped, ino power. 
...:.'iU 
tjmL£\'ZJ.hv i<.-:\.'i;hftHnii,-.Tl(iKa.; 
i 
,,, t 11. <:ujiJ>ti t u safo rcAiuvul 
a c t i o n . 
I ...-. UBLiuii rt-juoiiiE de:iptrfatc and no g e n e r a t o r s Arv 
I w. 1 1 dejuob crew. 
• 
J 
.1 /iiiii.liil^Ai;CLa^allflii: 
A 
•. .i...il P r o j e c t C o i l i n g 
AuDiorized 
[•> 
'...llii Ku!id3 Authorized 
for 
Mil.iyaliuji Conti a r t s at> of 
b / 8 / b 9 
0 
i,. . nui r.urci for Mitigaliuii 
C o n t r a c t e 
: I. 
£»,ount UbiijiaVcJ t o 1>C« LB3042 
. b 
KBtiBbled BApcnditurco as of 
1 1 / 5 / ^ 8 
: 
ttaJanoe 
hekinininii 
1 
Amount O b l i ^ a t n J to D'H EE30BB 
'; 
h.-il juatnd E^i'tind 1 tuj'B& aa of 
3 0 1 5 2 3 
nofc.h'• li ing itnlaucu 
.-...i.^ji.t ObUtutesil 
tu bOh ttSO'/S 
• 1,640,000 
1,262,000 
250,000 
148,686 
100,114 
500,000 
-0-
600,000 
250,000 
. J 
U.S. ENVIROHMENTXL PROTECTION AGENCY 
POLLUTION REPORT 
M 
Region II 
Response and Prevention Branch 
Edison, Nev Jersey 08837 
(201) 548-8730- Commercial and TTS 
24 Hour Esergenc; 
DATE: November 17, 19 89 
T0{ C. Sidamon-Eristoff, 
EPA 
W. Xuszynski, EPA 
8. Luftig, EPA 
R. SalXie, BPA 
J. Xarshall, BPA 
O. Pavlou, EPA 
ERD, WE-548B 
(E-Xail) 
B. Sprague, EPA 
0. Zachos, BPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
LEPC 
TAT 
Eight 
(8) 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Kajor 
Virgin Island Chemical Company (VIChem) 
St. Croiz, US Virgin Islands 
800 Lab Chemicals, 400 Drums, 22 Tanks 
Ground vater, Caribbean Sea 
POLREP NO.: 
SITE NO.: 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
1. 
SITUATION; 
A. 
Site damage from hurricane Hugo vas minor. Portions of the 
perimeter fence vere Icnoclced dovn. 
Ko spills of materials 
attributed to storm, despite damage to roof of cne lab. 
ERCS 
contractor (OE Materials) directed to mobilise to site to repair 
perimeter fence, and if possible, sample, stabilise (overpack), 
and segregate materials. 
2. 
ACTION TAKEN: 
A. 
November 9, 1989, OSC receives vaybill.s for tvo generators 
and bobcat, shipper informed Response Manager that pick-up truck 
is still in San Juan. OSC and Response Manager go to port to clear 
Customs and arrange for transport of generators and bobcat from the 
port to the site. After clearing Customs, OSC and Response Manager 
accompany transporter to dock and see that the pick-up truck is 
also at the port. OSC contacts shipper and is given vaybill for 
pick-up truck, and eventually clears Customs vith some difficulty. 
Generators are 10 kv and not 100 kv generators. Apparently, the 
retailer shipped the vrong size generators, OEM had purchased tvo 
100 kv generators. May be able to supply enough pover for the 
301524 
O 
i i - " ' * i -
/ 
F £.10 ST r. : '.. I >. 
I 
i 
i. 
K i i t J u t v t e d 
L A I - O I U I i t u x ' e ^ 
a u 
o f 
J I 
KoBaiiilng Dalajjce 
\j 
li.M.bl iguted Balance 
RoBiij.ning 
!•: 
h.-.i it-ulc of Totul Expendi turefi 
li 
DuLc- f o r A l l M i t i g a t i o n 
C o n t r a c t s 
I 
. •.;,;.-.; 
K x L r u i i U r o i 
C O i i t B 
. 
VhT bnlary/LiftVcl aa of 
11/03/89 
KPA u a l u r ^ / t r a v e l a& ui' 13/6/68 
;i 
iiiu.1 l-ixi-enditiJicb X of $2 M i l l i o n 
; - . 
:-...{txHii of Ti.'tol P r o j e c t 
C e i l i n g 
•i J . M ' _ . 
KUTUhB 
POLRKPS 
, / 
FDKTJjCOMlMG K.. liUbMJTTKD BY 
- 0 -
250,000 
-0-
149,888 
16,234 
15,300 
9.11 
9.9Z 
Dduglas7K. 
l o d A s t , 
On-Soene C o o r d i n a t o r 
Response and 
P r e v e n t i o n Branofa 
DATB RKLBASBD. fi\.o.l6K:^ 
301525 
office trailer lighting and air conditioning, but these generators 
vill not supply adequate lighting for inside the varehouse and 
labs. OSC considers demobing crev. 
OEM can airlift a 100 kv generator through American Airlines, 
however EPA vill have to f&z American a recjuest since the airline 
can only airlift emergency relief supplies for private companies. 
OSC coordinates vith EQ-Contracts attempting to get actual 
subsistence for ERCS contractor. Contracting Officer and RPB Chief 
call back OSC and inform him that CO haa authorised actual 
subsistence for ERCS and vill send OSC a memo confirming this 
matter. 
Ths cloan-up tech vho stepped on a nail yesterday vas informed 
by the local police last night that his vife is in the hospital (no 
phones available at hotel). This clean-up tech demobed today. 
B. 
November 10, 1989, OSC completes POLREP 7 and gives to TAT 
for distribution. OEM having difficulty finding a 100 kv generator 
vhich vill fit on air craft. Generator vhich does fit inside jet 
vill have to be purchased in Columbus, Ohio and driven to JPX 
Airport by 0700 hours tomorrov in order reach St. Croiz Airport by 
tomorrov afternoon. Pev transporters vork over the veekend, so ve 
vill have difficulty^ getting the generator delivered from the 
airport to the site. Due to the xineertainty that a generator vill 
be airlifted to the site, OSC requests EPA to ask rsMA if EPA can 
rent, buy or borrov a generator, this appears doubtful since VIChem 
is a superfund action and not hurricane relief related. OSC goes 
to Eess and requests a generator from Eess. P. Rube* of Bess vill 
look into it and ask that the OSC return tomorrov since Eess does 
not have vorking phones. OSC also asks Mr. Rubee if he thought 
that Eess may consider recycling some of the materials from the 
VIChem site. Ee replied that Eess vas not interested. 
Stairs built for office trailer. ERCS begins staging of lab 
reagents and drums. 
Generators are hooked up for lighting in 
varehouse (minimal lighting) and office trailer air conditioning. 
Demand from office trailer is too great and generator vorks for no 
more than ten minutes. 
OSC informed that tvo people at the PEMA Disaster Pisld Office 
Annex have come dovn vith Dengue Pever. 
OSC informs medic. 
Response Manager and TAT. Crev morale drastically affected by this 
news. Ask ERCS and TAT to research Dengue Pever. 
While staging thirty of the drums in the varehouse, tvo of 
the drums developed leaks. These drums appeared to be in good 
condition, but use of a drum cart as opposed to a remote handling 
drum grappler, vas apparently too much rough handling. 
ERCS 
experienced break-through in respiratory protection (Level C). 
TAT conducted Eot Zone perimeter air monitoring and found seven 
units on the hnu. All Eot Zone operations cease. 
301526 
OSC receives the folloving information on Dengue Pever from 
TAT: 
Description-acute, febrile epidemic disease, mosquito 
transmitted virus. 
Incubation 3-15 days, usually 5-6 days. 
Symptoms-seldom fatal, tvo fever periods vith intermission, skin 
eruptions similar to measles, severe pain in muscles and joints, 
high temperature, lazy, loss of appetite, diminished urine, 
irritability. Treatment-no specific treatment, analgesic sedative 
treatment. 
A safe removal action cannot be conducted at this time. 
Additional equipment and supplies are necessary. Island conditions 
vill have to improve or stabilise. 
OSC demobs crsv except for Response Manager, Poreman and Pield 
Clerk. 
TAT informs OSC that air monitoring shov no readings above 
one unit along the Eot Zone perimeter. 
C. 
November 11, 1989, ERCS secures eq^uipment on-site and posts 
varning signs on building entrances. 
OSC goes to Eess and is 
inforsdd that overnight Eess had tvo generators stop vorking. Eess 
has no extra generators to loan to EPA. OSC informed that 125 kv 
generator is on American air freight and vill arrive at airport . 
this afternoon at 1500 hours. ERCS looks for security firm to 1 
guard site vhile EPA/ERCS are off-site. 
Ko security services 
available on St. Croiz. ERCS vill look for security guards on St. 
Thomas, hovever either no phones or not ansvering. 
ERCS and OSC receive 125 kv generator at airport. 
Pev 
transporters are available over veekend, so car carry-all is hired. 
This process takes tvo hours even though site is less than one mile 
from airport. Carry-all is also used to transport bobcat from port 
to site. OSC must clear generator through Customs on Monday. 
D. 
November 12, 1989, OSC picks up Chief, RPB at airport and 
tours the site vith him. 
E. 
November 13, 1989, vaybill for generator has not arrived at 
American air freight office yet. OSC leaves mote for other EPA 
OSCs on island to clear generator through Customs vhen vaybill is 
available. 
OSC flies to Kevark, NJ. 
7. 
November 14, 1989, J. Rotola clears generator through Customs. 
OSC had previously decided to leave the trailers containing drum 
overpacks at the port until ERCS is remobilised to the site. The 
monthly rental charge for these trailers is minor, the port may be 
more secure than the site, and ve may use trailers to store drums 
vhen they arrive on-site. 
ERCS informs OSC that they have found a security service on 
Puerto Rico. This service vill cost $4000-$5000 per veek for a 24 
301527 
.: i 
hour guard service. 
It is the OSC's opinion that this guard 
service is too costly, vill have minimal impact on security (may 
make the site less secure) and is not necessary. 
Chief, RPB 
concurs vith this rational. Security measures vill involve regular 
visits to the site by EPA, TAT and possibly DPNR. 
TAT distributes Polrep 7. 
3. 
FUTURE PLANS AND RECOMMENDATIONS: 
A. 
Deliver all remaining medical supplies, electrical supplies 
drum over packs and sorbents to the site. 
B. 
Remobilization for sampling, segregation and stabilisation 
activities tentatively scheduled for January, 1990. 
301528 
4. 
PINANCIAL ACCOUNTING: 
A. CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
$1,840,000 
$1,262,000 
$200,000 
B. UNOBLIGATED MITIGATION PUNDS REMAINING 
C. COSTS A BALANCES as of 11/12/89 
DCN 
KE3042 
KE3069 
KE3073 
KE3085 
Subtotal 
Other Costs 
Estimate of Total 
Expenditures to Date 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
17% 
PERCENTAGE OP $2 MILLION 
16\ 
TAT 
$105,000 
$0 
OBLIGATED 
AMOUNT 
$250,000 
500,000 
250,000 
262,000 
$1,262,000 
S Of 11/03/89 
s Of 11/17/89 
MITIGATION 
22% 
EXPENDED 
AMOUNT 
$250,000 
28,178 
0 
0 
$278,178 
16,234 
22,576 
$316,98$ 
SPA 
11% 
BALANCE 
471, 
250. 
262, 
$983, 
$0 
,822 
rOOO 
,000 
,822 
TAT 
15% 
PINAL POLREP. 
PUTURE 
POLREPS 
PORTECOKING, k SUBMITTED BY 
Douglas R. Xodama, 
Cn-Scene Coordinator 
Response and 
Prevention Branch 
DATE RELEASED ^O^. O.l'^gl 
301529 
U.S. ENVIRONMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
Region II 
Response and Prevention Branch 
Edison, New Jersey 08837 
(201) 548-8730 - Commercial and FTS 
24 Hour Emergency 
DATE: January 10, 19 90 
TO: C. Sidamon-Eristoff, EPA 
W. Muszynski, EPA 
S. Luftig, EPA 
R. Salkie, EPA 
J. Marshall, EPA 
G. Pavlou, EPA 
E. Schaaf, EPA 
ERD, Washington, 
(E-Mail) 
B. Sprague, EPA 
G. Zachos, EPA 
P. Geiabert, EPA 
A. Smith, VIDPNR 
LEPC, VIDPNR 
TAT 
POLREP NO.: 
SITE NO.: 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
Nine (9) 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
800 Lab Chemicals, 400 Drums, 22 Tanks 
Ground water, Caribbean Sea 
1. SITUATION; 
Site conditions remain the same. 
2. ACTION TAKEN: 
A. December 5, 1989, OSC certifies Invoice 001. 
B. January 8, 1990, EPA, TAT and OH Materials travel to St. 
Croix. 
C. January 9, 1990, OH Materials, EPA, TAT mobilized on site 
for the first phase of the VI Chem removal. Two trailers 
containing overpack drums cleared through customs. 
D. Phone service was returned to the site along with 
electrical service via the use of an on-site generator. 
E. A contingency planning meeting was held on January 10, 
1990, with the local government agencies to inform them of 
the removal action being taken at VI Chem. Site visit by 
local responders scheduled for January 11, 1990. 
301530 
m 
?. 
A public notice will be placed in the Daily New newspaper 
as soon as possible informing the public of the VI Chem renoval 
action. The administrative record was placed in the DPNR office 
on St. Croix for public access. 
G. Additional OH Materials personnel were mobilized to the 
site on January 10, 1990. 
FUTURE PLANS AND RECOMMENDATIONS; 
A. The overpacked drums will be delivered to the site from 
the port authority on January 11, 1990. 
B. TAT will sample public wells in .area to determine if 
there is a change in the level of chloroform contamination. 
C. Sampling and stabilization will commence as soon as 
mobilization is complete. Anticipate starting on Friday, January 
12, 1990. 
FINANCIAL ACCOUNTING 
A. CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
TAT 
$1,840,000 
$1,262,000 
$200,000 
$105,000 
B. UNOBLIGATED MITIGATION FUNDS REMAINING 
C. COSTS & BALANCES as of 1/10/90 
DCN 
OBLIGATED 
EXPENDED 
BALANCE 
AMOUNT 
AMOUNT 
KE3042 
$250,000 
$250,000 
$0 
KE3069 
500,000 
53,304 
446,696 
KE3073 
250,000 
0 
250,000 
KE3085 
262.000 
0 
262.000 
SUBTOTAL 
$1,262,000 
$303,304 
$958,696 
OTHER COSTS 
TAT Salary\Travel as of 1/5/90 
26,786 
EPA Salary\Travel as of 1/10/90 
24.576 
Estimate of Total 
Expenditures to Date 
$354,666 
301531 
D. CEILING PERCENTAGES 
TOTAL PROJECT. MITIGi 
19% 
PERCENTAGE OF $2 MILLION 
18% 
^TION 
• 24% 
EPA 
12% 
TAT 
26% 
FURTHER 
POLREPS 
FINAL POLREP 
FORTHCOMINGXSUBMITTED BY / ^ . . ^ t . 
^y^-^-iXaj^ [-AN \ 
' "Douqlas <k. «6dama 
Dougli 
On-Scene Coordinator 
Response and 
Prevention Branch 
DATE RELEASED ///i/^o 
301532 
•JsS 
m 
U.S. ENVIRONMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
DATEt January 13, 1990 
Region II 
Response and Prevention Branch 
Edison, New Jersey 08837 
(201) 548-8730- Commercial and FTS 
24 Hour Emergency 
TO: C. Sidamon-Eristoff, 
EPA 
W. Muszynski, EPA 
S. Luftig, EPA 
R. Salkie, EPA 
J. Marshall, EPA 
G. Pavlou, EPA 
E. Schaaf, EPA 
ERD, WH-548B 
(E-Mail) 
B. Sprague, EPA 
G. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
LEPC 
TAT 
POLREP NO.X 
SITE NO.: 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
Ten (10) 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
600 Lab Chemicals, 400 Drums, 22 Tanks 
Ground water, Caribbean Sea 
1. 
SITUATION: 
A. 
St. Croix Security Kennels have removed their dogs from the 
site. There is currently only one on-site resident, hired by 
VIAG for site security. Site conditions remain the same. 
2. 
ACTION TAKEN; 
A. 
January 11, 1990, two additional phone lines were installed, 
received and unloaded two trailers containing overpack drums, 
cook trailer brought on-line, additional crew mobilized to site 
bringing total crew to twelve. The microwave phone system was 
demobed due to lack of a functioning phone line at the relay 
station. Approximately 200 feet of phone line was stolen at this 
location affecting not only the relay station, but at least 30 
residences upstream from the break in the phone line. 
301533 
A bull wandered onto the site and was chased off by the 
owner. 
DPNR, Fire Marshall, and EMS visited the site. OSC and 
Health and Safety Officer visited the St. Croix Hospital. 
Hospital will not be rebuilt until July, 1991 at the earliest. 
EMS encouraged OSC to make own arrangements for airlifting 
injured personnel to San Juan. 
OSC contacted USCG-MSO San Juan and requested USCG Search 
and Rescue to be on standby for airlifting site personnel to San 
Juan Medical Central. OSC was informed that the response time to 
St. Croix was at least one hour. OSC offered the opportunity for 
USCG to visit the site and observe clean-up operations. 
B. 
January 12, 1990: information was gathered from labels of 
lab reagents and drums, drums were numbered, initiated, packaging 
and overpacking of bagged and drummed material, two additional 
unknown cylinders were discovered near dog kennels. OSC 
coordinated with VIAG. One electrician demobed bringing total 
crew to eleven. 
C. 
January 13, 1990: 69 drums were overpacked, inventory of lab 
reagents continued, drum grappler repaired with on-site welding 
equipment, caps of unknown cylinders were removed and 
photographed. Photos will be mailed to cylinder specialists for 
possible identification. Air monitoring in labs and warehouse 
showed some elevated readings during clean-up activities. EPA 
coordinated with the Deputy Chief of Public Safety, to notify the 
Golden Grove Correctional Facility when site activities are 
concluded for the day; this will be done daily. 
D. 
A public notice will be placed in the Daily News newspaper 
on January 16, 1990 informing the public of the VI Chem removal 
action. The administrative record was placed in the DPNR office 
on St. Croix. If necessary a copy of the Administrative Record 
will be placed in the DPNR office on St. Thomas. 
3. 
FUTURE PLANS AND RECOMMENDATIONS 
A. TAT will sample public wells in area to determine if there is 
a change in the level of chloroform contamination. 
B. Sampling and stabilization may be completed by January 26, 
1990. 
301534 
/ 
r 
FINANCIAL 
ACCOUNTING! 
A. CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
TAT 
«1,640,000 
*1,262,000 
S200,000 
$105,000 
r 
B. UNOBLIGATED MITIGATION FUNDS REMAINING 
«0 
C. COSTS & BALANCES as of 1/12/90 ' 
DCN 
KE3042 
KE3069 
K:E3073 
KE3085 
Subtotal 
Other Costs 
TAT SalaryNTravel as 
EPA SalaryNTravel as 
Estimate of Total 
Expenditures to Date 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
22*/. 
PERCENTAGE OF »2 MILLION 
217. 
OBLIGATED 
AMOUNT 
$250,000 
500,000 
250,000 
262,000 
$1,262,000 
of 1/12/90 
of 1/13/90 
MITIGATION 
277. 
EXPENDED 
AMOUNT 
$250,000 
91,482 
0 
0 
$341,482 
43,932 
25,776 
$411,190 
EPA 
137. 
BALANCE 
408, 
250, 
262, 
$920, 
$0 
,518 
,000 
,000 
,518 
TAT 
427. 
FUTURE 
^ 
FINAL POLREP 
FORTHCOMING X SUBMITTED BY_^2i^AAi^aJl_S^/^:^!^ilIY^C^v,^ 
DouglasO R. Kodama, 
On-Scene Coordinator 
Response and 
Prevention Branch 
DATE RELEASED 
| U ^ M Q 
U.S. ENVIRONMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
301535 
U.S. ENVIRONMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
DATEt January 16, 1990 
Region II 
Response and Prevention Branch 
Edison, New Jersey 08837 
(201) 548-8730- Commercial and FTS 
24 Hour Emergency 
TO: c. 
u. 
s. 
R. 
J. 
G. 
E. 
Sidamon-
Muszynsk 
Luftig, 
Salkie, 
Marshall 
Pavlou, 
Schaaf, 
•Eristoff, 
EPA 
: i , EPA 
EPA 
EPA 
,, EPA 
EPA 
EPA 
ERD, WH-54BB 
B. 
G. 
P. 
A. 
(E-Mai 
Sprague, 
Zachos, 
Gelabert 
.1) 
EPA 
EPA 
:, EPA 
Smith, VIDPNR 
LEPC 
TAT 
POLREP NO.: 
SITE NO.: 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
Eleven (11) 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
800 Lab Chemicals, 400 Drums, 22 Tanks 
Ground water, Caribbean Sea 
1. 
SITUATION; 
A. Site conditions remain the same. 
2. 
ACTION TAKEN: 
A. 
January 14, 1990, 96 drums overpacked to date, samples 
collected from 21 drums, unknown lab reagents temporarily secured 
on-site, known lab reagents secured in drums with sorbent, 
options explored for sampling of drum containing potentially 
shock-sensitive tetrahydrofuran, one additional cylinder found 
on-site. 
B. 
January 15, 1990, label information gathered from all 
cylinders. Inspection of reactor tower revealed a minor amount of 
residual product in these vessels. This material will be 
removed. Gathering of outdoor drums/containers was initiated, 52 
drums sampled (73 to date), securing of known lab reagents 
301536 
m 
completed, and inventory of unknown lab reagents completed. 
Sample techs experienced skin irritation (protective clothing 
breakthrough) while sampling benzy1 chloride drums and flammable 
vapors present from sampling triethylamine. Hot Zone was 
evacuated until ventilation reduced to safe levels. A public 
notice was published in the Virgin Islands Daily News newspaper 
informing the public of the VI Chem removal action. OSC 
coordinated with VIAG. 
C. 
January 16, 1990, gathering, documentation and overpacking 
of outdoor drums completed, 10 drums sampled (83 to date). OHM 
had a car stolen the night of January 15/16. TAT previously had 
a car stolen the night of January 7/S. OSC reviewed options for 
sampling of unknown lab reagents, on-site treatment of shock-
sensitive materials, and known and unknown cylinders. Breathing 
air in short supply and it may be difficult obtaining additional 
A i r . 
TAT sampled WAPA public wells in Area to determine if there 
is a change in the level of chloroform contamination. The on-
site well was sampled for priority pollutant and bacteriological 
analyses. Two wells owned by the Virgin Island Port Authority 
could not be sampled because power had not been restored to the 
pump. 
3. 
FUTURE PLANS AND RECOMMENDATIONS 
A. One chemist will be demobed on January 18, 1990'bringing 
total crew to ten. 
B. Unknown lab reagents are scheduled to be remotely opened on 
January 22, 1990. 
C. Drum sampling, sample shipment, and analytical arrangements 
will be completed. 
D. TAT will conduct asbestos sampling of material on the reactor 
and bulk material. 
301537 
4. 
FINANCIAL ACCOUNTING; 
TOTAL PROJECT 
MiriGATION 
EPA 
$1,840,000 
$1,262,000 
$200,000 
B. 
UNOBLIGATED MITIGATION FUNDS REMAINING 
C. 
COSTS & BALANCES as of 1/16/90 
DCN 
KE3042 
KE3069 
KE3073 
KE3085 
OBLIGATED 
AMOUNT 
$250,000 
500,000 
250,000 
262,000 
EXPENDED 
AMOUNT 
$250,000 
123,800 
0 
0 
$1,262,000 
Subtotal 
Other Costs 
TAT SalaryNTravel as of 1/12/90 
EPA SalaryNTravel as of 1/16/90 
Estimate of Total 
Expenditures to Date 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
247. 
PERCENTAGE OF $2 MILLION 
227. 
MITIGATION 
307. 
$373,800 
43,932 
26,976 
$444,708 
EPA 
137. 
TAT 
$105,000 
$0 
BALANCE 
$0 
376,200 
250,000 
262,000 
$688,200 
TAT 
427. 
FINAL POLREP 
FUTURE 
POLREPS 
FORTHCOMING 
.SUBMITTED BY 
3*^ 
DATE RELEASED 
Doug l a p R. 
Kodama>-./ 
On-Scene 
C o o r d i n a t o r 
Response 
and 
P r e v e n t i o n 
B r a n c h 
301538 
U.S. ENVIRONMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
DATE; January 19, 1990 
Region II 
Response and Prevention Branch 
Edison, New Jersey 0B337 
(201) 548-8730- Commercial and FTS 
24 Hour Emergency 
TO: C. Sidamon-Eristoff, 
EPA 
W. Muszynski, EPA 
5. Luftig, EPA 
R. Salkie, EPA 
J. Marshall, EPA 
6. Pavlou, EPA 
E. Schaaf, EPA 
ERD, WH-548B 
(E-Mail) 
B. Sprague, EPA 
G. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
LEPC 
TAT 
POLREP NO.: 
SITE NO.: 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
Twelve (12) 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
Approximately 566 Known Lab Chemicals, 590 
Unknown Lab Reagents, 210 Drums, 22 Tanks 
Ground water, Caribbean Sea 
1. 
SITUATION; 
2. 
Site conditions remain the same. 
ACTION TAKEN; 
A. 
January 17, 1990, arrangements were made with the Department 
of Public Safety and the Virgin Islands Police Department to 
utilize police issued .22 caliber r i f l e s i a r remote opening of 
unknown lab reagents on site. A police represenative will notify 
the prison officals and remain on site during the activity. 
Continued overpacking drums; 37 drums were sampled and 120 
drums have been sampled to date. EPA coordinated with VITEMA and 
USCG. Cylinder specialist, believes that the two unknown 
301539 
cylinders are probably inert gases. 
The Department of Public Safety will also provide 
information on the procedures and permits necessary to obtain 
explosives on the island for detonating the unknown cylinders and 
shock-sensitive materials on site. 
B. 
January 18, 1990, two represenatives from the U.S. Coast 
Guard Marine Safety Office in San Juan, Puerto Rico mobilized on 
site for observing a hazardous waste site and clean-up. The two 
were given a tour of the hot zone and removal actions utilizing 
level "B" personal protective equip.oent. One chemist was 
demobed, total crew now stands at ten; EPA coordinated with USCG, 
VITEMA and Public Safety. 17 drums sampled (137 to date). 
C. 
January 19, 1990, results from the bacteria sample analysis 
of the on-site 250,000 gallon water storage tank indicated severe 
coliform infestation of the water poses a significant health 
risk. All personnel on-site were warned not to use the water. 
Containerization of lab reagents has been completed. A 
total of 10 drums were filled. Two c,abinets are being used for 
storage of reactive and shock-sensitive materials until such time 
as they can be detonated. Unknown lab reagents are stored on 
shelves until they can be remotely opened. 
Drum sampling and overpacking has been completed. A total of 
174 drums have been sampled. Device fabricated for collection of 
liquid and solid unknown lab reagents, during the remote opening 
of these containers utilizes a .22 caliber rifle. Remote opening 
of these containers scheduled for 1/22/90, TAT informed 
neighboring businesses of this activity, EPA coordinated with on-
site resident, VITEMA and Public Safety. 
3. 
FUTURE PLANS AND RECOMMENDATIONS 
A. Unknown lab reagents are scheduled to be remotely opened on 
January 22, 1990 
B. Sample shipments and analytical arrangements will be 
completed. 
C. On site storage tanks will be sampled. 
D. TAT will conduct asbestos sampling of material on the reactor 
and bulk material. Virgin Island Port Authority wells will be 
sampled once power to them has been restored. 
E. ERCS contractor will be demobed from the site until 
analytical results are obtained, disposal options are addressed 
and phase two is initiated. 
301540 
-a 
'm 
4 . 
FINANCIAL 
ACCOUNTING 
A. 
CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
$1,840,000 
$1,262,000 
$200,000 
B. 
UNOBLIGATED MITIGATION FUNDS REMAINING 
C. 
COSTS & BALANCES as of 1/19/90 
DCN 
KE3042 
KE3069 
KE3073 
KE3085 
Subtotal 
Other Costs 
Estimate of Total 
Expenditures to Date 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
267. 
PERCENTAGE OF $2 MILLION 
247. 
MITIGATION 
327. 
EPA 
147. 
TAT 
$105,000 
$0 
OBLIGATED 
AMOUNT 
$250,000 
500,000 
250,000 
262,000 
$1,262,000 
of 1/19/90 
. of 1/19/90 
EXPENDED 
AMOUNT 
$250,000 
147,838 
0 
0 
$397,838 
51,305 
28,476 
$477,619 
BALANCE 
$0 
352,162 
250,000 
262,000 
$864,162 
TAT 
497. 
FINAL POLREP 
FUTURE 
POLREPS 
FORTHCOMING k SUBMITTED BY 
-iS^ 
Dougld^^ R. Kodama, 
On-Scene Coordinator 
Response and 
Prevention Branch 
3 01541 
DATE RELEASED T,^. "Z'^, \ <^ ^ Q 
U.S. ENVIRONMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
Region II 
Response and Prevention Branch 
Edison, New Jersey 08837 
(201) 548-8730- Commercial and FTS 
24 Hour Emergency 
DATE: January 23, 1990 
TO: C. Sidamon-Eristoff, 
EPA 
W. Muszynski, EPA 
S. Luftig, EPA 
R. Salkie, EPA 
J. Marshall, EPA 
G. Pavlou, EPA 
POLREP NO.: 
SITE NO.: 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
1. 
SITUATION; 
ERD, WH-54BB 
(E-Mail) 
B. Sprague, EPA 
6. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
LEPC 
TAT 
Thirteen (13) 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
Approximately S66 Known Lab Chemicals, 590 
Unknown Lab Chemicals, 210 Drums, 240 Empty 
Drums, and 22 Tanks. Possibly Asbestos and 
Dioxin Containing Materials 
Ground water, Caribbean Sea 
A. 
Drum sampling and stabilization have been completed. 
2. 
ACTION TAKEN; 
A. 
January 20, 1990, sampling of all tanks and reactor vessels 
completed, QANQC of samples and drum logs, general clean up of 
warehouse area completed, list of chemicals needing dioxin 
analyses provided by OHM. Three five gallon containers of. 
potentially dioxin contaminated material sampled. Three bids for 
analytical work provided by OHM, low bid, ETC labs will be used. 
Decon trailer's water tank chlorinated. Equipment serviced. 
B. 
January 21, 1990, device for collection of unknown lab 
reagents completed, all drums in warehouse restaged and placed on 
pallets, warehouse floor cleaned, completed sampling of spent 
personnel protective clothing and paints, initiated documentation 
301542 
for shipment of samples. 
C. 
January 22, 1990, OSC coordinated with VI Police Department 
and informed of proper procedures for shipment of explosives to 
St. Croix. VI Police Department also provided two .22 caliber 
rifles for the remote opening of unknown lab reagents. 
Remote opening of unknown containers successfully completed. 
Paints secured in drums on—site. Most samples packaged and 
prepared for shipment. General site clean up conducted. 
D. 
January 23, 1990, bulked, unknown lab reagents solidified, 
sampled and secured in three drums in warehouse. Shipment of 
samples initiated. Initiate final clean up activities and 
securing of site. 
3. 
FUTURE PLANS AND RECOMMENDATIONS: 
A. 
Finalize shipment of all samples. 
B. 
TAT will conduct asbestos sampling of material oo the 
reactor tower and bulk material. Virgin Island Port Authority 
wells will be sampled once power to them has been restored. 
C. 
OSC through DPNR will inform applicable local agencies of 
the completion of this phase of the removal action. List of 
chemicals, their location on-site and a video tape of this phase 
will be distrbuted to these agencies in the near future. 
D. 
Analytical, transportation and disposal coordination. 
E. 
Demob for this phase. 
F. 
In approximately two months, on—site detonation of shock-
sensitive, explosive materials, off—site (on-island) detonation 
of known and unknown cylinders, crushing of empty drums, and if 
appropriate treatment of dioxin-containing materials. 
4. FINANCIAL ACCOUNTING 
A. CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
TAT 
$1,840,000 
$1,262,000 
$200,000 
$105,000 
B. Ifl^OBLIGATED HITIGATION FUNDS REMAINING 
$0 
301543 
C. COSTS & BALANCES as of 1/21/90 
# 
DCN 
KE3042 
KE3069 
KE3073 
KE3085 
Subtotal 
Other Costs 
TAT SalaryNTravel as 
EPA SalaryNTravel as 
Estimate of Total 
Expenditures to Date 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
27X 
PERCENTAGE OF •2 MILLION 
257. 
FUTURE 
POLREPS 
. 
FINAL POLREP 
FORTHCOMING, 
7 
OBLIGATED 
AMOUNT 
$250,000 
500,000 
250,000 
262,000 
$1,262,000 
of 1/19/90 
of 1/23/90 
MITJGATION 
33Z 
)(. .SUBMITTED 
EXPENDED 
AMOUNT 
•250,000 
166,019 
0 
0 
$416,019 
51,305 
29,113 
$496,437 
EPA 
15X 
1 
BY fisu-^^rtNsi^ ^ ' 
BALANCE 
$0 
333,981 
250,000 
262,000 
$845,981 
TAT 
497. 
JWfvV«^3. 
Dougla^ R. Kodama, 
On-Scene Coordinator 
Response and 
Prevention Bi 'anch 
DATE RELEASED ijx^ao 
301544 
X . 
\- — 
y 
MAY2ii.oQg 
U.S. ENVIRONMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
ff^y r 
Region II 
Response and Prevention Branch 
Edison, Nev Jersey 08837 
(201) 548-8730 - Commercial and FTS 
24 Hour Emergency 
DATE: May 18, 199 0 
TO: C. Sidamon-Eristoff, EPA 
W. Muszynslci, EPA 
S. Luftig, EPA 
R. Sallcie, EPA 
J. Marshall, EPA 
G. Pavlou, EPA 
E. Schaaf, EPA 
ERD, WH-548B, 
(E-Mail) 
B. Sprague, EPA 
G. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
LEPC, VIDPNR 
TAT 
POLREP NO.: 
SITE NO.: 
POLLUTANT: 
CLASSIFICATION! 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
Fourteen (14) 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
Approximately 566 Known Lab Chemicals, 590 
Unlcnown Lab Chemicals, 210 Drums, 240 Empty 
.Drums, and 22 Tanlcs. 
Ground vater, Caribbean Sea 
1. SITUATION: 
Emergency Response to a report of a fuming drum. 
2. ACTION TAKEN; 
A. May 9, 1990, 4 TAT personnel and Adalberto Bosque of the EPA 
Caribbean Field Office arrived on-site in Emergency Response to a 
report of a fuming drum. TAT suited up in Level B with SCBA's to 
assess the situation. The fuming drum, Drvim No. 29, was found in 
the rear of the warehouse. After Edison EPA was informed that the 
drum vas still fuming and that drum was in a bulging condition, EPA 
decided to mobilize the ERCS contractor. 
B. May 10, 1990, tvo ERCS contractors arrived on site and one TAT 
vas demobilized. 
ERCS made an entry along with TAT and EPA in 
Level B. The ERCS contractor loosened the lid of the overpaclc in 
order to dissipate the pressure build-up, exited Hot Zone, 
conducted literature search for benzyl chloride, initiated plans 
to transfer chemical, made a request for shipment of necessary 
301545 
equipment (i.e., poly overpack drums. Level A PPE, teflon pump). 
Benzyl chloride is a corrosive liquid and a severe slcih irritant. 
An incident involving sampling of benzyl chloride drums during 
Phase I at VIChem occurred on January 15, 1990 and is documented 
in POLREP #11. In the previous incident, sample techs experienced 
s)cin irritation vhile sampling benzyl chloride drums, the Hot Zone 
vas evacuated -until-safe .^ir levels were .reached, and the OSC 
decided that it was not necessary to continue sampling of benzyl 
chloride drums. 
C. May 11, 1990, tvo additional ERCS contractors arrived for a 
total of four ERCS on site. 
Equipment was piclced up at the 
airport. ERCS contractor is delayed due to condensation build-up 
inside the drums during shipment. Tvo ERCS in Level A suits on an 
air line entered the Hot Zone. Two TAT and the EPA representative 
entered in Level B with SCEA's. Three men were on baclcup. Level 
B personnel didn't handle the drums. The fuming drvim was found to 
have a bung not in the bung hole but off to one side sitting on the 
top of the inner-drum. Apparently, benzyl chloride reacted vith 
moisture in the air to form hydrochloric acid fimes. Except for 
the un-secured bung, the inner-drum was assessed to be in good 
condition. ERCS secured the bung and used lime based cement as an 
absorbent/neutralizer. 
D. May 12, 1990, ERCS contractor performed a site clean-up before 
demobilizing. The site electric generator was in operation during 
the day. 
E. Other site activities durinq emergency response 
While on-site during the emergency response, ERCS contractor had 
their ordinance specialist assess site for the on-site detonation 
of shoclc-sensitive materials that is planned for June 1990. A 
suitable on-site area was located. Also, ERCS noted that the EPA 
phones, which are in the office trailer, were not in service and 
that an ERCS 12,000 gallon waste treatment pool was missing. 
F. Other activities 
- February 2, 1990, OSC received a call from Dave Weston of 
VIAG. He said that a stranger was on the site during the past 
three days claiming that he was providing security for EPA. 
Dave told him to leave site yesterday but noticed today that 
hand tools, lawn mower, etc. are missing. 
Dave got the 
license plate number of the stranger's white Chevrolet pic)cup 
and he will follow up on this. 
- March 2, 1990, OSC updated Paul Simon of ORC on status of 
Removal Action and on March 5, 1990 the OSC mailed him a 
complete set of Polreps (nos. 1-13). 
- March 5, 1990, OSC reviewed analytical results collected from 
materials potentially containing asbestos. 
None of the 
insulation on the reactor tover or bul)c material with hand-
301546 
.3 
t 
written asbestos labels had any detectable levels of asbestos. 
They all were comprised of a cellulose-type material. 
April 11, 1990, due to the significantly increased SPCC 
activities associated with recent oil spills, OSC duties vere 
transferred, vith branch chief approval, to the former AOSC, 
John Higgins, and the former OSC, Doug Kodama, assumed the 
AOSC position. 
• 
April 24, 1990, separate letters were sent to Commissioner 
Smith, members of the VI Local Emergency Planing Committee, 
and VITEMA updating them on the Removal Action status and plan 
for Phase II. List of chemicals, their location on-site and 
a video tape of Phase I were distributed to these agencies. 
April 26, 1990, OSC letter was transmitted to Commissioner 
Smith requesting VIDPNR approval for use of the Anguilla 
landfill, or an alternate site, for detonation of cylinders 
containing both Icncvn and un)cnown hazardous substances. 
May 1, 1990, the AOSC received a call from Jim Sutherland of 
VIAG. He complained that EPA conducted a very shoddy job, cut 
electric lines, blev up phone junction box, interfered vith 
their business, is storing additional hazardous waste on site. 
AOSC disagreed with his statements. He stated that VIAG will 
seelc compensation. He also sated that he wants the equipment 
trailer to be .moved next to the decon trailer. 
The AOSC 
agreed that this could be done during Phase II. 
May 15 & 16, 1990, OSC met with TAT in Edison and discussed 
the chemical analytical data on water samples collected from 
the on-site water tanX and Fairfield Wells Nos i t 2. TAT was 
instructed to provide summary tables and a narrative summary 
on the cjuality of the data to the OSC by May 25, 1990. Based 
on these discussions, the data is of good quality and 
indicates no exceedances of Drinlcing Water Maximum Contaminant 
Levels. However, since sample collection was both incomplete 
(WAPA wells were not sampled because they vere not operating) 
and perhaps not representative (Fairfield well pumps had been 
inactive, as a result of Hurricane "Hugo", and were just 
turned on the morning of sampling), additional well sampling 
will be conducted during Phase II. 
May 16, 1990, OSC discussed Phase II plans with Jeff Bodi of 
ERCS and instructed that a worlcplan be submitted for this worlc 
by May 25, 1990. Also, we discussed whether ERCS had any 
responsibility for the fuming drum and whether ERCS should 
absorb some of these costs. The OSC will discuss matter with 
AOSC, TAT, and the contract DPO prior to concluding the 
matter. 
May 15. & 18, 1990, OSC discussed the status of the Removal 
Action with ORC Attorney Carol Burns, who was recently 
assigned VIChem. She informed OSC that ORC is proceeding with 
placing a lien on the VIChem property. I faxed her a copy of 
this POLREP on May 18. 
301547 
f 
- 
• ' 
3. FUTURE PLANS AND RECOMMENDATIONS: 
A. ERCS completes lab pac)c, paint waste, and empty drum disposal 
arrangements as soon as possible. 
B. ERCS develops Phase II worlcplan by May 25, 1990. 
C. TAT completes Phase I drinlcing water data summary by May 25, 
1990. 
D. TAT completes Phase II field sampling plan by May 25, 1990. 
E. ERCS must have all supplies and equipment necessary for Phase 
II shipped to St. Croix via Tropical Inc. in Miami by May 29, 1990. 
F. 
Mobilization for Phase II is scheduled for June 11, 1990. 
Phase II will consist the off-site detonation of cylinders, the on-
site detonation of shoclc-sensitive lab reagents, crushing of empty 
drtims, and the disposal of lab pacXs, paint waste materials and 
empty drums at a mainland hazardous waste incinerator. 
G. 
The OSC will prepare an Action Memo requesting additional 
monies and a twelve month time limit extension for the completion 
of VIChem. 
H. Drum compositing scheme for waste incineration .analysis must 
be finalized by ERCS, approved by EPA, waste analysis conducted, 
and drum disposal arrangements finalized for actual drum disposal 
in Phase III, which is planned for the autumn of 1990. 
I. The OSC will review the results of the dioxin data analyzed 
from the three five (5) gallon containers. 
301548 
'% 
4. FINANCIAL ACCOUNTING 
A. 
CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
— 
- 
. $ 1 , 8 4 0 , 0 0 0 
$ 1 , 2 6 2 , 0 0 0 - . 
$ 2 0 0 , 0 0 0 -
B. ' UNOBLIGATED MITIGATION FUNDS REMAINING 
C. 
COSTS & BALANCES a s Of 4/24/90 
TAT 
$105,000 
$0 
DCN 
KE3042 
KE3069 
KE3073 
KE3085 
Subtotal 
Other Costs 
TAT Salary\Travel as 
EPA Salary\Travel as 
Estimate of Total 
Expenditures to Date 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
33* 
PERCENTAGE OF $2 MILLION 
30t 
FURTHER 
POLREPS 
X POLREP 
FORTHCOMING_> 
OBLIGATED 
AMOUNT 
$250,000 
500,000 
250,000 
262,000 
$1,262,000 
Of 1/12/90 
Of 5/18/90 
MITIGATION 
41% 
L SUBMITPED BY 
EXPENDED 
AMOUNT 
$250,000 
268,049 
0 
0 
$518,049 
43,932 
40,630 
$602,611 
' 
EPA 
20% 
ZZJLI 
BALANCE 
$0 
231,951 
250,000 
262,000 
$743,951 
TAT 
42% 
•t^,9c-^ 
DATE RELEASED 
John H i g g i n s 
On-Scene 
C o o r d i n a t o r 
Response and 
P r e v e n t i o n Branch 
3 0 1 5 4 9 
•
^ 
f 
• 
/bty'^Xy) 
m 
:S 
U . S . ENVIRONMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
Region II 
Response and Prevention Branch 
Edison, New Jersey 08937 
(201) 548-8730- Commercial and FTS 
24 Hour Eioergency 
DATE: June 13, 1990 
TO: C. Sidamon-Eristoff, 
EPA 
W. Muszynski, EPA 
S. Luftig, EPA 
R. SaUia, EPA 
J. Marshall, EPA 
G. Pavlou, EPA 
ERD, WH-548B 
(E-Mail) 
Sprague, EPA 
Zacho«, EPA 
Gelabert, EPA 
Smith, VIDPNR 
B. 
6. 
P. 
A. 
LEPC 
TAT 
POLREP NO.I 
SITE NO.: 
POLLUTANT t 
CLASS1HiCATI ONJ 
SOURCE! 
LOCATION: 
AMOUNT: 
NATER BODY! 
1. 
SITUATION: 
Fifteen (15) 
4V 
Lab ChemicalSi Alcohols, Solvents, Acids 
Majnr 
Virgin Island Chemical Conp^ny (VlChaa) 
St. Croix, US Virgin Islands 
Approximately 366 Known Lab Chemicals, 590 
UnknOMn Lab Chemicals* 210 Drums, 240 Ejtpty 
Drums, and 22 Tanks. Possibly Asbestos and 
Dioxin Containing Materials 
Ground wateri Caribbean Sea 
Initiation of Phase II Be«ov«l 
I details. 
See previous polreps for Phase 
2. 
ACTION TAKEN: 
A, June 5, 1990, OSC discussed bids for waste analysis of 
composite drum samples with ERCS and Rick Haworth, Region 1 DSC. 
Based on the discussions the' OSC directed ERCS to contract with 
the second low bidder, " Analab**! for disposal analysis. 
301550 
^ 
I 
B. June 7, 1990, as requested, AOSC transmitted memo to Regional 
Administrator Sidamon-Eristoff that furnished detail on the May 
1, 1990 phone conversation between the AOSC and Jim Southerland 
of VIAG. 
C. June 11, 1990, all personnel arrived on Bt. Croix. OSC and 
TAT visited site and spoke to Andy with Infinity Services, who is 
a sub-lea*ee of a portion of the warehouse. Infinty Services 
was inforfped that they could not access the hot zone during 
clean—up activities. 
D. June 12, 1990, OSC discussed clean-up status and plans with 
Jim South»erlwnd of VIAG. He reiterated his complaints, which are 
docureentsd in P0LREP«I14 and in the June 7, 1990, memo fro* the 
AOSC to the Regional Administrator. However, he was calm and 
agreed that EPA and E.RCS could utilize space for storage of 
equipment and supplies in the warehouse. He also agreed that 
EPA could use his phone to aake credit card calls. 
EPA, TAT and ERCS (7) mobilized on site. 
ERCS started site 
CBt-up and reported a set of aluminum «iteps stolen "from the 
galley trailer. 
In addition, phone lines to the command post 
were cut. VITELCO was notified and indicated that phone service 
may be restored at the end of the weak. 
EPA *nd TAT met witli D«tv» Canegata, Assistant Commiccioner of 
DPNR to discuss cylinder detonation. 
In addition, EPA and TAT 
flket with Delroy Richards, Chief of the Department of Public 
Safety to request police assistance with the detonation. Police 
agreed to accompany detonation convoy from site with two police 
cars and to seal off landfill from public during operations. 
TAT also met with Fire Marshall Cyprian King tn rpquest A tirt 
truck and EMS service for the detonation. 
E. June 13, 1990, site set-up continues. ERCS mobilized five (5) 
personnel on site and demobilized one (i) personnel. A chemist 
from Ch«m Waste arrived on site to supervise the lab pack 
operation. Breathing-air and a port-a-john were delivered to the 
site. 
EPA and TAT held a Contingency Meeting with the following 
agencies: DPNR, VI Fire, Bureau of Corrections, Department of 
Health, ERCS. In addition EPA, TAT, ERCS and two represenatives 
from DPNR visited the detonation site (Anguilla landfill). 
WAPA and VIPA were notified by TAT that the Fairplain wells »6 
and *9} and VIPA wells fl and «2 will be sampled i o r 
halogenated hydrocarbons. 
A press release will be placed in the Daily News newspaper on 
Friday June 10, l990 informing the publii. of the temporary 
road and landfill closing during the detonation activity. 
301551 
:
• 
ERCS began re-staging the overpacked drums according to 
their compatabjlity classes delineated by the analytical 
results. 
ERCS restored phone service to the command post. 
3. 
FUTURE PLANS AND RECOMMENDATIONS: 
A. TAT will prepare minutes of June 13, 1990 Contingency 
Planning Meeting. 
B. Detonation of shock sensitives and of cylinders off-site at 
landfill on Saturday »orning June 16, 1990 in accordance with 
the Ordinance Plan. 
C. TAT will provide all necessary notifications regarding the 
detonation, including St. Croix Prison, Police, Fire, EMS, DPW 
St. Croix STP, Alexander Hamilton Airport, FAA, and businesses 
near the airport and landfill. Also, TAT will notify the NRC of 
the environmental ralease within one hour after final detonation. 
TAT will also conduct air monitoring. 
D. ERCS and Chem Waste will initiate labpacking on June 14, 
1990J ERCS equipment and supplies will be delivered on June 14, 
1990. 
E. Drum crushing will be initiated the week of June 16, 1990. 
The sixteen drums containing Benzyl chloride will be transferred 
to poly 55 gallon closed-top drums and overpacked inside 65 
gallon drums. 
F. The OSC will review the results of the dioxin data analyzed 
from the three five (5) gallon containers. 
G. TAT will perform sampling of the WAPA and VIPA wells. 
301552 
« 
' 
. 
•* 
4 . 
FINANCIAL ACCOUNTING 
A. CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
TAT 
•1,040,000 
il,262,000 
«200,000 
S105,000 
B. UNQBLIBATED MITIGATION FUNDS REMAINING 
SO 
C. COSTS & BALANCES as of 6/13/90 
DCN 
OBLIGATED 
EXPENDED 
BALANCE 
AMOUNT 
AMOUNT 
KE3042 
»250,0OO 
^250,OOO 
>0 
KE3069 
500,000 
327,999 
172,001 
ICE3073 
250,000 
0 
250,000 
KE30a5 
262,000 
O 
262,000 
Subtotal 
»1,262,000 
«577,999 
»684,001 
Other Costs 
TAT SalaryNTravel as of 6/13/90 
58,326 
EPA SalaryNTravel as of 6/13/90 
46,097 
Estimate of Total 
Expenditures to Date 
•682,422 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
MITIBATION 
EPA 
TAT 
37X 
46X 
23X 
56X 
PERCENTAGE OF »2 MILLION 
34X 
FUTURE 
POLREPS 
V 
CT ") D 
/I 
FINAL POLREP 
FORTHCOMING /\ SUBMITTED BY ^"--^i e*-''^--^- f-f-wAO>(,..^o 
John Wiggins 
vjC 
On-Scene Coordinator 
Response and 
Prevention Branch 
DATE RELEASED ^^/.^^-^^^g^ ^ ^ / ^ 9 0 
301553 
.4 
CCT I i 1990 
U . B . 
ENVIRONMENTAL P1?nTFr.TinN AGENCY 
POLLU1 ION REPORT 
R e g i o n 
I I 
R e s p o n s e 
and P r e v e n t io.n 
B r a n c h 
E d i s o n , 
Wew J e r s e y 
08B37 
<2013 t>4G-8730- Cotr.mercial 
^nd 
FTS 
24 Hour 
Emergsrncy 
DATE: J u n e 16, 
1990 
TO: C. 
S i d a m o n - E r i s t o f f , 
EPA 
W. M u s z y n s k i , 
EPA 
S. L u f t i g , 
EPA 
R. S a l k i e , 
EPA 
J . 
M a r s h a l l , 
EPA 
G, P a v l o u , 
EPA 
ERD, WH-548B 
( E - M a i l ) 
Rnragiio. 
FPA 
Z a c h o s , 
EPA 
G e l a b e r t , 
EPA 
S m i t h , 
VIDPNR 
8 . 
G. 
P. 
A. 
LCPC-
TAT 
POLREP NO. I 
S I T E NO.I 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUN1 I 
WATER BODY: 
S i x t e e n 
(16) 
. 
4V 
Lab Chemicals, A l c o h o l s , Solvent*, 
Acids 
Major 
Virgin Icland Chemical Company (ViChcm) 
St. Croix, US Virqin Islands 
Appruximatcly 5CG Known Lab Chmmicals, S90 
Unknown Lab Chemicals, 210 Drums, 240 Empty 
Drums, and 22 Tanks. Possibly Asbestos and 
Dioxin Containing Materials' 
Ground water, Caribbean Sea 
1. 
SITUATION; 
Phase II Removal Action continues. 
2. 
ACTION TAKEN; 
A. June 14, lyyo, ERCS continues labpacking and drum cogregation. 
Box trailer with ERCS supplies uoH delivered to the site frnn the 
ship container port. Also, airport containers with ERCS equipment 
were delivered to the site ana were unloaded. 
TAT speaks to Dave Caney^La (DPNR) about a press release informing 
the public of the detonation and obtain"^ Mr. Canegata's Approval 
to release the notification. 
TAT investigates a well drilling operaliun on the east side of the 
301554 
til C^mm cito no>r fh« usiPCi F.iirnlrtlnt Wall t6i «I.S. Geologic 
burvey was installing wiylil (0) cbservaiion wel 1 c as part nf A 
series of ground water flow-monitoring wells in the brackish 
aqui fer. 
Todd Shank of DPNR stops by the site to inform EPA that thi» Dept. 
of Public Works (DPW) is hesitant about the detonation taking place 
at the landfill. 
ERCS explosive expert arrives o»i *ite. 
CPA, TAT and explosive 
expert visit detonation site. 
CRCH iMtcsr-« ePA 
n* prftStpnc; trancwurtino Cylinders and "-.hock 
sensitives from VI Chem to landfill. EKCS requests a waiver of 
RC1RA tr Ancportat ion rpgulations and not to hold ERCS harmlesa if 
somethiftq Qoea wrcnj during transpwft. 
CPA infefMcd Pf^Cfi that th* NAtinnrtl Contingency Plan (NCP) allows 
EPA to transport hazardous materials in emergenty situations. It 
challenged, EPA would exhibit credentials, however, it is unlikely 
for EPA to be challenged since the Police Dept. and DPNR are a part 
OT tne exercise. EPA infwrjutrJ CRCC •iha* OCC did not have authnrlty 
to 
write 
the 
requested 
hold-harmless 
waiver. 
Subsequent 
consultations with ERCS and tPA contract offiti.»ls revealed that 
EPCS is covered by liability insurance. 
EPA faxed January well ixsrftpl ing data summary to Susan Shaw nf EPA's 
Region 2 Water Management Division (WMD), 
At UMT7 request, EPA directed TAT to investigate the Texaco 
gasoline station on Centerline Rd. east of FrederikStpd to observe 
at wei I digging w«»* yulnW on. 
TAT reported no activity At that 
station and no artivity At the other two Texaco stations nearby 
rrederikstfcfU. 
EPA, TAT and ERCS have a meeting to discuss detonation operations. 
B. June 15, 19VO, press r*»l ease noiifying the public of detonation 
was not in the Virgin Island Daily News newspaper. 
En.yil'.fml"'* exprr* and TAT vicit with H r ^ CJnlpf CyBrJiij Kif^d 
to give details about detonation for June 16, 1990. 
ERCS continues to lab pack and segregate drums. 
TAT, EPA and DPNR meet with several DPW officials and receive 
approvals from Mr. Slater, landfill supervisor, and Mr. Hanson, 
sewerage treatment plant supervisur, contingent upon the approval 
of the acting DPW Commissioner, who is on travel in St. Thomas. 
Mr. Canegata of DPNR subsequently informs EPA thai DPW approval 
for dotonatinn at the landfill was received. 
TAT called Del r uy Ri^-hords, Chief of Public Safety »nd gavi- ({K>L.4i1s 
of the detonation. 
301555 
Cyf^rian King, of the Vl Fire DepI-. dRlivcred the cxplosivoc permit 
to ERCS on the VI Ch^m site. 
FRr.fi inforras EPA of problems with transporting explosives to the 
island. 
Detonators and ptrf forstor charges are still In Tex«». 
They will not arrive* until Monday. 
When questioned, ERCS stated 
that the transporter verbally confirmed o«i Tuesday, June 12, 1990, 
that the shipmeni h.id bean transported. 
Another shipment of 
explosives JS on tne island ^lur^rj «t the quarry locked up anfj the 
owner is on Puerto Rico until next week. 
Numerous attempts to 
expedite matters failed. 
EPA and TAT contact all necassary agencies to inform then of the 
postpoMfr/nent of tho detonation and to schedule a Cor»Lingeney 
Planning Meeting at DPNR offices for 10:00 AM Tuesday, June 19, 
1990. EPA informed tKUls" tnat tnsrtr will Lc .,,., ve>\*U an Sunday. 
EPA questioned ERtE -bw«l the »*a%uc of tha drum rrii'Sh opBritO'' 
and equipment. ERCS did not knov when equipment would arrive, 
ERCG informed EPA that their (ERCG) lab (ETC) mad« a mistake *nd 
used all of the samples from the acid liquid compatibility grouping 
snri thai additional sampling was needf»rt. ^iso, samples from drum 
numbers 132 and 136 generated reactions (ie. elevated temperature* 
and gas evolution). From drum markings, it is suspected that these 
drums contain Muriatic acid And Hydrochloric acid and should be 
included in a sep/irate waste stream. ERCS wanted to know if it was 
okay to composite samples oo site. 
EPA informed ERCS that 
n.-»rk,Toino *nd rA«pnniting of sample from the acid liquid group 
would be at ERCS expense and that on site compositing of nAapI«r v«» 
inappropiate due to lack of adpnuate laboratory facilities. 
Explosive expert will work as a laborer and be billed accordingly 
until detoi)«tion is back on track. 
C. June 16, 1990, the Daily News newspaper released an article 
informing the public of the postponed detonation. 
In addition, 
the Daily N P W S mentioned that there was no nvw% release notifying 
the public of tho proposed detonation. However, the article did 
not mention that this omission was due to their failure to print 
the public notice furnished to xhem by TAT oi, June 14, 1990. 
ERCS fiiii*nes l«bpacking ww» k and contJnuec overgtckinq. 
A drum 
(#81) of Benzyl acetate mixed with Acetic acid (glacial) which is 
• fl^mmiblo o»^9*nic ;arirl And is the nnly drum in a single waste 
stream. 
If the drum cannot be neutralized or diluted to a non-
flashpoint condition, disposal analysis and transportation cost 
will 
approximate »8500, as it nay require its own SeaLand 
container. A bench scsle experimenl was performed. A small portion 
of the Benzyl acetate and Acetic acid mix w<a> diluted with water 
to see if the two would separate (Benzyl acetate insoluble in water 
and Acetic acid soluble in water). 
Results were inconclusive. 
It is decided to ship the «^tor.k quart sample to ETC for bench scale 
301556 
, 
I 
testing lo requii-ed dilution. Final rlrt er niinat Ion ef how to handle 
rlriim number 81 will be made priur Lu Phane 1X1. 
ERCS starts and completes packaging of additional sample stock 
iiifc-ultrJ for d i ^ ^ u ' - ^ l 
AHAlycic And disposal. 
3. 
FUTURE HLANS AND RFnOMMENDATIONCi 
A. On June 19, 1990, there will be m Contingency Planning Meeting. 
B. Remainder of explosives are to arrive on St. Croix, June IB, 
1990. 
C. Detonation of shock sensitives and cylinders off-cite at 
landfill will be resth&duled during the Continqency Planning 
Meet ing 
n. TAT will crovide all nu't^ksary not i f i rat ions regarding the 
detonation, including St- Croix Prison, Police, U r e , CM3, DPW 
St. Croix STP, Alexander Hamilton Airport, FAA, and businesses ne^r 
the airport and landfill. 
Also, TAT will notify the NRC of the 
environmental release within one hour after final detonation. TAT 
will also conduct air monitoring. 
E. Drum crushing will be initiated the week of June 10, 1990. The 
sixteen drums containing Benzyl chloride will be transferred to 
poly 55 gallon closed-top drums and overpacked inside BS gallon 
drums. 
r. Tho DSC will review thr results of tho dioxin dat;% AnalyrttJ 
from the three five (5) gallon containers. 
,v 
6. TAT will perform sampling of the WAPA and VIPA wells nearest 
the site. 
301557 
•1 
1 . 
FINANCIAL ACCOUNTTNQf 
A. 
CEILINGS 
THTAi PROJECT 
MITIGATION 
EPA 
•1,640,000 
$1,262,000 
S200,000 
B. 
UNOBLIGATED MITIGATION FUNDS REMAINING 
C. 
COSTS fc BALANCES as of 6/X6/90 
DGN 
KE3042 
KE3069 
KE3073 
KCOOOS 
OBLIGATED 
AMOUNT 
S250,000 
500,000 
2:30,000 
2fi?.0O0 
EXPENDED 
AMOUNT 
•250,000 
375,081 
0 
O 
$1,262,000 
Subtotal 
Other Costs 
TAT SalaryNTravel as of 6/16/90 
EPA S.ilaryNTravel ac of 6/16/90 
Estimate of Total 
Expenditures to Date 
D. CEILING PERCENTAGES 
TnTAJ PROJELT 
MIT I OAT ION 
40X 
SOX 
PERCENTAGE OF *2 MILLION 
37Z 
«625,081 
63,366 
48,097 
»736,544 
EPA 
24X 
TAT 
•105,000 
SO 
BALANCE 
•0 
124,919 
2bO,000 
262,000 
•636,919 
TAT 
607. 
FINAL POLREP 
FUTURE 
POLREPS 
_FORTHCOMING 
SUBMITTED BY 
John h i g g i n s ^ ^ C 
gy^ns 
>-'(^ 
On-Scene C o o r d i n a t o r 
Response and 
t-revention BrMui.ii 
DATE RELEAStU 
'''^. '"??A 
301558 
I • i 
U . S . 
ENVIRONMENTAL PROTECTION AGENCY 
P O L U m O N REPORT 
Region II 
Response and Prevention Branch 
Edison, Nev Jersey 08837 
(201) 548-8730- Concnercial and FTS 
24 Hour Emergency 
DATE: June 20, 1990 
TO: C. Sidamon-Eristoff, 
EPA 
W. Muszynski, EPA 
R. Caspi, EPA 
R. Sallcie, EPA 
J. Marshall, EPA 
G. Pavlou, EPA 
ERD, WH-548B 
(E-Mail) 
' B. Sprague, EPA 
G. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
liEPC 
TAT 
POLREP NO.: 
SITE NO.: 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
1. 
SITUATION; 
(17) 
Seventeen 
4V 
Lab (^lemicals. Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, DS Virgin Islands 
Approximately 566 Known Lab Chemicals, 590 
Unlcnown Lab Chemicals, 210 Dirums, 240 Empty 
Drums, 2uid 22 Tanlcs. Possibly Asbestos and 
Dioxin Containing Materials 
Ground water, Caribbeem Sea 
Phase II Removal Action continues. 
2. 
ACTION TAKEN: 
A. June 18, 1990, ERCS mobilized a subcontractor (drum crush 
operator) on site and continued overpacking . 
Initiated and 
completed labpacking, waste paint inventory and drum segregation. 
An air freight container was delivered to the site. 
ERCS resampled drum numbers 81, 163 and 164 for disposal analysis 
and waste streaun. 
This was the only additional drum sampling 
301559 
I . ' 
conducted in Phase II. 
ERCS will nanifest, with material safety data sheets (MSDS), the 
drums containing Benzyl chloride as a seperate waste stream. ERCS 
indicated that the Benzyl chloride may have to be put in one gallon 
charges. It was then decided that the Benzyl chloride will not be 
repacked vintil it is known how Chem Waste and other disposal 
facilities will acx:ept the Benzyl chloride. This may not be Icnovn 
until completion of Phase II. 
In addition, EPA directed ERCS to contacrt "Velsicol", the 
manufacturer, as to returning the drums of Benzyl chloride, which 
have manufacturer seals. 
Cyprian King, Fire Cliief re-certified the explosive permit. 
EPA contacted the following : Jet Research in Dallas, Arrow zind 
Four Star, both in San Juan, several times and successfully 
arranged for explosives to be delivered to St. Croix at 1330 hours. 
Explosives arrived at 1400 hours and were cleared through Customs 
by EPA and ERCS. 
ERCS informed EPA that drum crushing equipment is in Port 
Elizeibeth, NJ. EPA was informed that equipment would be in St. 
Croix at 14 00 hours on June 19, 1990. 
EPA apprised ERCS that they (ERC:S) and their subcontractors have 
managed equipment and supply delivery inadequately. It took zm 
extended effort by EPA to get the explosives in St. Croix. 
EPA faxed and received back a fax of release form for transmittal 
of Uranyl acetate and Merciiry (metallic) compounds to Poly 
Sciences, Inc. a recycling/reusing facility. 
B. June 19, 1990, EPA, TAT, DPNR and ERCS attended a Contingency 
Planning Meeting to set a new date for the detonation. 
EPA, TAT and ERCS 
meet with the Deputy Commisioner of DPW to 
schedule a new date for the detonation. 
ERCS sampled drum numbers 81, 163 and 164. ERCS also overpacked 
t h e spent wet cell batteries on site. In addition, ERC:S completed 
labeling of l2±>packs. 
ERCS informed EPA that there is a problem with a five (5) gallon 
can of asbestos and mineral spirits (flashing cement). This roofing 
material (mineral spirits) caruiot be landfilled and 
cannot be 
incinerated. Dave Martin, of Chem Waste attempted to see if Chem 
Waste would accept the material. A material profile was sent. 
ERCS informed EPA that they are "uncomfortable* shipping a glass 
container of Mercury (metallic) to Poly Sciences, Inc. ERCS stated 
that they would prefer shipping the material in a welded steel 
conical container,which is the single package specification for air 
shipment of Mercury for DOT and Intemational Air Transport 
301560 
# 
Association (LATA) regulations. 
EPA indicated that this would 
entail the following: package shipment, receipt, clearing customs 
and VI excise tax and transferring Mercury from glass container to 
steel container. EPA then recommended that ERCS proceed with 
alternate packaging (overpacking) in accordance with DOT and lATA 
shipping regulations. ERCS questioned whether EPA was compelling 
them to do something that they (ERCS) was "uncomfortable" with. 
OSC responded that he would sign the shipping papers. 
Drum crushing equipnient was shipped from JFK airport, but did not 
arrive in St. Croix as it vas taken off the plane in St. Thomas. 
C. June 20, 1990, TAT provided all necessary notific:ations 
regarding the detonation, including St. Croix Prison, Police, Fire, 
EMS, DPW , St. Croix STP, Alexander Hamilton Airport, FAA, and 
businesses near the airport and landfill. 
ERCS completed restaging of drums. 
EPA discussed packaging of Mercury with ERCS. 
ERCS chemist 
informed EPA that he has contacted All-PAK 2md that they informed 
him that their container is acceptable for overpacking the glass 
container of Mercury. 
EPA indicated to ERCS that they should 
further safeguard shipment by placing materialin overpacked metal 
can with vermiculite . ERCS agreed to overpack materials, but is 
still uncomfortable. OSC signed shipping papers. 
Drum crushing equipment ai-rived on St. Croix emd will be delivered 
tomorrow. 
3. 
FUTURE PLANS AND RECOMMENDATIONS: 
A. Detonation of shock sensitives and cylinders off-site at 
landfill will take place on June 21, 1990. 
B. TAT will notify the NRC of the environmental release within one 
hour after final detonation. 
C. Drum crushing will be initiated upon arrival of the drum 
crushing equipment. 
D. TAT will perform sampling of the WAPA and VIPA wells nearest the 
site on June 22, 1990, contigent upon CLP Lab selection. 
E. Transportation of labpacked materials and paint waste will be 
coordinated with mini-removals at DVI on June 25, 1990, and June 
26, 1990. 
F. Phase II Site Demobilization. 
G. The OSC will review the results of the dioxin data analyzed froa 
the three five (5) gallon containers. 
301561 
• ^ 
f " 
# 
4 . 
FINANCIAL ACCOUNTING 
A. CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
$1,840,000 
$1,262,000 
$200,000 
B. UNOBLIGATED MITIGATION FUNDS REMAINING 
C. COSTS & BALANCES as of 6/20/90 
DCN 
KE3042 
KE3069 
KE3073 
KE3085 
Subtotal 
Other Costs 
Estimate of Total 
Expenditures to Date 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
421 
PERCENTAGE OF $2 MILLION 
38% 
FUTURE 
POLREPS 
FORTHCOMING 
TAT 
$105,000 
$0 
OBLIGATED 
AMOUNT 
$250,000 
500,000 
250,000 
262,000 
$1,262,000 
of 6/20/90 
of 6/20/90 
MITIGATION 
51* 
EXPENDED 
AMOUNT 
$250,000 
398,823 
0 
0 
$648,823 
68,706 
49,867 1 
$767,396 
EPA 
25* 
BALANCE 
$0 
101,177 
250,000 
262,000 
$613,177 
TAT 
65 
FINAL POLREP 
SUBMITTED BY 
John Higgins 
On-Scene Coordinator 
Response and 
Prevention Branch 
li 
DATE RELEASED 
301562 
/\:yV^O 
zy 
U.S. ENVIRONMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
Region 11 
Response and Prevention Branch 
Edison, New Jersey 0883/ 
(201) 548-8730- Commercial and FTS 
24 Hour Emergency 
POLREP NO.: 
SITE NO.: 
POLLUTANT: 
CLASSIFICATION! 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
DATE: June 23, 1990 
TO: C. Sidamon-Eristoff, 
EPA 
W. Muszynski, EPA 
R. Caspe, EPA 
R. Salkie, EPA 
J. Marshall, EPA 
G. Pavlou, EPA 
ERD, WH-54BB 
(E-Mail) 
B. Sprague, EPA 
G. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
LEPC 
TAT 
Eighteen (18) 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
Approximately 566 Known Lab Chemicals, 590 
Unknown Lab Chemicals, 210 Drums, 240 Empty 
Drums, and 22 Tanks. Possibly Dioxin 
Containing Materials. 
Ground water, Caribbean Sea 
1. 
SITUAjriDN: 
Phase 11 Removal Action continues. 
2. 
ACTION _ T^KEN: 
A . 
J u n e 
2 1 , 
1 9 9 0 , 
d e t o n a t i o n 
o f 
s h o c k 
s e n s i t i v e s 
o r 
r e a c t i v e 
m a t e r i a l s 
and 
c y l i n d e r s 
c o n d u c t e d 
b e t w e e n 
0 6 0 0 - 0 8 0 0 
h o u r s 
a t 
A n g u i l l a 
l a n d f i l l . 
EPA n o t i f i e d 
NRC o f 
t h e 
e n v i r o n m e n t a l 
r e l e a s e 
w i t h i n 
a 
h a l f - h o u r 
301563 
bIRCS initiated and completed drum crushing. 
ERCS prepared galley 
trailer for demobe. ERCS demobed explosive expert. 
B. June 22, 1990, EPA (Higgins) and TAT (Bechtel) demobed from 
site. 
ERCS 
demobed 
foreman 
and 
drum 
crush 
operator 
(subcontractor). 
ERCS 
continued 
general 
site 
clean-up 
and 
preparation 
for 
demobi1i zation. 
Box trailer for labpacked materials and paint waste arrived on 
si te. 
C. June 23, 1990, Dave Martin from Chem Waste informed EPA that 
the box t r a i l e r delivered to site is owned by "Tropical" and they 
a r e not allowed to transport hazardous waste. 
Loading of labpacks onto appropiate boxtrailer postponed until 
arrangements can be made with hazardous waste transporter. 
ERCS demobed three personnel from site. 
3. 
FUTURE PLANS AND RECUMMENDATIONS; 
A. TAT will perform samplinq of the WAPA and VIPA wells nearest 
the site on June 25, 1990. 
B. Transportation of labpacked materials and paint waste will be 
coordinated with mini-removals at UVI. 
Scheduling of hazardous 
waste transportation is unknown at the present time; and may be 
determined on June 25, 1990. 
C. Phase II Site Demobilization. 
D. The OSC will review the results of the dioxin data analyzed from 
the three five (5) gallon containers. 
301564 
-. 1 
^ • 
PJ.NANCJ AL ACCOUNTING 
A. 
CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
SI,840,000 
SI,262,OOO 
S20O,00O 
B. 
UNOBLIGATED MITIGATION FUNDS REMAINING 
C. 
COSTS & BALANCES as of 6/20/90 
DCN 
KE3042 
KE3069 
KE30/3 
KE3085 
Subtotal 
Other Costs 
Estimate of Total 
Expenditures to Date 
TAT 
S105,0O0 
so 
OBLIGATED 
AMOUNT 
S250,000 
500,000 
250,000 
262,000 
SI,262,ooo 
of 6/20/90 
of 6/20/90 
EXPENDED 
AMOUNT 
S250 
398 
S648 
68 
^9, 
S767 
,000 
,823 
O 
0 
,823 
,706 
,867 
,396 
BALANCE 
101, 
250, 
262, 
•613, 
SO 
177 
ooo 
000 
.177 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
427. 
PERCENTAGE OF S2 MILLION 
387. 
FUTURE 
POLREPS 
L POLREP 
F0RTHC0M1NG_X 
MITIGATION 
517. 
&\ n-
SUBMITTED BYJV, 
EPA 
257. 
\\ rx i 
- V) ^ 
r 
3-o<W\52rV\r 
TAT 
657. 
\ 
\ 
v<>5\Avi*iSl 
John Hoggins 
On-Scene Coordinator 
Response and 
Prevention Branch 
-W
DATE RELEASED 
301565 
U . S . ENVIROhiMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
Region 
I I 
Response and P r e v e n t i o n 
Branch 
E d i s o n , New J e r s e y 
08837 
(201) 
548-8730- Commercial and FTS 
24 Hour Emergency 
POLREP NO.: 
SITE NO.: 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
DATE: J u l y 12, 
1990 
TO: C. 
S i d a m o n - E r i s t o f f , 
EPA 
W. Muszynski, EPA 
R. Caspe, EPA 
R. S a l k i e , EPA 
J . M a r s h a l l , EPA 
G. Pavlou, EPA 
ERD, WH-548B 
(E-Mail) 
B. Sprague, EPA 
G. Zachos, EPA 
P. G e l a b e r t , EPA 
A. Smith, VIDPNR 
LEPC 
TAT 
Nineteen (19) 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
Approximately 566 Known Lab Chemicals, 590 
Unknown Lab Chemicals, 210 Drums, 240 Empty 
Drums, and 22 Tanks. 
Possibly, Dioxin 
Containing Materials 
Ground water, Caribbean Sea 
1. 
SITUATION: 
Phase II of Removal Action completed. 
2. 
ACTION TAKEN: 
A. June 25, 1990, VITELCO restores phone service. TAT samples VIPA 
and WAPA wells, packages samples, and ships samples via FedEx. 
This completes all TAT work on-site. Dave Martin of ChemWaste 
informs EPA that Trailer Marine Transport (TMT) is a certified 
hazardous waste transporter. TMT spots box trailer on-site for 
labpack loading. 
B. June 26, 1990, EPA reviews ERCS memo regarding theft of 
treatment pool and aluminum stairs between Phase I demob (1/24/90) 
and Phase II mob (6/11/90). 
ERCS demobilizes the galley trailer and air compressor. The bomb 
box is picked up at the site for .transport to EPA, Edison. 
ERCS contacts John Bergman of Velsicol regarding the possible 
301566 
reclaim of the eight, 55 gallon benzyl chloride drums. Velsicol 
vill consider and contact EPA. 
ETC informs OHM who informs EPA that additional compatibility 
testing revealed unacceptable reactions for drum nos. 159 and 75 
within the acid liquid group and dnim no. 133 within the base 
neutral group. Additional four quart samples are taken from each 
of these drums. ERCS also informs EPA that the bench scale testing 
for d m m no. 81 indicated that neutralization of the acetic acid 
would generate 3-4 additional drums of waste. 
AOSC informs ERCS of his approval to reimburse ERCS for replacenent 
of aluminum stairs and treatment pool. The basis for this decision 
is EPA's prior determination, as documented in a November 27, 19S9 
EPA letter to ERCS, to not provide security while off-site. 
EPA informs ERCS to provide landfill/incineration analysis for the 
crushed drum sample. 
C. June 27, 1990, ERCS packages samples for drum nos 81,75, 159, 
and 133 and arranges transport via Four Star Transport to San Juan 
Airport where the samples will be shepherded by TAT, who will 
retain the services of a custom clearance broker, and will be 
transferred to FedEx for delivery to ETC, Findlay. 
Dave Martin of ChemWaste packages the 1 quart glass container of 
mercury waste and ships material to Bethlehem Apparatus, 
Hellertown, PA. (EPA IDI PAD002390961). 
Box trailers, loaded with labpacks, are transported to the 
container port and clear U.S. Customs. 
Phase II demobilization completed. ERCS and EPA leave site. 
D. June 29, 1990, AOSC discusses compliance status of Trade Waste 
Incinerator (TWI) with Region V and there is no problem with 
sending CERCLA wastes. Also, the status of Bethlehem Apparatus is 
discussed vith Region 3 and they are in compliance. 
TAT delivers Detonation Report Summary. 
OSC mails letter to Mr. Cherra Hyliger, Deputy Commissioner of 
Operations for the Public Works Department, detailing the June 21, 
1990 detonation of VIChem hazardous waste materials at the Anguilla 
Landfill and addressing his concerns regarding pubic health. 
E. July 2, 1990, AOSC arranges to meet Dave Martin of ChemWaste at 
Port Everglades to clear hazardous waste through. U.S. Customs. 
FedEx informs ERCS who informs EPA that Analab is not an approved 
lab for the receipt of "soil from a foreign land", which was the 
shipping paper description for the crushed drum samples. ERCS 
arranges for the sample to be transported to the NYTEST lab, which 
is a US Dept. of Agriculture and US (^istoms approved lab, for 
analysis. 
301567 
TAT informs EPA that the driim sanples are still in San Juan at the 
Four Star Company and that TAT cannot provide the transfer services 
requested by EPA because such work would constitute "personal 
services". 
EPA holds several heated discussions with the TAT 
leader and the TAT Zone Management before TAT agrees to provide the 
requested transfer sezrvices. The VIChem drum samples clear customs 
and leave San Juan via FedEx. 
Off-Site Facility Selection checklists completed for TWI and 
Bethlehem Apparatus are approved by Bruce Sprague. 
F. July 3, 1990, ERCS informs EPA that the mercury product and 
Uranyl acetate arrived at Polysciences intact. 
OSC discusses the matter of the stolen aluminum stairs and 
treatment pool with the Contract Officer, Tim Grier. He agrees 
that, since EPA decided not to demobilize equipment and to not 
provide security vhile off-site (as documented in the November 27, 
1989 letter), replacement of this equipment is an eligible cost and 
he approves of the expenditure. 
G. July 5, 1990, AOSC arrives in Florida and meets with U.S. 
(Customs officials and Crcwley Maritime Corp. at Port Everglade. 
Customs inspector is confused as to the appropriate "PL No." to be 
entered on Customs Form 7523 and requests EPA to return tomorrow. 
H. July 6, 1990, VIChem and St. Croix "mini-removal* hazardous 
waste clears Customs (PL No. is 3209.90*00004). Crowley trailers 
are inspected by AOSC and all dmms are intact, no leaking or 
damaged drums. 
Drums are transferred from Crowley trailer to 
ChemWaste Truck by ChemWaste. ChemWaste Truck, which is placarded 
"Dangerous", "Poison", and "Flammable", departs Port Everglade. 
I. July 9, 1990, OSC reviews status and plans for disposal 
analyses. 
ERCS agrees to furnish revised bulking scheme and 
informs EPA that drum samples are scheduled to arrive at Analab 
today for 21 day turnaround analysis. 
J. July 10, 1990, OSC discusses possible reclaim of the benzyl 
chloride drums with Mr. Bergman of Velsicol. He informs OSC that 
he had passed the matter on to Velsicol, Memphis and that someone 
from that office should have contacted EPA. 
OSC informs Mr. 
Bergman that he would again contact him if no word is heard from 
other Velsicol representatives. At this point, reclaim of this 20 
year old product does not appear to be promising. 
OSC directs ERCS to furnish drum location map and inventory of 
unused supplies at VIChem. 
301568 
3. 
FUTURE PL^NS AND RECOhtMENDATIONS: 
A. The OSC vill prepare an Action Memo requesting a twelve month 
time limit extension. 
B. The OSC will review expended and expected costs and determine 
whether a request for additional monies is necessary. 
C. The OSC will review the results of the dioxin data analyzed from 
the three five (5) gallon containers. 
D. TAT vill complete Phase II photodocumentation. 
E. TAT vill complete Phase II well sample analysis summary. 
F. Analab vill complete disposal analyses. 
G. ERCS will transmit analytical data to EPA and procure drum 
disposal facility. 
H. Phase III will be planned and mobilized. 
301569 
4 . 
FINANCIAL ACC0UN7TNG 
A. 
CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
$ 1 , 8 4 0 , 0 0 0 
$ 1 , 2 6 2 , 0 0 0 
$ 2 0 0 , 0 0 0 
B. 
UNOBLIGATED MITIGATION FUNDS REMAINING 
C. 
COSTS & BALANCES a s o f 
6 / 2 3 / 9 0 
TAT 
$ 1 0 5 , 0 0 0 
$0 
DCN 
KE3042 
KE3069 
KE3073 
KE3085 
Subtotal 
Other Costs 
TAT Salary\Travel as 
EPA Salary\Travel as 
Estimate of Total 
Expenditures to Date 
D. CEILING PERCENTAGES 
TOTAL PROJECT j 
45% 
PERCENTAGE OF $2 MILLION 
41% 
FURTHER 
POLREPS 
AL POLREP 
FORTHCOMING_X 
\ . 
OBLIGATED 
V 
AMOUNT 
$250,000 
500,000 
250,000 
262,000 
$1,262,000 
Of 7/6/90 -
of 7/12/90 
MITIGATION 
54% 
._ SUBMITTED BY. 
DATE RELEASED^^ 
EXPENDED 
BALANCE 
AMOUNT 
$250,000 
$0 
434,673 
65,327 
0 
250,000 
0 
262,000 
$684,673 
$577,327 
80,880 
62,387 
$827,940 
EPA 
TAT 
31% 
77% 
^ ^ > y 
John Higgins 
On-Scene Coordinator 
Response and 
Prevention Branch 
ZVUii^^-i. A-K^O 
3 0 1 5 7 0 
u 
U.S. ENVIRONMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
/^^GumQA 
^n. 
Region II 
Response and Prevention Branch 
Edison, Nev Jersey 08837 
(201) 548-8730- Commercial and FTS 
24 Hour Emergency 
POLREP NO.: 
SITE NO.: 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY; 
1. 
SITUATION; 
DATE: August 3, 1990 
TO: C. Sidamon-Eristoff, 
EPA 
W. Muszynski, EPA 
R. Caspe, EPA 
R. Salkie, EPA 
J. Marshall, EPA 
;E.Schaff, EPA» 
G. Pavlou, EPA 
ERD, WH-548B 
(E-Mail) 
B. Sprague, EPA 
G. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
LEPC 
TAT 
Twenty (20) 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
Approximately 566 Known Lab Chemicals, 590 
Unknown Lab Chemicals, 210 Dmms, 24 0 Empty 
Drums, and 22 Tanks. 
Possibly, Dioxin 
Containing Materials 
Ground water, Caribbean Sea 
Emergency response to a report of a fuming drum. 
2. 
ACTION TAKEN: 
A. July 24, 1990, Jim Southerland of VIAG informs EPA that a dnim 
housed in the warehouse at VIChem is fuming. The OSC contacted TAT 
and ERCS and instructed them to prepare for site mobilization. 
B. July 25, 1990, the OSC and 1 TAT personnel arrive on-site and 
determined the fuming drum to be drum no. 22. A review of the drum 
logs indicated that this vas one of sixteen drums containing benzyl 
chloride. Benzyl chloride is a corrosive liquid, a severe skin 
irritant, and will volatilize to form hydrochloric acid. 
A 
previous response to a fuming drum emergency was conducted in May 
1990 and is the main subject of POLREP #14. The OSC confirmed ERCS 
mobilization for the next day. A single site telephone line (#809-
778-2199) was operational. 
TAT vas instructed to furnish a 
301571 
-.-.s 
# 
m 
Material Safety Data Sheet (MSDS) for benzyl chloride in the event 
that it became imperative to ship this material off St. Croix. 
C. July 26, 1990, the OSC visited the Virgin Island Department of 
Planning and Katxiral Resources office in Christiansted and informed 
Mr. Leonard Reed of the emergency situation at VIChem. 
3 ERCS 
mobilize to site in the late afternoon. The plan to stabilize the 
fuming drum, to inspect all other benzyl chloride drums, to obtain 
additional sample from drum #81, and to ship the benzyl chloride 
samples stored on-site is discussed. 
OSC informs ERCS that 
material transfer of benzyl chloride to poly drums will only be 
conducted if the drum is fuming because of drum deterioration. 
Generator vas started and all electric equipment functioned. 
However, only the single site telephone line was operational. Only 
2-150# air cylinders, vhich will be needed to supply the ERCS 
airline, are full. 
C. July 27, 1990, no site telephone line is operational. Based on 
previous arrangements, OSC utilizes VIAG phone line with his EPA 
AT&T card. 
TAT purchases 2 floor fans, which will be used to 
ventilate the warehouse, and obtains a fax of benzyl chloride MSDS. 
ERCS enters Hot Zone in Level B Acid Splash Suits. ERCS loosens 
overpack lid of fuming drum #22, obtains additional 3 quarts of 
sample from drum #81, and informs OSC that drum #26, another benzyl 
chloride drum, is fuming lightly. ERCS packages samples for drum 
no. 81 and 3 quart samples of benzyl chloride. ERCS drops off 5-
150# air cylinders for recharge. After warehouse is, ventilated, 
ERCS reenters Hot Zone, removes overpack lids for all sixteen 
benzyl chloride, reinstalls missing bungs on drum nos. 22, 26 and 
21, stabilizes these drums with lime, replaces overpack lids, and 
returns drums to pallets. OSC warehouse inspection indicates that 
the drums have been successfully stabilized. 
TAT arranges transport of samples via Four Star Transport to San 
Juan Airport (SJA) where the samples will be transferred to FedEx 
for shipment to the mainland. TATL Henne, who had conferred with 
TAT Zone management, instructs TAT member Bechtel that TAT cannot 
procure the customs broker services necessary at SJA, as this would 
constitute "personal services". Without success, OSC discusses 
matter with TATL Henne and reminds him of the two previous 
occasions in January and June, 1990 when TAT provided the same 
services being requested. OSC confers with Jennifer Johnson, who 
was standing in for the EPA TAT project officer, Karen Tomimatsu. 
After conferring with Sue Anderson, Ms. Johnson advised OSC to 
contact Ms. Tomimatsu on Monday. OSC responded that there was a 
need to settle this issue but that the problem at hand had to be 
resolved this afternoon. OSC instructed ERCS that they would have 
to provide for clearing sample packages through U.S. Customs in San 
Juan. 
D. July 28, 1990, ERCS picks up a7x3 delivers the 5 fully charged 
air cylinders to VIChem. OSC again inspects warehouse; inspection 
indicates that the drums have been successfully stabilized. EPA, 
TAT, and ERCS demob site. 
301572 
# 
E. July 31, 1990, OSC reviews and approves VIChem Invoice #6. 
F. 
August 1, 1990, OSC drafts request to the Regional 
Administrator for. exemption from the 12 month time limit and an 
increase to the total project ceiling. If approved this increase 
would establish a new total project ceiling of $1,950,000. 
G. August 2, 199 0, OSC and jJp€__R.otola, the OSC for the Virgin 
Island mini-removals, review the costs being charged by ChemWaste 
for the joint labpack disposal. Manpower costs are distributed 
based on the site entry logs whereas transportation and disposal 
costs are apportioned by the weight of labpacks at each site. Total 
costs to be charged to VIChem for ChemWaste services is $53,066.10. 
3. 
FUTURE PLAJJS AND RECOMMENDATIONS; 
A. The OSC vill review the results of the dioxin data analyzed from 
the three five (5) gallon containers. 
B. TAT vill complete Phase II photodocumentation. 
C. TAT vill complete Phase II well sample analysis summary. 
D. Analab vill complete disposal analyses.' 
E. ERCS vill transmit analytical data to EPA and pirocure drum 
disposal services. 
F. Phase III will be planned and mobilized. 
301573 
4 . 
FINANCIAL ACCOUNTING 
A. 
CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
$1,840,000 
$1,262,000 
$200,000 
B. UNOBLIGATED MITIGATION FUNDS REMAINING 
C. COSTS & BALANCES as of 6/23/90 
DCN 
KE3042 
KE3069 
KE3073 
KE3085 
OBLIGATED 
AMOUNT-
$250,000 
500,000 
250,000 
262,000 
EXPENDED 
AMOUNT 
$250,000 
434,673 
0 
0 
$1,262,000 
Subtotal 
Other Costs 
TAT Sa1ary\Travel as of 7/6/9 0 
EPA Salary\Travel as of 7/12/90 
Estimate of Total: 
Expenditures to Date 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
45% 
PERCENTAGE OF $2 MILLION 
41% 
MITIGATION 
54% 
$684,673 
80,880 
62,387 
$827,940, 
EPA 
31% 
TAT 
$105,000 
$0 
BALANCE 
$0 
65,327 
250,000 
262,000 
$577,327 
TAT> 
77% 
FINAL POLREP 
FURTHER 
POLREPS 
F0RTHC0MING_2(_ SUBMITTED B 
DATE RELEASED 
John Higgins 
On-Scene Coordinator 
Response and 
Prevention Branch 
301574 
c 
cc r 2 4 I9-; 
m 
U . S . 
EN-VIRONMENTAL PROTECTION AGENCY 
POLLUTION REPORT 
Region II 
Response and Prevention Branch 
Edison, New Jersey 08837 
(201) 548-8730- Commercial and FTS 
2 4 Hour Emergency 
DATE: September 7, 1990 
TO: C. Sidamon-Eristoff, 
EPA 
W. Muszynski, EPA 
R. Caspe, EPA 
R. Salkie, EPA 
J. Marshall, EPA 
E. Schaff, EPA 
G. Pavlou, EPA 
ERD, WH-548B 
(E-Mail) 
B. Sprague, EPA 
G. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
LEPC 
TAT 
POLREP NO.: 
SITE NO.: 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
1. 
SITUATION; 
Twenty One (21) 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
Approximately 566 Known Lab Chemicals, 590 
Unknown Lab Chemicals, 210 Drums, -24 0 Empty 
Drums, and 22 Tanks. Including, Dioxin 
Containing. Materials 
Ground water, Caribbean Sea 
# 
Disposal arrangements underway for Phase III. 
2. 
ACTION TAKEN; 
A. August 6, 1990, OSC reviews total waste analysis data for 
suspected dioxin-containing material. This material consists of 
two (2) five gallon containers of "Weedox". Total waste analysis 
data for this material indicate that 2,3,7,8 Tetrachlorodibenzo-
dioxin (TCDD) was not detected but significant levels of Octo-
chlorodibenzodioxin (OCDD) and Heptachlorodibenzodioxin (HpCDD) 
and furans were measured. OSC contacts Paul des Rosiers, Chair-
man of the EPA Dioxin Disposal Advisory Group, regarding disposal 
options for the "Weedox" herbicide and OSC faxes Paul a copy of 
the Analytical Data Summary. 
301575 
-ej 
B 
^ 
B. August 7, 1990, OSC revievs TAT costs with TATM Bechtel. TATM 
Bechtel informed OSC that certain TAT preliminary assessment-
type costs vere planned to be be transferred from TAT's Removal 
Account for VIChem to TAT's Preliminary Assessment Account for 
VIChem. Accordingly, TAT has been furnishing cost figures vhich 
vere adjusted downward for POLREP purposes. Hovever, since the 
Technical Direction Document (TDD) for the VIChem Preliminary 
Assessment is closed out, there is no possibility of proceeding 
vith the planned transferral. Therefore, all future POLREPs, 
including this POLREP, will shov all current TAT costs charged to 
the VIChem Removal Action. 
C. August 10, 1990, Paul des Rosiers contacts OSC and informs OSC 
that because of the small quantity of the "Weedox" material and 
the absence of TCDD, he recozimends that the "Weedox" be applied 
on-site vith respiratory protection in accordance with 
manufacturer instructions. According to Paul's 8/13/90 memo to 
the OSC, such application "will result in the promotion of UV 
photolytic destruction of not only the active ingredients but the 
CDD's (dioxins) and CDF's (furans) as well." Furthermore, the 
alternative of removing and disposing of this material requires 
pretreatment to reduce the CDDs and the GDFs and there are no 
permitted facilities in the U.S. to accomplish this requirement. 
D. August 31, 1990, Regional Administrator approves Action Memo 
granting a time limit extension and increasing the total project 
ceiling to $1,950,000. 
E. September 4, 1990, ERCS informs OSC that all disposal analyses 
have been completed. OSC directs ERCS to solicit for drum 
disposal. 
F. September 7, 1990, OSC revievs ERCS draft, disposal 
solicitation letter. VIChem drum disposal will be coordinated 
with drum disposal for St. Croix mini-removals. Upon selection 
of disposal company, ERCS will prepare waste profiles for OSC 
review and approval. 
3. 
FUTURE PLANS AND RECOMMENDATIONS; 
A. TAT will complete Phase II photodocumentation. 
B. TAT will complete Phase II well sample analysis summary. 
C. ERCS will procure disposal facilities for VIChem drummed 
waste. 
D. Phase III will be planned and mobilized. Project exigencies 
and EPA budget constraints indicate that Phase III mobilization 
will occur sometime after the latter half of October 1990. 
301576 
FINANCIAL ACCOUNTING 
A. CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
$1,950,000 
$1,516,000 
$200,000 
B. UNOBLIGATED MITIGATION FUNDS REMAINING 
C. COSTS i BALANCES as of 7/25/90 
DCN 
KE3042 
KE3069 
KE3073 
KE3085 
OBLIGATED 
AMOUNT 
$250,000 
500,000 
250,000 
262,000 
EXPENDED 
AMOUNT 
$250,000 
500,000 
10,489 
0 
$1,262,00,0 
Subtotal 
Other Costs 
TAT Salary\Travel as of 8/31/90 
EPA Salary\Travel as of 9/7/90 
Estimate of Total 
Expenditures to Date 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
50% 
PERCENTAGE OF $2 MILLION 
49% 
MITIGATION 
50% 
$760,489 
152,261 
71,649 
$984,399 
EPA 
36% 
TAT 
$195,000 
$254,000 
BALANCE 
$0 
0 
239,511 
262,000 
$501,511 
TAT 
78% 
FINAL POLREP 
FURTHER 
POLREPS 
FORTHCOMING_X SUBMITTED BY 
DATE RELEASED 
John Higgins 
On-Scene Coordinator 
Response and 
Prevention Branch 
301577 
U.S. ENVIRON-MENTAL PROTECTION AGENCY 
POLLUTION REPORT 
DATE: November 8, 199 0 
Region II 
Response and Prevention Branch 
Edison, New Jersey 08837 
(201) 548-8730 - Commercial and 
24 Hour Emergency 
TO: 
FTS 
Sidamon-Eristoff, 
Muszynski, EPA 
Caspe, EPA 
Salkie, EPA 
Marshall, EPA 
Pavlou, EPA 
Schaaf, YiVhTyy 
ERD, WH-548B, 
(E-Mail) 
Sprague, EPA 
Zachos, EPA 
Gelabert, EPA 
Smith, VIDPNR 
VIDPNR 
C. 
W. 
R. 
R. 
J. 
G. 
I? 
B. 
G. 
P. 
A. 
EPA 
LEPC, 
TAT 
POLREP NO.: 
Site NO.; 
POLLUTANT: 
CLASSIFICATION; 
SOURCE: 
LOCATION: 
AMOUNT; 
WATER BODY; 
1. 
SITUATION; 
(22) 
Twenty Two 
4V . 
Lab Chemicals, Alcohols, Solvents, Acids 
Ma j or 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
Approximately 566 Known Lab Chemicals, 590 
Unknown Lab Chemicals, 24 0 Drums, 24 0 Empty 
Drums, and 22 Tanks. 
Ground vater, Caribbean Sea 
Disposal arrangements underway for Phase III. 
2. 
ACTION TAKEN: 
A. 
September 21, 1990, OSC received copy of ERCS disposal 
solicitation letter with list of bidders. Since one of the bidders 
is an ERCS subsidiary company, OSC directed ERCS to instruct 
bidders to mail all bids to OSC to avoid the potential for ERCS 
conflict of interest. 
B. 
October 3, 1990, The videotape of the June 1990 detonations 
was distributed to: all local officials who participated in 
coordinating the detonation; the US Coast Guard in San Juan, vho 
observed the detonations; and Sherrel Henry, the RPM. 
301578 
C. 
October 5, 1990, OSC evaluation of disposal bids indicates 
that incineration of the 17 drums of benzyl chloride to be 
prohibitively expensive. 
Only one disposal company bid on the 
Benzyl chloride wastestream. ChemWaste Management bid $170,000. 
for transferal of material from drums to 1 gallon charges, and 
transportation and disposal of material; an alternate bid of 
$130,000. vas submitted by CWM for on-site treatment. OSC decides 
to explore recycling this material. 
D. 
October 9, 1990, Based on their overall low bid for 
transportation and disposal and their prior experience disposing 
of labpacked material in June 1990, OSC selects ChemWaste 
ManagejTient, Inc. (CWM) for disposal of drummed material. Hovever, 
OSC writes letter to CWH requesting a clarification of their bid, 
especially CWM proposed transportation costs ($426/drum). 
E. 
October 18, 1990, OSC completed a "Compendium of Well Water 
Data Collected 
at VIChem by EPA from 1986 to 1990." Over this 
period, there vere five separate sampling events at seven different 
locations. 
The 
data 
consistently 
indicated 
Chloroform 
contamination. The Compendium, complete vith a three dimensional 
color graphic plot, vas distributed to the RPM and VIDPNR and it 
vill be appended to the OSC Report. 
F. 
October 23, 1990, CWM letter reduced transportation costs to 
$3 3 0/drum vhich is acceptable to OSC. 
G. 
October 24, 1990, OSC met vith D & O Chemical company 
representatives and discussed their interest in accepting 17 drums 
of Benzyl chloride product. 
The meeting went well. 
The OSC 
examined company files, including DEA import forms and invoices for 
Benzyl chloride, and determined that the company is a legitimate 
concern actively engaged in importing and wholesaling Benzyl 
chloride. Transportation arrangements vere discussed and vill be 
finalized prior to Phase III mobilization. 
H. 
November 1, 1990, OSC presented a slide show of the 
detonations at the OSC National Conference held in Washington, D.C. 
The presentation was well received with avid interest displayed by 
OSC's in attendance. 
I. 
November 8, 1990, OSC hand delivers signed waste profiles for 
twenty-one wastestreams of drummed material at VIChem for submittal 
to CWM for approval. 
3. 
FUTURE PLANS AND RECOMMENDATIONS 
OSC vill complete plans for removal and disposal of drummed 
material at VIChem. 
301579 
• i 
FINANCIAL ACCOUNTING 
A. CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
TAT 
$1,950,000 
$1,516,000 
$200,000 
$195,000 
B. UNOBLIGATED MITIGATION FUNDS REMAINING 
$254,000 
C. COSTS & BALANCES as of 10/27/90 
DCN 
OBLIGATED 
EXPENDED 
BALANCE 
AMOUNT 
AMOUNT 
KE3042 
$250,000 
$250,000 
$0 
KE3069 
500,000 
500,000 
0 
KE3073 
250,000 
69,000 
181,000 
KE3085 
262,000 
0 
262,000 
Subtotal 
$1,262,000 
$819,000 
$443,000 
Other Costs 
TAT Salary\Travel as of 8/31/90 - 
152,261 
EPA Salary\Travel as of 11/3/90 
77,650 
Estimate of Total 
Expenditures to Date 
$1,048,-911 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
MITIGATION 
EPA 
TAT 
54% 
54% 
39% 
78% 
PERCENTAGE OF $2 MILLION 
52% 
FURTHER 
POLREPS 
FINAL POLREP 
FORTHCOMING_J(_ SUBMITTED BY 
DATE 
John Higgins 
On-Scene Coordinator 
Response and 
Prevention Branch 
RELEASED /V J^^^-^^WyJ^^^-TS^/?^Q 
3 0 1 5 8 0 
- 4 
\ 
U . S . 
ENVIRON-MENTAL PROTECTION AGENCY 
i 
j 
POLLUTION REPORT 
DATE: November 15, 19SO 
Region II 
TO: 
Response and Prevention Branch 
Edison, New Jersey 08837 
(201) 548-8730 - Commercial and FTS 
24 Hour EmBergency 
C. Sidamon-Eristoff, 
W. Muszynski, EPA 
R. Caspe, EPA 
R. Salkie, EPA 
J. Marshall, EPA 
G._ Pavlou, EPA 
tiE. schz^Bif yzpky 
ERD, WH-548B, 
(E-Mail) 
B. Sprague, EPA 
G. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
LEPC, VIDPNR 
TAT 
EPA 
POLREP NO. ; 
Site NO.: 
POLLUTANT: 
CLASSIFICATION: 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY; 
Twenty Three (23) 
4V 
Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
Approximately 566 Known Lab Chemicals, 590 
Unknown Lab Chemicals, 240 Drums, 240 Empty 
Drums, and 22 Tanks. 
Ground vater, Caribbean Sea 
1. SUMMARY OF VANDALISM INCIDENT: 
A. The VIChem Site demobilized on July 27, 1990. During the past 
three veeks, thieves made several break-ins at the Site. Equipment 
left on-site vas stolen and the trailers vere ransacked. 
The intruders broke into the drum storage room and tampered vith 
approximately 40 drums. 
The yellow poly-overpacks previously 
holding the drvims were stolen and removed from the Site. 
On Saturday November 10, 1990, Mr. Adalberto Bosque of the EPA 
Caribbean Field Office (CFO) and TATM's Bechtel and Mentzel arrived 
on the Site and assessed the extent of the situation. 
ERCS 
mobilized to the Site on Sunday November 11, 1990. 
A crew of ERCS and TAT righted the drums, placed fiber pack drums 
on pallets and spread lime inside the warehouse to neutralize 
spilled acid. 
The U.S. Attorney on St. Croix and local enforcement agencies are 
conducting a criminal investigation. 
3 01581 
2. SITUATION/BACKGROUND 
A. See Previous POLREP. 
B. The VIChem Site demobilized in July 1990 vhile EPA awaited 
approval to dispose of the approximately 240 drums remaining in the 
varehouse. 
During this demobilization ERCS and TAT left equipment and gear 
on-site to be used in the final phase of the removal. The decision 
to leave gear on-site vas made due to the high cost of shipment off 
and back on to the island. 
At the time the Site vas demobilized VIAG was preparing to operate 
an alcohol dewatering facility on the property. 
VIAG's owner 
maintained offices in the building on-site. 
3. ACTIONS TAKEN 
A. On Friday, November 9, 1990, the VI Department of Planning and 
Natural Resources (DPNR) inspectors notified EPA a break-in had 
occurred at the VIChem Site. EPA/TAT immediately responded to the 
Site to conduct a preliminary investigation in order to ascertain 
the extent of damage. 
B. On Saturday, November 10, 1990, EPA/TAT arrived at the Site at 
0800 hrs. Mr. Bosque informed OSC of the following observations 
made and recorded by EPA and TAT: 
1. A new "Gateway" was cut into the fence surrounding the 
property. A well-worn pathway had been created in the 
vegetation. This path was obviously made by vehicular traffic 
over a period of time. 
2. The EPA/TAT office trailer had been broken into and 
ransacked. Thieves stole any items which may have had 
any commercial value including chairs, coolers, fax 
machine, five telephones and other items. 
Expendable 
personal protective equipment was not removed. 
The 
intruders apparently entered through a broken window. 
3. The ERCS equipment storage trailer and the decontamination 
trailer were broken into and ransacked. Some items stolen 
included tools, power tools, a washer and dryer, shovels, non-
sparking drum tools, radios and other response gear. 
In 
addition, the four tires on the decon trailer were stolen. 
The ERCS pick-up truck vas stripped of tvo tires, the battery, 
mirrors, radiator, one door and the vindshield vas broken. 
4. VIAG offices vere also ransacked. 
301582 
5. The drum storage area vas also broken into. The intruders 
removed the lids from approximately 42 yellov poly overpacks 
and tipped the contents onto the floor. Several drums were 
broken in this process. Twenty-seven fiber drums containing 
powders, including salicylic acid, were removed from overpacks 
in the front storage room. 
Fifteen poly drums containing 
liquids, including glacial acetic acid, sodium hydroxide and 
other corrosive material, were removed from overpacks in the 
back room. 
Liquid corrosive material vas observed on the 
backroom floor. 
Apparently, this spillage was the former 
contents from Drum # 159 that had contained a corrosive liquid 
but is now empty. This spillage was entirely contained within 
the varehouse. 
6. Items vhich vere not stolen and are apparently in good 
condition are the 125 KW generator, the bobcat, the trailers 
themselves, four SCBA's and other gear. A full inventory is 
available. 
7. On the top level of the distillation tower evidence was 
found that a vagrant had been sleeping on-site. A bed and 
food were found by EPA/TAT. 
After consulting with Mr. Angel Rodriguez', who is the EPA OSC on-
scene at the Muriatti Site in Puerto Rico, OSC activates ERCS to 
respond to the Site and directs ERCS to utilize the Response 
Manager (RM) and two Response Technicians from the Muriatti Site. 
The local police were notified of the incident and dispatched an 
officer to the scene. The VI Police will drive by Site but are 
unable to provide full time security. 
C. On Sunday, November 11, 1990, DPNR visited the Site, agreed to 
coordinate efforts with EPA, assisted in the provision of security, 
and provided EPA with hand-held radios. 
DPNR informs EPA that 
yellow overpacks vere spotted at a St. Croix housing development, 
which is within one mile from the Site. 
Also, DPNR took the 
initiative on the subsequent criminal investigation. DPNR efforts 
in assisting EPA are exemplary. ERCS crew arrives on Site. 
At 
TAT directive, TATM Devine mobilized to site. 
D. On Monday, November 12, 1990, ERCS and TAT make a Level "B" 
Site entry and uprighted the overturned drxims. The trailers were 
cleaned and reorganized. 
At TAT directive, TATM Bergmueller 
mobilized to Site. 
E. On Tuesday, November 13, 1990, ERCS placed all fiber drums on 
pallets and spread six bags of lime around the drums to neutralize 
and stabilize the spilled material. 
A full inventory of all equipment remaining on site was made. 
Also, ERCS was directed to develop a list of stolen equipment and 
a list of equipment necessary to conduct future removal activities 
at the Site. 
301583 
VIDPNR Enforcement vent before the St. Croix Magistrate to obtain 
a seach warrant for the planned raid. When the Magistrate was 
infonr.ed of the nature of the vandalism he instructed VIDPNR to 
coordinate vith Federal Criminal Enforcement Agencies. VIDPNR 
contacted the U.S. Attorney on St. Croix and a meeting vas 
arranged. 
As discussed vith the OSC, Mr. Bosque contacted Mr. Jay Harrison 
of the FBI. Mr. Harrison explained that the FBI had only 2 agents 
in the USVI and they vere stationed in St. Thomas. 
He vould 
contact FBI Offices in Puerto Rico to see vhether they could 
participate in the investigation. 
Mr. Bosque met with the U.S. Attorney's Office on St. Croix, DPNR 
Enforcement, and the local police to discuss the criminal 
investigation and plans. 
A Strike Force raid is planned for 
Thursday, November 15, 1990. 
Besides vandalism at VIChem, the 
Strike Force is also concerned with illegal drug activity at the 
housing development. 
TATM's Mentzel and Bergmueller demobilized from Site. 
The fence surrounding the property was repaired. 
OSC and Mr. Bosque discussed situation with Mr. Gary Nurkin of ORC. 
ORC will contact Mr. Jim Peters of the U.S. Attorneys Office in St. 
Croix and is willing to advise OSC in the event OSC is requested 
to testify before a Grand Jury. OSC leaves messages at OEP, OCI 
and for Mr. Andy Prachak of the CFO. 
OSC contacted Mr. Southerland of VIAG at his home in St. Croix. 
Mr. Southerland informs OSC that vandalism has been ongoing for the 
past three weeks. OSC asked why he did not contact EPA directly, 
or through VIDPNR. • He replied that his files, including his 
personal telephone directory was ransacked and that he did not 
think to go through VIDPNR. He further stated that he encountered 
vandals at Site but he alleged that he did not receive strong 
police support. Police apprehended but released a vandal for no 
apparent good reason. He indicated to OSC that he was abandoning 
VIAG operations at VIChem. 
OSC contacted ChemWaste Management (CWM), the selected disposal 
company, for the purpose of expediting planned disposal activities 
by temporarily storing VIChem drummed material prior to approval 
from disposal facilities. He felt that this could be done, as 
early as the first week in December 1990, but that he would have 
to check with CWM Memphis facility. 
E. On Wednesday, November 14, 1990, TAT assisted the U.S. Attorney 
with preparation of the search warrant affidavit. Mr. Bosque, 
TATM's Bechtel and Devine, and 3 ERCS demobilize Site. 
301584 
Mr. Chris Miller of OCI contacted OSC. OCI will not get involved 
in the criminal investigation of vandalism at VIChem because OCI 
is responsible for pursuing "environmental" crimes. For example, 
if the warehouse spillage reached outside the building to the soil, 
OCI would then be involved. 
Mr. Andy Prachak, ORC Attorney at the CFO, contacted OSC and OSC 
updated him on status of criminal investigation. 
ERCS subcontracts for twenty-four hour security at the Site. 
F. 
On Thursday morning, November 15, 1990, a Strike Force raid 
lead by the VI Police was conducted and 8-10 yellow overpacks were 
recovered and the names of the thieves were learned. ERCS foreman 
assisted the raid, established 24 hour security at the Site, and 
demobilized. 
4. FUTURE PLANS AND RECOMMENDATIONS; 
A. 
EPA will cooperate with the ongoing VI Police criminal 
investigation and any subsequent criminal prosecution. 
B. Drum removal is tentatively scheduled for December 1990. 
301585 
FINANCIAL ACCOUNTING 
A. CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
TAT 
$1,950,000 
$1,516,000 
$200,000 
$195,000 
B. UNOBLIGATED MITIGATION FUNDS REMAINING 
$254,000 
C. COSTS & BALANCES as of 10/27/90 
DCN 
OBLIGATED 
EXPENDED 
BALANCE 
AMOUNT 
AMOUNT 
KE3042 
$250,000 
$250,000 
$0 
KE3069 
500,000 
500,000 
0 
KE3073 
250,000 
69,000 
181,000 
KE3085 
262,000 
0 
262,000 
Subtotal 
$1,262,000 
$819,000 
$443,000 
Other Costs 
TAT Salary\Travel as of 8/31/90 
152,261 
EPA Salary\Travel as of 11/3/90 ' 
77,650 
Estimate of Total 
Expenditures to Date 
$1,048,911 
D. CEILING PERCENTAGES 
TOTAL PROJECT 
MITIGATION . 
EPA 
TAT 
54% 
54% 
39% 
78% 
PERCENTAGE OF $2 MILLION 
52% 
FURTHER 
^ — ^ 
POLREPS 
K 
\ 
D 
/ I-
FINAL POLREP 
FORTHCOMING_X_ SUBMITTED BY ^^^ [ o-KLw^ M ^ ^^''"'^-^ 
John Higgins 
On-Scene Coordinator 
Response and 
Prevention Branch 
DATE RELEASED K ^ Cr-Cr-c^-'tM^iS'k^/^^Q 
301586 
>\kyO 
U.S. ENVIRONMENTAL PROTECTION AGENCY 
FINAL POLUmON REPOR-y 
DATE: October 25, 1991 
Region II 
Response and Prevention Branch 
Edison, New Jersey 08837 
(201) 548-8730 - Commercial and FTS 
2 4 Hour Emergency 
TO: c. Sidamon-Eristoff, EPA 
W. Muszynski, EPA 
K. Callahan, EPA 
R. Salkie, EPA 
J. Marshall, EPA 
G. Pavlou, EPA • 
E. Schaaf, EPA y^ 
C. Berns, EPA 
ERD, WH-548B, 
(E-Mail) -
B. Sprague, EPA 
G. Zachos, EPA 
P. Gelabert, EPA 
A. Smith, VIDPNR 
Y. Canegata, VIDPNR 
TAT 
POLREP NO.: 
Site NO.: 
POLLUTANT: 
CLASSIFICATION; 
SOURCE: 
LOCATION: 
AMOUNT: 
WATER BODY: 
Thirty (30) 
4V 
'Lab Chemicals, Alcohols, Solvents, Acids 
Major 
Virgin Island Chemical Company (VIChem) 
St. Croix, US Virgin Islands 
Approximately 566 Known Lab Chemicals, 59 0 
Unknown Lab Chemicals, 240 Drtuns, 24 0 Empty 
Drums, and 22 Tanks. 
Ground water, Caribbean Sea 
1. SITUATION 
The final phase of site cleanup operations was completed in April 
1991. 
This removal action, which was been pending the final 
disposal of all hazardous material, was completed on October 24, 
1991. 
2. ACTIONS TAKEN 
A. On April 26, 1991, Chem Waste Management (CWM) informed OSC 
that a tractor-trailer containing 21 drums from Wastestream / 5 
(base neutral liquids) was involved in an accident while en route 
to CWM's Lake Charles facility. The accident occurred at 2 AM this 
morning when the truck jack-knifed and collided with an automobile. 
A pregnant female passenger in the automobile was taken to the 
hospital for observation and released the next day with no reported 
problems. No drum material was spilled, the drums were transferred 
to another trailer, and transported to the disposal facility later 
this morning. 
301587 
J i 
, y ^ -* y r ' /,. 
4. FUTURE PLANS AND RECOMMENDATIONS; 
A. Complete review of upcoming 1900-55 forms and invoices. 
B. Completion of OSC Report in FY '92. 
C. Coordinate with ORC on enforcement case. 
D. The OSC will continue working on closing this project out. 
ERCS has requested reimbursement for-approximately $57,000. 
vorth of supplies and equipment that vere stolen or damaged 
during the November 1990 vandalism incident. A complete reviev 
of costs by the OSC, as requested by the Contract Officer, vill 
require that ERCS submit additional documentation. 
5. KEY ISSUES 
In accordance vith the Action Memo and -the CERCLA Off-Site 
Compliance Policy, the following materials were disposed of at off-
site facilities during clean-up activities: over 8,000 pounds of 
laboratory chemicals; 189 - 55 gallon drums of hazardous waste 
chemicals; 40 - 85 gallon drums of miscellaneous hazardous waste 
(i.e., drained batteries, contaminated PPE, and contaminated floor 
sweepings); and 240 crushed empty drums. Approximately 590 unknown 
laboratory containers were opened remotely on-site by rifle and the 
contents solidified into 3 - 5 5 gallon drums that were included in 
drvun disposal operations. 
The following materials were disposed of through ori-site/off-site 
treatment or recycle: 11 compressed gas cylinders and 70 pounds of 
shock-sensitive chemicals were detonated; 43 - 55 gallon drums of 
virgin product were recycled; and 2 five gallon containers of 
herbicide were sprayed on site. 
-^-^•;-
The final draft of the .Site ::.Inspection report was submitted by FIT 
to EPA (ESD) on September *s4r^s=i^l9 91. 
The in-house FIT data 
validation for organic and inorganic data was completed but only 
the inorganic data^has received EPA final approval. Groundwater^, 
data r indicated-^chlorof orm Jcontjimination in ' thel^^^ 
ug/L) :and thie two downgradient public jwaterrrsupp^ 
Fairplains /9 (12ug/L) and Fairplains / 8" (12ug/L) ": The "onTsite. 
soil^andiisediment'? sample - data also "indicated, contaninatjion. The 
Pre-Remedial and Data Support Section will review the SI"i^report and 
determine whether a Hazard Racking Score package is warranted. 
« 
There are no hazardous laboratory or drummed materials remaining at 
the site. The possible remediation of suspected contamination of 
groundwater, soil, and sediment originating from VIChem will be 
considered under the National Priority List system for priortizing 
site remediation as required by S300.425 of the National 
Contingency Plan. 
301588 
«. 
DISPOSITION OF WASTES 
Wastestream* 
labpactt of Chen1cil« 
Kediua 
Solid t H o u t d 
Quantity 
7990 pound* 
Treataent 
Tncfnentlon 
Disposal 
O * Tradg Wind Incliy.-atof 
Hgigrdous CylIndent 
Cai 
n 
evllrxfert 
Detonation 
AnqulUi l a n d f i l l . St. Crelx 
Shock-Serai tlve Otet*. 
SoUd I l i q u i d 
7D pocnd* 
Detonation 
Anguilla I a n d f f U , St. Croix 
Uranyl Acetate 
Solid 
100 grann 
»ecycl> 
Polysclence*, tne. 
Mercury 
Solid 
1 pouid 
tecygU 
Polysciences, Ine. 
•Veedox* Herbicide 
Liquid 
2/5 q. drum 
On-site Spraying 
VlCTea. St. Croix 
1 - Organic liquid* 
l i q u i d 
U/55 g. drjM 
Tnclrieratlon 
Holllna, Deer Part, Tx. 
2 - Organic liquids 
l i q u i d 
13/55 g. drvjns 
Incineration 
t o l l l n s . Deer Park. Tx. 
Flan. Organic l l q . 
l i q u i d 
19/35 g. druns 
Incineration 
Solllrta. Deer Park, Tx. 
t - Flaffl. Organic U q . 
liquid 
11/55 9. druns 
Incineration 
B e l l l r a . Deer Park, Tx. 
; - Base N e u t r i r U q . 
liquid 
21/55 9. drtra 
Wastevtr treat. 
CUM lake Qiarles. l l . 
6 - Base Keutral U q . 
l i q u i d 
17/55 a. dnjns 
Incineration 
Kollins, Deer Park, Tx. 
7 - Bate neutral Sol. 
Solid 
21/55 fl. drum 
l a n d f i l l 
VM Ewelle. Ala. 
7A- Base Meutral Sol. 
Solid 
15/55 g. drvjns 
l a n d f i l l 
CiM Enelle. Ala. 
8 - Acid l i q u i d * 
l l q j i d 
15/55 
fl.dnjra 
trclrSeratlon 
> o l t i n * i Deer Parkj Tx. 
9 - Organic Solid* 
Solid 
6/55 g. dram 
Incineration 
H o l l i r a , Deer Park, Tx. 
9A- $*Hcyllc Acid 
Solid 
27/55 S' drLiaa 
lecyclt: 
PtO Oienlcal/Pfltter O.eia. 
gnolewood.nj/ltidqefield.llj 
10- Chlor. Org. U q . 
Uquid 
1/55 g. drum 
Incl.-teratfon 
t o l t i n * . Deer Park, Tx. 
11- f l a n . Org. U q . 
IIquid• 
1/55 g;'dnjm 
Tnclneratlbn 
XolHraj Deer Part. Tx. 
12- Base Meutral U q . 
l i q u i d 
1/55 fl. drum 
Inclneritlen 
Rollln*, Deer Park, Tx. 
13- Acid l i q u i d 
l i q u i d 
1/55 flJ druM 
Iheirteriitioo 
8oUtn«. Deer Park. Tx. 
15- Tartaric Acid 
Solid 
6/55 g. drum 
landfiU 
OM Eielle^ Ala. 
17- HCHA Effoty Druig 
Solid 
2tO dnim 
landfiU 
CW Epelie; Al*: 
20- Benzyl Chlortd* 
Uquid 
16/55 8- drum 
tecyclt 
DiO Oienic*l/Jame Fine Che«. 
Englewocd.WJ/Bound Brook.MJ 
OraIned Batterie* 
Solid 
3/as 
flf.-drum 
l a n d f i l l 
CJM Eaeller Ala^ 
Battery Add 
Uquid 
3/5 fl. drum 
Wastevtr. treat. 
CW ttodel City, WT 
line/Floor Sweeping* ''' 
Vol id'^ 
7/85 fl. drum 
l a n d f i U 
OM E ^ t U . Ala. 
Protective Clothing 
Solid 
29/85 fl. drum 
Incineration 
TVl. Sauqet. t l 
Protev-tive Clothing 
Solid 
l/tS g. drug* 
Incineration 
EM5C0. l i t t l e Bock, Ki 
Sanple Glasswar* 
Solid 
(/5 fl. drum 
Incineration 
EWSCO, little Bock, A» 
* Murfaert preceding certain MstettrcaMS identify those uattettrcaiw accordinQ to tK« bulking tchene. 
WS MM, wat a one drua wastettreaa the content* of which were spilled during v*r>dalt«a. WS i 16, 18, 
and 19 were Uastettream* for th* St. Croix 'Minl-Reneval** project that were bid and disposed of with 
VIChem waste but charged under the St. Creix •>tinl-»effovals* pre)ect. 
301589 
FINANCIAL ACCOUNTING 
A. 
CEILINGS 
TOTAL PROJECT 
MITIGATION 
EPA 
TAT 
$ 1 , 9 5 0 , 0 0 0 
$ 1 , 5 1 6 , 0 0 0 
$ 1 5 0 , 0 0 0 
$ 2 4 5 , 0 0 0 
B. CONTINGENCY COSTS 
$39,000 
C. UNOBLIGATED MITIGATION FUNDS REMAINING 
$154,000 
D. COSTS & BALANCES as of 7/30/91 
DCN 
OBLIGATED 
EXPENDED 
BALANCE 
AMOUNT 
AMOUNT 
KE3042 
$250,000 
$250,000 
$0 
KE3069 
500,000 
500,000 
0 
KE3073 
250,000 
250,000 
0 
KE3085 
262,000 
262,000 
0 
KE0036 
100,000 
7,658 
92,342 
Subtotal 
$1,362,000 $1,269,658 
$92,342 
Other Costs 
TAT Salary\Travel as of 3/29/91 
219,361 
EPA Salary\Travel as of 10/25/91 
147,250 
Estimate of Total 
Expenditures to Date 
$1,63 6,269 
E. CEILING PERCENTAGES 
TOTAL PROJECT 
MITIGATION 
EPA 
TAT 
84% 
84% 
98% 
90% 
PERCENTAGE OF $2 MILLION 
82% 
301590 
The above accounting of expenditures is an estimate based on 
figures known to the OSC at the time this report was written. The 
OSC does not necessarily receive specific figures on final payments 
made to any contractor(s) . Other financial data which the OSC must 
rely upon may not be entirely up-to-date. The cost accounting 
provided in this report does not necessarily represent an exact 
monetary figure which the government may include in any claim for 
recovery. 
FINAL POLREP X 
FURTHER 
POLREPS 
FORTHCOMING 
SUBMITTED B 
A , ^ - > - ^ 
DATE RELEASED 
John Higgins, P.E. 
On-Scene Coordinator 
Response and 
Prevention Branch 
• 
301591 
virgin Island Chemical Cocpany Removal Investigation, St. Croix, U.S.V.l, 
* 
Site inspection conducted January 31, 1989 
* 
AOO drums inventoried 
* 
^00 lab reagents inventoried 
* 
8 steel tanks vlth liquids 
^ 
* 
4 full tanks of ethanol 
* 
Sodium metal; Ethyl ether; Phosphorous pentoxide; Diisobutyl 
aluminum hydride pose serious threat 
* 
Dog kennel operating on site, ovner living on site 
* 
PRP actively using site 
* 
St. Croix prison } mile downwind 
* 
Air monitoring results on site equivalent to background 
301592 
From: Kichael Mentzel TAT-2 ^ A t 
Jeif Bechtel TAT-2 
To: 
Doug Kodama OSC 
U.S. EPA Response and Prevention Branch 
Subject: Virgin Islands chemical Company (VI CHEM) Removal Evaluation 
and Site Investigation preliminary report. 
Data: 2/2/89 
INTRODUCTION 
On Tuesday January 31, 1989 the U.S. EPA Response and Prevention Branch 
conducted a Removal Evaluation and Site Investigation at the Virgin "island Chemical 
Company (VI CHEM) site in St. Croix U.S. VI. This action is in reply to a request 
from George Pavlou, associate director Enforcement programs dated 1/23/89. 
PERSONNEL 
Doug Kodama 
' 
(201) 906-6905 
U.S.EPA RiP Branch 
" 
Edison N.J. 
Adalberto Bosque 
(809) 729-6915 
U.S.EPA CFO 
Santurce PR 
Michael Mentzel 
(201) 225-6116 
Jeff Bechtel 
Edison N.J. 
TAT-2 
Arnaldo Martinez 
(809) 723-8A66 
TAT-21 
Santurce PR 
Francine Lang 
(809) 773-0565 
Leonard Reed 
St. Croix VI 
Henry Thomas 
Greg Rhymer 
V.I. Department of Planning and Natural Resources 
(DPNR) 
301593 
A. LABORATORY 
Over ^ 0 containers of laboratory reagents and unknown liquid and solid 
Ejaterlal are located in this area. Room 22 is the main lab area. Room 18 is 
the lab storage area, Room 15 contains unmarked glassware and Room 11 contains 
only a few items. Some of the more nefarious items of note are as follows: 
1. Sodium metal (2 boxes). Water reactive. 
2. Ethyl Ether (6 cans). Potential explosive. 
3. Diisobutyl aluminum hydride (4 lecture bottles). Spontaneously combusts 
in air. 
A. Potassium cyanide (2 bottles). Poisonous. Stored near acids, potential for 
release of hydrogen cyanide gas. 
5. Phosphorous pentoxide (1 bottle). Reactive. 
6. Two Flanmable storage cabinets containing various materials and unknowns. 
7. Two office type storage cabinets. One cabinet has spilled toaterlal on the 
top shelf which has dripped downward to mix vith other chemicals. 
Many other chemicals exist in the laboratory,as well as many containers 
vith unknown materials. Refer to table I for a listing of the known chemicals. 
All the chemicals which had dates are at least five years old. 
B. DRUM STORAGE VAREHOUSE 
In the main warehouse (Room 3,A,5 and 6) are located approximately 
AOO drums, of these, 200 are green painted drums which have the words ETHYL 
ALCOHOL stenciled on the lid. The condition of the ethyl alcohol drums vary 
from fairly sound to extremely deteriorated. Some cf the drums consist of 
only a rusted shell vith gaping corroded holes. A rough estimate shovs that 
100 are empty and 100 contain some type of material. This material may be 
some type of sludge. Other materials found are as follovs: 
1. Laboratory unknowns (75 containers less than i gal.) 
2. Methanol (5x 55 gal.) 
3. Glacial acetic acid (I3x 55 gal) 
4. Benzyl acetate (22x 55 gal.) 
5. Toluene (lOx 55 gal.) 
6. Antifreeze/glycol (19x 55 gal.) 
7. Benzyl chloride (28x 55 gal.) 
8. Salicilic acid (27 fiber drums) 
9. Methyl isobutyl carbinol (12x 55 gal) 
10. Sodium hydroxide (12x 55 gal.) 
11. Bulging drum, unmarked (1) 
12. Drums in vhich some type of reaction has taken place, lid popped off (2) 
13. Many other drums vith contents as shown in table 2 
IA. Drums of unknown material. 
15. Paint (97x 5gal. 21x Igal.) 
16. Cylinder chlorine (1 bad condition). Cylinder hydrogen chloride (1) 
A cistern is located in room 2. PVC pipe leads to a pumping system outside 
the building. One drum of sulfonic acid is broken and leaking it'contents. 
301594 
OUTSIDE CROUyBS 
An inspection of the reactor and centrifuge buildings revealed various 
production materials including lubricating oils; propane, oxygen and acetylene 
cylinders; filter media; ethanol; assorted paints and some sodium hexa-oeta 
phosphate. Some of the oil drums are leaking. 
Scattered around the facility are eight stainless steel tanks with quantities 
of unknown liquid varying from empty to three quarters full. A large storage 
tank is on site along with numerous pressure and reaction vessels. 
Fourteen large green storage tanks are also on-site. Ten are planned to be used 
in the alcohol dehydration project. Four of the ten are full of ethanol. The 
other six are empty. The remaining four not being used are empty and unsound. 
Mr. Southerland stated that- -sludge was removed from these tanks when his company 
began operation.. 
Mr Southerland is a partner in the alcohol dehydration project being undertaken 
by VIAG Fuels Inc.on the site. Mr Southerland was interviewed in order to gain 
information about present activities on site. VIAG uses some of the office 
space in the main building. 
301595 
i^ACHKEfJT A 
iland CbAfflioal SltO 
T^cationt 
gt Croix, U,8, y.I.. 
The Island cheaical eite is located on the Isl&nd's South side 
n*ar tha west end (Figure 1). The site is situated on route 66, 
approxiaately 0.5 miles due north of the Alexander Hamilton 
Airport. The site covers approximately 3 acres and is bordered 
to the north by an intermittent stream that originates on the-
north side of the Island and discharge into the Caribbean eea. 
A number of r*«idenc«s are located as close as one-tenth of a 
mile from the site. In addition, several well fields are located 
in the vicinity of th* «ite. --- 
_ 
In connection with sale of assets of Island Chemical Cospany(ICC) 
to Virgin Island Chemical (VICC), in October, 1984, Enviro-
Science^ Inc. (ESI) was retained to investigate the ICC site. 
The inve$tigat^onj:onducted-by^,ESI,,revealed that both'^ofithelpits^ 
andvth"e;rarea5:iroui*i3thl^ 
were contaminated with ' 
ToltJene' and Pyt'i<3iS« (^i-Snire 2). 
Following the discovery of the contaaination, ESI removed and/or 
treated soma of the contaminated material at the Site. 
Additional investigations are necessary, however, to evaluate the 
nature and extent of any remaining contamination" at the site and 
the threat, if any, posed by such contamination. 
ESI haa submitted a RI/PS work Plan to address the additional 
investigations that are necessary and EPA has coamented, ESI is 
now revising the Work Plan. 
Tha Votk.PlAn, however, does not address & possible renoval of 
cheaicals stored in a portion of the main building owned by vice. 
The Virgin Island Company is in the process of finalizing the 
sale of this &ain buildincf. 
On Koveaber $th EPA and DPKR conducted a sita inspection of the 
aain buildin^r* The aite inspection revealed that & portion of 
the building contains large amounts of stored cheaicals in bags 
and druaa. Some of the cheaicals includedi 
sodiua hydroxide, 
toluene, eulfaaic acid(granular), potassium sulphate and benzyl 
chloride. Many of the bags and druas have ruptured and have 
spilled all ever the floor. There are pools of liquids, and 
powders over various parts of the floor. There are druns with 
portions of their sides rusted; others ehowed danger signs, such 
aa bulging, pitting, and visible accuaulation on soae druns. 
w 
301596 
ISIA}JD CKtHTC^L S I T ^ 
gite History 
The 3.5-acre site is owned by Charles_JL_-^t-a£^ey^_.Iac. On Hay i, 
1969 Steffey leased tha property to Houston Cheaical Industries, 
Ino. 
Houston Cheaical assigned the lease to-CSTlbe cEenica! 
Coapany Inc., (subsequently known as Pierrel Aaerica, Inc.) on 
March 20,1972. 
. 
" 
^ 
— 
on June 30, 1978—Pierrel Aaerica assigned the ground lease to 
CoopexiiAboratoriefiTijiIne,^ 
On October 30, 1979'-'Cooper 
LaBoratories assigned^the-iease to its subsidary. Island Cheaical 
conpany(ICC). On Kovesber-1, 1979 Cooper Laboratories told^ll"" 
of the -Stock "Of ICC to the pr^deccessor of Berlex Laboratories, 
Inc. 
(Berlex). 
on Septeaber 14,1984, ICC sold its assets to 
virgin Island Cheaical Coapany (VICC). (See figure 1 for break 
down b"Jf~o^7neTiShlpy'i 
site Operations 
- ^ — o f t ^ : 
|Berl<exS«icquired:§th^^ 
At 
"^Ke^tiae of purchase "tHe facility was in a non-siperational aode. 
Prior to the acqfuisition of the leasehold by Cooper, it is 
believed that the prior owners were in the pharaaceutical area of 
the cheaical industry and used the site to manufacture phenacetin 
and ethoxyquin. Cooper produced quinidine; operations vas halted 
in the aid-1979. 
Be^ex •revaapMs'^''the facility and operate"d for about t^o of its 
four' years of ownership. The facility produced prinarily 
quinidine from quinine. Production vas discontinued vhen the 
aethologies used produced a aore expensive product than never 
aethods used elsewhere in the industry. Tho plant did not 
operate for aore than a year prior to purchase by VICC. 
gtt» lnY»=>tigat.lon 
Enviro-Sciences, Inc. (ESI) vas contracted by Berlex to conduct 
an enviromnental study of the ICC sitel Under the contractural 
agreeaent between Berlex and VICC, ESI was responsible for 
certifying that the site vas environaentally clean and free of 
cheaical contamination; if not, the site had to be reaediated. 
ESI initiated a sit* evaluation in Septeaber, 1984 and continued 
the investigation into October. Contaaination vas found at 
several locations and a prelininary cleanup plan was subaitted to 
EPA. 
301597 
-2- 
- -
ISLAND CHKHICAL SITE • 
fq^ijqu-XlP AND PECO?-ygKDATTOy;<;: 
It is recoaaended that the TAT teaa evaluated the site to 
deterained if the site warrants a renoval action under CERCLA. 
In the interia, the following corrective actions should be 
iEpleaented: .Cheaicals in container that are leaking, rust&d 
etc., should be repackaged. Cheaicals should also be staged on a 
platfora so that water can not get to thea, 
E?A vill aail notice letters to PRP's to offer thea a chance to 
perfora a reaovai action, if the TAT teaa aaJces the detemination 
that one is necessary. 
In the interia, the site will be evaluated for possible inclusion 
on the NPL. All existing available data will be used for the HRS 
ocoring. 
301598 
CHEiMICAL NAME 
TABLE 1 
Laboratory Reagent Inventory 
COMPANY 
QTY 
STATE 
1,3-dinitroben2ene 
1-butanol 
1-chlorobutane 
1-propanol 
18-Crown-6 99% 
2,2-oxydiethanol 
2,6-dimethoxyben2oic acid99% 
2,6-ditertiarybutyl p-cresol 
2-hydroxyben2yl alcohol 99% 
2-hydroxyethyl ether 
2-methyl-1-butanol 99% 
2-methylbutyl ajnine 
3,3-diaethoxy benzidene 
3-hydroxybenzoin acid 
4-chlorobenzene sulfonamide 
4-hydroxy 4methyl 2pentanone 
4-hydroxyben2oic acid 
4-methylbenzo phenone 97% 
9-hydroxyflourene 
Acetic acid 
Acetone 
Acetonitrile 
Alkalinity C,D,E,G 
Aluminum Chloride 
Aluainum chloride 
Amaonium acetate 
Ammonium acetate 
Ammonium acetate purified 
Ammonium hydroxide 
Ammonium persulfate 
Ammonium persulfate 
Ammonium thiocyanate 
Amyl alcohol 
Arsenic trioxide 
Barium chloride 
Barium chloride 
Barium chloride 
Barium hydroxide 
Benzaldehyde 
Benzene 
Aldrich Chemical 
J.T.Baker Chemical 
MCB 
J.T.Baker Chemical 
Aldrich Chemical 
Kodak 
Aldrich Chemical 
Biesterfeld 
Aldrich Cheaical 
Aldrich Chemical 
Aldrich Chemical 
American Laboratorie 
Kodak 
Aldrich Cheaical 
Aldrich Cheaical 
Aldrich Chemical 
Aldrich Cheaical 
Aldrich Cheaical 
Aldrich Cheaical 
MCB 
Fisher Scientific 
Supelco 
Mogul Corporation 
Mallinckrodt 
Witco Chemical 
Fluka 
Aldrich Chemical 
Jarchem Industries 
Sargent Welch Scient 
J.T.Baker Cheaical 
J.T.Baker Chemical 
Fisher Scientific 
Mallinckrodt 
Fisher Scientific 
Drew Chemical 
Mallinckrodt 
Fisher Scientific • 
Fisher Scientific 
J'.T.Baker Chemical 
Tenneco Oil 
100 
500 
4 
500 
25 
1 
25 
500 
25 
1 
10 
15 
100 
100 
100 
500 
50 
50 
g 
ml 
L 
al 
g 
xg 
g 
g 
g 
3cg 
g 
g 
g 
g 
g 
g 
g 
g 
2x25 g 
2x5 
4 
lb 
L 
1 box 
4x2 
1 
500 
1 
2 
250 
500 
2.5 
•500 
500 
1 
oz 
lb 
g 
kg 
Jcg 
g 
al 
kg 
g 
g 
pt 
2xll3g 
1 
• 
500 
1 
1 
500 
qt 
g 
lb 
lb 
al 
2xlgal 
solid 
liquid 
liqaid 
liquid 
solid 
liquid 
solid 
solid 
liquid 
liquid 
liquid 
liquid 
solid 
solid 
solid 
liquid 
solid 
solid 
solid 
liquid 
liquid 
liquid 
liquid 
solid 
solid 
solid 
solid 
solid 
liquid 
solid 
solid 
liquid 
liquid 
solid 
liquid 
solid 
solid 
solid 
liquid 
liquid 
301599 
Benzhydrol 
Benzoic acid 
Benzoin 
Benzoin 98% 
Benzophenone 
Benzophenone 
Benzophenone 
Benzophenone 99+% 
Benzoyl chloride 
Benzyl acetate 99% 
Benzyl alcohol 
Benzyl benzoate 
Benzyl chloride 
Ben2yl chloride 
Benzyl cinnamate 98% 
Benzyl ether 
Benzy ltrietJiylammoniu=chl ori 
Bismuth subnitrate 
Bromine 
Bromophenol blue 
Brucine sulfate 
Buffer solution pH 10.00 
Buffer solution pH 4.00 
Buffer solution pH 7.00 
CAO-3 BHT 
Calcium sulfate anhydrous 
Cello-Seal 
Chloride F 
Chlorodiphenyl aethane 98% 
Chloroform 
Chromotropic acid >Ta salt 
Cinnamaldehyde 
Citric acid anhydrous 
Citricacidtrisodiumdihydrate 
Cobalt chloride 
Color standard 4 
Congo red 
Copper metal 
Cupric sulfate 
Cupric sulfate 
DPD #1,2,3 Reagents 
Dibenzo 18-Crown-6 98% 
Dibenzoyl tartaric acid 
Dichloroethane 99% 
Dichlorophenyl aethane 99% 
Dichlorotoluene 99% 
Diethylene glycol 
Diisobutyl aluminum hydride 
Diphenylmethane 99% 
Diphenylthiocarbazone 
Eosin Y 
Ether anhydrous 
Ethoxyguin 
Ethyl acetate 
Ethyl acetate 
Ethyl benzene 
Ethyl ether 99% 
Ferric ammonium sulfate 
Kodak 
Mobay Chemical 
Fluka 
Aldrich Chemical 
Aldrich Chemical 
K&S Chemical 
Upjohn 
Aldrich Chemical 
Mobay Chemical 
Aldrich Chemical 
Mallinckrodt 
Aldrich Chemical 
unknown 
Velsicol 
Aldrich Chemical 
Aldrich Chemical 
Aldrich Chemical 
MCB 
Fisher Scientific 
Fisher Scientific 
Fisher Scientific 
Fisher Chemical 
Fisher Scientific 
Fisher Chemical 
Sherwin Williams 
W.A.Hammond Drierite 
Fisher Scientific 
Mogul Corporation 
Aldrich Chemical 
Fisher Scientific 
Fisher Scientific 
un>:nown 
J.T.Baker Chemical 
Aldrich Cheaical 
Fisher Scientific 
unknown 
Fisher Scientific 
Fisher Scientific 
Fisher Scientific 
Mallinckrodt 
Taylor Chemical 
Aldrich Cheaical 
Knoll Fine Cheaicals 
Aldrich Chemical 
Aldrich Chemical 
Aldrich Chemical 
Fisher Scientific 
Texas Acres 
Aldrich Cheaical 
Fisher Scientific 
Aldrich Chemical 
Fisher Scientific 
unknown 
Aldrich Chemical 
MCB 
Dupont 
Fisher Scientific 
Fisher Scientific 
100 
1 
2x1 
g 
lb 
ka 
4x50Gg 
500 q 
1 bag 
500 
50 
1 
100 
1 
100 
4 
500 
100 
1 
25 
1 
113 
5 
1 
500 
500 
500 
. g 
g 
lb 
g 
pt 
g 
oz 
g 
g 
kg 
g 
lb 
g 
g 
oz 
ml 
Bl 
ml 
1 bag 
4x5 
25 
3 
100 
4 
25 
2x1 
500 
1 
2x1 
1 
25 
500 
500 
500 
3x1 
50 
1 
1 
25 
100 
1 
4 ( 
500 
25 
25 
4 
4 
5 < 
lb 
g 
oz 
g 
L 
g 
kg 
g 
3cg 
lb 
oz 
g 
g 
g 
g 
oz 
g 
kg 
^9 
g 
g 
qt 
=yl 
g 
g 
g 
qt 
oz 
gal 
Sxlgal 
1 
qt 
6x500g 
500 g 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
liquid 
liquid 
liqjid 
liqjid 
liquid 
solid 
liquid 
solid 
solid 
liquid 
solid 
solid 
liquid 
liquid 
liquid 
solid 
solid 
liquid 
liquid 
solid 
liquid 
,. solid 
liquid 
solid 
solid 
solid 
liqaid 
solid 
solid 
solid 
solid 
liquid 
solid 
solid 
liquid 
solid 
solid 
liquid 
gas 
liquid 
solid 
solid 
liquid 
liquid 
liquid 
liquid 
liquid 
liqiud 
solid 
301600 
Ferric chloride 
Ferric chloride 
Ferric chloride anhydrous 
Ferric chloride anhydrous 
Ferrous ammoniua sulfate 
Formic acid 
Glacial acetic acid 
Hydrazine sulfate 
Hydrazine sulfate 
Hydrochloric acid 
Hydrochloric acid 
Hydroxylamine hydrochloride 
Hydroxylamine hydrochloride 
Iodine 
Iron chloride anhydrous 
Isoamyl alcohol 
Isobutyl alcohol 
Lead acetate 
Lead nitrate 
Lithium perchlorate 
Magnesium sulfate 
Medical oxygen 
Mercuric chloride 
Mercuric oxide 
Mesityl oxide 
Methanol 
Methenamine 
Methyl alcohol 
Methyl orange 
Methyl red 
Monochlorobenzene 
N-methylaniline 
Na salt of ME salicylate 
Niacin N.F. 
Nitric acid concentrated 
Nitrobenzene 
Non aqueous buffer soln. 
Nutrizyme 
Oil #3 
Paraffin oil 
Paraformaldehyde 
Paraformaldehyde prills 91% 
Perchloric acid 
Phenol red 
Phenopthalein 
Phenylhydrazine. .. 
Phenylhydrazinehydrochloride 
Phosphorous pentoxide 
Piperazine 
Potassium bromide 
Potassium butoxide . 
Potassium chloride 
Potassium cyanate 
Potassium cyanide 
Potassium dichromate 
Potassium ferrocyanide 
Potassium hydroxide 
Potassium hydroxide 
unknown 
Fisher Chemical 
Pennwalt Corporation 
Kodak 
Fisher Chemical 
unknown 
Fisher Chemical 
Fisher Scientific 
Fisher Scientific 
MCB 
Fisher Chemical 
Fisher Scientific 
MCB 
Fisher Scientific 
BASF 
Fisher Scientific 
J.T.Baker Chemical 
MCB 
Fisher Scientific 
Aldrich Chemical 
Fisher Scientific 
MSA 
Fisher Scientific 
Fisher Scientific 
Aldrich Chemical 
Fisher Scientific 
Fisher Scientific 
Mallinckrodt 
Fisher Scientific 
Fisher Scientific-
PPG Industries 
Kodak • 
Sattra Chemical 
Nepera Chemical 
J.T.Baker Chemical 
Fisher Scientific 
Beckman Instmments 
Merck 
Frich Oil 
Fisher Scientific 
MCB 
Celanese Cheaical 
MCB 
Fisher Scientific 
Fisher Scientific 
Fisher Scientific 
Fisher Scientific 
Fisher Scientific 
MCB 
Fisher Scientific 
Callexry Chemical 
Beckman Instruments 
Fisher Scientific 
Fisher Scientific 
Fisher Scientific 
Fisher Scientific 
Mallinckrodt 
Fisher Scientific 
100 
1 
al 
lb 
5x50Cg 
500 
1 
200 
5 
4 
100 
2X6 
3x1 
1 
4 
500 
500 
500 
500 
1 
100 
500 
500 
g 
lb 
g 
lb 
02 
g 
lb 
L 
kg 
oz 
g 
g 
ml 
ml 
lb 
g 
g 
g 
1 cyl 
2xl00g 
500 
100 
4 
500 
g 
g 
L 
g 
1 gai 
113 g 
2x10 g 
10 
1 
oz 
kg 
1 bag 
250 
2X8 
1 
1 
2 
g 
lb 
qt 
pt 
oz 
5 gal 
1 
1 
1 
2X8 
5 
1 
4x4 
2 
1 
100 
qt 
qt 
lb 
lb 
g 
oz 
oz 
lb 
lb 
g 
5x500g 
50 
2X6 
1 
500 
500 
3 
2x1 
500 
g 
oz 
lb 
g 
g 
kg 
lb 
-^g_ 
301601 
liquid 
solid 
solid 
solid 
solid 
liquid 
liquid 
solid 
solid 
liquid 
liquid 
solid 
solid 
solid 
solid 
liquid 
liquid 
solid 
solid 
solid 
solid 
gas 
solid 
solid 
solid 
liquid 
solid 
liquid 
-solid 
liquid 
liquid 
solid 
solid 
- liquid 
liquid 
liquid 
solid 
liquid 
liquid 
liquid 
solid 
liquid 
solid 
solid 
liquid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
• 
potassium iodide 
Potassium iodide 
Potassium periodate 
Potassium platinate 
Potassium sulfate 
Potassium sulfate 
Potassium sulfate 
Potassium thiocyanate 
Resorcinol 
Salicylaldehyde 99-^% 
Salicylic acid 
Salicylic acid 
Salicylic acid sodium salt 
Sicapent 
Silica gel dessicant 
nitrate 
nitrate 
Chloride 
acetate 
acetate anhydrous 
acetate anhydrous 
amide 
benzoate 
benzoate 
benzoate 
benzoate 
Sodium borohydride 
Sodium carbonate 
carbonate anhydrous 
chlorate 
dichromate 
formate 
Sodium hydride 
Sodium hydroxide 
Sodium metal 
Sodium nitrite 
Sodium nitro ferricyanide 
Sodium sulfate 
Sodi\am tartrate 
Sodium tartrate 
Sodium thiosulfate 
Succinic anhydride 
Succinic anhydride 
Sulfamic acid 
Sulfanilic acid 
Sulfite 0,P,Q 
Sulfuric acid 
Tetraphenolboron sodium 99% 
Thiopene 
Total alkylinity indicator 
Tributyl borate 
Trichloroethylene 
Triethyl borate 97% 
Triethylenediamine 
Weedox C/R 250 herbicide 
Xylene 
Zinc chloride 
Zinc chloride anhydrous 
Silver 
Silver 
Sodium 
Sodium 
Sodium 
Sodium 
Sodium 
Sodium 
Sodium 
Sodium 
Sodium 
Sodium 
Sodium 
Sodium 
Sodium 
Drew Chemical 
Fisher Scientific 
Fisher Scientific 
Varlacold Chemical 
Indiana Army Ammo Plant 
Aldrich Chemical 
un3cnown 
Fisher Scientific 
Koppers 
Aldrich Chemical 
Aldrich Chemical 
Aceto Chemical 
Aldrich Chemical 
MCB 
Davison Chemical 
J.T.Baker Chemical 
Sargent Welch Scientific 
Fisher Scientific 
Sattra Chemical 
Niacet Corporation 
CDF Chimie Noth America 
Farchan Research T-ab 
Sattra Cheaical 
Dastech International 
Ishihara Corporation 
Pfizer 
Fisher Scientific 
Fisher Scientific 
Mallinckrodt 
Hooker Cheaical 
Fisher Scientific 
unknown 
Thiokol/Ventron Division 
Mallinckrodt 
RMI 
Fisher Scientific 
MCB 
Fisher Scientific 
J.T.Baker Cheaical 
Fisher Scientific 
Fisher Scientific 
MCB 
Aldrich Cheaical 
Fisher Scientific 
H&S Cheaical 
Mogul Corporation 
J.T.Baker Chemical 
Aldrich Cheaical 
Kodak 
Drew Cheaical 
Aldrich Cheaical 
Mallinckrodt 
Aldrich Chemical 
Air Products 
Southern Mill Creek Prod, 
Fisher Scientific 
Fisher Scientific 
Mineral Research 
i 
qt 
2x500g 
100 g 
5 
g 
250 g 
500 g 
50 
g 
500 g 
3 bags 
100 g 
100 g 
500 g 
100 g 
2.8 L 
2x1 qt 
1 
oz 
30 
g 
500 g 
3 bags 
250 'g 
2x500g 
500 g 
1 bag 
1 bag 
250 g 
100 lb 
4x25 g 
1 
kg 
1 
lb 
1 box 
10 kg -
5 
lb 
1 
lb 
500 g 
2 boxs 
2x500g 
4 
oz 
500 g 
2 
oz 
6xll3g 
2x1 lb 
6x250g 
2x1 kg 
500 g 
1 bag 
3x2 oz 
10 lb 
25 
g 
100 g 
1 
qt 
750 g 
1 
pt 
100 g 
250 g 
. 2x5gal 
5x1 L 
500 g 
1 
lb 
301602 
liquid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
liquid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
"solid 
solid 
solid 
solid 
solid 
liquid 
liquid 
solid 
liquid 
liquid 
liquid 
liquid 
liquid 
solid 
liquid 
liquid 
solid 
solid 
p-chlorobenzene sulfonamide HiS Chemical 
2 bacs 
<^oi -^ 
p-naptholbenzein 
Fisher Scientific 
25 
g 
l o U -
p-toluenesulfonicmonohydrate Aldrich Chemical 
500 q 
kkk 
pH indicator A 
Mogul Corporation 
2 
oz H L T -
z Miscellaneous unknowns 
on site lab glassware 
280bot 
miTk^ 
z Miscellaneous unknowns 
on site one oz bottles 
238bot 
liq-ji-^-
301603 
TABLE 2 
Drum Inventory 
Chemical Name 
Company 
Qty 
State 
Acetone 
Acetylene 
Activated carbon 
All-veather patch material 
Amersite 2 
Ashland MeOH 
-^Benzyl acetate 
Benzyl chloride 
Chlorine 
Chloroform 
Crofox 
Crystal Clear floor finish 
Degreaser 
Drewtrol 8500 
Ethyl alcohol 
Filteraid 
Glacial acetic acid 
'^Glycol 
Humisorb 
Hydrochloric acid 
Hydrogen chloride 
Insulation (asbestos??) 
Insulation fiberglass 
Lubricating oil 
Lubricating oil 
Magnesium sulfate trihydrate 
Methanol 
Methanol 
Methyl isobutyl carbinol 
Methyl isobutyl ketone 
Micro aedia filter sheets 
Oxygen 
Oxygen 
Paints 
Paints 
Paints 
Paints 
Para-phenetidin 
Pentosin 
Potassium acetate 
Potassium sulfate 
Powdered filter media 
Propane 
Purafil II 
Quinine sulfate 
Rinseline injector fluid 
Ashland Chemical 
VI Gas 
Calgon Corporation 
Revere Chemical 
Valley Freight Syst. 
Ashland Chemical 
Island Chemical 
Velsicol Corporation 
VI Gas 
unknown 
Cerfact T-=^boratories 
Cerfact Laboratories 
unknown 
Valley Freight Syst. 
unknown 
un>cnown 
Celanese Chemical 
Island Cheaical 
Culligan 
Certified Laboratory 
VI Gas 
unknown 
unknown 
Texaco 
Texaco 
Tomita Pharmaceutica 
Ashland Chemical 
unknown 
Van Waters & Rogers 
Ashland Cheaical 
Ertel Engineering 
VI Gas 
Santa Maria Gases 
unknown 
unknown 
International Paint 
International Paint 
unknown 
Deutsche Pentosin 
Jarchea Industries 
un3cnown 
Ionics 
unknown 
unknown 
Kiaafarma 
Bob Chamber Ltd. 
55 
G 
2 cyl 
30 baa 
55 
G 
55 
G 
5 
G 
21x550 
28X55G 
1 cyl 
55 
G 
55 
G 
2x20 G 
55 
G 
55 
G 
115x55 
10X30G 
13X55G 
20X55G 
30 
G 
55 
G 
1 cyl 
13 box 
7 box 
2X10 G 
5x55 G 
6x25kg 
5x55 G 
3X55 G 
12X55G 
55 
G 
18 box 
3 cyl 
1 cyl 
44x5 G 
53x1 G 
97x5 G 
21x1 G 
55 
G 
20 
L 
8xl00# 
50 bag 
2 boxs 
4 cyl 
15X10G 
20 
G 
55 
G 
liquid 
gas 
solid 
solid 
liquid 
liquid 
liquid 
gas 
liquid 
liquid 
liquid 
liquid 
liquid 
liquid 
solid 
liquid 
liquid 
solid 
liquid 
gas 
solid 
solid 
liquid 
liquid 
solid 
liquid 
liquid 
liquid 
liquid 
solid 
gas 
gas 
liquid 
liquid 
liquid 
liquid 
liquid 
liquid 
solid 
solid 
solid 
gas 
solid 
liquid 
liquid 
301604 
Rout 
Salicylic acid 
Salt 
Soda ash 
Sodium acetate anhydrous 
Sodium acetate anhydrous 
Sodium bicarbonate 
Sodium hexa-meta phosphate 
Sodium hydroxide 
Sodium hydroxide 
Spent toluene/acetone 
Sterling salt crystals 
Sulfamic acid 
Tartaric acid 
Thinner 
Thinner 
Toluene 
Toluene 
Triethylamine 
Waste oil 
z Empty drums 
2 Miscellaneous unknowns 
Cerfact Laboratories 
Rhone-Poulenc 
unknown 
Allied Chemical 
unknown 
Jarchem Industries 
Stauffer Chemical 
FMC 
Mantek 
Manuel del Valle Inc 
unknown 
unknown 
Dupont 
Pfizer Chemical 
unknown 
Advance 
Ashland Chemical 
unknown 
Air Products 
unknown 
unknown 
on site containers 
20 
G 
27drum 
2x30 G 
15x100 
50 lb 
200 lb 
8x1001 
200 lb 
55 
G 
12X55G 
2x55 G 
50 lb 
400 lb 
15x100 
6x1 
55 
3x55 
5x55 
55 
2x55 
130 
25 
G 
G 
G 
G 
G 
G 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
solid 
liquid 
liquid 
liquid 
solid 
solid 
solid 
liquid 
1 i qu i d 
liquid 
liquid 
liquid 
liquid 
n/a 
misc. 
301605 
S T . 
C R O I X 
^=r:Z-. 
,.''^--'-' 
- " • • • . : • . ' . • • : • • • . 
' • • - . y ^ 
.liit-[,\\V^ 
)•• -/-.^hotjCrcS-i \ 
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' y j \ u p f P t o t a y 
L J > - ^ ' 
y)\}pZy''-T-y^ 
v^ ^ 
AZ 
• -:.--••• 
' z k 
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• ^ ll • • ^ - . . i - 
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A...-. - -z -- \y 
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\--:..zy^yy V yyk::?-z-yp 
A- 7j-'Ai^^'T'y''''.:MA\yfr. i--Z\^$ 
''yzyyryA 
A'^-A ^vii-K {YV:^A^ZZA"' ' 
'>- • \ v IU-—<-•' • J 
r 
1—r—^<-r ' — V : 
r—.—=——v \v-Oi ..•L^-- T'. ^ ' • • . ^ - u - g ^ ^ ^ ^ 
•l.v- \ l--< 
\'-'^^:r:z>-z-kZ 
zi=<y • ' . \ y k \ \ ' 
kk^^,:yj^h^' • - k z y y y 
kz^^ 
' 
Izyz^^^'- ykhy- 
. —•jTsI 
v 
m^.>p^yy'^y<z 
•^kyirrsrifc;. 
y y y ^ : • rz 
', \ -
1 
: 
'l-i-l t - ^ ^ ^ - \ y t:\.: •.•z:.\::-e; S ^ ^ . i -^^ 
.-\|\-./ 
...•-• .!^y//yyk'k'^y'^y 
! 
'AAz¥/tPS fV*^-'i9:^i. V- 5- i . y' J ^ \ S ^ 
• ^pyz='k^ 
MkZA 
p;r^-'^}> 
A ) \ iV 
*]225——-
^;!1V 
\ «' I y-Ji y 
:".«• .•• V l T f— 
Al«un<3rr H i w * 
y.Kyi 
^ 
i"^-
SPIU. PRE^yENTION & 
EMERGENCY RESPONSE OMSlON 
rn.VNVociaum wiih ICTTcchnolo^ In<L.CCJonn»oo A.-ksvaciates. 
Inc_ Koourcr Applicsiions. |nc_ Coo/Rnouire Cunvulvints. Inc.. 
a n j tn^Tronrr^-nuJ Toxjcolo^ tnicmaiiooaJ. Inc. 
EPAPM 
KODAJi^A 
TAT PM 
MENTZEL 
FIGURE 1 
SITE LOCATION 
VI CHEM SITE 
ST. CROIX US VI 
301606 
Pt.AllT tNTXANCt 
SPIU PRr/E>moN & 
EMEHGcNCY RESPONSE DIVISION 
EPAPM 
KODAMA 
F l G i n ^ 2 
SITE DLACRA.M 
la Auociauon «>nLh ICF Tcchaotog}' lac_ C C Johnson tt Auociaio. 
l o c R o o u m Applk3tiona. I n c Cco/Koource Consulunu. Inc_ 
ind EnvironmcnLiJ Toxicolo^ (nterTuiionai. t n c 
TATPM 
KENT2EL 
VI CHEM SITE 
ST. CROIX DS VI 
301607 
.<: 
L o a d i n g 
D o t k 
:. A V . : . , 
COfvCRETE 
SURFACE 
':' 
W s ; « h Q u ^ ^ 
: - > - . -5 
26 
25 
23 
Wt 
20 Errr^ri'. 
-17 
IS I Jt.,-:iy 
•I 
^1 -"r 
4 
.r. 
^i^kk 
i^.izz 
• 
1 
•DRUMS 
(MT) 
t7??77T(MT) 
^ 3 ( M T ) 
^ 3 ( 3 / 4 ) 
.'-fa% 
^ ^ ^ 
-TANXS 
• 
=DRUMS 
•DRUM AREA 
LAB AREA 
=W0RX ARZA/NO CHEMICALS 
=0FFICE AREA 
(1/4) 
u 
L -'. 
l-+_.]_4-.J. •_^. 
— I -
L_4-_L_i_i._. ...^_L 
301608 
# 
APPENDIX I 
PHOTOGRAPHS 
301609 
Photo #1. Virgin Island Cheaical Company 
Alcohol dehydration apparatus 
Photo #2. Dog kennel operating on site 
301610 
Photo #3. Maintenance building 
Photo til. View of tanks, nain building, and alcohol 
dehydration unit 
301611 
Photo /5. Main building office area 23 
Photo /6. Area 22 lab in the main building 
301612 
Photo f l . Virgin Island Cheaical Company 
Sodiua metal in area 18 
Photo #8. Area 18 chemical and glassvare storage 
301613 
Photo *9. Incompatable storage of lab reagents 
Pho to *10. Incompatable and leaking storage of lab reagents 
,01614 
Photo *11. Incompatable and leaking storage of•lab reagent-
Photo ^i:. IncompacabU storage of lab reagents 
301615 
Photo #13. Paint cans in area 1 
Photo till. Cylinder of chlorine 
:,;jo*HAtfj::ni 
301616 
« —<u»fcwO»r^.**^..i,-.o.^ —*i 
Photo #15. Drums in area i ; note water on the floor 
Photo #16. Drum contents undergoing a reactlc 
301617 
Photo #17. Virgin Island Chemical Coapany 
Drums and debris in area 5 
Photo i l 8 . Drums in area 5 
301618 
Photo ='19. Deteriorating drums in area 6 
Photo ^20. Drums and floor contamination in area 5 
301619 
Photo ?21. Deteriorating bags in area 6 
Photo #22. Drums in area 6 
301620 
Appendix M 
Laboratory Results 
\WORKU4231\02\\VORKPLA.N.REP 
HAHDING LAWSON ASSOCIATES 
301621 
Laboratories Inc. 
Memorandum 
To 
From 
Date 
Subject 
J. Beck 
2.V. McKennon 
Occober 15, 19Si 
ISL.-!uND OiEMICAI. iNVtKCNXEMT.^L SAMPLES 
Cn 9/17/8i, we received several samples frc= Ir-/ Coher. of ir.virc Scisr.cas Ir.: 
for analysis fcr various organic components. 
VTe agreed to exa=ir.e the samples for volacile organics via GC cech-irues , 
ar.d Chen for ncr.volscile organics like cuinidine using H?I.C I2chr.i:--ss . 
Cur invescigacicn is conplece, and data is attached. 
3I5C'JS3I0N 
:. GC ANALYSIS 
Quantitable amounts of toluene were found in sanples T8-1 and ~ank-c. 
Also, quantitable aaouncs of pyridine were found in satrples D-1, D-2, 
and D-5. 
Qualitatively, the chromacograns were exaained for additional peaks. 
Samples S4-2, D-5, T8-1, and T8-2 contain an unknown peak eluting 
between the pyridine and toluene peak. Tank-8 had an unidentifiable 
peak which eluted shortly after toluene. 
II. HPLC 
Quantitable amounts of quinidine and/or quinine were found in 3-1, 
D-2, D-5, TS-1, Tank-8, Tank-4, and Tank-9. 
Qualitatively, the HPLC chromatograms in many cases have some unidentifi: 
early eluting peaks which are not related to quinidine, quinine, or 
any of the other cinchona alkaloids. 
DEPOSITION or SAMPLES 
On October 10, 1984, all samples were given to Al Kyles who is a 
representative of Enviro Sciences Inc. 
Note: Due to the extreme rush to analyze these samples, limited 
precautions were taken to protect either CC or LC columns. Total 
replacement cost for columns is approximately $960. 
M kr>^Yp 
D.W. McKennon 
DUM/hms 
Attachment 
Pyy.^.yyy^ 
R. Willis 
R. Wohl 
R. Milos 
I ^.Cohen/Enviro Sciences I 
301622 
c c . A.V.^YS-S* 
L.C. A-N-.V^YSIS-" 
S.O<?LE 
I2£:!T:?IC.^TICM 
5i.-l 
S.i-2 
S--2 
S i - -
S i - 5 u r f a c e 
D-1 
D - : 
D-3 
D--
D-3 
TS-I 
T 8 - : 
Tank-S 
Tar.k-4 
Tank-9 
Tank-7 
"Ji Sample 
r i - H i g h 
Cone. 
TOLLT-E 
N/D 
N/D 
N/D 
N/D 
N/D 
N/D 
N/D 
N/D 
N/D 
N/D 
694 pcm 
N/D 
13,880 ppm 
-
-
-
-
-
PY-RIDINE 
N/D 
N/D 
N/D 
N/D 
N/D 
920 ppn 
507 ppn 
N/D 
N/D 
3014 ppm 
N/D 
N/D 
N/D 
-
-
-
-
-
QU-N-D::;E 
C1VC-N.J>— 
N/D 
N/D 
N/D 
N/D 
N/D 
452 ppm 
55 ppm 
N/D 
N/D 
170 ppm 
274 ppm 
47 ppm 
4050 ppm 
8227 ppn 
N/D 
N/D 
N/D 
N/D 
QU:N:;;I 
N/D 
N/D 
N/D 
N/D 
N/D 
82 ppr. 
N/D 
N/D 
N/D 
N/D 
101 ppn 
N/D 
' 1 5 2 1 ppn 
2594 ppn 
354 ppn 
N/D 
N/D 
N/D 
N/D • None Detected 
•G.C. Reference Bk. 83-9, pp. 75-79, EGO 
**L.C, Reference Bk. 83-11, pp. 22-30, MSM 
301623 
Pi.sr-/ J 
:v / 
Laboratories Inc. 
Me.mcrsncL: 
To: 
Cr. '•?. B. Caldwell 
cc: w. :,^-
?.. Vic: 
Frc.-n: G. ?.UC^ 
Ca:e; 
Cc-cber 19, 1534 
Sutiec:: 
.---.alysis cf Scil Sajr.ples frcm Isl = .-.d Ch.a.T.ic3.1 by 
Headscacs-Gas .Cr_rcn:a-ccracr.v 
Three scil sa.T.plas received 10/15/84 frcn the Islar.d 
Charr.ical si^e v>'sra e.xami.-.ad by haadscaca gas chrcr-azc 
fcr the presence of toluer.s and =yridi.-.e. Tha rasulc 
ara listad in tha table belcw. 
Chrcrr.a-ccrar-.s cf tha 
three sa.Ticlas are attached. Ths larca caaks cbsarved 
ac tha becin.-.inc cf eac.n c.-.rc.tatccrachic run ar 
he heacscacs excer:.-.ent. 
Sa-=] 
Xoluana, 
:n 
K-22 I'A 
H-21 2-3 
.1 
<0.2 
none cstactad-
none datactsd 
"CO.2 
lone del 
1.2 
CD Limit of dataction ca. 0.1 cpm 
Quantitation was performed by standard addition (Ippr.) 
tc the sair.ple and comparison to the unspi.ked saiiiple. 
Chromatocrachv Conditions 
A. Toluene 
Column: 
6' x 2nra glass packed with 80/100 Carbocach C/ 
0.1% SP-1000 
Ta.T.ceraturss: Injector - 250°C Detactcr - 27S°C 
Oven - 1 min (§ 100"=C; 200°C 9 iS^C/rr.in 
Carrier: 
Nitrogen, 22 mi/min 
Detector: 
FID 
3. Pvridine 
• 
Column: 
4' x 2ra, glass packed with. 60/80 Carbopack 3 / 
4% Csriowax 20M/0.8% XCH 
.-.•.-j:i,?^.r:CVi3i^'-" 
301624 
'srr.z s JTi CJJTSS ; 
C a r r i a r 
Oven 
:r - 250-C 
De: 
120Cc 
i s c t h a r r 
r)7--^ 
3--^C 
5.0 grarr.s o f sa.rr.pla v e r a p l a c e d in a £0 ~ 1 serur. b c t - 1 ; 
was Healed with a Taflcn lined secf.:n".. Tha sealed ssr". 
beetle ccntaininc the sa—.pla was equilibrated, at 90^C : 
1-1.E hours. With a previously heated gas tig 
cf the headspaca vcl'ur^a frcm tha serum bcttle 
a.-.d cuicklv i.-.-ect=d into tha cas chrcmatcrrac 
t syrtn 
was with 
: a , 
0. 
•'.cMeal, T. a.-.d Hradar, C.V., 
J.i.OAC. 65, 
1 = 4-137 
(1982! 
Mctabcck Rafara.nc 
GI?,-1-143-145 
'£j.M/^, 
^i^:S 
G. I . Rude 
301625 
. c r i ; • t t u .ir.>,\ I' 
CO 
o 
cr\ 
to 
til 
I f j ^ I 
j INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
IIS? ROUli 10 RtNpOirH m*i KRSII 0)I69 
701 M< OilO 
uji^i-ivaeteixic.,,. lat.oi-atoru 
IIE.HOSPACE 
U t ' l ' o i t 
O n i c : 
Ociol.i.-r 9, 
IDfi'i 
I.a I). 
< 
3'if>2'i 
C o m p o u n d s 
d e t e c t e d 
i n 
p a r t e 
p e r m i l l i o n 
( m i l i g r a m a / k i l o g r a m s 
)Ory 
Wgt.Bas 
S.VMPLE SOURCE; 
S.AMPLE n.ATE: 
ENVIRO SCIEMCES 
SAMPLE ID: | . n Hole #20 
Sept. 
18-19, 19811 
T.AKE.X nV: A|,-,n_!..KY.!.£I 
AT I.AR DATE: 
9/2 7./fill 
i'( ( 
ClILOROMEni.A.K'E 
BUOMOMETIIASE 
^ 
niCIILOROniFLUORO.METIlANE. 
" • y 
Vl.WL CHLORIDE 
. 
/ 
^., . 
<r CHLOROETIIA.SIE 
y 
• 
METHVLE.XE CHLORIDE 
j 
Z> 
^ACETONE. 
TKlCHLOROFLUOROMETH.A.Vi;. . 
1,1-DICML0R0ETHYLE.\E 
1,1-D1CHL0R0ETHA.\E 
' 
• t-],2-DlCHL0R0ETHVLE\n.. 
LHLOROFOR.M 
T " 
' 
FKEO.V 115 
1 ,:-DJCllLOROETIIANE 
, l-BUTYL METHYL ETHER 
1 . 1 .1-TRlCHLOROETIIA.VE. 
. . 
CARBO.V TETRACHLORIDE 
BROMODICHLOROMETHANE 
1 ,2-DICIII.0HOI>R0PA.\E 
C-1 ,3-niCIII.OROPRnPENE 
t-l,5-niCIH.OROPK0PHSE 
TCE (TRICIILOROETIIYLENE). . 
niBRDMOCIILOIiOMETIlA.VE 
Hr.VIfNF 
Ill ISOPtiOPVL ETHER 
:-cin.oi(OETini\iNVL 
ETHER. 
HEX WE 
BROMOFORM 
1.1,2,2-irir(AciH.ORnFTin\E 
pri: 
(11 ri(ACiii.ni(ot;TiiviL.\L) 
HEPT.VVE 
TOMIL.VE 
CIILOKOnn.XZE.VE 
•. 
iETIIVLBENlENE 
n. I 6^ 
F o r 
t h e 
a b o v e 
l i s t e d 
v o l a t i l e 
p o l l u t a n t s , 
n o t h i n g 
i l e t e c t e i l 
a t 
n.oi|i|.m5ens i i i v i t y 
l e v e l . 
X 
O t h e r 
p e a k s 
d e l e c t e . l . 
F l u o r e t h y n e 
'^ 0 . ' . 5 ; 2-me t h y I | , r o , . a . u . I 0 . 2 0 ; p o . u a n e 
O . O I ; 
^ 
LT " Less t h a n , CT-fire;t(er 
tlian, \'I)»Noi d e t e c t e d , 
•'•NOrr: 
I'd-.. •, i l> I y from plastic; li.ii). 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
HEADSPACE 
I'L'port 
U n t e : 
Orioher 9, 
l9B'i 
l..il>. 
i 
3'i62!, 
IIW ROUll 10 RttjDOlM NiM <(RSI(OrU) 701 M< 01)0 
VOLATILE ORf.AMCS BY PIHUir A V Q I U P 
r.r/H.S 
Compounda d e t e c t e d 
i n 
p a r t e 
p e r 
m i l l i o n 
( m i l i g r a m a / k i l o i j r a m s j O r y 
Ugt.Bas 
S.AMPLE SOURCE: ENVIRO SCIEMtES 
SAMPLE 
I D : 
j , i 
(, | | „ | e 
//h 
SAMPLE DATE: 
S e p t . 
1 8 - 1 9 . 
198'i 
TAk'E.V BY: AJan_L^Ky!e_r 
AT LAB OATE: 
9 / 2 7 / 0 ' i 
U> 
o 
l-» 
a\ 
to 
-J 
CHLOROMETHANE 
BROMOMETHANE 
DICIILORODI FLUOROMETHANE, 
VINYL CHLORIDE 
CHLOROETHANE 
.. 
METHYLENE CHLORIDE 
ACETONE 
TRICHLOROFLUOROMETHANE.. 
1,1-DICHLOROETHYLENE 
1.1-DICHLOROETHANE 
I-1,2-DICHLOROETHYLENE.. 
CHLOROFOR.\| 
FREON 115 
1,2-DICHLOROETHANE 
I-BUTYL METHYL ETHER 
1,1,1-TRICHLOROETHANE... 
CARBON TETRACHLORIDE 
BROMODICHLOROMETHA.NE 
1 ,2-l)ICIH.OIl6IM(ni'\\i; 
C- 1 ,5-DICIII.nROPROPENE 
t - l ,5-niClllOROPROPENE 
TCE (TRICIIKMIOETIIYLENE). . 
0IBR0.M0CIIL0l;O^IETIIANE 
BENZENE. 
niISOPROPYL ETHER 
2-CIII.OROEIIIVLVlNVL 
ETHER. 
HE VANE 
BROMOFOR.M 
, 
1 , l , 2 , 2 - T r T R \ r i l l O R O E T I U V E . 
PCE 
(TETR.\flHOI!OElllYII;NE). 
HEPTANE 
TOLUENE 
CHI OROBENZENE 
ETHYLBENZENE 
X 
For 
t h e 
a b o v e 
l i s t e d 
v o l a t i l e 
p o l l u t a n t s , 
n o t l i i n g d e t e c t e d 
a t o . o i p p n e e n s i t i v i t y 
l e v e l . 
X 
O t h e r 
p e a k s 
d e t e c t e d . 
f l u o r e t h y n e 
- 0 . 3 8 ; 
2 - m c l h y l 
p r o p . u . . . l 
0 . 1 6 
„ 
, 
. . „ .
.
. 
, 
iVMOTF- 
I ' o b b i l i l v 
f I o m 
p l a b i l e 
liiii). 
LT - L e s s t h a n , G T ' C i c i i i c r t h a n , ND'Not d e t e c t e d , 
' " " ' t . 
Y 
I 
c . c r i . j t u ...;•.i,M'_: 
u . i t j r / u j a t 
z 
w 
o 
H 
o\ 
to 
00 
INDUSTRIAL 
CORROSION 
• MANAGEMENT 
INCORPORATED 
M7 ROUll 10 RtXPOirH NIM l(RS(< O'H) 701 ;>t>0)10 
•'>^'t':r Uloi-atortj 
HEADSPACE 
R e p o r t 
D a t e : 
October 9, 190't 
I.ill), i 3(,6?,6 
VOLATILE ORGANICS BY PHRGE ANIJiJjUP 
QC/MS 
Compounda d e t e c t e d i n p a r t a 
p e r m i l l i o n 
( m i l i g r a m o / k i l o g r a m s ) O r y 
WQi.Baii 
S.AMPLE SOURCE: ENVIRO 
SCIENCES 
S A M P L E ID: 
31 (i-|lole # 1 3 
SAMPLE DATE: 
Sept. I8-I9. igBlt 
TAKEN BY. A)an_L;KyJej: 
AT LAB DATE: 
9/2 7/0'! 
CHLOROMETHA.VE 
BROMOMETHANE 
DICHLORODlFLUOROMETHANE. 
VINVL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
TRICHLOROFLUOROMETHANE. . 
1.1-DICHLOROETHYLENE 
1 ,1-DICHLOROETIIANE 
l-l,2-DICHLOROETHYLENE.. 
CHLOROFOPv-M. 
FREON 115 
1 . 2 - D I C I I l O R O E T I I A N E 
t-BUTVL 
METHYL ETHER 
1 , 1 .1-TRICHLOROETHANE.. . 
CARBON TETRACHLORIDE 
BROMODICHLOROMETHANE 
1 .2-niCIII.0R:iPRnP\VE 
c- 1 .S-DlCIHv'ROPIiOPENE 
t - l .5-DICIIIOROPROPLNE 
TCE (TRICIH.OROETHVIENE). . 
niBROMOCIILOP.OMETIIANE 
BENZENE 
DlISOPROPYL ETHER 
2-CHLOROETHY IA INYL 
ETHER. 
IIEWNE 
BROMOFORM 
, 
1 , 1 , 2 . 2 - I L I R \ r i H . O R O r : l l l \ N E , 
Pr.r 
(TLIKACIIIOROEIHVILNE), 
HEPTANE 
T O I D E N E 
CHLOROBENZENE 
; 
, 
ETIIVLBENZENE 
_X 
For t h e above 
l i s t e d 
v o l a t i l e 
p o l l u t a n t s , 
n o t h i n g d e t e c t e d 
.n o . o i p p m s e n s i i i v i t y 
l e v e l . 
J 
O t h e r 
p e a k s 
d e t e c t e d , 
f i i . » r p i hynp ^ 0 , 3 1 ; 
2 - i i i e t t i y l 
p r o p . i i i n l 
" - K ' 
LT » Less 
t h a n , 
r i T ' C i r c a i e r 
t h a n , 
NI)=Not 
d e t e c t e d . 
••.NOTE: 
('<)s:.ilily 
friiiii p I 0 s I I c Iwni 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
k Z k k ' ^ " •"•:--"-^ ^'"-^'Vt-istdUH^,. LtiLoratoi-tj 
HEADSPACE 
R<'|"><t 
H a t e : 
Octol.ur 9, l98'i 
Lal). 
t 
3/,f,2-/ 
VOLATILE ORl'.ANICS BY PIIRrii; AND TIKP^ 
GG/.'llS 
Compounda d e t e c t e d in p a r t s per m i l l i o n 
(miligvtimo/kiloQrams)(*ry U.jt.Dd 
S.AMPLE SOURCE: ENVIRO SCIENCES 
SAMPLE ID: i, , Q „ „ | e 21 
lis? ROUll 10 RtNDOtrit NIM KRSII D»&9 
701 Sil 0)10 
SAMPLE DATE: 
S e p t . 
1 8 - 1 9 . 198'i 
TAKEN HY: A!c-.i>_L,u!<y.!£_r 
AT LAB HATE: 
9 / 2 7 / B ' i 
; 
1 
1 
! 
1 
1 
I. 
!. 
1 
••• 
1 
! 
! 
o 
; 
H 
i 
(X\ 
I 
IO 
! 
VO 
CHLOROMETHAN'E 
BROMO.\|ETHA.NE 
DICIILORODI FLUORO\IETIIANE, 
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
TRICHLOROFLUOROMETHANE. . 
1 ,1-DICHLOROETHYLENE 
1,1-DICHLOROETILANE 
l l ,2-DICHLOROETIIYLE-;E. . 
CHLOROFORM 
FKEON 115 
1.2-DICHLOROETHANE 
t-BUTVL METHVL ETHER 
1 .1 ,1-TRlCHLOROETILANE. . . 
CARBO.N TETRACHLORIDE 
BRO.MOD I CHLOROMETHANE 
1.2-i)iriii.oRopi(np\vE 
c-1 ,5-I)K:III.OROPI(OPI;NE 
t - 1 ,5-|l|CIII.OR0Plt0IM:KL 
TCE (TRlCHI.OROrillYl ENH). . 
DlRROMOrillOMO.MnTHANE 
BENZENE 
Ill ISOPROPYL ETHER 
2-rillOROLIIIVI.V INVI. ETHER. 
HEXANE 
BRt^MOFOR.M 
1 , 1 ,2,2-TEIR.\CIII.OROETllVNE 
p("L 
(Trik.vciii.oRnrriiviLNi.) 
IHPIVNE 
101 DENE 
CIHOIKMU NZL\C 
•. 
ElllVI BENZENE 
. . 
1 
X 
For t h e above 
l i s t e d 
v o l a t i l e 
p o l l u t a n t s , 
n o t h i n g d e t e c l c ; ! a t n.olppni sens i t i vi i y l e v e l 
X 
O t h e r 
p e a k s 
i l e t e c i e d . 
fJ.iJ2L^L'*Yi}.?"_?:_"§J_?llI'l''l.yL_!'!;".'J'2"" ' " • ' ' ^ • /^-"i'-' hyl - ' ' ' " - l " ^ " ^ " • ^ ' ; 
Dyi:Lt!.lnu-_i?:-Q?-- 
- 
- 
- 
-
IT • Less 
t h a n , 
r,T=C.i c i i i e r 
t h a n , 
Nl) = N(ii 
d c U L i c d . 
NOTE : ' r i . i . - j i ll I y 
f i d m 
p I .i s l i i; l>.i<). 
^ c- ^/, /^V 
Ervs» « i xtaxsi srx. 
CHAIU OP CUSTODY .^ICORD 
1» CC»»EU>J»0 RO.. CENVllXE. »6W JtJlSET 07SM 
I n s t a l l a t i o n : ZAt.cy Asj>s .Z^yc. 
S u r v e y No 
.'7<' Cfyiiafje^ yyyfayyy y7c»m,as 
Saaplera: (Signature) 
a. 
e ' 
rs CI 
CO 3 
S t a t i o n 
L c c a c i o n 
I 
D a t e 
T l a e 
S a n p l e Type! 
a 
Leap . vjrao 
•..,.. Z. 
/ S 
2^ 
y r - y f Z y y r -
X 
I 
y ' j 
/ 
I 
y s /s 
y 
/ 
¥ ' J 2 / 
R e l i n q u i s h e d 
b y : 
( S i g n . ) 
R e i m q u i s a e a 
b y : ( S i g n . ) 
R e c e i v e d 
b y : 
( S i g n . ) Date l1\.-3.^ 
( R e c e i v e d 
b y : ( S i g n . ) Date/Tiae 
Reiinquisned by: Ciiga.) 
.ved b y : ( S i g n . ) I D a t e / T i a « 
R e l l n q u l a h e d 
b y : 
( S i g n . ) 
R e c ' d by 
L a b o r a c o r y 
f o r 
f i e l d 
a n a l y s i s 
( S i g n . ) 
yz. 
D a t e / T i a e 
Dispatched by: (Sign.) 
Dace/Time lec^ 
f y i Laioracory 
yAvJAz^ 
D a t a / T l a e 
Method of 
S h i p m e n t : 
301630 
^?M% 
YORX LABORATORIES DIVISION 
CERTIFIED REPORT TRANSMIHAL 
REPORT NUMBER . 
30850-145 
DATE 
... Xcve.T.ber 12, 19 3 4 
CL;SNT 
£.-.viro-3ciences , inc. 
19 Cccela.".d ?.c3.d. 
Denville, New Jersey 
0 7 8 3 4 
ATTcNTlON Mr. Ijrr Cohen 
The above refefencec report is enclosed. Copies of this report and supporting cc:c 
will be relcinec in cu tiles in tne event ihey cre requir©a (cf future refecenca 
If there are any quesrions conceming tftis report, please do not hesitate to contact us. 
Any samples submitted to our Laboratory will be retained for a maximum of sixty (60) 
days from receipt ct tnis report, unless other oirangements are aesired. 
Naturally, as inthe pest, CLrslultwill be pleased to quote on any future recuirem.enrs 
you may hcve In ccditlon fo the service provicec we also offer the following: 
HazcnSous Waste Analyses 
Prccuc: Evaluoiion/R&O 
Wcrer and Wastewcrer Analyses 
Air end Process Gas Analyses 
• Incustnal Hygiene Surveys 
• Metallurgical Analyses 
• MIcrablological Analyses 
• Mess Spectrometry Services 
Robert Q. Bradley 
CA 
Vice President 
-.-iC. 
• tL'.c s:.->-v:e •r.,-r.c:''e • Mc.-coa Ccnracric^" 'Zt>.U,& • |2Qi) ;ii-.ii£a 
301631 
si 
••loveniber 12 , 19S4 
30350-145 
E>rviRO-SCIENCES, INC. 
19 Copeland Road 
Oer.ville , Ne^f Jersev 0733' 
Atte.':tion: Mr. Irv Cohen 
PU?.?OSS 
Nine (9) soil saaples were submitted to Yori Laboratories for 
deterrtinatlon of toluene and pyridine on a quantitative basis. 
Other compounds found in the samples were also Indentified and 
are reported on a seai-quantitative basis. 
The sait^ples •sere 
also analyzed for oil and grease. 
METHODOLOGIES 
The samples were analyzed 
for toluene using the dyna-mic 
headspace 
Gas 
Chromatograph/Mass 
Spectrometry 
method 
in 
accordance with Cher.ical Analysis of Sediments and Elutriate 
Testing, EP.\ 1979. 
A Tekmar Model LSC-3 Purge and Trap 
interfaced with an HP 5995C GC/MS/DS were used 
for the 
analysis. 
The samples were analyzed for pyridine and oil and grease in 
accordance with EPA/CZ-81-1 Procedures for Handling and Cheai-
cal Analysis of Sediments and Water Samples, May 1981. An ii? 
5995C GC/MS/DS was used for the pyridine analysis. 
RESULTS 
The results are listed in the following tables. 
Prepared by: 
Gail 0. Sprio 
Senior, Chemist 
snior. ^,nerais^; y 
Approved by: 
\ Z r L/.,-,I (J • \Au.u!i'<^~^ 
GDS/JCC/mz 
J.eiff|rey C. Curran 
ChiisfrX^Uetnist 
YWC. IMC • 2CQ Mojvcf Ti«npi>"r • iM-.-.oi.:.<- CO'-<-.t?ciicu O.V».'>a • • C m i^l-cai-i 
301632 
w 
TABLE 1 
ENVIRO-SCIENCES, IVC. 
TOLOENB AND PYRIDINE RSSnr.T^ 
IdenlS^Lior, 
i.kkkkiy . 
P y : - i d i . e 
u g / k g 
r o s b l 
<1 ,000 
<1 ,000 
< 1 , 0 0 0 
<1,000 
13 ,000 
2 6 , 0 0 0 
4 3 , 0 0 0 
< 1 , 0 0 0 
< 1 , 0 0 0 
20 Septic 
20 A-2' 
21 .\-2' 
2 1 .^-4 ' 
25 - 2' 
2 7 - 2 ' 
32 - 2' 
35 - 4' 
36 - 2' 
CAuger) 
540 
690 
15 
43 
210 
16 
15 
8 
7 
V^'C.-NC •2C:M:ii,t^-,>rz-..i:.!A..--r.t. r:.-r-..-..-::-..,:,^.. . , - „ , , ,,. ^..., 
301633 
...^—... ^^ ^-, 
1-7 
TABLE 2 
E^fVIRO-SCISNCSS. 
INC. 
Samole Identification 
Comoounds -ound 
' ' ^ " " u ^ ' ^ e f 
20 A - 2' 
methylene chloride 
chloroform 
benzene 
ethyl benze.".e 
Y'MC. INC • 2nO M.-«-»-r.^ T(yo,-;,i... >.;-.,.,-, 
.--y-f-ir "r.-.i-::e-^i'i •':-:-^t 2r-- iJ^ 
a ,400 
20 S e p t i c 
(Auger) 
1,1-methylene b i s - b e n z e n e 
a ,t^'j 
diphenyl methanone 
64,000 
methylene c h l o r i d e 
<5 
chloroform 
12 
benzene 
<3 
<5 
<5 
6S 
total xylenes 
500 
21 A - 2' 
methylene chloride 
<3 
chloroform 
<5 
trichloroethylece 
• <5 
benzene 
<5 
tetrachloroethylene 
<5 
ethyl benzene 
7 
21 A - 4' 
methylene chloride 
<5 
chloroform' 
<5 
benzene 
<3 
2 5 - 2 ' 
methylene choride 
<5 
chloroform 
5 
benzene 
<5 
27 - 2' 
methylene chloride 
<3 
chloroform 
19 
benzene 
<5 
3 2 - 2 ' 
methylene chloride 
<5 
chloroform 
<5 
1,1,1-trichloroethane 
<5 
benzene 
<; 
3 5 - 4 ' 
methylene chloride 
<5 
chloroform 
13 
1,1,1-trlchloroethane 
11 
benzene 
<3 
3 6 - 2 ' 
..methylene chloride 
<5 
chloroform 
<5 
benzene 
<5 
•Results are reported on a semi-<iuantitative basis. 
0.3 
2 .3 
0 .9 
2.4 
3 .3 
O.S 
0.5 
0.9' 
2.2 
2.S 
0.4 
1 .7 
0.4 
2.2 
0.6 
4.4 
4.2 
0 .8 
0.3, 
2.4 
0.4: 
1.6 
1.4 
0.2 
301634 
TASLH 3 
E-WIRO-SCISNCES. 
INC. 
OIL A2TD GREASE RF<?rTT.T<; 
.->' 
Sa.T.ple Identification 
20 Septic (Auger) 
20 
A - 2 ' 
21 A - 
2 ' 
21 .4. - 
4 ' 
25 - 
2 ' 
27 - 
2 ' 
3 2 - 2 ' 
3 5 - 4 ' 
3S - 
2 ' 
0: 
1.1 
_mg 
And Grease 
/ks Cacm^ 
241 
555 
1 ,500 
27.3 
89.S 
137 
50.6 
39.5 
,: 965 
301635 
Si'i 
INDUSTRIAL 
CORROSION 
UANAGEMENT 
INCORPORATED 
|lilM)>i\i It &uaOllH.ll(lllJltUItlUI IOIW««IM 
CLIEHT: 
ICNVtHO SClKNfiK - ICC (HerlcM) 
NJDiP I c i l l l i e u uiiiiKiiitj 
LaLoraiury 10 l U l 16 
s o n . SAMPLE 
REPORT DATE; .Inly T l , 19H5 
LAB i _ i m } l 
SAMPLE ID: llrnjo j l n u 112 
SAMPLE DATE: 
6/7/85 
SAMPLED BY; 
A. Kyluu 
VOLATILE ORGANICS BV PURGE AHO TRAP 
By CC 
•BTy/"tADSPACE 
AT LAB DATE: 
fi/m/flS 
CIILOROHETIIANE 
• 
BROMOMETHANE 
• 
VINVL CHLORIDE 
• 
CHLOROETHANE 
• 
METHYLENE CHLORIDE - - -
ACETONE 
I.I-OICHLOROETHVLENE --
I,I-DICHLOROETHANE **--
t-l,2-DICHLOROETHYLENE 
CHLOROfORH 
1,2-DICHLOROETHANE 
I-BUTYL METHYL ETHER --
I.I,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE --
BROMODICHLOROMETHANE --
1.2-DICHLOROPfiOPAN£ ---
Compounds detected In parts per tnllllon (ml 11 Igrams/k I lograms) dry weight basis. 
K 
^,c-l,3-DICIIL0R0P«0PENE 
— 
X 
'l-l,3-0ICIIL0R0PH0P£H£ 
! 
X 
TCE (TRICIIIOROtTHVLENE) 
) 
],2l,n 
M 
l,l.2-TRICIILnK0£TIIAHE 
6B 
10 
^Compounds co-elute (could be either material). 
LT-Left Than, CT-Creater Than 
dwb-Dry Weight Basis. 
X-Not Detected 
'DIBROHOCHLOROHETIIAHE 
BEN2ENE 
DIISOPROPYL ETHER 
2-CHLOROETIIVLVINYL ETHER 
BROMOFORM 
1,1,2,2-TETftACHLOROETHAHE 
PCE (TETRACIILOROETHYLEHE — 
TOLUENE 
-
CHL0R0BEH7ENE 
_ 
ETHYLBENZENE 
- 
_ 
H-XYLENE 
_ 
« I O-XYLENE 
P-XYLENE 
— 
**Teiraliydrofuran ( Phosgene also elute at this 
point. Numerical results are calculated for 
I,l-Olchloroethane only. 
s.6nn 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level o f : 
y 
Unknown peaks detected (retention t Imr,est Imated amount): Xyltinc-a 
IH; 11) iiiikiinwn liyilrociirlion pcwika raii[^£i;t; 
fron) 2 to 10 oK/klt- 
_ _ _ ____ 
. 
NOTE:Compound Identification Is based upon retention time matches with specific known standards. Confirmation 
of analysis using CC/MS Is required to positively Identify any materldl and/or amount detected. 
IKOUSTRI ApCOJJROS I mtiiCMT, YJ w:. 
yy 
^ — - ^ — . _ _ 
\f<^ 
• y ! 
Z J I i 
INDUSTRIAL 
CCRHCSiCN 
MANAGE'/ZNT 
INCORFGF^TED 
•.i:: ^ouTi -.0. .^incc'.-i'v. .-icw :y:rf a7aa5 ::•. ;-i-:2;c 
CLiz:;t: ;:r.":?.o scrz^tcts. ';tc 
c_i_wp^r SCL'?.£Z: 
ICC CEEP-iZIC^ ??.C_'iCT 
y 
V.'ascava;ar Ljboritsr-/ 12 i-'l-:.li 
ilCPC'C SACZ; 
.^uiusr If. 19 = : 
LA3 ••/ 
ii2SS2 
SAM?!.; I.;: 
Dr21.-. 
S.C<3L3: C A " : 
6 / ' / 3 5 
SA^Jir: 3Y: 
A. Kvlas 
soil. SA:-C?LE 
i.A3a?ACC5.v A:;AI.";:SZ£ 
.\r ' - ^ CACZ; 
-i/lS/ :5 
:lcn Tf 3lacx S o i l : 
p ^ ' ^ - ^ a ; a ^ 
Ser.= 5.-.a 
Coluer.e 
:-vl:ar.::er.e 
£:hyl: 
.«-;-:vlar.e 
0,?-Xvl=r.e 
0. IC 
Q.ZS 
0.22 
0.2? 
Simple has "Toiue.ie l i k e " or soLvenc odor. 
3..t. e.S'S ac 4Q !ns?/'<3 
R . r . 3 0 . 2 1 _c 
2 Sij/kg 
All rasulrs rapocrad ir. a5/'<.g. 
Ve cr.cr.k. /cu foe chis opporcunl;-/ co s-r.fe you. I: you have any quasctcr. 
p'.za.ss do r.oc hesicica co call. 
-\ 
l:^USZ^l.\L CC-L'.GSICN yjLNACiC-li:: 
L~/jng 
•cl. 
_.'"L.*ss Than 
Eduia. Tlcr.er.or 
Vice Presidenc 
301637 
. LAB NO. 42885 
Pit duplicata (liquid) Priority Pollutants +40 
(Process Pit) 
Saaples not analvzed because sample volume too stiai; 
301638 
• • • r i r m a i ' i a ^ ' ^ m 
INDUSTRIAL ^^^^ 
CORROSiON SA.MPLZ 
MANAGEMENT 
INCORPORATED 
[IJ2 RCUIE 10. RANOCCfH. NEW jERStT 073S9 
r01-S34-0330 
NJOE.' C e r t i f i e d Drinking Wac-r/ 
Wastewater Laboracory to ./litllo 
REPORT DATE: 
Julv 3 1 . n s s 
LAB H 
42936 & 42887-rn>?ng-
AA 
CLIENT:. 
iN-1 ?0 SCISNCIS 
SAMPLE SCURCE: 
SAMPLE DATE: 
6/14/85 
ICC (3erlax) 
SAMPLED BY: 
A.Xylea 
AT LAS DATE: 
PRIORITY POLLUTANT VOLATILE ORGANICS + ^0 
by GC/MS + I 5 PEAKS 
6/18/85 
Paramecer 
Result 
Paramecer 
Resul : 
acrolein" 
acrylonitrile* 
benzene 
bromoform 
carbon tetrachloride 
chiorobenzene 
ch i orod ibrwTicmethane 
chlorethane 
- - - . 
2-chloroethylvlnyl 
ether 
chloroforn 
dlchlorobrcmcmethane 
: 
1 ,1-d!chlorcethane 
1,2-dichlorcethane 
1 ,1-dichloroethylene 
220 
1 ,2-dichloropropane 
1 , 3-dichloropropy1ene 
ethylbenzene 
methyl bromide 
methyl chloride 
methylene chloride 
1 ,1,2,2-tecrachloroethane -
tetrachloroethylene 
toluene 
•. 
1,2-trans-dichloroethylene 
1,1,1-trichloroethane 
I,1,2-trichloroethane 
trichloroethylene 
vinyl chloride —•• 
Resulcs reported in mg/Vg (ppa), dry weight basis. 
LIS 
X 
1,560 
X 
•Detection Liait 
LT-Le5s than 
X=Not detected 
100 Dom 
OTHER COMPOUNDS DETECTED 
APPROXIMATE 
CONCENTRATIONS 
22 
1430 
l - c h l o r o - Z - s e t h y l benzene 
40 
benzyl a c e t a t e 
c h l o r o n e t h y l benzene 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
ET/Jag 
Edwia^Tlchenss-
Vice President 
V- A 
Pz> 
301639 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 MUTE 10. HlKOQl?^. NEW IIKTI 07U3 20Mi*Ji220 
CL 1 EMT: 
E^n^ISO SCIENCE 
NJOE? C e r t , 
. e d 
O r i n k i n c 
W a t i r / 
UasLe-rtoter 
L a b o r a t o r y 
10 . ? 1 H 1 1 S 
= .\^. 
REPORT DATE: July 3j. 
LAB I 
SOIL SAXPLZ 
L9S5 
^2386 & 42387 CCy.50SI~ 
SAMPLE SOURCE: ICC (Berlex) 
SAMPLE DATE:_iZiil2i___SAMPLED BY: A. Kvles 
.AT LAB DATF-- <./-'g/a-
PESTICIDE S PCB EXTRACTABLES 
PRIORITY POLLUTANTS + 1*0 
by GC/MS 
Pa rameter 
Result 
Aldrin 
LT 2-
a-3HC 
- 
L7 2 
b-BHC 
- — 
LT 2 
d-3HC 
LT 2 
g-SHC 
- 
- 
- 
— 
— 
LT 2 
Chlordane 
LT 12 
l»,U'-DOO 
— 
LT 3 
'»,'*'-00E 
- 
LT 3 
A,U'-ODT ----- 
- 
- 
LT 3 
Dieldrin 
-' 
LT 3 
Endosulfan I 
LT 3 
Endosulfan II 
: LT 3 
Endosulfan Sulfate 
; 
LT 3 
Endrin 
; 
•• 
LT 3 
Endrin Aldehyde 
LT 3 
Heptachlor 
LT 3 
Heptachlor Epoxide 
LT 3 
Toxaphene 
LT 12 
PC3-10'16 
IT 45 
PC3-1221 
- 
LT 45 
PC3-U32 
- 
LT 45 
PC3-12i*2 
LT 45 
PC3-12l4a 
— 
L-r (.tt, 
PC3-125^ 
- 
— 
LT 45 
PC3-126Q 
- 
- 
t-T 45 
All 
r e s u l t s a r e reported In sig/kg (ppm), dry veighc b a s i s . 
INDUSTRIAL CORROSION MGMT., INC, 
r H > » ^ ^ ^ ^ v r U 
fi.-Tvr:T / 
Edw i>^^ T i ch'TWior 
^— 
It 
ET/jmg 
V i c e P r e s i d e n t 
/QZ^ 
L T - L e s s 
T h a n 
X=»Noc 
D e t e c t e d 
301640 
rp 
% 
I N D U S ' ^ 
. , A L 
Wastewater L 
CORROSION ^ 2 1 ^ ^ ^ „^^„,^ „^^^._ 
M A N A G E M E N T 
^ ^ / 
42386 & 42aa7-rn'.ioo<;TTT 
INCORPORATED 
r a i o r y 
iQ ^ 11,1 1 6 
11S2 ROUIE 10. RANIXIPH. NEW JERSEY 07853 ai-5*l.03:0 
C L I E H T ; 
r S V I R O 
SCIENCES 
ICC (Berlex) 
SAMPLE 50URC-
SAMPLE DATE: 6/14/85 
SAMPLED BY: 
A.Kyles 
.AT LAB DATE:. 
6/13/3; 
BASE/NEUTRAL EXTRACTABLES PRIORITY POLLUTANTS + kQ 
by GC/MS 
+ 15 PEAKS 
X 
Parameter 
Result 
acenephthene —•-
acenaphthylene 
anthracene 
benzidine 
benzo(a)anthrac8nc 
benzo(a)pyrene 
3,'f-benzof luoranthene 
benzo(ghi)pery1ene 
benzo(k)fluoranthene 
bls(2-chlQroethoxy)methane 
b i s ( 2 - c h I o r o e t h y l ) e t h e r 
' 
b I s ( 2 - c h l o r o I s o p r o p y l ) e t h e r -
b l s ( 2 - e t h y l h e x y t ) p h t h a l a t e 
'»-brotiwpheny1 phenyl ether 
butylbenzyl 
p h t h a l a t e 
2-chloronaphthalene 
- - — - - - — - -
*i-chlorophenyl phenyl ether 
chrysene. 
dlbenzo{a,h)anthracene 
1 ,2-dIehlorobenzene 
1,3-dlchlorobenzene 
1 ,'»-d Ichlorobenzene — — - - - - - -
'3 i3-dlchlorobenzidlne 
. 
Parameter 
diethyl phthalate 
dimethyl p h t h a l a t e 
di-n-butyl 
phthalate 
2,'*-dlnl trotoluene 
• 
2 , 6 - d i n i trotoluene 
d l - n - o c t y l 
p h t h a l a t e 
I,2-dlphenylhydrazine(as 
azobenzene)-
fluoranthene 
fluorene 
— 
hexachlorobcnzf.ne 
hexachIorobuladiene 
hexachl orocycl open tad iene — 
---
hexachloroethane 
lndeno(l ,2,3-cd)pyrene 
i sophorone 
naphthalene 
nitrobenzene 
— 
N-n11rosodI methy I amine 
N-nltrosod i-n-propylamine 
N-nItrosod Iphenylamine 
----
phenanthrene 
pyrene 
--
I ,2,'»-trlchlorobenzene - — 
--—. 
Resu' 
Y 
X 
•7 
X 
r 
T 
X 
X 
X 
X 
_x_ 
None of the above listed Priority Pollutants detected at a sensitivity level of 
450 mg/kg (ppa) dry weight basia. ** . 
IT-Less Than 
X=Not Detected 
**Large dilution necessary due gp high concentration of benzyl ace: 
APPROXIMATE CONCENTRATION 
OTHER COMPOUNDS DETECTED 
benzyl acetate 
- - / / • rg/Ci benzene methanol 
l , l ' - [ o x y b i s 
(taethylene) 
bis]benzene 
170,000 
15,000 
4,000 
Chloromethyl benzene 
diphenyl methanone — 
9H-fluorene-9-one 
— 
- 4,400 
-30,000 
- 3,000 
All results reported in mg/lcg (ppm), dry weight basis. 
ET/iT 
INDOSTSIAL CORROSION MGMT.,".
301641 
iiWxr?K.-<=?' 
%f^-
w 
o 
cr. 
to 
INDUSTRIAL 
pORROSION 
MANAGEMENT 
L'J N I INCORPORATEO 
iiii»aniii.itAMioi>H.|<Yiiuitnaiu4 UI-U^IIM 
NJDEP Certified Drinking Udlcr/Uautcwd. 
Laboratory 10 Il<tll6 
son. SAMPLE 
REPORT DATF: 
-'"ly 31. ISQj 
LAB Jl A2afl6 & 42887 COHPOSTTE 
CLIEHT: 
-£HUliQ-SCltUCEa. 
SAMPLE SOURCE :__icc_XiluiiliixL 
SAMPLE DATE; 
fi/14/flS 
SAMPLED BY: 
k , Vy}.,^ 
AT LAB DATE: 
Jdl&JM. 
AGIO 
EXTRACTABLES 
PRIORITY 
POLLUTANTS 
+ tiO 
bv 
CC/HS4 IQ PEAKS 
ACID EXTRACTABLES PRIORITY POLLUTANTS » 10 Peaks 
2-chlorophenoi 
y 
2-nltrophenol 
X 
phenol 
X 
2,4,-dimethylphenol 
X 
2,<«,-dlchlorophenol -- 
' 
X 
pentachlorophenol 
X 
2,Ji-dlnl trophenol 
X 
'i.S-dlnltro-o-cresol 
x 
^-nltrophenol 
X 
2,'(,6-irlchlorophenol 
jj 
'i-chloro-J methyl phenol 
X 
None of Che obove liaced Priority PoIlucanCa dececced 
a t a senlstlvlcy level of 450 mg/kg (ppni) dry weight baalu 
OTHER COMPOUNDS DETECTED APPROXIMATE CONCENTRATIONS 
No other I'lienollc compounda detected ac a senalclvlt] 
of 500 mg/ku (ppm) dry welghc baula. ** 
INDUSTRIAL CORROSION M A N A G E M E N T , INC. 
** Large dilution neceBBary due Co high concencruclon 
of benzyl acecace. 
ET/Jmg 
LT-Lc$i Than 
X-Not Detected 
Edwl rt- T i cli<Jiior 
Edwl rt- T i cli<Jiior 
V i c e 
P r e s i d e n t 
iiixzni 
A% 
INDUSTRIAL 
CORROSION 
SOIL SA.MPLE 
HJDE? Certified Drinking Water 
Wastewater Laboratory 10 ^1^116 
MANAGEMENT 
INCORPORATED 
Ii'i; ROUll m. RiNooiPH. NtW j{RsiTo;itfi9 M I U4UIT(I 
n IFNT; 
ENVTRO SCIENCES 
REPORT DATE: 
-LL^ 
LAB / 42886 & 42387 Co=oosits 
SAMPLE SCURCE: ICC (Berlex) 
SAMPLE OATE: 6/14/85 
SAMPLED BY: 
A. Kvles 
AT LAB DATE:6/18/85 
PRIORITY 
POLLUTANTS + 40 
TOXIC POLLUTANTS: Metals, Cyanide and Total Phenols 
PARAMETER 
T o t a l 
Anti.TXiny 
Total Arsenic 
Total Beryl 1ium 
— 
Total Cadmium 
Total Chromium ---
Total Copper 
Total Lead -------
Total Mercury 
Total Nickel 
Total Selenium 
Total Silver 
Tota I Tha I 1 ium -••-
Total Zinc 
RESULT 
T T Iiq 
40.0 
LT 
2^87 
22.8 
592 
327 
688 
2.73 
134 
LT 
L.08 
iT 
7^48 
LT 66.2 
3.594 
Total Cyanide 
Total Phenol -
_L.44 
_1,Q1 
All results are reported in ag/Vg (ppm)', dry weight basis. 
We thank you for this opportunity to serve you. 
If you have any questions, pleose 
do not hesitate to call. 
Very truly yours, 
INDUSTRIAL CORROSION HGMT..INC. 
^ A^^j<r<rry~\ i Zzy 
Edwin TicheivQr 
-T^-e^ / 
ET/jmq 
LT»Less Than 
X=Not Detected 
Vice President 
/0£) 
301643 
(A) 
O 
M 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
son. SAMPLE 
NJDEP Certified Drinking Udter/Udstcwdte 
Laburdtory ID / U l U 
iiwtouii It uiicaini.Ma.«U4f(iui MIU4«IM 
CLIENT: 
ENyiRO SOIKNCK 
ICC (Iterlcx) 
REPORT DATE:_ 
LAB / ^111112. 
SAMPLE ID: 
•Inly 31.19(15 
J)ry(;r_ 
SAMPLE DATE; 
6/14/05 
SAMPLED BY: 
A. Kyleu 
VOLATILE ORGANICS BY PURGE AND TRAP 
By CC 
BTX/HEADSPACE 
AT LAB DATE: 
6/m/H5 
CHLOROMETHANE 
• 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE - — 
ACETONE 
1,1-DICHLOROETHYLENE -
1,1-DICHLOROETHANE **— 
t-l,2-DICHLOROETHYIENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER --
I.I,I-TRICHLOROETHANE -
CARBON TETRACHLORIDE --
BROMODICHLOROMETHANE --
1.2-DICHLOROPROPANE ---
Compounds detected In parts per million (ml 11Igrams/kllograms) dry weight basis 
X 
4.0 
340 
4.2 
i^Compounds co-flut« (could ba cither material), 
LT-Less Than, CT-Creater Than 
dwb-Dry Weight Basis. 
X-Not Detected 
^[C-I,3-DICIIL0R0PR0PENE 
't-l,3-DICIIL0H0PR0PENE 
^ 
TCE (TRICIIIOHOETHYLENE) 
^,1,1,2-TRICIILOROETIIANE 
'DIBROMOCHLOROMETHANE 
BENZENE 
DIISOPROPYL ETHER 
2-CHLOROETIIYLVINYL ETHER 
BROMOFORM 
1,1,2,2-TETRACHLOROETIIANE 
PCE (TETRACHLOROETHYLENE 
TOLUENE 
CHLOROBENZENE 
ETHYLBENZENE 
M-XYLENE 
-
wO-XYLENE 
P-XYLENE 
**Tetrahydrofuran ( Phosgene also elute at this 
point. Numerical results are calculated for 
I,I-Dichloroethane only. 
X 
X 
6.6 
X 
X 
X 
X 
X 
4,000 
X 
16.1 
17.7 
I S . I 
For tha above listed Volatile Pollutants, nothing detected at • sensitivity level of: 1 mn/Vn dml>. 
_Unknown peaks detected (retention timr,estimated amount): 
NOTE:Compound Identification It based upon retention time matches with sf>eclflc known stanJdrds. Confirmation 
of analysis using GC/HS Is. required to positively Identify any materldl and/or amount detected. 
illDIISTHIA!^ORflOSiON.»CMT,^|MC. 
t ! 
CHAIN 0? CUSTODY .RECORD 
It COPLAND TO.. DENVIUX WW JEPSTY 07834 
I n s t a l l a t i o n : 
ICC (Eeriex) 
Survey No.: 
o. 
a 
nj C 
in. 
Station Location 
Saaplers: (Signature) 
Date 
Analysis 
Tine 
Sampl - J -
e 
i y p e< 
u 
<-o3o . ij r a 0 
G f^ 
i.1 
• s 
o o 
2 -J 
Drain Line 
y^?zi 
Toluene 
6/5/85 
Identify the contents cr t.ne black soil 
sanple.] 
/ -
La'ooratory Pit 
' P 5 - ? ^ "b Pyridine 
6/14/85 
Laboracory Pit-duplicate ^ 
^ VGA j / ; ^ li4 
6/14/85 
[* Tise liait may have expired, if so do not run.] 
ly-^tia-^ 
i 
Pic-duplicats (liquid) Priority Pollutantb 6/14/85 -kkJl 
V(5 iTi-;.^ 
combine and 
Pit-Int erf ace (liquid/sl'jdgejX 
j-^j, 
6/14/85 
Pit-sludge 
t4.s.9&~/ 
j priority 
dis-;s 
tsollutants 
6/14/85 /P^A-c 
V 
v!/ 
Ona container has a vhite lump, segregate it and an lyze for 
ilne 
quinidine.] 
Dn •••er 
l y C y Mi- />^'-^f 
Toluene 
6/14/85 
Relinquished by: (Sign.) 
RecSlyed by: (Sign.) 
Relinquished by: (Sign.) 
yyy 
Received by: (Sign.) 
Date/Tiae 
Date/Time 
is.eiinquLsnea by : ( Sign. ) 
jRecaived by: (Sign.) 
Date/Ti 
Reiinqjiiatied 
by:/^Sign.) 
Rec'd by Laboratory 
for field analysis 
Dispatched by: (Sl/in.) 
r 
(Sign.) 
Date/Tiae 
y / 
Date/Tlm^[Rec'd for Laboratory 
by: 
D a t e / T i m 
' M A l ^ 
Method of Shipaent: 
Express Air Freight 
kl/uyyA/-
301645 
mm 
YCRX LABORATORIES DP/ISICN 
tg/r 
CERTIFIED REPORT TRANSMITTAL 
R=.=CRT NUMEg= 
: c g ; o - i i ? ; 
DAT 
•) = 
' z - : - . 
CUENT 
Er.vircsciar.css^ 
Ir.c. 
19 C = celar.c P.c^^ 
D e = v i i l e , NJ 
07334 
ATTcNTlCN 
Dr. A. Kyles 
Th.e cocve refe<-encsc raccn is enciosec. Ccpies cf T\'is reccn end succcrtng cere 
will t e rercinec: in cur !H*s in the even: ffiey cre recuireC fcr furure refefenca 
If there cre cny cuesricrti ccnceming this repcrt. piecse dc net hesitcre TO conrcc: us. 
Any scmoles suPmiKeQ tc Cur LcPcrcrcry will be rercined fcr c mcxin-.um cf sixr/ [iO] 
dcys from receipt of tni^r^iscrr, unless omer crrcngemenis cre cesirec. 
Ncojrcily, cs in the pcsT; o u ' srcff will t e piecsec to cucte cn cny fuu'e rec.uiremer:Ts 
ycu mcy neve. In ccciticfi ro the service provided, we else crfer ihe 'cilcwing: 
• Hc2c.-C3\:sWcsfeAnctyses 
. Prccuc: ?vciucticn/R&D 
• WcTerijrcv/csTewcTerAnclyses 
• Air one Ptccess Gcs Anclyses 
• indusrrct Hygiene Surveys 
• Mefcilur^jccl Analyses 
. Mlc-ocic^c9iccl Anciyses 
• Mess Sp^ctrcmeiTY Services 
w f y Tnjiy Y< 
Robert G-Brccley 
Vice President 
301646 
vrfT^=^---
?s. 
S e o t e n b e r 25, 1985 
30850-1195 
E^^VIKOSCIiNCSS , 
rac. 
19 Copeland 
Road 
D e n v i l l e , New J e r s e v 
07834 
Atte-'i-icn: 
Dr. A. 
K y l e s 
?'r~.:=CSS .:^D RESULTS 
E i g h t 
(8) 
s o i l 
sa.T.ples were s u b m i t t a c 
t:c York L a b c r a t c r i e s 
f c r 
a n a l y s i s . 
The sarr.ples were c r e c a r s c £.~c. a.nalyzed 
i.-. acccrda.nca 
w i t h P r o c e d u r e s 
f c r Hancli.-.c and Cha.^.ical A n a l v s i s cf 
S a c i - = n t 
and >:ater Sa.T.clas, £ ? A / C r - 3 1 - 1 . 
~ 
T.^.a r e s u l t s 
a r e recoct:ed 
in t h e follcwi.nc 
T a b l e s . 
P r s c a r e d by: Z J > x < k C ' P - C ^ 
D a n i e l r , 
otiz 
L a b o r a t o r y 
Manaeer 
Aoeroved 
bv: 
.y 
^ 
u^^ 
•a^£.t-&v f C 
C u r r a n 
/cHZeP Che-itist 
DFO/JCC/md 
r.vC. INC. • 2C:Q •Mor.'Cft Tvrr.cike • Monroe. Connecrcut C^Aio • [IZZ) 261-^i-i53 
• 
301647 
3 -
• 5 
T c l u 
CS» 
^*—-nC!!<e.;Mca-ce.C; ^""^ncu:C^44a.(:„,,2,, 
301648 
^&o 
P i t 
i - a o 
-Dii. 
i 
^-VC. ;MC. . 20Z .«. ''ic.-.-ce > 
>*'.=--^e-.V,onroe.Ccn.ne^.„..,^^. 
301649 
CO 
o 
M 
a\ 
tn 
o 
U 
INDUSTRIAL 
CORROSiON 
MANAGEMEhTT 
INCORPORATED 
ti-.i HUM u kuica. lit al a M till n u t i«iui«iM 
HJOEP C c r i i / i t i i Drink ing Wdlur/Wdilcwdier 
Ldbordlory 10 ,?l'il 16 
CLIENT: 
EKVIHO SCIENCES. I HP.. 
SAMPLE DATE: 
7 / l / f l 5 
ICC (IIEKI.EX) 
PliOlECT 
SAMPLED BY: 
E n v i r o 
S c i e n c e s 
REPORT DATE:_ 
IAD g 
iiriZtl 
SAMPLE I D ; 
\}£t^r_ 
.Aiiljii.sr 
IS,19H5 
AT LAB DATE: 
7 / l l / f l 5 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CtlROHATOGBAPllY/HEADSPACE 
Compounds detected in parts per m i l l i o n (ml IIIgrams/klloQrams) 
dry weight 
basis 
I .2-DICIILOROPROPAHE -
CHLOROHETIIANE 
UnOMOMfTllANE 
VINYL CIILOHJDE -
CHLOROETIIAHE -
METHYLENE CHLORIDE 
r — 
ACETONE 
-
»,I-DICHLOROETHYLENE 
. l.l-DICHLOROETHANE ** 
I-I,2-DICHLOROETHYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER 
-
I,I,1-TRICHLOROETHANE 
CARBON TETRACHLORIDE 
• 
BROHODICHLOROMETHANE 
'"'Compounds co-elute (could be either material). 
LT-Lest Than 
dwb-Dry Weight Basis. 
GT"Creater Than 
X-Hot Detected 
^|C-l,3-0ICIII0K0PfinpfNE 
'|-I,3-0ICIIL0R0P«0PEN£ 
TCE (TRICIILOROETIIVLEME) 
^,I,I,2-TRICHL0R0£TIIANE___ 
'OIBROHOCHLOROHETIIAHE 
BEN2EHE 
01ISOPROPYL ETHER 
--
2-CIILOROETIiyLVINYL ETHER -
BROMOFORH 
-
1,1,2,2-TETRACHLOROETIIANE -
PCE ( TETRACHLOROETIIYLEHE)-
TOLUENE - 
- 
--
CHLOROBENZENE 
ETHYLBENZENE 
--
. . . . K 
X 
X 
i 
. 
. . X 
! 
X 
: 
X 
Jf 
i 
X 
; 
X 
Q^J 
X 
**Tetraliydrofuran t, Phosgene also elute at this 
point. Numerical results are caluclated for 
1,1-Dichloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 
mg/kg dwb. 
Jf 
Unknown peaks detected ( r e t e n t i o n time, estimated amount) 
niiinuroiiii otlier liyilrociirlioii pcukii, 0.02 to Q.l iii|;/k); 
^ v 
NOTE: Compound identification is based upon retention time 
matclies with specific known' standards. Confirmation 
of analysis using CC/MS is required to poslllvely 
INODSTHIAI. COHHOSIOH HGHT.. INC. 
Pflwiii TIclicnor, Vice PreiiileiK 
•- 
\ , 
'•• 
1 
! 
1 
1 
U) 
o 
H 
a\ 
tn 
H 
'•n 
INDUSTRIAL 
CORROSION 
MANAGEMEf/T 
INCORPORATED 
IDIKUII K lAaMkni M o i i U K I I I t i IOI 1114110 
I 
NJDEP C e r i i f i e d Drinking 
Uuicr/Wuitcwuicr 
Laboratory ID n h \ 1 6 
REPORT DATE: 
LAB I 
/.WS? 
Ain;ii.st 
l5.19flS 
CLIENT; 
ENVIRO SCIENCES, INC. - ICC (HEKI.EX) PIIO.IECT 
SAMPLE DATE: 
7/1/85 
SAMPLED BY: 
Enviro Sciences 
SAMPLE 10: 
Dryer 
VOLATILE ORGANICS BY PURGE ANO TRAP 
CAS CHROMATOGRAPHY / HEADSPACE 
AT LAB DATE; 
7/11/fl^ 
Compounds detected In parts per million (milligrams/kilograms) dry weight basis 
CHLOROMETHANE 
j, 
BROMOMETHANE 
* 
VINYL CHLORIDE 
x 
CHLOROETHANE 
x 
METHYLENE CHLORIDE 
7 
X 
ACETONE 
- 
2.0 
l.l-DICHLOROETHYLENE 
- 
X 
1,1-OICHLOROETHANE ** 
- 
X 
t-l,2-01CHLOfiOETHYLENE 
X 
CHLOROFORM 
X 
1,2-OICIILOROPROPAHE 
^,c-l,3-DICIIL0R0PnnPENE__. 
't-l,3-DICIILOR0PR0PEH£"" 
TCE (TRICHLOROETHYLENE) 
^, 1,1,2-TR I CIILORO£TilAHE_ 
'DIBROHOCHLOROMETHANE 
1,2-OICHLOROETHANE 
t-BUTYL METHYL ETHER 
^ 
1 .1,1-TRICHLOROETHANE 
CARBON TETRACHLORIDE 
BROMODICHLOROMETHANE 
• 
iiCompoundi c o - e l u t e (could be e i t h e r 
m a t e r i a l ) . 
LT-Less Than 
dwb-Dry Weight 
Basis. 
GT-Greater Than 
X-Not Detected 
BENZENE 
---
DIISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER -• 
BROMOFORM 
• 
1,1,2,2-TETfiACIILOROETHANE • 
PCE ( TETRACHLOROETHYLENE)-
TOLUENE -
CHLOHOUENZENE --
ETHYLBENZENE 
" 
- L ^ 
**Tetrahydrofuran i Phosgene also elute at this 
point. Numerical results a r c caluclated for 
1,1-Oichloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensllivity level of 
Unknown peaks detected (retention time, estimated amount )_j/L.j)L£_i5_|]n;/liii 
mg/kg dwb. 
NOTE: Compound Identification Is based upon, retention time 
matches with specific known standards. Confirmation 
of analysis using CC/MS is required to poslllvely 
f j f 
identify any material t n d / o r amount detected. 
niDIISlHIAl. COHHOSIOH MGMT.. INC. 
fdwiii Tichenor, Vice President 
^ 
iT;,-^"^ 
trfmomkic:a^X2STiC. 
1 • COf^UkHO P O , DtKVTUl. NCW jePSFT OTSU 
CHAIN OF CUSTODY RECORD 
tM'l. 
yH-
z^y^ 
ys-b 
•PS\ 
yy 
-
I n s t a l l a t i o n : 
Vdcl J / P ^ / y k 
S u r v e y 
N o . : 
u 
•—* °-
a 
• 
ra 
c 
VJ a 
S t a t i o n 
L o c a t i o n 
, 
—J L^^y'^-.-S, 
/<^^<'/---v-
• * ^ 
"V* 
' 
^ 4 
^ 
V4 
P t ^ e 
k r r 
r^ / 
'PZyyy^t.yy, 
" 
y 
Z 
y ^ 
' 
• 
- ^ 
' 
y y . y y ^ 
• 
A'-U<z-r:y^ 
R e l i n q u i s h e d 
b y : 
( S i g n . ) 
^A.yyyf-y 
R e l i n q u i s n e d j ^ y : 
( S i g n . ) 
R e i i n q u i a n e d 
b y : 
( i j i g n . ) 
R e l l n q u l a h e d 
b y : 
( S i g n . ) 
D i a p a t c h e d 
b y : 
( S i g n . ) 
D a t e / T i m * 
S a a p l e r s : 
( S i g n a t u r e ) 
C a t e 
T i a e 
i 
yyA^y 
y . - e c ^ ^ 
A/Z^ic<y 
/X^y 
'^Ju/y 
Ajkc-y 
'r 
<• 
* 
'r 
y r 
, 
-J-
y , t*/t.y 
y 
Sample 
Type! 
wOBp . 1 k j c a o 
— T t - ; 
u « 
c 
O n 
LJ 
• c 
o o 
^ 
/ 
X 
Y 
V 
yt 
> 
R e c e i v e d 
b y : 
( S i g n . ) 
R e c e i v e d / b y : 
( S i g n . ) 
R e c e i v e d 
b y : 
( S i g n . ) 
R e c ' d 
by 
L a b o r a t o r y 
f o r 
f i e l d 
a n a l y s i s 
| ( S i g n . ) 
1 R e c ' d 
f o r 
L a b o r a t o r y 
| b y : 
/ 
/ 
/ 
/ 
/ 
D a t e / T i a e 
'!>i!y r.-^ 
D a t e / T i a e 
r 
D a t e / T i a e 
D a t e / T i a e 
| 
D a t e / T i m e 
Method 
of 
S h l p ; n e n t : : 
y 
, / 
/ 
1 
, ^ k S r ^ : / P ^ ^ ^ ^ ' ' ^ ^ 
301652 
YORK LABORATORJI5 DIVISION 
CERTIFIED REPORT TRANSMIHAL 
R£.=CRT NUMBEf^ 
;C5:0-12S3 
DATS 
Sa--
. a - 
•?= 
I o s : 
CLIENT 
AHSNTiCN 
ir.vir=scianc=s, l:ic. 
19 Copelar.d Xcad 
Denville, JTJ 
0783i. 
Dr. A. Kvlas, 
Th.e ccove referencec r%ccrT is enclosed. Ccpies ci tnis reccrr end succcrcng CCTC 
will be rercjnec in ourSlftS in ine event ttiey cre rec'jirec fcrfurure reference. 
If there cre cny quesT;of« ccnceming this repcn, pf'ecse Co nor hesitate to conTCcrus. 
Any samples submirteci ?c our Lcbcrctcr/ will be retcined fcr c rr.cximum cf sixr/ .;*Q) 
ccys from receipt of thu reccrr, unless other cn-cngerrienrs cre Pesirec. 
Ncturctly. cs in fhe pcst our srcff will be pleased tc cucte cn cny futu-e recuirerr.er.ts 
ycu may hcve. In ccc.licn to the service provicec we else offer the following: 
. Hc:c.-ccus Wcste Analyses 
• Product SvcluctiorvR&D 
• Water cr.d Wastewater Ana ly ses 
• Air cnQ Process Gas Anciyses 
• Industry! Hygiene Surveys 
-• Merclhjrgtcal Analyses 
• Mic-obiclcgiccI Analyses 
• Mess Screctrcmetry Services 
Vec^y Truly Youri 
RoceffQ.Brcaley 
/ 
Vice President 
' 
r.vc. :.NC. • : : : ;.ic.-.rc2 r<,^^:.;3 • ••vic.--=8. ccrr.ec-z-^: • ^ i ^ i • •;::;•; z=-\ 
301653 
Secteraber 25, 1985 
30850-1233 
ENVIROSCrSNCES, INC. 
19 Ccceland Road 
De.nvllle, New Jersev 
07334 
At:te.-.ricn: Dr.-A. Kyi*s 
PUH2CSE AND R ; S " L T S 
Si.-c (o) scil sa.Ticlss were submitt^ed tc York Labcra-cries fcr 
analysis. Tbe sampi^S were cracared ar.d analvzed in acccrda.-.ce 
T.he results ara repQ^-l^c i.-i the follcvi.-c Tables. 
Pracared by: 
-,...li- ^ ^ L - ^ 
Daniel ?\ 
o t t 
Laboratory Mar.aaer 
3^£rcey C, Curran 
DFC/JCC/md 
•mc. :.Mc. • : : ' Mc.-a*i« ru.T.=::^e-;vicnrca.conrect:=utC6'i45 -vz:;; :;t-
301654 
TABLE 1 
^ ^ 
30850-1283 
^ ^ ^ ^ S l ^ - I l e n t a i c ^ t i c T ^ 
5434 - . , , , , , 
, ^ , ^ ^ ^ 
l 2 i H e n e . . _ u c ^ 
5435 - c r y e r , 
7 / 1 / 8 5 
920 
V^.VC.'.VC.ZCaMc.-ro^^-^ 
, 
CUtO<i^S.(3n,;-.,.^l^, 
301655 
TABLE 2 
30850-1233 
E^VIROSCIENCHS, T^C^ 
Sa-nriple 
I c e r . t l ' i c a t i c n 
5436 - Lab ? i t , 
* 1 , 7 / 1 / 8 5 
5437 - Lab P i t , 
# 2 , 
7 / 1 / 8 5 
5433 - Lab P i t , 
* 3 , 
7 / 1 / 8 5 
5439 - Lab P i t , 
# 4 , 
7 / 1 / 8 5 
?yrici.-.e> 
ue/:<c 
1 ,100 
3,400 
<150 
<150 
"Ave, INC. • 2CC .Mcrs<» niT-.piKS- Mcnrce. Cannecttcur06^*3 ••;2:21 :*-!~ii£5 
301656 
t. : 
I' 
i ? 
-J 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
iiilMuii lo.iUMoarH.wwjiiiSiroiii xnsimiKi 
IIJIlLI' C u l t i l i c i l 
U i i n k i i i y W d l L i V W j b l c W a l Ul 
L < i l i U i a l u i y 
ID l l \ ' i \ 16 
REPORT OATE: 
l-AO * 
Vifi/Q 
Aiiniisr 
I 5 , j 9 n 5 
CLIEHT; KNVIHO SClKNCi:.';, INC. 
SAMPLE DATE; 
7/I7/»S 
\cc (iii:i<i.i:x) piio.ii'CT 
SAMPLED BY: 
Liiv/ro Scicncco 
SAMPLE ID: 
Orynr. 
AT LAB DATE: 
7/25/(15 
VOLATILE ORGANICS BY PURGE AMD TRAP 
GAS CHROMATOGRAPHY / HEADSPACE 
Compounds detected In parts per mill Ion (milligrams/kilograms) dry weight basis 
CIILOROHETIIANE 
BROMOMETHANE 
VINYL 
CHLORIDE 
- 
-
CIILOROETIIAHE 
METHYLENE CHLORIDE 
-
ACETONE 
I,1-DICHLOROETHYLENE 
I,I-DICHLOROETHANE ** 
-
t-I,2-OICHLOROETHYLENE 
JL 
X 
AA.. 
Z& 
1,2-OICIILOROPROPAHE 
X_ 
^,c-l,3-DICIIL0R0PR0PEHE 
' t - l ,3-DICIILOROPROPEME 
" 
— 
TCE (TRICIMOROETIIYLEHE) 
X_ 
^,1,1,2-TRICHLOROETHANE 
'OIBROMOCIILOROHETIIAHE 
— 
CHLOROFORM 
1,2-DICIILOROETHANE 
t-BUTYL METHYL ETHER 
-
1,1,1-TBICHLOROETIIANE 
CARBON TETRACHLORIDE 
- 
• 
BROMODICHLOROMETHANE 
• 
'''Compounds co-elute (could be either material). 
LT-Less Than 
dwb-Dry Weight Basis. 
GT-Greater Than 
X-Not Detected 
BENZENE 
--
DIISOPROPYL ETHER 
2-CIILOROETHYLVINYL 
ETHER -
BROMOFORM 
• 
1,1,2,2-TETRACIILOROETIIAHE • 
PCE ( TETRACHLOROETHYLENE)-
TOLUENE 
CHLORODENZEHE 
-
ETHYLBENZENE 
0.07 
0.36 
**Tetraliydrofuran & Phosgene also elute at this 
point. Numerical results are caluclated for 
1,1-Oichloroelhane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 
mg/l<g dwb. 
J^ 
Unknown peaks detected (retention time, estimated amount) niiinerniifi olilmr liytlrocarlion peaks 0.01 to 1 mp/k^ 
NOTE: Compound Identification Is based upon retention time 
matches with specific known standards. Confirmation 
of analysis using GC/MS Is required to positively 
CT/ 
identify any material ind/or amount detected. 
INDUSTRIAL CORROS|ONi HGHT., INC. 
yky 
o> ,w^ 
XJHtJOSTX. 
CaAI3 OF CUSIODY a2CQ2D 
ittssmyx aa.ooaamsi.tKm jBimrr Qtxtn 
I n a c a l l a t : -°°*- 2rk(L 
: ^ ^ 
Surv«7 H o . : 
Samplara: 
( 3 i j n a t u r « ) 
a 
U3 
Station Location 
/ 
Data 
Tiaa 
j 
2" 
Saapla Typa 
« 
(.osp. 
v>rao 
o « 
• e 
a o 
^(i<6?f 
y !/S<yCyZ k Ag pyyy. 
y'S^^ / y P .^^f>Ka/.c J 
A^p^yyyy^) 
/<£>/»rf 
y 
^ 
z< 
/ 
y/ 
/., / yCyyrP^fii,) 
o 
^ 
/ 
-r 
/ZPy//e/ry Aal^cy/S^/S •7^p<Z} 
// 
y/ 
><. 
^ 
y^ycyyi 
'y^ 
Aikaodz. 
Syy^ycy:^ yLoti,^ .^y y./y^ /ry.^/rs.y^/— 
yyar" /=r,f£yy*jo ^y^ryc yf/^-r^/i... rvyvyejy 
yy^.a <g^yy/et£ji. Z^tej^y^py^^ y9y7icuys~ 
RFiiaqui3h.e<i by: 
( S i j a . ) 
Rayiicquished 
by: 
(Sign^/) 
R a x i n q u i a n a a 
by: 
( 2 1 g 3 . ) 
Racalvad by: 
( S i g n . ) 
Aecaivad by: (jSlgn. ) 
D a t a / X i a * 
D a c a / T i a a 
jlecalvaa by: ( S i g n . ) 
O a t a / I i s a 
Raiiaqulshad by: (Sign.) 
Rac'd by Laboratory 
for fiald analyaia 
(Sign.) 
D a t a / T i a a 
Dispacciiad b y : 
( S i g n . ) 
Data/Tiaa Rac'd for Laboratory 
by: 
Data/Tia« 
Method of Shipaent: ckkyL/yA!!/ p2Py /k^/^Azk' 
301658 
INDUS,rllAL 
CORROSiON 
MANAGEMENT 
INCORPORATED 
NJC£.= C = . Cifisd Orinkl.ig -.Vare.-V" 
Wastewater Laboratory ID .^lljlo 
.: 6 -
REPORT 0A7E:_ 
LA a .^ 
^"^18 
••August: 
15,1985 
1152 aOUIE 10. .PANCCLrH. NC.V JE.^Srf 07863 :Q1-5E4-:320 
CLIENT: 
Z:rr?.0 SCIHNCZS. IVC, 
SA.MPLE SOURCE: 
ICC r B E ? X r n 
^-'-'-•'-Cl 
SA.V?LI ID: 
St.C.rni-r. 
SAMPLE DATE: - « H « I O W » - 
SAMPLED BY: 
Al K v l e s 
.AT LAB DA-r: 
7/22/85 
WA: 
PRIORITY POLLUTANT VOLATILE ORGANICS 
bv 
GC/HS 
Pa rane!:er 
acrolein* 
a c r y l o n i t r i l e ^ 
benzene 
brcrr.oform 
carbon t e t r s c h l o r i d e 
chlorobenzene 
ch 1 orod ibrcr.cmechane 
chlorethane • 
2-chloroethy1Vinyl 
e t h e r -
chloroform 
di ch lorcbrcp.cr^ethane 
1 , 1-dichloroethane 
1 , 2 - d i c h l o r o e t h a n e 
I , 1-d Ichloroethylene 
Result 
X 
O.Oi 
Parameter 
I,2-dichiorcpropane 
I,3-dichloropropy1ene 
ethylbenzene 
methyl brcrr.ide 
methyl chloride 
methylene chloride 
1,1 ,2 , 2-tetrachloroethane -
tetrachlcrcechyIene 
toluene 
1 , 2 - t r a n s - d i c h l o r o e t h y l e n e 
I , 1 , 1 - t r i c h l o r o e t h a n e 
1 , I , 2 - t r i c h l o r o e t h a n e 
tricTiloroethy lene — 
vinyl chloride 
Resulcs reporced in mg/l (ppm). Dececcion liaic 0.001 ag/1 (ppm), 
*Dececcion Llnit: 0.1 ag/l 
Rssult 
E T / j m g 
INDUSTRIAL CORROSION 
MGMT.,INC, 
Edwin 
T i c h e n o r 
V i c e 
P r e s i d e n t 
LT=Less Than 
• •X'^m: Dececced 
301659 
m 
. iiNuuoi...iAL 
CORROSiON 
MANAGEMENT 
INCORPORATED 
Laooratory 10 
,116 
REPORT OATE: 
Augusc Ij.igS 
tv" 
LAB i . 
4i41S 
1152 SOUTH 10. S>NCOL?H. HtH JERSO 07863 201 534.0330 
CLIEHT: 
-^r-r-'n ^r'^^vr^';. ivc. 
SAMPLE -SSL'SC;: 
ICCf 3E?J.-:t') 
St. Croi-t 
SAMPLE DATE: ••rV-"-- 
SAMPLED BY: 
Al Kvles 
AT LAB OATEu 
yyy^t^ty.^r'yy 
WATER 
PESTICIDE S PCS EXTRACTABLES 
PRIORITY POLLUTANTS 
bv GC/MS 
Parameter 
Result 
Aldrin 
LT 0.01 
a-3HC 
- 
— — LT 0.01 
b-3HC 
LT 0.01 
d-3HC 
t l 0.01 
g-3HC 
LT 0.01 
Chlordane 
LT 0.02 
!•,«•'-000 
— 
LT 0.01 
i4,t»' -DDE 
LT 0.01 
'«,'«'-DOT 
- 
- 
LT 0.01 
Dieldrin 
. 
LT 0.01 
Endosulfan 
I 
LT 0.01 
Endosulfan II 
. 
LT 0.01 
Endosulfan Sulfate 
LT 0.01 
Endrin 
LT 0.01 
Endrin Aldehyde 
'• 
LT 0.01 
Heptachlor 
• 
LT 0.01 
Heptachlor Epoxide 
LT 0.01 
Toxaphene 
; 
LT 0.02 
PC3-I016 
— 
— 
- 
LT 0.01 
PC3-1221 
LT 0.01 
PC3-1 232 
LT 0.01 
PC3-12'»2 
LT 0.01 
PC3-1248 
LT 0.01 
PCS-US'* 
— 
LT 0.01 
PC3-1 260 
r 
- LT 0.01 
All 
r e s u l t s reported In mg/l (ppm). 
INDUSjaiAL 
CJliiOSI, 
Edv< in T i c h e n o r 
ET/jmg 
V i c e 
P r e s i d e n t 
LT=Le s s 
t h a n 
X=»Not 
d e t e c t e d 
7/22/85 
, INC, 
301660 
u> 
o 
INDUSTRIAL 
CORROSION 
UANAGEMENT 
INCORPORATEO 
ii>2*0Kifit.kutcoini.MmMuiinui 
M I M I O M 
HJULI' C c r t l l l c d Ul iiikliiij 
Wuicr/Ud^tcwjtcr 
Laboratory ID I l ' i l l 6 
fiEPDRT OATE: 
Aii)!iiiit 
15,1905 
LAB H 
A A } 3 
CLIENT: 
KNVIRO .SCIKNni'.S, I N C . , 
SAMPLE SOURCE^ 
SAMPLE DATE; Jinluuiuiv» 
ICO (ui:iii.i:x) |'KO.II;CT 
SAHI'I.K II): ST. <:ro(K 
SAMPLED BV; 
y^JZ'cyy^Jlr^ 
Al Kylea 
AT LAB DATE: 
l l l l l ^ ^ 
BASE/NEUTRAL 
Parameter 
• Result 
acenaphthene 
X 
acenaphthylene 
X 
anthracene 
X 
benzidine 
X 
benzo(a)anthracene 
X 
benzo(a)pyrene 
X 
J . ' i - b e n z o n u o r a n t h e n e 
X 
benzo(ghl)perylene 
; 
X 
benzo(k)fluoranthene 
X 
b I s (2-chloroethoxy)methane 
X 
bls(2-chloroethyl)ether 
- 
X 
b l s ( 2 - c h l o r o l s o p r o p y l )etlier 
X 
bis(2-eihylhexyl)phthalate 
X 
^-broniophenyl phenyl ether 
X 
butylbenzyl phthalate 
X 
2-chloronaphthalene 
X 
'i-chlorophenyl phenyl ether 
X 
chrysene 
X 
dlbenzo(a,h)anthracene 
X 
1,2-dlchlorobenzene 
X 
1,3-dlchlorobenzene 
X 
I ,'i-dlchlorobenzene 
X 
3 , 3 - d l c h l o r o b e n z l d l n e 
X 
None nf tliu uliovu I ' r l o r l l y I'ol liiliiiit u ilutuctuil 
**Otlier compound!! see Aiiiieiuliini I 
LT"Less Than 
EXTRACTABLES PRIORITY POLLUTANTS 
bv GC/MS 
Parameter 
diethyl phthalate 
-
i l l m d i i y l 
pill II.I I •Itu -
dl-n-butyl phthalate — : 
2,'i-dlni trotoluene 
- 
--
2,6-dIni trotoluene 
di-n-octyl phthalate 
I,2-diphenylhydrazine (as azobenzene) 
fluoranthene 
fluorene 
hexachlorobenzene 
hexachlorobutadiene 
hexachlorocyclopentadiene 
hcxachloroeiliane 
indeno(1,2,3-cd)pyrcne 
Isophorone 
naphthalene 
n i trobenzene 
N-nltrosodlmethy I amine 
N-nlt rosodI-n-propylamine --• 
N-nltrosodiphenyI amIne 
phenanthrene 
pyrene 
"-
I ,2,11-1 rich lorobenzene 
lit 11 ijuiiul C IV I ly level of 0.(11 inf,/I (|i|iiii) 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
Result 
X 
F/)i.i in T i r hcnr^r 
:^i'i 
^fJDE? Carcified Drlzxing Vacar/ 
Wascewacer Laboracory ID v l i l l a 
REPORT DATZ: August 15.1985 
LAS 'i i'iiia 
a.i£>rr: 
ET.IRO SCIINCZS, I:^C. 
SAMPLE SOLUCE: 
SAJ^LE DATE: 
ICC (Berlex) 
SAXPLZ ID: 
Sc. Croi-x 
SA^CLZD 3Y: 
Al. Kvles 
.AT L.A3 DATZ: 
7/22/S5 
y 9 j Z * y y f / j — 
BASZ/NELTRAL ZXTRACTA3LZS PRIORirf PGLL'uTA-NTS 
ADDE>roL^. I 
0~-:Z7. COMPOUNDS DETZCTZD 
by GC/MS 
?3ra=ecer 
becxaldehyde 
chlcronechyl benzene 
benzene mechanol 
phenyl acecace 
diphenyl mechane 
Resulc 
3. 
0 
24 
26 
0 
0 
0 
3 
0 
0 
u. 
.4 
l-l'-ioxybis(mechylene]bts benzene 
All resulcs are reporced ia mg/l (ppm). 
We chank you for chis opporcunicy co serve you. If you have any quescions, 
please do noc hesicace co call. 
INDUSTRIAL CORROSION M.ANAGZMZNT, INC. 
ZT/jmg 
end. 
LT=Lass Than 
Edwin TicSenor 
Vice Presidenc 
301662 
r g . 
ic 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJOE? Certified Drinking Water/ 
Wastewater Laborator/ 
ID j i U l l o 
REPORT 0ATE:__Aji23i^ 
1152 ROUIE 10. SAXOOU'M. .Sfi* IIRSVI 07869 
201Si4-0130 
LAB .¥ 
4Adl8_ 
CLIE.NT: 
ENVIRO SCIZNCZS. INC. 
SAMPLE SCURCE 
ICC (3ZRLZZ) PROJZCT 
ST. Crol.T 
SAMPLE DATE: 
<-..'>...--TT 
SAMPLED BY: Al Kvles 
yPJ^ycyrpy/ 
ACID EXTRACTABLES 
PRIORITY POLLUTANTS bv GC/MS 
AT U B DATE :__:_JLillli5_ 
WATER 
Parameter 
2-chlorcphenol 
2-n i t rcche-iol • 
Resulc 
pnenol 
2,'»-dir>ethyl phenol 
2,4-dichlorophenol 
2, l* ,6-tr ichlorophenol 7--
pentachlorophenol 
2,'•-dini trophenol 
i*,6-dini t r o - o - c r e s o l 
i(-n i trophenol 
A-chloro-3 methy! phenol 
None of che above Prioricy Pollucancs dececced ac a sensicivicy level of 0.01 mg/l (>• 
OTHER PEJLKS DETECTED: benzoic acid (? 3 ag/l 
ET:jmg 
lT=»Less Than 
"X=»Not Detected 
NOUSTRIAL CORROSION M G M T . , INC 
Edwin Tichenor 
Vice President 
301663 
L-e 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
lis; ROUIt 10. BANCClPM. Nt)» JtflStr OJiifiJ 
?01iJ4QlVI 
CLIEKT: 
Z:r'7IR0 SCIZNCZS INC. 
NJO£? C - j r t i f i e d 
Oriniiing 
Water 
U j s i e w a t e r 
L a b o r a t o r y 
10 j ' l A l I S 
REPORT OATE: 
i , . „ . « - 
T •= 
l o a c 
' " • • 11 'w 
. .. 1 ^ y - -r 
LAB / 44418 
SAMPLE S C U R C E L 
SAMPLE DATE: 
ICC (3ZRLZX) PROJECT 
SAMgt-Z ID: Se. Croix 
riffsss:;:^ SAMPLED B Y : ^J- ^v^gg 
ypy^^y^rr 
,Pt'X LAB DATE.-
7/22/35 
PRIORITY 
POLLUTANTS 
WATER SAMPLE 
TOXIC POLLUTANTS: 
Metals, Cyanide and Total Phenols 
PARAMETER 
Tocal Anci.Ticny -
Total Arsenic --
Tota1 Bery11ium 
Total Cadmium --
Total Chromium • 
Total Copper 
Total Lead 
:-• 
Total Mercury --
Total Nicitel 
— 
Total Selenium 
Tota1 SIIver --
Total Thai Iium 
Total Zinc 
Total Cyanide 
Total Phenol -
RESULT 
r T 
LT 
LT 
TT 
0, 
ft. 
^
• 
0 
0 
0 
q 
n 
n 
n 
n 
n 
4 
0 
0 
v.i 
005 
013 
003 
027 
n s 
on 
nm 
0*^0 
OITi 
nos 
O^q 
fi'i 
.053 
•1$! 
All results are reported in ag/i (ppm). 
Ue thank you for this opportunity to serve you. 
If you have any questions, please 
do not hesitate to call. 
Very truly yours, 
INDUSTRIAL CORROSION MGMT.,INC. 
£T/jmq 
LT'Less Than 
X=Not Detected 
J.^ 
Edwin Tichenor 
Vice President 
301664 
C f 
trv»oMxaex3srKm 
CHAia OF CUSTODY RSCOID 
11 coti-fcxa ao. oonnxL K » j w i cm* 
I n a t a l l a t i o n : 
7~y*y 
Surv«7 Ho,: 
S*«pl«r«: (3ljn«tur«) 
k^^yk'yp^y^ 
l-l 
Scatlon Locatioa 
Data 
Tla« 
S a a p l * T7p« 
^ o a p . -Ajca o 
o « 
o o 
I 
I 
I 
I 
<A/^ 
ypyyyyyy y^-yyyyrr^yj -r 9^0 
Xyp/ekcy/kyyo 
k. \y 
yiy^^^ yZy^ A^k^ 
A 
R e l i n q u i s h e d b y : ( S i g n , ) 
Received by: ( S l j a . ) 
I D a t « / T i a « 
. l e i l n q u i s n e a b y : ( S i « n . ) T" 
R e l l n q u i a n e a by: ( S i g n . ) 
XZZI^.L.^J, 
7./? i" 
_•>•(<-
RecBlvea by: J S i g n , ) D a c e / T i a e 
Relinquiahad by: (Sign,) 
Recelvea by: (Sign.) Date/Tiae 
Rec'd by Laboratory 
for field analysis 
(Sign.) 
D a t e / T i a e 
D i a p a t c h e d b y : ( S i g n , ) 
D a t e / T i a e Rec'd for L a b o r a t o r y 
i D a t e / T i a e 
by: 
r 
-Method of S h i p m e n t : 
^ 
. 
. yP<y • ckyci^.^^ 
'/^^y 
301665 
..ii:2^:i^-jiy:.Z^?i'^-r'a^'Ti.-%i 
to 
o 
bil 
LU 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
llimOUK 10. KlNOCiPllHfWJEIISK 0)111 lOIMIOlM 
II.)DI:P C o r i i f i u i l DiiiiKJiKj l/al er/V/ds lewaier 
Laboriiiory 
ID ; I 'il 16 
REPORT DATE: 
^i;i!LL'!!!L'!;l_L2JOQl. 
I-AI) ; 
/.VlfiZ 
CLIENT: 
l-NVTKO SOTF.NCI- - ICC lll'HI.KX I'liaiKCT 
SAMPLE DATE: 
August 7, 1985 
SAMPLED BY: 
K i w i r o 
SCUMICH 
SAMI'I r ID: 
i.,ii, I'll 
ri'lf.S 
AT IAD DATE: 
Aii);ii.sr 9. I'IflS 
CHLOROMETHANE 
BROMOMETHANE 
VINYLCHI.ORIDE i 
CHLOROETHANE ---
HETHYLENE CHLORIDE ---
ACETONE 
I, I-DICHLOROETHYLENE -
1,1-DICHLOROETHANE ** 
t-l,2-DICIIL0R0ETHYLENE 
CHLOROFORM 
1,2-DICIILOROETIIANE 
t-BUTYL METHYL ETHER -
I,1,1-TRICHLOROETHANE • 
CARBON TETRACHLORIDE -• 
BROMODICHLOROMETHANE -• 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CHROMATOGKAPHY/ HEADSPACE 
Compounds detected In parts per million (mi I 11 grams/k i logrdiiis) dry weight basis 
^ - - - 
X 
0.32 
1,2-DICIU-OROPROPANE 
c-1 ,3-DICIIIOROPROPFIIE 
t - l ,3-DICIIIOHOI'KOI'rHi;'"' 
TCE (TRICIILOROETIIYLCIIE) 
1,1 ,2-TRICIILOROETIIAIIE 
0.02 
0.02 
'DIBROMOCHLOROMETHANE 
BENZENE 
DIISOPROPYL ETHER --
2-CIILOROETIIYLVINYL ETHER -
BROMOFORM 
1,1 ,2.2-TETRACIILOROETIIANE -
f>CE ( TETRACIILOROETIIYI.ENE)-
TOLUENE 
- - -
CIILOROIIENZrilE 
ETIIYLDENZEIJt 
-
X 
X 
X 
X 
X 
JA 
X 
X 
X 
n. 
X 
0. 
M 
ni 
"Compounds c o - e l u t e 
( c o u l d be e i t h e r 
m a t e r i a l ) . 
LT=Less Than 
dwb=Dry Weight 
Basis. 
GT=Greater Than 
X=Not 
Detected 
••'••^Tel rahydrofiiran C Phosgene also e l u t e at 
t h i s 
p o i n t . 
Numerical 
r e s u l t s are c a l u c l a t e d 
for 
1,1-Dichloroethane 
o n l y . 
For the above l i s t e d V o l a t i l e P o l l u t a n t s , nothing detected at a s e n s i t i v i t y 
level of 
0,01 
mg/kg dwb. 
j { 
Unknown peaks detected ( r e t e n t i o n time, estimated amount) 
Xylem.'s .iiipriix.O^Ofj nm/kiidwb 
NOTE: Compound I d e n t i f i c a t i o n 
Is based upon r e t e n t i o n 
lime 
matches w i t h s p e c i f i c known standards. Confi unaiion 
of a n a l y s i s u s i n g GC/MS is required to ( l o s i l i v e l y 
i d e n t i f y any m a t e r i a l 
anil/cir ainnunt 
detected. 
INI)|I;;TI!I/\I. COKKOSION HANAOI-MKNT, INC. 
izi^j/(fpL-^.c 
'l. i c l l . l 1 .1 
. / I.U'V i'liI: /I'l'l.'S i I I L M I 
£ 
U) 
o 
M 
;fe'i'i 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
JNCORPORATED 
I I S K I k l K i j M'CHOIKPIi.linkJIIISEt 01161 
20ISK41JU 
CLIENT: 
NJDEP Cell i i i n l Diiiil.iiiy V/aier/V/as I ev;u l e r 
l.abcir.iioiy 
ID ; 1 'il 16 
REPORT DATE: 
Si'pfiMnlu-r 
I2.19fl5 
LAB .f 
''i')l(il 
FN'yiRo scrnNCK - ^r.c. m-m.Kx I'ltn.ir.cr 
SAMPLE DATE: Aiipust 7. ]9fl5 
SAMPLED BY: 
F.nviro Science 
SAMPLE ID: l.,i|, l>(l: //V.)fi6 
AT I.AII OATE: 
August 9. 10R5 
CHLOROMETHANE 
BROMOMETHANE 
VINYL CHLORIDE -
CHLOROETHANE 
HETHYLENE CHLORIDE ---
ACETONE 
---
1,1-DICHLOROETHYLENE -
I ,1-DICHLOROETHANE ** 
t-l,2-0ICIIL0R0ETHYLENE 
CHLOROFORH 
I,2-DICHLOROETHANE ---
t-BUTYL METHYL ETHER -
I ,1,1-TRICIILOROETIIANE 
CARBON TETRACHLORIDE -• 
BROHOD ICIILOROMETHAIIE -• 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CHROMATOGRAPHY/ HEADSPACE 
Compounds detected In parts per million (milligrams/kilograms) dry weight basis 
X 
0,27 
I ,.2-Oirill.OROPROPANE ---
...c-i ,3-niciii.nROPRnPENE 
' • ' l - l ,3-DICIII.0U0n(0l'CIIE'" 
TCE 
(TRICIILOROETIIYLENE) 
,,I,I.2-TRICHLOROETHANE 
••'DIBROMOCHLOROMETHANE 
0,02 
0.01 
BENZENE 
DIISOPROPYL ETHER 
2-CIILOROETIIYLVINYL ETHER -
BROMOFORM 
l.l,2,2-TETRACIIL0R0ETIIANE • 
PCE ( TETRACIILOROETIIYI.ENE)-
TOLUENE 
CHLOROIlENZriin - -
ETIIYI.DENZENE 
J.t2L 
X 
"Compounds co-elute (could be either material), 
LT=Less Than 
dwb=Dry Weight Basis. 
GT-Greater Than 
X=Not Detected 
•"•"Tet rahyilrofuran t Phosgene also elute at this 
point. 
Numerical results are caluclated for 
1,1-Dichloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 
Unknown peaks detected (retention time, estimated amount) 
nig/kg dwb. 
NOTE: Compound Identification is based upon retention time 
matches with specific known standards. Confirniation 
of analysis using CC/MS is required to positively 
identify any material and/or ainnunt deiecied. 
iN'DiisriiiAi. f:oi(i(n.';TON HANAGLMLNT, 
kdy. 
INC. 
: i \ l i . : 
• ' • / •'' l . i V i l u : / I ' l L';; i I I L M I 
A 
O 
H 
00 
M 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
IKlbdRPORATED 
ii&iiuxnt io.*>iipo^hi.iri<tJifisi(bfit9 201 ii4<i])a 
NJDEP C e n i f lull niiiil.iiiy \/aier/Was tewaier 
Lahoralory 
ID / I ' l l 16 
REPORT nATE:__Soi.re!!!!.er_Lia9fli. 
LAB H 
/iVIfi/, 
C L I E N T : 
Kt^yiRO .SCTI'NCE - TCC HFKI.KX 
I'HO.II'CT 
SAMPLE DATE: 
Aupiist 7. 1985 
SAMPLED BY: 
Elnvlro Science 
SAMPI r ID: 
l.iili I'It //S')67 
AT LAB DATE: 
Aiii'iuit 9. 10(15 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CHROMATOGRAPHY/ HEADSPACE 
Compounds detected In parts per million (milligrams/kilograms) dry weight basis 
CHLOROMETHANE 
X 
EROMOHETHANE 
7 
VINYL CHLORIDE -r 
CHLOROETHANE ---- 
• 
METHYLENE CHLORIDE 
ACETONE 
1,1-DICHLOROETHYLENE --
1,1-DICHLOROETHANE * * -
t-l.2-0ICIILOfi0ETIIYLENE 
CHLOROFORH 
1,2-DICIILOROETHANE 
t-BUTVL METHYL ETHER - -
I,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE - -
BROMODICHLOROMETHANE - -
0.23 
0,03 
O . l l 
I ,2-DICIILOROPROPAIJE -
,.,c-l ,3-DICIII.ORnPROPfllE 
" ' t - l ,3-DICIILtW<OPROI'CIIE 
TCE (TRICIILOROETIIYLENE) 
- -
, , 1,1,2-TRICHLOROETHANE 
•'oiBROMOCHLOfiOMETIIANE 
BENZENE 
DIISOPROPYL ETHER 
2-CIILOROETIIYLVINYL ETHER -• 
BROMOFORM 
I ,1 ,2,2-TETRACIILOROETIIANE -
P'CE ( TETRACHLOROETHYLENE)-
TOLUENE 
CIILORODENZCNE 
ETHYLBENZENE 
0.01 
0^05 
"x" 
0.0/| 
^Compounds co-elute (could be either material). 
LT=Less Than 
dwb=Dry Weight Basis. 
GT=Greater Than 
X=Not Detected 
-•"Tetrahydrofuran C Phosgene also elute at this 
point. 
Numerical results are caluclated for 
1,1-Dichloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 
o.OI 
X 
Unknown peaks detected (retention time, estimaled amount) 
Xylene —O.IIL' m^/ki; (Iwlj 
mg/kg dwb. 
NOTE: Compound I d e n t i f i c a t i o n 
is based upon r e t e n t i o n 
time 
matches w i t h s p e c i f i c 
known standards. 
Confirmation 
of a n a l y s i s u s i n g GC/MS is required to 
( l o s i i i v e l y 
i d e n t i f y any m a t e r i a l 
anil/or amtiiint d e l e c t e d . 
INDIISTIilAI. COkllOSIOH MANAGKHKNT, i NC. 
ziz.y^/./tX^ 
'A.\7^-r-.r^. 
'i: i Vli,' I .1 ! i . / I.ev' iiii. / I ' r i . ! ; i i l u i i l 
• 
y .V 
9tfJ9omxsexssnc 
CaAI3 0? CUSTODY RSCORD 
J^V 
<.'~4 H 5 
11 c=m»« MO-oeMvxL >«• xnerr r m 
I n . t a l l a t i o n : 
y ^ ^ 
k ^ . y ^ y 
Survey H o . : 
* 
m ^ 
i 
• 
' 
<• 
C 
S t a t i o n 
L o c a t i o n 
Samplers: ( S i g n a t u r e ) 
i 
y^yyyy 
\ 
Data 
u 1 
1 
Tiae 
Saaple 
TypJ 
- o a p . -vjcao 
^m 
f . 
O 
« 
_o _o 
Zz^y^d^ kyP^^^^) 
\ -Ay^^k^ya.-^ \ 
1 V 
1 / 1 
-.^3i Ps.y'S/ZklA^^ZZZZ^ikLitiy^ 
• 
\ 
-t.o--i S-i 1 • yy^ryy/Z kZTZyyiyyZey^ 
-. z 
"<l 
y A 
i n q u i s h e d 
by: 
( S i « a . ) 
\ 
k 
\\. 0 
-ix..y^J^. i^yy.^^.^ 
// 
z7:^^J\ 
\ y 
^ 
^v^^l 
1 \ 
\y-
• 
.Received by: ( S i g n . ) 
i D a t e / T i a « 
]C^. r 
. l , ^ ^ ^ r ^ 
] 
^-/a^tfi 
i n q u i s h e a 
by: 
( S i g n , ) I 
/ 
K e l i n q u i a n a a 
Uy: 
( S i g n . ) 
R e l i n q u i s h e d 
b y : 
( S i g n . ) 
D i a p a t c h e d b y : 
( S i g n , ) 
Recelvea b y : y ( S i g n , ) i D a t e / X i a e 
j 
RecBiveo by: 
( S i g n , ) 
jRec'd by L a b o r a t o r y 
f o r f i e l d 
a n a l y s i s 
( S i g n . ) 
D a t e / T i a e Rec'd for 
L a b o r a t o r y 
by: 
D a t e / T i a e 
i 
D a t e / T i a e 
1 
P a t e / T l a e 
i 
1 
1 
• 
1 
iMethod of 
S h i p a e n t : 
^ 
-^ 
301669 
YCRX LAJ30RATORIE5 DlVISiON 
y.',7/. 
CE.^TlFiED REPORT TRANSMITTAL 
RE=CRT NUMBER. 
•G85C-l3i3 
DATr 
Se::5=ber 2 5 . 1955 
CLIE.NT 
Hr.vircscissiias, Inc. 
19 Copeland. 5.Qad 
Denville, >t-,J 07834 
ATTiNuCN 
J:yle3 
The ccove referencaC 'reccrr is enc!ose<3. Copies cf ttnis reccrr cne succcrrtng cc:c 
will be rercinec in cuxfiles in me event iriey cre recuirec ter rurure reference. 
If mere cre cny quesicns ccnceming fhis reccn, p.e<zzQ Co ncf hesifcrs fo ccnrco: La. 
Any scmples submirttC to cur Lcccrcrcry will Ce retcineo fcr c rr.cxin',um cf sixr/ [60] 
ccys frcm receipt cf TUS rfepcrr, unless ottier crrcngemenis cre Cesirec. 
Ncujrclly, cs in trie pes;, oxj stcfl will be piecsec tc cucte cn cny tutue recuirerr.er.ts 
ycu mcy hcve In cccittcn TO itie service provicec we ciso offer tne Icllcwinc: 
• Hczcrccus Wcste Anciyses 
• PrccL!tttEvcluction/Rai.D 
• VVcr^ crK2 Wcstewcter Anciyses 
• Air QftC.^rccess Gcs Anciyses 
• • incvaSTict Hygiene Sun/eys 
• MeicjturgiccI Analyses 
• Micratioicgiccl Anciyses 
• MG5$ ScecrcmeiTV Services 
Very Toily Yc 
PUi{ 
i?cbertcarcCley 
Vice PresiCenr f 
TUC. IMC. • 2CC .Mc.-,-^^ KiT.c:xe• .Vic.-.rce. Ccrnec-curCii^o • ; - ; 3 ; Z~'.—^l 
301670 
Septie.T.cer 25, 1985 
30850-1342 
E^^/rHcscIEMcrs, INC. 
19 Ccceland Head 
Cenvllig, Nev Jersev 
07334 
At:ta.':{:i.on: Dr. A. Kylsa 
r'.-~..r C b c .-l^•^ i<£^joU.^J 
Four (4) soil samples were suc.-^iicted tc York Lai:cr2cori£3 fcr
analvsis. T.'-.e sa.TicI^g were crsparsd a.-.d analyzed in acccrda.-.ce
""•if- PrccecLjrss fcr -Ha.ndli.-.c a.^'d Che.-jcal .Analvsis cf S^di.r.s-.-
and AJTar Sa.-.cles . i: j.X/'cS-5 i - i . 
' 
T.'ie r = SL:Ics ara rspc?^%d i.': t.ne follcwi.-.c Tables. 
bv: 
y^yt^i 
Acoroved bv 
DFO/JCC/rr.d 
Daniel F. o^t 
Labcrat.qry Manaeer 
O / / 
r 
i^y 
!yAy ^ 
y y 
y/^.. 
T'/C, INC. • 2Ca Mc.-rc% Ti^rp-xe• -Monrca Ccnnecrcwt Ci^3 • r:C3) 26l-.:.:53 
301671 
TABLE 7 
^C.I,NC..::G,MC,-.', •ce "urcike • Mcs-^e. Cc.-„-.9crcu7 
C<i^a.;2Ca) 241^1453 
301672 
TABLE 2 
^ 
20850-1343 
^52220SClENCZsllNC 
^ ^ - l e _ ^ d e n ^ ^ ^ i ^ 3 ^ ^ 
J^, 
5751 - La'=: p i ^ 
^^ 
5752 - Lab p i . 
.^ 
<150 
<150 
V-VC. :NC. . irr, 
'^='^r^n„e.Mon.eCcnnec.=.o...a.(203,2.l.a.:S 
301673 
m 
YORK LABORATORIES DIVISION 
CERTIFIED REPCRT TRANSMITTAL 
^ ^ 
REPORT NUMBER 
30850-1^^^ 
DATE 
Sepcasber 25, 1955 
CUENT 
E:iviroscisncas» 
l a c . 
19 Cooeiand ?.Qad 
Denville, NJ 
0783^ 
AHENTICN 
Dr. .\. Xyles 
The cCove reference reccrr is enclosed. Copies of this report end supccrring ccrc 
will be reicined in ou? files in the even: they cre required fcr furure reference. 
If there are cny quesTions ccnceming ihis repcrx, piecse do net hesitcre to ccnrcc: us. 
Any samples sufcmittecj to cur Lcccrctcry v/iil be retained fcr c mcximurn of six?/ [60] 
days from receipr of tt^5report, unless other crrcngements cre cesirec. 
NcTurclly, cs in the pest cur stcft will be pleased to cuote on cny future recuiremenrs 
you mcy hc/e. in cdctticn tc the service provided, we ciso offer the following: 
• Hczcrccus Wcste Analyses 
• Product £vclucticrvR&D 
• Wcter end Wcstewcter Analyses 
• Air crvi Prccsss Gos Anciyses 
. • IndLWKtcl Hygiene Surveys 
' MeTQihrgiccI Analyses 
• Mlcrcfciotogiccl Anciyses 
• Moss Specrrcmetry Services 
Toily 
RccertGLBrc 
Vice President 
•r.'iC. ;.NC. • ICC Mc.-rpsa :.JT.Z:-<B • :'vlcnrc9. Ccrnscrcut '2z'ici--.ZZ: 
301674 
September 25, 1985 
30850-1444 
ElMVIROSCIENCES, INC. 
19 Ccceland Road 
Denville. New Jersev 
07834 
Atte.ntion: Dr. A. Kyies 
PURPOSE -AND RESULTS 
Five (5) soil sa.T.ples were submitted to York Laboratories 
anaiysis. 
The sar.pl.es were prepared and analyzed in acc; 
ancs with Rrccedurea fcr =a.".dlinc and Che-tiical .^.nalvsi; 
Sedi.~enr a.nc >7a-er Sa;?.cles, E?A/CE-a 1 -1 . 
" 
The results are repor^fed in the fcllcwina Tables 
Precarec bv: 
y k y ^ 
' \ J 
ADorovec 
Daniel ?» -Qtr 
Labcracorv. Manager 
a .-^-.yk. (A. /A,,.,.... 
^ s f r e y Q» Curran 
DFO/JCC/md 
r.VC. ;NC. • zee Wcr«:e ruT.c:i<e • Mcrrca Ccnnectcut Zti/il • f.203', 2a•l-u.,iiSa^ Jt^ «- rs a 
301675 
?5. 
--' 
^ 
TABLE 1 
-5 
30850-1444 
E>ryiR0SCI2NC2S, rNC. 
Sample I d e n t i f i c a t i o n 
T o l u e n e , 
uc/:<c 
O^Z-^V 
ICC B e r l e x , 8 / 7 / 8 5 1:00 
360 
r.VC. :NC. • ICC .Mcnrce^onpike • Mcp--ca Ccnnecrcu: C6443 • {20311^,-:^^^ 
301676 
TABLE 2 
3 0 8 5 0 - 1 4 4 4 
ENVTROSCIENCES, 
INC. 
S a m o l e I d e n t i f i c a t i o n 
p v r i d i n 
ICC B e r l e x - 
Lab P i t , 
8 / 7 / 8 5 
12:00 
2 , 7 0 0 
ICC B e r l e x - 
Lab P i t , 
8 / 7 / 8 5 
12:00 
<150 
VVVC. INC. • I-C Mcrrcs Tirr;c:Ke • Mcnrce, Ccr.necr.cu: Cd-icS • ^IZZ] Zi'.-^-^h A -c '-- '^ 
301677 
cs. 
TABLE 3 
30850-1444 
ENVTROSCIENCES, INC. 
VOLATILE PRIORITY PCLLOTANTS 
All results reported in ug/l. 
# 
Ccmrcund 
chloromethane 
brcmomechane 
vinyl chloride 
chloroethane 
me-hyla.ne chloride 
trichlorofluorcmethanfe 
acrolein 
acrylonitrile 
1 ,1-dichloroethene 
1 , l-dichloroechane 
trans-1 ,2-dichloroeth«.ne 
chloroform 
1 ,2-dichloroethane, 
1,1,1-trichlcroe-han^ 
carbon tetrachloride 
bromodichloromethane • 
2-chloroethylvinyl ether 
1 ,2-dichloropropane 
trans-l,3-dichloroprQcene 
trichloroethyle.ne 
benzene 
cis-1 ,3-dichlorcprop^n.e 
dibromochlorcme-nane 
1 ,1 ,2-trichlorcethan.^ 
bromoform 
tetrachloroethyle.ne 
1 ,1 ,2-2-teT:rachloroe*thane 
toluene 
chlorobenze.ne 
ethvl benzene 
Samcle Identificaticn 
ICC Berlex 
ICC Berlex ICC Berlex 
Lab P i t 
Lab P i t 
Lab •=--
8/7/85 3:00 8/7/85 3:00 3/7/3= 
"-nn 
<1Q 
<10 
<10 
<1Q 
<1Q 
<10 
<100 
<1Q0 
<10 
<1Q 
<10 
<'io 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<1Q 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
22 
<1Q 
<10 
<10 
<10 
<1Q 
<10 
<10 
<10 
<100 
<100 
<10 
<10 
<10 
<10 
<10 
< ] 0 . 
< i o '• 
, <10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
21 
<10 
<10 
<1C 
<'iO 
<-. Q 
<':Q 
<'. c 
<10 
^ 1 r n 
<1G0 
<1Q 
<10 
<10 
<10 
<10 
<10 
<:c 
<ia-. 
<10 
<10 
<!0 
<10 
<'0 
<1Q 
<":o 
<10 
<'0 
<10 
<10 
350 
<10 
< i O 
r.vc. iNC. • 2CC .Mcr-ta \:r-.pixe • MorrcaCcnnectcu:O.t-i^i • iZZZ\ 261-4^= 301678 
i — 
Berlex Labs, Inc. 
St. Croix, VI 
VID80651095 
Table I 
Results of Organics Analysis on Samples 
j 
1 
Mm 
"""" 
• 
Organic Compounds 
Toluene 
Flourene 
Bis(2-ethylhexyl)Phtha-
-late 
Benzophenone 
Di-n-octyl Phthalate 
Chloroform 
Benzene 
Di-n-butyl Phthalate 
Sample^ 
087001 
ug/kg 
460 
9200 
13000 
15^000000 
Sample// 
087002 
ug/kg 
560 
1300 
4700 
2600000 
500J 
Sampled 
087003 
ug/kg 
420 
16000 
SampleQ 
087004 
ug/kg 
440 
1900 
4200 
200K 
200K 
i 
I 
1 
Sampled 
087005 
ug/kg 
360 
51000 
600J 
Sample// 
087006 
ug/kg 
400 
36000 
2000 
, 
75000 
Sample #087001 - Aerated Soil Composite from Storage Room (left side) 
- '' 
Sample #087002 - Aerated Soil Composite from Storage Room (right side) 
Sample #087003. - Surface Soil Composite from North Side of Lab Waste Drainage Area 
Sample #087004 - Subsurface Soil Conposite from North Side of Lab Waste Drainage Area 
Sample #087005 - Surface Soil Composite from South Side of Lab Waste Drainage Area 
Sample #087006 - Subsurface Soil Conposite from South Side of Lab Waste Drainage Area 
K " Actual value known to be less than value given 
J • Estimated value 
Blank Space - Material Analyzed but not detected 
301679 
1 
•j£-
n<V1IOM«INTAl r t o T i m o N 
A O I M C T - 
I I O I O N K 
Environmental Services Division 
I01J0N, MfW J H U T 
M t l 7 
N « a k « f 
• t 
C«iit«i*«ri 
SV7Cc3 
1 
I 
I 
\ 
D*scrip«i«ii af | a a » U » 
f a n t m A t M s i k f l a t » « « t i k l l i t T («c S«Byl«: 
«,/^/i J5 
\ama\t 
N « * k a r 
tali»««ltW«^ l y : 
t«Ufl4wUli«W l y : 
ft*cai*a4 
l y : 
I c u i y t ^ l y : 
t « l M ^ v i f W « ^ l y r 
» r 
ft«taiv«rf 
l y : 
l a i t ' i T t ^ l y : 
Tia* 
T i - t 
TiB. 
0«t« 
0«« 
D M * 
» • ! • 
t»««wi i«f a « « t * •> tmnaiy 
lama— i— U««|» al Ci<i*4y 
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INDUSTRIAL 
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INCORPORATED 
iisj »oui£ IU. IIAMOOL!^. ^en tihstr O^JSK :UI.SI4.«JJO 
NJDE? C e r c i f i e d Dririk.i.-:g Wacer/U'as:: 
Laboracory ID :/lAil6 
RZPORT DATZ: 
March 5. 
L935 
LAB II 
5 2^63 
PRIORITY POLL'JT.A.NT 
LA30R.\T0RY A.NALYSIS 
CLIZ.NT: E:.'VIR0 SCIZNCZS IMC. 
S.-^MPLZ 
SAMPLE 
UNITS: 
SOURCE: 
ID: C-l 
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X 
X 
! 
X 
X 
1 
X 
1 
X 
X 
X 
X 
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. X 
X 
V 
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1 
NC - Non-caicuabie .RPD due co value(s) less chan dececcion limic. 
dub - D r y Weig.hc Basis 
X = Hoc Analyzed 
LT - Less Than 
INDUSTRIAL CORROSION MAxNAGZMZNT, INC. 
RPD » Relative percenc difference. 
RSL/dlh 
R ^ 
P ////Jy ik. 
cnard S. L*^vf^ 
jfcnard S. 1.4. 
r e s i d e n t 
' 
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INDUSTRIAL 
CORROSION 
MANAGE.MENT 
INCORPORATED 
1152 ROUTE '0. MuiOCLPH. .ItW .EJUET 37S69 
:0I-5J4-J33a 
NJDE? Cercified Drinking Wacer/yascevacer 
Laboracory ID //14116 
RZPO.RT DATE: March 5 
LAB If 52464 
1996 
PRIORITY POLLUTANT 
LA30.R.\T0.RY ANALYSIS 
CLIZNT: ENVIRO SCIZNCZS. INC. 
SAMPLZ 
SA.MPLZ 
UNITS: 
SOURCE 
ID: C- 2 
--
Is: 
,- \ 
.and 
drv 
Chemica 
veishc 
1 Co. 
b s. '^" s 
SAMjiLZ DATE: 
SAMJ'LZD BY: 
AT LAB DATE: 
M_\TRIX: Soil 
-oX^-,=>--. 1 Q' 
Alan Xvlss 
Februarv 21. 
1 cc i 
1 C I A 
iParam.e car 
S amp 1e 
Resulc 
dvb =• Dry Weighc Basis 
X » Noc Analyzed 
LT » Less Than 
Xinimum 
Dececcion 
Mecncc 
Blank 
.•i.nalvsis 
.-SLncimonv 
Arsenic 
X 
X 
1 
i 
X 
! 
X 
V 
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i 
X 
1 
X 
i 
X 
Cadmium 
Chromium 
1 
CoDoer 
Lead 
Mercurv 
LT 0.23 
1 
LT 0.23 
LT 0.23 
15.4 
3S.3 
22.0 
LT 0.103 
Nickel 
! 
X 
Selenium 
1 
X 
Silver 
Thallium 
Zinc 
Phenol 
X 
X 
57.S 
X 
Cvanide 
J 
X 
LT 0.21 
LT 0.21 
LT 0.5 9 
LT L.3 
LT 0.103 
X 
LT Q.r? 
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X 
1 
X 
1 
X 
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X 
1 
X 
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1 
0.97 
i 
X 
X 
! 
X 
1 
X 
1 
I 
1 
I 
RSL/dlh 
INDUSTRIAL CORROSION MANAGEMJINT. INC. 
gr±£hard S. lev<£ne 
P r e s i d e n c / 
301683 
INDUSTRIAL 
CORROSION 
MANAGE.MENT 
INCORPORATED 
.IU KOUfE 10. WKOCUM. Hly».;VtSlt 07SS9 ZOt-iU-OZZO 
NJDE? Cercified Drinking War.-/Vasc=v, 
Laboracory ID •/14116 
R£?ORT DATZ: .March 5. 1986 
LAB it 
52465 
, 
PRIORITY POLLUTANT 
LABORATORY ANALYSIS 
CLIZNT: ENVIRO SCIZNCZS, INC. 
SA.MPLZ 
SAMJ'LE 
UNITS: 
SOURCE: Island Chemical Co. 
ID: 
G-3 
r.s,''kE(-3on) drv veishc basis 
SAMJ'LE DATZ: 
S.i_M?LED 3Y: 
AT LAB DATZ: 
Tebruarv 1?. 
Alan Kvles 
Zabrua^'.* '^' 
i_ c c ; 
19Ef 
M-ATRIX: Scil 
dwb •• Dry Weighc Basis 
X - Noc Analyzed 
LT =- Less Than 
RSL/dlh 
Paramecer 
Ancimonv 
Arsenic 
' 
Bervllium 
Cadmium 
Chromium 
CoDoer 
Lead 
.Mercurv 
Nickel 
Selenium 
Silver 
Thallium 
Zinc ' 
Phenol 
Cvanide 
Sampla 
Resulc 
V 
V 
X 
T - p T? 
I c -
33.3 
' 4. =; 
T-T" n, '01 
X 
X 
X 
X 
129 
X 
! 
X 
1 
1 
Minimum 
| 
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j 
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1 
1 
Y 
1 
i 
V 
1 
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! 
TT 0.21 
1 
1 
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- • 
1 
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! 
X 
i 
X 
1 
X 
1 
X 
1 
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X 
X 
Mac.-.cc 
Blank 
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.,. 
-,-
Y 
T T n -!-> 
T - 
n 
-11 
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1 
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n 
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INDUSTRIAL CORROSION MANAGEMZNT.INC. 
Pochard S. lieviiie 
P r e s i d e n c 
^ 
301684 
r 
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INDUSTRIAL 
CORROSION 
MANAGEME.NT 
INCORPORATED 
NJDE? Cercified Drinking Vacer/Wasce--
Laboracory ID r^l4115 
M 
.i Murt 10. WJ«OOL«I. .itw jtRSEY i i u i 
M\-iu-iiza 
RZPO.RT D.A,T£: M?.rch 5, 
1986 
LAB It 
32466 
PRIORITY POLLUT.^.MT 
LA30PA.T0.RY ANALYSIS 
CLIENT: 
ENVIRO SCIZNCZS INC. 
SAMPLZ 
S.A^-PLZ 
UNITS: 
SOURCZ: Island Chemical Co. 
ID: G-4 
me''ks''t;rm'* drv veishc basis 
• S.-iiMPLZ DATE: 
SAM-PLZD BY: 
AT LAB DATE: 
e Druar-' 
1 Q _ 
1 OS, 
M-ATRIX: 
Spji 
Paramecer 
.-.ncimonv 
Sample 
Resulc 
.Minimum 
Dececcion 
Limi! 
M e c.-. c c 
Blank 
.^nalvs: 
.Arsenic 
Bervllium 
X 
Cadmium 
LT 0. 
LT 0.22 
0.2: 
Chromium 
12.0 
LT 0.20 
LT 0. 
Coooei 
7<; 
.T 0.5 7 
Lead 
I 7 7 
L.3 
T T ! 
Mercurv 
LT 0.102 
LT 0.102 
LT 0.1C 2 
Nickel 
Selenium 
Silver 
Thallium 
Zinc 
37.1 
LT 2.1 
0.9^ 
Phenol 
Cvanide 
dwb » Dry Weighc Basis 
X - Noc Analyzed 
LT - Less Than 
RSL/dlh 
INDUSTRIAL CORROSION MANAGEMJiNT, INC. 
Ri£hard S. 
L^ilifi 
P r e s i d e n c f 
'w(yiy>*'^ 
301685 
# 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
a NXiiE 10. HAAOOLP^. NEW jEfistr o/isa 
:oi-ii*.ujjo 
NJDZP Cercified Drinking Wacer/'-'ascev 
Laboracory ID i/14ll6 
^ 
RZPORT DATZ; M^rch 5 . 1°.= -
LAB it 5 2 4 6 7 
PRIORITY POLLUT.\NT 
LABORATORY ANALYSIS 
CLIZNT: ZNVIRO SCIZNCZS INC. 
SAM-PLZ SOURCZ: Isla 
SAMPLE ID: G-5 
Cha-ical Co. 
UNITS: 
ms./ke'^-om') drv 
;asis 
' SAMPLZ DATZ: Februarv 19. 19S6 
SAMJ'LZD BY: 
AT^..^ yy-'^c 
AT LAB DATZ: 
MJ>ITRIX: 
<;. 
.1 ' 
1 Q C ; 
;c'--
Paramecer 
1 
1 
1 
Sample 
i 
Resulc 
Minimum 
Dececcion 
L imi c 
'—1 
Mechcc 
1 
31anl< 
I 
Analvsis 
1 
1Ancimonv 
jArsenic 
dwb - Dry Weighc Basis 
X - Noc Analyzed 
LT - Less Than 
RSL/dlh 
Bervllium 
Cadmium 
Chromium 
Coooer 
! 
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Mercurv 
Nickel 
Selenium 
Silver 
Thallium 
Zinc 
Phenol 
Cvanide 
X 
LT 0.23 
17.1 
36. 1 
20. 2 
LT 0.105 
X 
X 
X 
X 
57.2 
X 
1 
X 
X 
! 
LT 0.23 
! 
LT 0.21. 
! 
LT 0.50 
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LT 1.3 
1 
LT 0.105 
! 
X 
X 
! 
X 
X 
1 
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X 
X 
X 
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LT 0.21 
LT 0.5C 
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1 
1 
1 
1 
X 
X 
X 
X 
0.95 
X 
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1 
1 
1 
1 
1 
INDUSTRIAL CORROSION MANAGZHZNT,INC. 
1/Ty^i, 
(.ichard S./LeVdne 
Presidenc 
301686 
c 
I? i'l 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
t\%l ROUIE IQ. fUMXlLPH. t e n JEASET a7I«9 201014.0^^11 
NJDEP Cercified Drinking Wacer/ 
Laboracory ID ^14116 
REPORT DATZ: March 5. iQg6 
LAB it 52468 
"<i3 -s-ace r 
PRIORITY POLLUTANT 
LABORATORY .^ALYSIS 
CLIZNT: ZNVIRO SCIZNCZS INC, 
SAM-PLZ SOURCZ: Island Chemical Cc. 
S.AM-PLZ ID: 
G-6 
UNITS: -.T.^^^r 
1 
-» - c - c 
SAM-fLi: DAT:L: Februarv 19". 195 5 
SAMPLED BY: .:^lan Kvles 
.kT LAB DATZ: ^»-„,.,,_.. -i 
' C C A 
M-\TRIX: c„,-i 
iParamecar 
1 
Sample 
I 
Resulc 
Minimum 
Dececcion 
Limic 
Mechcc 
j 
Blank 
Analvsis 
1 
dwb - Dry Weighc Basis 
X - Noc Analyzed 
LT - Less Than 
Ancimonv 
Arsenic 
Bervllium 
Cadmium 
1 
1 
t 
1 
i 
i 
Chromium 
' 
Coooer 
Lead 
Mercurv 
Nickel. 
Selenium 
! 
1 
Silver 
Thallium 
Zinc 
Phenol 
Cvanide 
X 
X 
X 
^.0 
46.5 
40.0 
32. a 
LT 0.122 
X 
X 
X 
X 
349 
X 
X 
1 
T T 
T T 
LT 
LT 
LT 
LT 
X 
i 
X 
i 
X 
i 
0,23 
' 
0,25 
: 1 
0.71 
! 
1.6 
1 
0.122 
X 
1 
X 
1 
X 
X 
2.6 
X 
X 
LT 
T f 
LT 
T_7 
LT 
X 
1 
X 
1 
X 
1 
0.2= 
i 
0.25 
1 
0.71 
i 
1.5 
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! 
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1 
X 
i 
1 
X 
1 
X 
i 
X 
1 
1.2 
! 
1 
X 
: 
1 
1 
1 
1 
RSL/ dlh 
INDUSTRIAL CORROSION MANAGEMENT,INC. 
7 / M Z ^ /(//7yyy^ 
Ridhard S. Lfvi.1^ 
Preside! 
I S. Leva 
mc 
[/ 
301687 
n 
•i I 
i i i 
1 
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INDUSTRIAL 
CORROSION 
MANAGE.MENT 
INCORPORATED 
•ij •<ourt :o. SXCCL.IN. itwjt.iiCf 0/1(69 :oi-5j<-oa:;u 
.NJDZP Cercified Drinking Wacer/Wasceva-; 
Laboracory ID .'/'14115 
.RZPORT DATZ: March 5. 1985 
LAB /; ^lifia 
PRIORITY POLLUTANT 
LABORATORY A.NALYSIS 
CLIZNT: ENVIRC SCIZNCZS INC. 
SAMPLZ 
S.^MPLZ 
UNITS: 
SOURCZ: Island Chemical Co. 
ID: G--
— c ' '.' c •' — '^—1 ^ .'•* •^•T 'v'2 ' '7'^ r n 3 c -' c 
SAMPLZ DATE:Februarv 19! 19=6 
SAMPLED BY: Alan Xvles 
-AT LAB DATE: Februarv 21. ICC — 
M-ATRIX: So--"' 
(This resor: :orm concains boch che original sample resulc and che spike recover-.'.) 
1 
1 
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Samole 
Resul: 
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Added 
1 Soikec ! 
i Sample j 
' Resulc ! 
. 
7R 
Concrol 
Limics 
for JR 
^'.inimum 
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Limic 
M 5 : r. 0 c 
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.Analvsis 
lAnc ir.cn V 
75-125 
I 
Arsenic '• 
Bervllium ! 
Cadmium 1 
Chromium. 1 
Coooer • 1 
Lead 
Mercurv 
' 
Nickel 
! 
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Silver 
' 
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Phenol 
Cvanide 
X 
X 
1 
1 
2.4 
! 
71.1 
! 
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45.4 
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X 
X 
1 
X 
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X 
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851 
X 
X 
X 
X 
1 
1 
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1 
0.004 
X 
X 
X 
X 
1 
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X 
i 
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1 
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i 2.39 
i 2.92 
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X 
1 
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X 
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X 
! 
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X 
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1 X 
1 
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1 
1 
1 
1 
1 
1 
X 
175-125 
X 
1-7 5-125 
103% 
75-125-
119% 
175-125 
83% 
175-125 
106% 
75-125 
• 88% 
I75-I25 
X 
75-125 
X 
175-125 
X 
175-125 
X 
75-125 
103% 
'r75-125 
X 
I7 5-125 
X 
^75-125 
% ! 
%r 
% 1 LT 
% ! LT 
% 1 LT 
mt 
% 
LT 
LT 
- 1 
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% 1 
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7. 
7. ILT 
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X 
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0. 
0; 
0. 
1. 
0. 
X 
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1 
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25 
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72 
T_T 
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121 
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T 
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1 
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%R =» Percenc Spike Recovery 
NR = Noc required. 
Scandard addicion performed-
dwb =» Dry Weighc Basis 
X » Noc Analyzed 
LT =• Less Than 
The spiked sample resulc is based on che soil 
in solucion. 
Ic does noc direccly reflecc che 
final mg/kg dry weighc basis resulc of Che 
sample. 
RSL/dlh 
INDUSTRIAL CORROSION MANAGEMENT.INC. 
c 
UL//lAyf./Alyy-
301688 
Ricl^^rd S. L&v/znkl/ 
fe 
L'J 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
IISJ WUIE 10. .^xOCU'^'. MtW .WSET J/S69 : a i - i 4 l - J J ^ 
NJDE? Cercified Drinking 
Laboracory ID •/141i5 
5 rtacer;^a; 
cevacer 
RZPORT DATZ: M^ 
L.\3 // 5 24 70 
1 Q 5 A 
PRIORITY POLLUTANT 
LABORATORY .ANALYSIS 
CLIZNT: ZNVIRO SCIZNCZS INC. 
S-AM-PLZ 
SAM-PLZ 
UNITS: 
SOURCZ 
ID: G-
_~,"^--
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3 
., 
Isl 
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an -
Co. 
ba=-
_' SAMPLZ DATZ: Februarv 
SAM-PLZD BY: 
AT LAB DATZ: 
il = -
Con..-. 
•<v-= = 
. 3 • » - • - 
"^ ^ 
: C C X 
.MATRIX: Cn-'i 
1 
Paramecer 
Ancimonv 
! 
1 
Arsenic 
Bervllium 
Cadmium 
Chromium 
Coooer 
Lead 
Mercurv 
Nickel 
Selenium 
Silver 
Thallium 
Sample 
Resulc 
Y 
X 
V 
LT 0.2 3 
2C . 4 
32-3 
19.4 
LT 0.093 
X 
1 
X 
X 
X 
Minimum ' 
Dececcion 
Limic 
X 
i 
Y 
! 
X 
! 
LT 0.23 
1 
LT 0.21 
' 
LT 0.60 ' 
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LT 1.3 
LT 0.093 
X 
X 
X 
X 
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Y 
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Cvanide 
76.2 
X 
X 
LT 0.44 
X 
X 
0.99 
' 
X 
• 
Y 
dwb - Dry Weighc Basis 
X - Noc Analyzed 
LT » Less Than 
RSL/dlh 
INDUSTRIAL CORROSION MANAGZMZNT,INC. 
RL6h 
P 
idhard S. L^vl 
residenc 
/ 
AiAyAA. 
301689 
3 
! f , 1 i 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
-Ml HOuIt 10. SAJiCCUM. >£W ;EMtT a;!59 :<il-5a4<jJM 
-NJDZP Cercified Drinking Wacer/Wascevacer 
Laboracory ID :/14il6 
RZPO.RT D.\TZ:- M_2rch 5, 19S6 
LAB li' 3 24 7 L 
PRIORITY POLLUTANT 
LABORATORY ANALYSIS 
CLIZNT: ZNVIRO SCIZNCZS INC. 
S-AM-PLZ 
SA.MPLZ 
UNITS: 
SOURCZ: Island Chemical Co. 
ID: 
G-o 
_
^ 
.••..-. ^ _ . , _ - , 
^ _ . , 
._.o , • _ • _ _ 
• _ . _ - • -
• SAM-PLZ DATZ: Februarv 19; 19S6 
SAMPLED BY: Alan Kvles 
AT L.AB DATZ: -Q•-.-., = -.. 71 
, a z -
MATRIX: c^,-i 
r'aramece; 
Ancimonv 
S amp1e 
Resulc 
X 
Minimum 
Dececcion 
Limic 
X 
aian.-; 
Analvs: 
Arsenic 
Bervllium 
Cadmium 
LT 0.23 
LT 0.23 
LT 0. 
dwb » Dry Weighc Basis 
X =» Noc Analyzed 
LT » Less Than 
RSL/dlh 
Chromium 
Coooer 
Lead 
Mercury 
Nickel 
Selenium 
Silver 
Thallium 
Zinc 
Phenol 
Cvanide 
19.3 
34. 9 
2' . 4 
LT 0.113 
X 
X 
X 
X 
75.7 
X 
X 
LT 0.21 
! 
LT 0.61 
1 
LT 1.1 
LT 0.113 
X 
X 
1 
X 
X 
LT 0.44 
X 
X 
LT 0.21 
! 
LT 0.51 
1 
LT 1.1 
i 
LT 0. 113 
1 
X 
1 
X 
X 
• 
i 
0.9? 
1 
X 
X 
i 
1 
INDUSTRIAL CORROSION 
MANAGZM-ZNT.INC. 
Ri^ard S. Laving 
Presidenc 
C 
301690 
INDUSTRIAL 
CORROSION 
MANAGEME.NT 
INCORPORATED 
.12 flourE 10. (UNOCLPM. Ntiii JE.HSET oithi 
joi-s«4.oj;a 
NJDEP Carcified Drinking Wacer/Wascavace: 
Laboracory ID ^14116 
RZPORT D.ATE: Mjzr: 
LAB it 52472 
5. 193; 
?-RIORITY POLLUTANT 
I-ABORATORY ANALYSIS 
CLIZNT: ^vVTRO SCIZNCF-. rvc. 
S.JMPLZ 
SA-MPLE 
UNITS: 
SOURCZ: 
ID: G-
rT,c-/'<^''^ 
Is 
• 
' ^ 
n-n^ 
.and 
r-'-.r 
Chemi 
ve"' ""^ 
ca 
r 
1 
•n 
Co. 
3 e - c 
SAM-PLZ DATZ: 
SAM-PLZD BY: 
AT L-AB DATE: 
M J ^ T R I X : 
<;n-
Februarv 19. 
Alan Kvles 
r=,-.,_,,-_,, ->• 
1 
1_ cc-
! c c -
j 
Paramecer 
Ancimonv 
Arsenic 
Bervllium 
Cadmium 
Chromium 
Coooer 
Lead 
-Mercurv 
Nickel 
Selenium 
Silver 
Thallium 
Zinc 
Phenol 
Cvanide 
Sampla 
Resulc 
Y 
X 
X 
LT 0.30 
30.6 
62.7 
16.5 
LT 0.106 
X 
V 
.V 
X 
X 
66. 5 
X 
X 
1 
1 
Minimum 
| 
Dececcion 
1 
Limic 
1 
X 
' 
X 
i 
X 
i 
LT 0.30 
! 
LT 0.27 
LT 0.77 
i 
LT 1. 4 
LT 0.106 
X 
X 
X 
X 
LT 0.56 
X 
x 
Mechcc 
.Analvsis 
x 
X 
X 
i 
1 
LT 0.30 
LT 0.-7 
1 
LT 0-77 
i 
LT 1.4 '- 
1 
LT 0.106 
X 
Y 
! 
X 
X 
1.3 
1 
I 
X 
Y 
1 
! 
i 
1 
t 
i 
dwb - Dry Weighc Basis 
X " Noc Analyzed 
LT » Less Than 
RSL/dlh 
INDUSTRIAL CORROSION MANAGEMENT,INC. 
A / y y ^ 
R^c'hard S.'yLaKC^dhe 
Preside: 
1 S. i-
snc / 
301691 
l\ 
r.ii 
i 
I ' l 
.k : : 
! 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
l U J - U U l l IU KAlrUUl.l'n I t W J l H i L T 0/3»M 
lUI )•< UJJU 
NJDE? Cercified Drinking Wacer/Wascevac: 
Laboracory ID (/i4116 
.REPORT DATE: 
March 5. JOfift 
L.\2 it 52473 
PRIORITY POLLUT.A-NT 
L.A30R.AT0RY A-\ALYSIS 
CLIZ.NT: ENVI.RO SCIENCES INC. 
SAMPLE 
S.-^-MPLE 
UNITS: 
SOURCE: Isiand Chemical Co. 
ID: G-11 
ma/ke i':3-3m) drv veishc basis 
' SAMPLE DATZ: February 19. 19S6 
SAMPLED BY: 
Alan Kvles 
AT L.A3 DATE: Februarv 21. 195 6 
MATRIX: 
Soil 
1 
i • 
1 
1 params cer 
'.Ancimonv 
iArsenic 
i 
s 
! 
R 
1 
1 
1 
ampl 
esul 
X 
X 
e 
c 
1 
M 
De 
i 
i 
inimum 
ceccion 
Limic 
X 
X 
M=..-cc 
Blank 
.Analvsis 
Y 
X 
Bervllium 
Cadmium 
Chromium. 
X 
LT 0.34 
41.1 
X 
LT 0.54 
LT 0.49 
X 
LT 0.54 
LT 0.49 
ICoooer 
1 .4 
LT 
Lead 
12.8 
LT 2.5 
T "" 7 ^ 
Mercurv 
' 
Nickel 
' 
Selenium 
1 
Silver 
Thallium 
Zinc 
Phenol 
Cvanide 
LT 
8 
0.194 
X 
X 
X 
X 
71 
X 
X 
LT 
LT 
0.194 
1 
X 
1 
X 
X 
1 
X 
1 
5.1 
1 
X 
1 
X 
LT 0.1 
X 
X 
X 
X 
2. 3 
Y 
X 
?4 
i 
i 1 
1 
dwb = Dry Weighc Basis 
X = Noc Analyzed 
LT =• Less Than 
RSL/dlh 
INDUSTRIAL CORROSION MANAGZM-Z.NT, INC. 
'/VhitJL 
Lchard S. 
Presidenc 
301692 
I 
il k 
CO 
o 
M 
to 
U> 
. , - 
INDUSTRIAL 
I ' I . 
CORROSION 
r . y l 
MANAGEMENT 
UI i 
INCORPORATED 
IISI ItOUK 10. (UHOOIPII. NEW JfASt V 0?a6J ;0I S>< ()]]0 
HJDEP r.eri i f ied D r i n k i n g 
Waier/V/ui.leviater 
l . a h o r a i o i y 
ID i l ' i l l 6 
REPORT HATE: 
H;,rnl. ID, 19R6 A:l -' 
CLIEHT:_ENyTRO_saiKNCES^Na._:^Ifi].an!LJ]lieifilcaLJ:.(Wfliiy_ni:Qjcct_ SAMPI E lf):_G-i 
-z 
' 
SAMPLE n A T E : F e b r i i n r v 
1 9 . 1986 
SAMPLED BY:_ 
ALnn_KyIea 
^^T LAR DATE: i.-ciiniary 2 1 , 10»6_ 
VOLATILE ORf.ANICS DY PURGE ADD TRAP 
; . 
By 
fiC/HS 
- 
HEADSPACE 
Compounds d e t e c t e d 
In p a r t s p e r m i l l i o n 
(mi 11 igranis/k i lofjroins) 
dry weight 
b a s i s , 
CIILOROHETIIAHE 
BROHOHETIIANE 
VINYL CHLORIDE 
-
CHLOROETHANE 
HETHYLENE CHLORIDE 
ACETONE 
1,1-DICHLOROETHYLENE -
1,1-DICHLOROETllANE 
t-l,2-DICHL0R0ETHyLENE 
CHLOROfORH 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER --
I,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE --
BROHODICIILOROHETIIANE --
- N l ) _ 
J J I ) _ 
- N l ) _ 
. N i ) _ 
-Nl)_ 
JJ I I -
NI) 
_.N!L 
_N!L 
_N!L 
-NIL 
J ! L 
..NIL 
ND 
1,2-DICIII OROPROPANE 
c-i,3-niciiinRoi'Rnpi:NE 
- - -
l-l,3-niCIIL0R0PR0l'ENE 
- - -
TCE (TRICIIIORnLTHYLENE)--
1,1,2-TRICIII.OROETIIANE 
DIDROHOCIILOROHETIIAHE - - - -
BENZENE 
DlISOPROPYL ETHER 
--
2-CHLOROETIIYLVlNYL ETHER • 
BROMOFORH 
1,1,2,2-TETRACHI.OROETHANE 
PCE (TETRACHLOROETHYLENE) 
TOLUENE 
CHLOROOENZENE 
ETHYLBENZENE 
• 
Nil, 
• 
N!)_ 
N!l_ 
NIL 
NIL 
_ H ! L 
NIL 
_ H ! L 
NIL 
__N!)_ 
NIL 
N|)_ 
_ N ! L 
.Nn_ 
— N I L 
LT=Less T h a n , G T = G r e a t e r T h a n , 
Nn=Nou 
D e t e c t e i l 
dwb-Dry Weight 
B a s i s 
SIMtUOOATI' KI'CnVKKll'S: 
d^ motbylene c b l n v l . l e - 60% 
' ' H ' 
II I'll 
d.. 
t o l u e n e - 
12 5% 
- 131% 
X 
For t h e above 
l i s t e d 
V n l n t l l e 
P o l h i l a n t s , 
n n l h l n g d e l e c t e d a l a s e n s l l i v i l y 
level of 
0 . 0 2 m|;/l<|',(ppin) 
ilwb. 
I 
• 
* 
' 
•* 
Other compounds delected:^ 
i^ 
, 
Li-
•••I...I 
• 
TNI)ll#iaAI, C,a\AtWl()U HANAGI'MI^NT, TNC^ 
.. /ck.{AU A/{/-/.•( r^i \'{yyyZzz. _ 
• 
• ' 
• 
' 
•• 
< 
A / i 
/ l l 
. . . . I 
I , , , , , . 
^ 
o 
M 
VO 
I
, I 
INDUSTRIAL 
' j . 
CORROSION 
• 
' I 
MANAGEMENT 
J I J 
INCORPORATED 
nil ROUl 10. MNOOini. M(wjifts(yo;i(i JDI sitoi^o 
NJOEP Ceriified Drinking Water/Wastewater 
Lahoralory If) //I'd 16 
REPORT PATE: _M,,rch_|n._]9ft6_ 
L A D // 
v^/,r,/, 
CLIENT: ENVIRO .SnTjENOE.S TNO. - T.slnnd Chcmlcnl rnwpnnv Prolect 
SAMPLE DATE; FebrMarv 19. 1986 SAMPLED BY: 
Alan_Kyle3 
SAMPLE ID: f;-2 
•:|/.'>i.-, 
_AT IAR DATE: Pcl.nii-iry 2 1 . 19116 
VOLATILE ORGANICS BY PURGE AND TRAP 
By 
GC/MS 
r 
HEADSPACE 
^yi 
Compounds detected In parts per million (mi 11igrams/kilograms) dry weight basis. 
CIILOROHETIIANE 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
HETHYLENE CHLORIDE 
ACETONE 
1,1-DICHLOROETHYLENE -• 
1,1-DICIILOROrTIIANE 
t-l,2-DICHL0R0ETIIYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER --
1,1,1-TRICIILOROETHANE -
CARBON TETRACHLORIDE --
BROMODICHLOROMETHANE --
— N I L 
_ N I L 
NIL 
NIL 
NIL 
Nl) 
Nl) 
Nl) 
N l ) _ _ 
Nl) 
un 
Nl) 
Nl) 
NU 
1,2-DICHLORnpROPANE 
— - - -
c-l,3-DICIII0RnpR0ITNE 
- - -
t-l,3-0ICHIOROI'R0l'tNE 
- - -
TCE (TRICIII.OROETIIYIENE)--
1 ,1 ,2-TRICIIl OROETHANE - - -
PIBROHOCIILOROMETIIANE 
BENZENE 
- - -
01 ISOPROPYL ETHER 
2-CIII.OROETIIYLVINYI. ETHER • 
DROMOEORH -
1,1,2,2-TETRACIILOROETHANE 
PCE (TETRACIILOROETMYLENE) 
TOLUENE 
CHIORODENZENE 
ETHYLBENZENE 
• _ N ! 1 
:„nn 
• _ H I } 
' 
— N l ! 
. 
_ N I ) 
_ n i ) 
_ N I ) 
_ N l l 
_ i i n 
__NI> 
_ N I 1 
Ml) 
Nil 
Nl) 
N|) 
LT=Less Than, GT=Greater Than, ND-Not Detected 
dwb=Dry Weight BasIs 
5L'!!!?Q^.'^TLl!!!?f:f}^!:!'.!!:5' ''2 merliylene'chloride - 6/(% 
(I. toluene 
11 I'll - 126% 
(I . toluene - 1 1 't% 
X 
For tho above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 ni|;/ke(n()m) duh. 
Other compounds delected: 
i 
''' '• ' 
: / 
(NDiWTiaAi. c.omuyjjm iiANAotHKNT, rue. 
/ U k / u ( y / { ( / y A . n ^ 1L •• • -"••"• 
I 
i 
'M 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
)IS)fUXn( 10. R<NOO(ni.MWJ(RSEV 07169 201 i l 4 « } ] a 
# 
o 
o^ 
vo 
cn 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID yCl'il 16 
REPORT DATE:_M,-,rc!iJ|),_19ft6_ 
LAR // «/,6S 
CLIENT; ENVTRO SCTENCE.S. TNO. - T.slnnd Chcmlcnl 
Coinpany P r o l e c t 
SAMPLE I D : _ ( ; - ] 
• • ' ' ' :'!••••• 
SAMPLE DATE; February 
19. 
19R6 SAMPLED BY: 
Al2!LKyIS5 
^^^ " ^ " '^'^TE: Fe!,r,,nry_21^J9n6_ 
VOLATILE ORGANICS BY PURGE AND TRAP 
By 
GC/MS 
-. HEADSPACE 
...' I -
• ' • 
^ 
. 
Compounds detected In parts per million (milligrams/kilograms) dry weight basis. 
CHLOROMETHANE 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE ---
ACETONE 
1,1-DICHLOROETHYLENE -
1,1-DlCIILOROETHANE 
t-l,2-D|CIIL0R0ETIIYLENE 
CHLOROFORM 
1,2-DICllLOROETilANE 
- - - -
t-BUTYL METHYL ETHER - -
l.l,l-TRICHLOROETIIANE -
CARBON TETRACHLORIDE 
- -
BROMODICHLOROMETHANE 
- -
N|)_ 
NIL 
NIL 
NIL 
N[L 
Nn_ 
NIL 
Nlll 
NU_ 
NIL 
N n _ 
NP 
NP 
N P . _ 
Nl) 
1,2-DIClll OROPROPANE 
c-l,3-DlClliOROPROPrNE 
- - -
l-l,3-DICIII0K0PI(0PEIIE 
- - -
TCE (TRICHI.OROETIIYLENE)--
I ,1,2-TRICIIL0R0ETI1AI(E 
- - -
DIBROHOCIII.OROHETIIANE 
BENZENE 
DIISOPROPYL ETHER 
2-CHI.OROETHYLVINYL ETHER • 
BROMOFORM 
1,1,2,2-TETRACIII.OROETHANE 
PCE (TETRACHLOROETIIYLENE) 
TOLUENE 
CHLOROBENZENE 
ETHYLBENZENE 
• 
N n _ 
Nl) 
Nl) 
Nl) 
ND 
, Nl) 
Nl) 
ND 
. Nl) 
N D _ _ 
Nl) 
Nl) 
NU 
Nl) 
Nl) 
LT=Less Than, GT=Greater Than, ND=^Not Detected 
dwb=Dry Weight Basis 
^L'llHOL'.ATLHl'frL'V''•'!!''•-'= ''^ methylene' chloride - 9fi% 
liient 
57% 
li. t o l u e n e - 61% 
lU'lt 
For the above l i s t e d V o l a t i l e 
P o l l u t a n t s , n o t h i n g d e t e c t e d at a s e n s i t i v i t y 
l e v e l o f 
0.02 mp,/k|;(p|)iii) iK/h. 
Other compounds d e l e c t e d : 
> 
INDUJ y 
,1'iiiAi. (:Qrtj;«,';ini) HAMAnriitiNT, inc. 
• 
/ 
f / / 
y<.//A%/ /^^f-i^ 
1. 
w 
o 
l - » 
vo 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
IISI ROUIE 10. RANDOtni. IKW JlHsrv 071(9 201 i l l Olio 
J ••• 
NJDEP C e r t i f i e d D r i n k i n g W a l e r / W a s l e w a i e r 
l a b o r a t o r y ID ij'I'il 16 
. 1 . I 
• 
• • l A l i . - ^ ] 
REPORT DATE:__H.n-cb 10,- 19fl6i'-.'ri 
I An § 
52466 
ykA 
I.-' 
CLIENT; ENVTRO SCTENOES. INC. - T.slnnd niiemlcal Ooinpnnv P r o l e c t 
SAMPLE ID:_(:_/i 
SAMPLE DATE; F e b r u a r y 19. 1 9fl6 SAMPLED BY: 
:AJn!i_KyJe!i 
AT IAR DATE :_p,.ijrunL-y_2L_lQD6-
VOLATILE ORGANICS DY PURGE AND TRAP 
By 
GC/MS ,- 
HEADSPACE 
i. -'A'-
. • 
I . .,.'••; 
I 
• ' 
• 
Z ' Z ' I 
Compounds d e t e c t e d In p a r t s p e r m i l l i o n ( m i l l i g r a m s / k i l o g r a m s ) dry w e i g h t b a s i s . 
CIILOROHETIIANE 
BROMOMETHANE ---
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
I.I-DICHLOROETHYLENE 
-
1,1-DICIILOROETHANE 
t - l . 2 - D I C I I L 0 R 0 E T I I Y L E N E 
CHLOROFORM 
1,2-DlCHLOROETHANE 
t-BUTYL METHYL ETHER --
1,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE --
BROMODICHLOROMETHANE --
.Nil 
- N l ) _ 
J J U _ 
JIU 
-1ID_ 
JJQ-
-NIL_ 
J l l i _ 
J^l)__ 
_NI)__ 
_N}) 
j j ) 
_N|) 
Nl) 
I,2-DICHIOROPROPANE 
c - l , 3 - D l C I I I 0 R 0 P R 0 P E t l E 
- - -
t - l , 3 - D I C I I I 0 R 0 P R 0 P E N E 
- - -
TCE 
(TRICIIIOROETHYLENE)--
1 ,1 ,2-TRICIILORflETIIANE 
- - -
DI BROHOCUI.OROHt THANE 
BENZENE 
Dl ISOPROPYL ETHER 
2i-CIIL0R0ETIIYLVINYL ETHER • 
BROMOFORM 
I ,1 ,2,2-TETRACIil.OROETHANE 
PCE 
(TETRACHLOROETHYLENE) 
TOLUENE 
CHLOROBENZENE 
ETHYLBENZENE 
„.N!L 
„ N ! L 
_!!!L 
__.N!L 
__N!L 
_ H ! L 
_I!!L 
_l!!)_ 
—liiL 
_.N!L 
H!)_ 
_ N n _ 
__.NP._ 
_ N ! L 
ND 
.5!J!!!!!?flAT!:J?!'l'f^y!r!!ll-'i= ''^ "'etbylcne cblnrl.le - 100% 
<l toluene - 70% 
LT-'Less Than, GT=Greater Than, ND-Not Detocte.l 
'"'" ~ ^'^^ 
dwb'=Dry Weight Oasis 
X 
For the above listed Vol al 11 e Pol lut ant s , nothing delected at a st.-ii'.. il I v i Iy level of (].(]2 m(;/k|'(ppm) duii 
Ot her compotinds de I ec I ed: 
'). 
)\\?/n/\ 
]mu?/Y\<u\, oniTifn^nN HANACKMRNT, INC. 
///A/2yJ%J/AAtt\. •: .... 
CO 
o 
vo 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
IIS2 ROUIE 10. RANOOini. NIW JERSEY 07et9 201 Sa4 01)0 
I ••* 
NJDEP Certified Drinking W a t e r / W a s t e w a t e f 
Laboratory ID yfi'il 16 
, 
:,. 
: -i^i.' ,'.: . .1 
t 
. ' i . ' f • . * 
•* 1 
• 
I 
* 
• 
• 
• • 'Z^iZA' ^ ' ' 
.•' 
REPORT DATE: Marcl. 10. 19n6'i.''li:U ' •.•' : 
LAD // 52/,67 
•t'r. 
CLIENT; ENVTRO S C T E N C E S , T N C . - Tsland Chemical Compnny Project 
SAMPLE in:_C-5 
SAMPLE DATE; February 19. 1906 SAMPLED BY; 
Alan Kyles 
y\y 
AT LAR DATE: 
I'ebruary 21. I9fl6 
VOLATILE ORGANICS BY PURGE AND TRAP 
§L_£lZi1 S - IIEAD S PAC E 
CHLOROMETHANE -
BROMOMETHANE - 
--
VINYL CHLORIDE 
CHLOROETHANE 
HETHYLENE CHLORIDE 
ACETONE 
1,1-DlCHLOROETIlYLENE -• 
1,1-DICHLOROETHANE 
t-l,2-DICHL0R0ETIIYLENE 
CHLOROFORM 
1,2-DICliLOROETHANE 
t-BUTYL METHYL ETHER --
I,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE --
BROMODICHLOROMETHANE — 
•: '\\Zi-i.A^ 
i. zy 
C o m p o u n d s detected In parts per million (mi 1 1 igrams/k i lograms) (Iry welgitt b a s i s . 
_ N ! 1 _ 
_ N ! > _ 
_m 
_ N U _ 
_ N I ) _ 
_ N I ) _ 
_ N ! I _ 
_NIL_ 
_NP._ 
_ N P _ 
_ N ! } _ 
. N Q — 
_N!)_ 
-NP— 
. U P _ 
1,2-DICIil OROPROPANE 
c-l,3-DICIII.OHOI'ROI'rNE 
- - -
t-l,3-DICIM0R0PR0PENE 
- - -
TCE (TRiCIII OltOETIIYLENE)--
1 ,1 ,2-TRICIILOROETIIANC 
DIBROMOCIILOROMCTNANE 
BENZENE 
DIISOPROPYL ETHER 
2-CIII.OROETIIYLVINYI. ETHER • 
BROMOFORM 
I ,1.2,2-TETRACIILOROETIiANE 
PCE (TETRACHLOROETHYLENE) 
TOLUENE 
CHLOROBENZENE 
ETHYLBENZENE 
ND 
_N|) 
JJl) 
_.Nn 
_NP 
Jin 
_N|) 
JI!L_ 
-NIL_ 
_NI)_ 
JI!I_ 
JI!L_ 
_N|) 
_N|1 
J M 
SIlItltOCATI' 
ltl'CnVI'ltlli:.S: 
LT=Less Than, GT=Greater Than, ND=Not Detected 
dwb-Dry We I gilt BasI s 
(1-2 mntbylene chloride - 97% 
(I, toluene - 67% 
IIKIl - 66% 
X 
For the above l i s t e d V o l a t i l e P o l l u t a n t s , nothing detected at a sen;, i I i v I i y liivel of 0.02 mc/kcCppiii) ilul). 
Other compounds delected: 
^ 
' '' ' 
• 
INnilknitlAl, COIi/oyON IIANACI'MENT, IIJC, 
CJ 
o 
M 
<Ti 
VO 
00 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
IS2 ROUIE 10. RANOOini. NEWJERSIr07169 
201 i t 4 0310 
N.IDEP C e r t i f i e d D r i n k i n g 
V/ater/V/aslev-^ater 
Laboratory ID /?I'll 16 
• ^ ; ; '/[ 
REPORT n A T E : _ M a ! : c ! . J O , _ i 9 n 6 _ l L l 
LAB II 
v2/i6H 
'•••. . 
CLIENT; ENVTRO .SCTENCES. TNC. - T.slnnd Cbemical Compnny Project 
SAMPLE \0:j]-.f^ 
SAMPLE DATE; February 19. 1986 SAMPLED BY: 
.AJan^KyJen 
AT LAD DATE: [.yuniary 21. 19n6 
VOLATILE ORGANICS BY PURGE AND TRAP 
By GC/MS - HEADSPACE 
Compounds detected In parts per million (milligrams/kilograms) dry weight basis, 
CHLOROMETHANE 
BROMOMETHANE --
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
• ACETONE -- 
- 
• 
1,1-DICHLOROETHYLENE -• 
1,1-DICIILOROETIIANE 
t-l,2-D|CHL0R0ETIIYLENE 
CHLOROFORM 
1,2-DICIILOROETHANE 
t-BUTYL METHYL ETHER - -
I,I,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE - -
BROMODICHLOROMETHANE - -
_ND 
_ N n _ 
_NI)_ 
_NIL_ 
_NIL_ 
_NI)_ 
_N|)__ 
JJIL_ 
_NI)__ 
_NIL_ 
-Nl)_ 
JIII— 
_Nn_ 
-NIL_ 
_NII_ 
1,2-DiCIILOROPROPAIIE 
c-1 ,3-DirillOROPROI'LNE - - -
t - 1 , 3 - 0 1 CIII OROI'ROPfNE - - -
TCE (TRICIII OROLrilYI.ENE)--
I ,1,2-TRICIII OROETHANE - - -
DIBROHOCHIOROMETHANE 
BENZENE 
DIISOPROPYL ETHER 
2-Clil.OROETIIYLVIIIYL ETHER • 
DR'OMOFORM 
1 .1 , 2, 2-TETRACIII OROETHANE 
PCE (TETRACHLOROETHYLENE) 
TOLUENE 
CHLOROBENZENE 
ETHYI.DENZENE 
NP 
N P _ 
Nil 
Nl) 
l l l ) _ 
__N|) 
_ _ N P 
Nl) 
l-JU 
N U _ 
Nl 
111 
NU_ 
NU_ 
NU_ 
SIIRUOCATI': RKCOVI'.ltlKS 
tl-^ motliylene 
c h l o r i d e 
66% 
n/i% 
LT=Less Than, GT=Greater Than, ND=Not Detected 
dwb=Dry Weight Basis 
d.. 
t ( i l i i e i \ e 
II I ' l l 
59% 
For the above listed Volatile Pollutants, nothing delected at a sensitivity level of 0.02 m(;/k|>,(ppm) iluli. 
Other compounds deled ud: 
. 
I . 
INDIl^fia^/l. jltil^KJION^I.ANACLUKNT, INC. 
//k^y/ yyn't-<- • 
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INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROUIE 10. HANOOlhl. NEW JERSEY 07669 
201 i a i 0110 
t 
1 
I. 
r 
•;;. 
t 
it 
i, 
NJDEP C e r t i f i e d 
D r i n k i n g 
W a t e r / W a s t e w a t e r 
L a b o r a t o r y 
ID / y i ' i l 16 
REPORT DATE: 
M.ircli 
1 0 . 1 9 ( 1 6 ^ 
LAD .// 
r?./,()<} 
) i ' l n v 
CLIEHT;_EHV.iRO_SGIENCES-JNn.^_Ialaiid_Ghei!ilGflLCQn)nnny_PcQj£ct 
SAMPLE in:_j;_7 
SAMPLE DATE: pciiruai:x_l5-^lQf]6_SAMPIfD BY: 
Alan.Kyles 
AT IAD OATE: 
l / . i | . n i n r v 
2 1 . 
19R6 
VOLATILE ORGANICS BY PURGE AND TRAP 
By 
G C / M S 
- 
H E A D S P A C E 
Compounds 
d e t e c t e d 
I n p a r t s 
p e r m i l l i o n 
( m i l l i g r a m s / k i l o g r a m s ) 
d r y w e i g h t 
b a s i s i 
CHLOROMETHANE 
BROMOMETHANE 
VINYL 
CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
1,1-DICHLOROETIIYLENE 
-• 
1,1-DICIILOROETIIANE 
t - l , 2 - D | C I I L O R 0 E T H Y L E N E 
CHLOROFORM 
1,2-DlCHLOROETIIANE 
t-BUTYL 
METHYL ETHER 
- -
1,1,1-TRICIILOROETIIANE 
-
CARBON TETRACHLORIDE 
- -
BROMODICHLOROMETHANE 
- -
_ _ N I ) 
NU 
NU 
ND 
NU 
NU 
NU 
NU 
NU 
ND 
ND 
ND 
J I L 
..NIL 
ND 
1,2-DICIII.OROPROPANE 
c - 1 ,3-DICIIIOROI'ROIMNE 
- - -
t - l ,3-DICIIIOROPROPLNE 
- - -
TCE 
(TRICIII OROLTHYIENE)--
1 ,1 , 2 - T R I C I I I OROETHANE 
- - -
DIBROMOCIIIOROMETIIAIIE 
BENZENE 
DlISOPROPYL 
ETHER 
2-CIII.OROETIIYI.VINYI. 
ETHER • 
BROMOFORM 
1 ,1 ,2,2-TETRACIII.OROETHANE 
PCE 
(TETRACHLOROETHYLENE) 
TOLUENE 
- -
CHLOROBENZENE 
ETHYLBENZENE 
_ND_ 
_NP_ 
_N!L 
J!!L 
J U L 
_N!L 
_m_ 
J!!}_ 
-NIL 
-NIL 
-till, 
-.NIL 
-!IP_ 
.NIL 
ND 
LT-Less Than, GT=Greater Than, ND=Not Detected 
dwb=Dry Weight Basis 
SURROGATE JIKCOVI'lt I MS: .Ij metbylene chloride - 111% 
•'ll 
^ " ' 
RKll 
-
( I . 
t o l u e n e 
- 
126% 
X 
F o r 
t h e 
a b o v e 
l i s t e d 
V o l a t i l e 
P o l l i i l a n l s , 
n o t h i n g 
d e l e c t e d 
at 
a s e n s i t i v i t y 
l e v e l 
o f 
0 . 0 2 mB/l<i;(ppm) 
d u b , 
X 
O t h e r 
compounds 
<'elec l e ( l : | | y d i - o c / j i |io|!_llT._^^LI!l|ll,_!J|!IU!}!<.._Oi !> .!!!li/!^i:(ll'.'!;..' I ! . ' I Y . ! ! ' J l ! ! ! ! u ) _ J 
'1 
im\\'.i7i<\Zf.A.i]nny\(fii 'MANACEMENT, INC. 
iii;i/Ruf: cimuYimi MAI 
////(Uy y J/,At. / 
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CO 
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;^;i'i 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
IIS2 ROUIE 10. RANOOini. NEW JERSEr 07)69 201 i64 OUO 
NJOEP Cert ified Drinking Water/Was Iewater 
Laboratory ID Al'il 16 
,.y/z 
REPORT D A T E : _ j j a r c b 
m . 
1906 ' " 
LAO i 
--,2/.70 
:••• -• 
CLIENT; 
ENVTRO SCTENCES. TNC. - Tslnnd Cbemical Compnny P r o l e c t 
SAMPLE ID: 
C-D 
SAMPLE DATE;Kebninrv 19. 19n6 
SAMPLED DY; 
^Xnn__KyJ[es 
AT LAR DATE: 
F e b r u a r y 2 1 , 1906 
VOLATILE ORGANICS BY PURGE AND TRAP 
By 
GC/MS 
- 
HEADSPACE 
Compounds d e t e c t e d In p a r t s p e r m i l l i o n 
( m i l l i g r a m s / k i l o g r a m s ) dry weiglit 
b a s i s , 
CIILOROHETIIANE 
-
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
HETHYLENE CHLORIDE 
ACETONE --r---
1,1-DlCIILOROETHYLENE 
-
1,1-DICHLOROETIIANE 
t-l,2-DICHLOROETHYLENE 
CHLOROFORM - -
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER - -
1,1,1-TRICIILOROETIIANE -
CARBON TETRACHLORIDE 
- -
BROHODICIILOROHETIIANE 
- -
NP 
N!) 
_ _ N P 
_ i l P 
NP 
NP 
_:_NP 
N P _ _ 
NP 
NP 
NP 
Nl) 
. 
NP 
N!) 
I,2-DICHIOROPROPANE 
c - 1 ,3-DICIIIOROI'ROI'ENE 
- - -
t - l , 3 - P I C I I I 0 R 0 P R 0 P E N E 
- - -
TCE (TRICIII OROETHYI E N E ) - -
1 ,1 ,2-TRICin.OROETIIANE 
- - -
DI OROHOCIILOROMETHANE 
DEN2ENE 
- - -
DIISOPROPYL ETHER 
2-CliLOROETiiYLVINYL 
ETHER • 
BROMOFORM 
1,1,2,2-TETRACHLOROETIIANE 
PCE 
(TETRACHLOROETIIYLENE) 
TOLUENE 
CHLORODENZENE 
--
ETHYLBENZENE 
_Np_ 
_L'P_ 
_.N|L 
-NIL 
_N|L 
_N!L 
-L'lL 
-MIL 
-NP_ 
-NIL 
-NP_ 
-NP_ 
-NP_ 
-NIL 
Nl) 
LT=Less Than, GT=Greater Than, ND=Not Detected 
dwb=Dry Weight Basis 
SIIUHmWiTE KI'COVKUIKS: dj methylene chloride 
d. toluene - 72% 
HI'11 - 5y/. 
10/,% 
X 
For the above listed Volatile Pollutants, nothing detected at a sens i t i v i I y ii:vi;l of O.DZ mi;/k(;(p|im) dub 
Other compounds detected: 
\ 
•_ 
^ ^ 
1II0II.;^IIIAK ('-(Wm:.il)U IJANACKMKNT, INC. 
I, 
J 
fc.:.,. ili 
i 
. ^ 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1162 ROUIE lO.RAMOOU^I. HEW JERSEY 07669 
201 661 0330 
L 15 I'l 
w 
o 
i-» 
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o 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID ,^l'il 16 
REPORT nATE:_^|;,^.ci,_in._10Q6. 
IAD f__s:j/,/| 
CLIEHT: 
ENVTRO SCTFNCIl.S TNC. - Tiilnnd Cbemical Conipnny P r o j e c t 
SAMPLE 10: j j - i j 
• 
SAMPLE DATE:_Fei>iugE^_[9^i9fi6_SAMPLED 
DY: 
.Alfln_KyIfi2 
^AT IAD DATE: February 2 1 . 19R6 
VOLATILE ORGANICS BY PURGE AND TRAP 
By 
GC/MS 
- 
HEADSPACE 
Compounds d e t e c t e d 
In p a r t s per m i l l i o n 
( m i l l i g r a m s / k i l o g r a m s ) 
dry weight 
b a s i s , 
CIILOROHETIIANE 
BROMOMETHANE 
VINYL CHLORIDE -
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
--• 
1,1-DICHLOROETHYLENE -• 
1,1-DICIILOROETHANE 
t-l,2-DICHLOROETHYLENE 
CHLOROFORH ---
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER --
1,1,I-TRICHLOROETHANE -
CARBON TETRACHLORIDE --
BROMODICHLOROMETHANE --
_N!L_ 
_N!L_ 
„NP_ 
INP_ 
_NP_ 
_NIL_ 
-NIL-
-Nil-
M ) -
.Nl)_ 
M\— 
- N n _ 
.ND_ 
.NU_ 
1,2-Dirill OROPROPANE 
c-l,3-DICHI0R0PR0PENE 
- - -
t - l ,3-niCIII.OROPROPENE 
- - -
TCE (TRICIII OROETHYI EHE)--
1,1 ,2-TRICIII OROETHANE 
DIBROMOClll OROMETHANE 
BENZENE 
DlISOPROPYL ETHER 
---
2-CIIIOROETIIYI.VINYI. ETHER • 
BROMOFORM 
1 ,1 ,2,2-TETRACIII OROETHANE 
PCE (TETRACIIIOROETIIYLENE) 
TOLUENE - - - 
- - 
--
CHIORODENZENE 
ETHYLBENZENE 
NIL 
' N I L 
-NIL 
..NIL 
ND 
_Nn 
AllL 
_-NP_ 
-NIL 
-NIL 
-NIL 
-NP_ 
-NIL 
-NIL 
ND 
LT=Less Than, GT=Greater Than, 
ND=Not 
Detected 
dwb=Dry Weight 
Basis 
SIIKimCATE HECnyr.ltlES: 
(bi m e t b y l e n e 
c b l o r l . l e 
I iieiu 
611% 
102% 
d . 
t o l u e n e 
- 76% 
IIFII 
For 
the above l i s t e d V o l a t i l e P o l l u t a n t s , 
n o t h i n g d e t e c t e d al a s e n s i t i v i t y 
level o f 
0.02 m|;/kt',(ppm) 
di;b. 
Ol her compounds de I ec I e d : 
\ 
; 
IMnnc'Ti/. /TT-iv;;:: 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
ll32ROUIf 10. RANDOini. NEW JERSEr 07669 201 Sai 0}30 
NJDEP Ceriified Drinking Water/Wastewater 
Laboratory ID /'I'll 16 
REPORT DATE LHarcb J0._19L1(L 
IAD II 
r,?/,7T 
CL I ENT; ENVTRO SCTBHCE.S. T^C. - Tslnnd CheiHlcnl Company Pro | cct 
SAMPLE I P:._j;-I I 
SAMPLE DATE: February 19. I9ft6 SAMPLED BY: 
Al nn Kyles 
AT IAR DATE: 
Februnry 21, I9R6 
VOLATILE ORGANICS BY PURGE AND TRAP 
• 
By G C / M S - H E A D S P A C E 
Compounds detected In parts per million (milligrams/kilograms) dry weight basis. 
U) 
o 
M 
o 
lO 
CIILOROHETIIANE 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
HETHYLENE CHLORIDE 
ACETONE -
1,1-DICHLOROETHYLENE -• 
1,1-DICIILOROETIIANE 
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
-
1,2-DICHLOROETIIANE 
t-BUTYL METHYL ETHER - -
1,1,1-TRICHLOROETIIANE -
CARBON TETRACHLORIDE - -
BROMODICHLOROMETHANE - -
. N P _ 
. N l > _ 
. . N l l _ 
J ^ l l _ 
_NL 
_ N U _ 
_ N U _ 
_ N U _ 
. - N U _ 
-Na__ 
JJU__ 
J i n _ 
_ND_ 
_NI)_ 
ND 
LT=Less Than, GT=Greater Than, ND=Not Detected 
dwh-'Dry Weight 
Basis 
1,2-DICIILOROPROPANE 
c-l,3-DICIIIOROPROI'ENE 
- - -
t-l,3-DIClliOROPROPENE 
- - -
TCE (TRICIII OROETHYI ENE)--
1,1,2-TRICIU OROETHANE - - -
DIDROMOCIII.OROMETIIANE 
DEN2ENE 
DIISOPROPYL ETHER --
2-CIIIOROETIIYLVINYI. ETHER • 
BROMOFORM 
1,1,2,2-TETRACIIlOROETHANE 
PCE (TETRACHLORflETHYLENE) 
TOLUENE 
CHLOROBENZENE 
ETHYLDENZENE 
__NI1 
_ N | ) 
__LJ|) 
__NP 
Nl) 
__N1) 
NO 
_ N U 
_ N U 
— N i l 
Nil 
Np 
iip 
Nl) 
un 
-WATER 
SIIUUOCATE RECOVER I K.S: 
i\-^ m e t b y l e n e 
c l i l o r i d e 
- 
T l ) [ % " 
173% 
d.. 
t o l u e n e 
It I'll 
16T% 
X 
For the above l i s t e d V o l a t i l e P o l l i i l a n l s , 
n o t h i n g d e l e c t e d at a s e n s i t i v i t y 
I r v d 
o f 
s iij-./l (ppli)-wiii ei 
(1. I mc/l^;(|'|"") " "n I I 
Oilier compoiiiuls del ec I ed: 
_^ 
UYi 
iNi)ii.';;yi( 
/i 
iLyin/vi. cnHHO?;iijN HANACF.MFNT. mc. 
////k f. /y{ k 1-^ 
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» . 
..b 
»1 
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:|l 
• 
# 
b 
I 
Jl. 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
IIS2 ROUIE IO.IUlHDO(rtl.UIWJERSElD7l69 201 3I««]30 
n 
L'J 
SAMPLE 
SOURCE: 
ENVTRO SCIENCES 
SAMPLE 
DATE: 
February 19. 19R6 
State C e r t i f i e d Drinking Water/Wastewater L a b o r a t o r y ID # l ' i l l 6 
REPORT 0 A T E : _ A i . r l L ^ L _ 1 9 ( i 6 
LAB y}'__5/LS0i 
SAMPLE 
ID ••_Cn!!!|!0!iJ te_nC 
C-6 .'md (;-7 
TAKEN 
D Y : _ A U < y i < l « . 
AT LAB DATE : Fel.runry 2 1 . I9D6 
KEACriVATEl) DATE: A p r i l 10. 1906 
EP T O X I C I T Y 
TEST 
l e a 9 b ? . l S _ A n a l v 5 ] s J C F R _ y o l _ . J i 5 , _ N o . 3(1) 
PARAMETERS 
TESTED 
I n o r g a n i c Chemicals by AA 
A r s e n i c 
Barium 
Cadmium 
Chromium 
Lead 
Mercury 
Selenium 
S i l v e r 
-
TEST 
as 
I.T 0 
RESULT 
mg/l 
.005 
1.2 
I.T 0 
I.T fl 
0 
I.T 0 
I.T 0, 
I.T 0. 
.02 
02 
2/. 
010 
OOS 
01 
MDI, 
I.T (I.DO'i 
I.TJ).;| 
1:0:.!?L 
l.'rj).D2_ 
l,TJ).D6 
j . l M ) . ()I () 
1,'r 0,1)02 
I.T 0,0) 
METHOD 
MAXIMUM PERMISSIBLE 
!!!:^i^!^ 
Concerit r a t jon as mo/1 
I.T 0,005 
5.0 
I.T 0.5^_ 
100.0 
l.r 0.02 
1.0 
l.r 0.02 
. 
5.0 
br_().oi6_ 
5.0 
l.r 0.010 
0.2 
i.rj)j^05 
' - 0 
l.r 0.03 
5.0 
//////////////////////////ii/////i//////////////////////////////////////////////^^/^/^/^^^/^^^^^/y//^////^//yyy^y 
All 
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s t a l e d . 
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to 
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q u e s t i o n s , p l e a s e d o n o l h e s i t a t e to c a l l . 
RSL'dlh 
e n c I . 
If y o u h a v e a n y 
V e r y 
t r u l y y o u r :• , 
I N D U S T R I A L 
C O R R O S I O N 
H(;HT.,INC 
kycA:^J>y k>- kiZi^c-,.,&./ 
Rlclinnf S. I.evliie • 
k / / , 
Preaident 
^•^ 
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oc-
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p, 
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Iba e e / T i m e 
R e c e i v e d 
b y : 
( S i g n . ) 
O a c e / l ' l n i r : 
Rec e i v e t i 
by : 
K S i g n . ) Da ce / T i m e 
R c i i n q u i s h e a 
by : 
(. S i g n . ) 
R e l i n q u i s h e d 
b y : . ( S i g n . ) 
R e c ' d 
by 
L a b o r a c o r y 
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f o r 
f i e l d 
a n a l y s i s 
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D i s p a c c h e d 
b y : 
( S i g n . ) 
D a c e / T i m e 
R e c ' d 
f o r 
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par. e / T i m e 
b y : n. {j. f u<—-
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301704 
'V^^fl?(^ <k^o6 Pry 
C y - I 
18 CC*^LANO TO.. D€MVIU-E. NEW JtSSEY 07JJ4 
CHAIN OP CUSTODY RECORD 
Installacion:^^^^ ^ ^ k ^ r ^ ^ y k ^ ^ / i ^ 
Survey No . : 
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Saaplers: (Signature) 
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Relinquished by: (Sign.) 
Rei.inquis2ie^d. by: C Sign . ) 
Received by: (Sign.) Date/i 
Reiinquisned by: (Sign.) 
Received by: (Sign.) Dace /-
Relinquished by: (Sign.) 
Received by:(Sign.)Dace/ 
Rec'd by Laboracory (Dace/ 
for field analysis 
(Sign.) 
Dace/Time 
R e c ' d 
f o r 
L a b o r a c a r y 
Method 
of 
S h i p m e n t : 
77 
D a c e / 
301705 
(^. .iir ,' 
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CHAIN OP CUSTODY RECORD 
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Installation: y ^ 
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Survey No . : 
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Station Location 
Samplers: (Signature) 
Date 
Tiae 
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RexinquiS'hea by: (Sign. ) 
Rexinquisnea by: (Sign.) 
Relinquished by: (Sign.) 
•yy y y 
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^ y y 
Dispatched by: (Sign.) 
Received by: (Sign.) Date/Tiae 
Received by: (Sign.) iDate/Tiae 
Received by: (Sign.) Dace/Tiae 
Rec'd by Laboracory 
Date/Tiae 
for field analysis 
(Sign.) 
Date/Tine Rec'd for Laboratory 
by' 
Mechod of Shipment: 
D a t e / T i c e 
<v ^ y . 
301706 
. I / - M 
LU 
CO. ..-iOSION 
MANAGEMENT 
INCORPORATED 
NJDE? C^.r:. .ed Drir.kir.s V£r = r/:;£s:2--a: 
Laboracory ID;/ 14116 
REPORT DATE: Mav 2. 1986 
LA3 f?. 5 3581 
1152 SCUTE 10. RANOOlPH. NEW JESSEV 07369 
201-53--0230 
CLIENT: 
E^TVIRO SCIENCES INC - I s l a n d Cher.ical 
P r o j e c t 
SA:-1?LE SOURCE: 
Tank U 
SAINPLE DATE: March 12, 1986 
TAKEN 3Y: A. Kvles AT LAB DATE: y.arch 20, 19:6 
LABORATORY ANALYSIS 
REPORT 
=ARA:-!E-ER 
RESULT 
Eenzoauinone 
30' 
siuorenone 
70% 
If you should have any quescions, please do not hesicace co call. 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
(ichard S./Lev^fie 
Presidenc 
RSL:dlh 
301'70'7 
INDI TRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROUTE 10. RANDOLPH. NEW JERSEY 07869 
201-3J4-O230 
iVJDE? Cercified Drinking Vacar/^Cascavata; 
Laboracory IDi-' 14116 
REPORT DATE: M.av 2. 1986 
LAB it 53582 
CLIENT: ENVIRO SCIENCES INC. - Island Cheaical Proiect 
SAMPLE SOURCE: Tank 7 
SAMPLE DATE: March 12, 1986 
TAKE:'; 3Y: A. Kyles AT LAB DATE: :-terch 20. 
.A-BORATORY .ANALYSIS 
REPORT 
?.i^A:-!ETER 
RESLT-T 
Benzophenone — 
Fluorenone 
Unknown Alkane 
39.6" 
43.8" 
16.62 
If you should have any quescions, please do not hesitate to call. •'; 
INDUSTRIAL CORROSION M.ANAGEMENT, INC. 
Richard S. 
President 
.eve;ne 
RSL:dlh 
. - •-*! - .r-
301708 
INDU^.RIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDE? Certified Drinking Vaca: 
Laboracory ID;/ 14116 
REPORT D.ATE: Mav 2, 1986 
LAB it 
53533 
•>aj cava car 
1152 ROUTE 10. RANOOLPH. NfiV JERSEY Q73S9 
201-52<S-O320 
CLlENT: 
Ey.'IP.O SCIENCES INC. - Island Cheaical Proiect 
SAMPLE SOURCE:- Tank 
SA_MPLE DATE: 
March 12. 1986 
TAKEN BY: A. Kvles AT LAB DATE: 
M=rch 20. 1^=6 
-ABORATORY .ANALYSIS 
REPORT 
P.AR.AMETE?. 
RESL'L'; 
Benzophenone 
Fluoenone -r— 
iD . / /. 
14.3% 
If you should have any quescions, please do noc hesicace co call. 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
Presidenr 
RSL:dlh 
301709 
y. J 
.UK; 11 r-ULLUirtiNi 
V U L A T i L t 
UKbnN. 
ANALYSIS 
LABORATORY ID #14116 
LAB i? 
53583 
PARAMETER 
Chloromethane 
Bromomethane 
Vinyl Chloride 
Chloroethane 
, 
Methylene Chloride 
1,1-Dichloroethene 
1,1-Oichloroethane 
Trans-1 ,2-Dichloroethene 
Chloroform 
1,2-Dichloroethane 
1,1,1-Trichloroethane 
Carbon Tetrachloride 
Bromodichloromethane 
1,2-Dichloropropane 
Trans-1,3-Oichloropropene 
--• 
Trichloroethene 
Dibromochloromethane 
1,1,2-Trichloroethane 
Benzene 
cis-V,3-Dichloropropene 
2-Chloroethylvinyl ether 
Bromoform 
Tetrachloroethene 
1,1,2,2-Tetrachloroethane --• 
Toluene 
Chlorobenzene 
Ethylbenzene 
Total Xylenes 
*Dichlorobenzenes noc analyzed under chis mechod 
' CLIENT: ENVIRO 
SAMPLE SOURCE 
GC/MS Method 624* 
Tier II Deliverables 
_ 
SCIENCES INC. - Isla-r: 
Tank 8 
RESULT 
ug/ kg 
U 
U 
u 
U 
u 
u 
u 
U 
U 
u 
u 
TI 
n 
u 
TT 
u 
- u 
U 
u 
u 
u 
U 
u 
u 
8000 
u 
u 
u 
METHOD 
BLANK 
ug/kg 
U 
u 
u . 
T7 
rr 
TT 
T-
U 
IT 
U 
r' 
IT 
U 
tT 
u 
u 
u 
u 
u 
u 
u 
u 
u 
u 
2. 7J 
U 
U 
U 
Che-icai 
MDL 
ug..'kg 
100 
100 
1 nr\ 
ino 
1 on 
100 
• '"r i ' 
100 
1 on 
lOQ 
1 on 
• ^ 
1 no 
100 
100 
100 
100 
100 
100 
-
100 
.100 
100 
100 
100 
. 
100 
100 
100 
100 
100 
Analyzed by GC/MS Mechod 625. 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
301710 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
U52 ROUTE 10. RANDOLPH, NEW JERSEY 07869 
201-58-:-0230 
NJDE? C a r c i f i e d 
Drinking 
Wacar/Vascavace: 
Laboracory ID;/ 14116 
REPORT DATE: 
Mav 2, 
1986 
LAB •? 
53584 
CLIENT: 
EN'VIRO SCIENCES INC. - I s l a n d Cheniical Proiect 
SA:-IPLE SOL-RCE: 
Tank 9 
SAI-:PLE DATE: March 12, 1986 
TAKZN BY: A. Kvles AT LAB DATE: March 20. 19S6 
LABORATORY ANALYSIS 
REPORT 
'.IRAI-IETER 
RESLT.T 
p-Pheneridine 
89. 1% 
Unknown arcsacic M'.v'=217 
10.9% 
If you should have any quescions, please do noc hesicace co call. 
INDUSTRIAL CORROSION MANAGEMENT, INC 
Richard S .^Lavine 
President 
RSL:dlh 
301711 
# 
lh l'j 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
REPORT DATE: Mav 2, 1986 
LAB it 53589 
1152 ROUTE 10. RANCOLrH. HVN JERSEY 07859 201-:a4-02;0 
CLIENT: 
E^TVIRO SCIENCES INC. - 
I s l a n d 
CheTnical 
P r o i e c t 
SANIPLE SOURCE: 
Tank 
U 
LABORATORY .ANALYSIS 
REPORT 
P.ASAM-ETER 
RESULT 
Benzophenone 
64.8% . 
Fluorenone 
35 . 2% 
If you should have any q u e s c i o n s , p l e a s e do noc h e s i c a c e to 
c a l l . 
INDUSTRIAL CORROSION M-ANAGEMENT, INC 
Rf chard S. LflZiii& 
P r e s i d e n t 
RSL:dlh 
(3 
NJDE? Carcified Drinking Wacer/Vascevaca: 
Laboracory IDi/ 14116 
SAMPLE DATE: March 12, 1985 
T.AKZ:'; BY: A. Kvles 
AT LAB DATE: March 20, L = = -
301712 
ts^ 
/ 
^ ,• y / 
r - t 
C H A I N OF 
C U S T O D Y 
'j:r>c : ^ sczTtCZS inc. 
> • • - ' • • " • 
3 6 6 - 6 2 5 5 
Sena 
fleoprt 
To: y ^ y y ^ ^ J c y j y ^ C t ^ 
y y y y c r x 
. u i l a t i tion: 
ySCiP^y/y 
y/yyyyryen,^ 
<^c-yjr<S<Zy) 
..Tiolinq Series: 
(ZAiy.'-t.J yct-r/tr,.-^ 
Samoieris) 
Nane: 
y<<:r:^y y . yr^yy.-
I b i g r a :ij.-s: 
X:.. y yz-^. 
y y ^ t ^ y f f y ^ 
mole Identification Samoli ng 
Location Point 
Samel ing 
Gate 
Samoling 
Time 
Samole Tyoe 
Analysis 
Come. 
Graa 
Recuirec 
No. C I 
v-cr. ; a i n e r s 
<' ."/<-
9 ^ 
/yy^AA f'Z 
/<p-/2. y>^ 
y 
/<i-
/ 
y.d~ I 
'' p 
1 
1 
ry 
' / 
\ 
j 
^ y ' AO 
1 
1 
'/ 
1 
t 
! 
- 
1 
X 
y 
y 
\c<?~ .J,(X— 
1 
/ 
\ A ^ .z<y 
^ 
\. 
£ 
i 
/ 
! 
'^ 
/ / 
/ / 
/<? 
A^ 
y. 'i'/-
^/ /<y 
• 
< i 
oy.Tiy 
eiinauisnea 3y: CSign.3 
;eiincuisnec 3y: CSign.] 
Receivea 9y: CSign.] 
Gate/Time 
1 
1
Receivea By: CSign.] 
Date/Time 
leiincuisnec- To L a o o r a t o r y ay: (Sign.3 
Receivea For Laboratory Sy: (Sign.) 
C ate/Time 
4 e i n o a Of 
Relincuisr.ment: 
Name Of Laooratory: 
ANALYSIS Rg.QUIPgD 
out cooe m prooer column] 
Priority ooilutant^--lO: 
Petroleum hyarocaroons: 
Volatile organics CGC]: 
Volatile organics CGC/MSh 
,Cyanides: 
CODE 
I 
ANAL'^'SIS 
CCCS 
i 
A N A L ' ^ S I S 
COOE 
I 
ANAL'^SiS 
CCCE 
01 
02 
03 
( ^ 
05 
Nickel: 
Chromium: 
Arsanicr 
Coooer: 
Laad: 
Mercury: 
Antimony: 
06 
07 
08 
09 
10 
1 1 
12 
Zinc: 
Cadmium: 
Selenium: 
Silver: 
Barium: 
COO: 
BOO: 
13 
14-
IS 
IS 
17 
18 
19 
301713 
^01 
PRK FY POLLUTANT VOLATILE ORGANIC / 
LABORATORY ID il4116 
LAB it 53362 . 
.YSIS 
r 
CLIENT: E^rviRO SCIENCES - I s l a n d Che-
SAHPLE SOURCE 
0 8 5 - 2 5 1 - E S I 
'" ac 
GC/MS Method 624 * 
T i e r 
I I 
D e l i v e r a b l e s 
METHOD 
PARAMETER 
RESULT 
BLAMK 
MDL 
SPIKE 
DUP SPIKE 
RPD 
ug/kg 
ug/kg 
ug/kg 
Chloromethane 
u 
u 
lo 
200 
; Aj, 
33 
oromomethane 
L^ 
U 
10 
2-0 
19; 
?: 
Vinyl Chloride 
u 
u 
10 
156 
127 
. 
"tt~ 
Chloroethane 
u 
U 
10 
44 
LL: 
CQ 
Methylene Chloride 
u 
7 .:J 
10 
122 
lOL 
T ^ 
1 ,1-Oichl oroethene 
'• 
- 
u 
U 
10 
90 
9; 
T " ; 
1,1-Oichloroethane 
u 
u 
IQ 
90 
L-:6 
Tg^ 
Trans-l ,2-Dichlcroethene 
U 
U 
10 
105 
11: 
y _ 
Chloroform 
• 
U 
7.3 J 
10 
IQ6 
119 
1,2 
1,2-Oichloroethane 
U 
U 
10 
106 
132 
22 
1,1,1-Trichloroethane 
U 
U 
10 
112 
121 
7.7 
Carbon Tetrachloride 
U 
U 
10 
104 
131 
39 
Bromodichloromethane 
U 
U 
10 
98 
153 
44 
1,2-Oichloropropane 
U 
U 
10 
104 
116 
g 
Trans-1 ,3-DTChloropropene 
U. 
U 
10 
104 
12G 
L4 
Trichloroethene 
U 
U 
10 
125 
132 
4.7 
Dibromochloromethane 
U 
U 
10 
118 
137 
15 
,1 ,2-Trichloroethane 
U 
U 
10 
96 
125 
26 
Benzene 
- 
U 
2.0 J 
10 
' 100 
105 
^ _4_^ 
cis-1 ,3-0ich1oropropene 
U 
" 
U 
10 
10^ 
11= 
13 
2-Chloroethylvinylether 
U 
U 
LQ 
102 
119 
15 
Bromoform 
U 
U 
LQ 
98 
U4 
38 
Tetrachloroethene 
U 
U 
10 
114 
72 
45 
1,1 ,2,2-Tetrachloroethane 
U 
U 
10 
76 
58 
15 
Toluene 
U 
4.9J 
10 
102 
65 
44 
Chlorobenzene 
U 
U 
10 
104 
116 
11 
Ethylbenzene 
- 
U 
U 
10 
114 
110 
• _3_J 
Total Xylenes 
- 
— 
U 
U 
10 
130 
115 
12 
*Dichlorobenzenes noc analyzed under chis mechod. 
Analyzed by GC/MS Mechod 625. 
3 01714 
1 • f. i'l 
PP'ORITY POLLUTANT VOLATILE ORGANIC ANALYSIS 
LABORATORY ID #1 41 U 
LAB # 53363 
CLIENT: ENVIRO SCIENCES 
Island Cha-ic2! ?: 
SAMPLE SOURCE 
085-252-ESI 
GC/MS Method 624* 
Tier I I Deliverables 
PARAMETER 
Chl oromethane 
Bromomethane 
Vinyl 
Chloride 
Chloroethane 
Methylene Chloride 
• 
1 ,1 -Dichloroethene. 
1 ,1-Oichloroethane 
Trans-1,2-Dichloroethene 
Chloroform 
1 ,2-Dichloroethane 
1 ,1 ,1-Trichloroethane 
Carbon T e t r a c h l o r i d e 
Bromodichloromethane 
1 ,2-Oichloropropane 
Trans-1 ,3-Oichloropropene 
. 
Trichloroethene 
Dibromochloromethane 
'• 
. 
1,1 ,2-Trichloroethane 
Benzene 
, 
cis-V,3-Dicnloropropene 
2 - C h l o r o e t h y l v i n y l ether 
= 
Bromoform 
Tetrachloroethene 
1 ,1 ,2 ,2-Tetrachloroethane 
^ 
Toluene 
Chlorobenzene 
Ethylbenzene 
Total Xylenes 
*Dichlorabenzenes noc analvzed under chis mechod. 
RESULT 
ug/kg 
u 
u 
153 
HETriOD 
BLANK 
ug/kg 
u 
f * 
U 
y 
7 07 
4.9-
MDL 
; g 
; Q 
To" 
10 
10 
• c 
To' 
IQ 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
Analyzed by GC/MS Method 625. 
301715 
-^ 
PP^ORITY POLLUTANT VOLATILE ORGANIC ANALYSIS 
LABORATORY ID 11411. 
LAB i 53364 
CLIENT: zyviRO SCIENCES - Icland C-^-ical ?-
SAMPLE SOURCE 85-252-E5I 
k__ 
GC/MS Method 624* 
Tier II DelIverabl es 
PARAMETER 
Chloromethane 
Bromomethane 
Vinyl 
Chloride — 
Chloroethane 
Methylene Chloride 
1 ,1-Oichloroethene 
1 ,1-Dichloroethane 
Trans-l ,2-Dichloroethene 
Chloroform 
1,2-Dichloroethane 
1 ,1 ,1-Trichloroethane 
Carbon Tetrachloride 
Bromodichloromethane 
1 ,2-Dichloropropane 
Trans-l,3-Dichloropropene 
-
Trichloroethene 
Dibromochloromethane 
1 ,1 ,2-Trichloroethane 
Benzene 
cis-V,3-Dichloropropene 
2-Chl o r o e t h y l v i n y l e t h e r 
Bromoform 
Tetrachloroethene 
1 ,1 ,2 ,2-Tetrachloroethane 
Toluene 
Chlorobenzene 
— 
Ethyl benzene 
— 
Total Xylenes 
*Dichlorobenzenes not analyzed under chis mechod. 
RESULT 
ug/kg 
S.-3 
U 
4.4B 
U 
2.SJ 
U 
HETriOD 
BLANK 
ug/kg 
T: 
"JHT 
4.9J 
MDL 
10 
10 
10 
10 
10 
•0 
JJL 
JJL 
l.Q 
10 
10 
10 
10 
- 10 
10 
10 
10 
10 
10 
10 
10 
10 
Analyzed by GC/MS Method 525. 
301716 
. 1 
. \ j r : . ' i i 
PULL'J I rtit I VQLATiLE 
ORGAN" 
LABORATORY ID #1 41 ,, 
LAB i 
53365 
ANALYSIS 
CLIENT: ENVIRO SCIENCES - Island Che=ical Pro-
SAMPLE SOURCE 08?-2' •-3i-
e.c: 
GC/MS Method 624* 
Tier II Deliverables 
, PARAMETER 
Chloromethane 
Bromomethane 
Vinyl 
C h l o r i d e 
• 
Chloroethane 
Methylene Chloride 
• 
1 ,1-Dichloroethene 
1 ,1-Dichloroethane 
Trans-1 ,2-Dichloroethene 
; 
Chloroform 
1 ,2-Dichloroethane 
1 ,1 ,1-Trichloroethane 
Carbon Tetrachloride 
Bromodichloromethane 
1,2-Dichloropropane 
Trans-l,3-Dichloropropene 
; 
, 
Trichloroethene 
Di bromochloromethane 
1,1 ,2-Trichloroethane 
Benzene 
• 
ci s-l",3-0ichl oropropene 
2-Chl oroethyl vinyl ether 
—'• 
Bromoform 
Tetrachloroethene 
1 ,1 ,2 ,2-Tetrachloroethane 
Toluene 
Chlorobenzene 
Ethyl benzene 
• 
Total Xylenes 
*Dichlorobenzenes noc analvzed under this method. 
RESULT 
ug/kg 
U 
a 
Q T5 
METHOD 
BLANK 
ug/kg 
U 
2.0J 
4 Q T 
MDL 
10 
1 n 
To" 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
10 
Analyzed by GC/MS Method 625. 
301717 
r-k 
Tk\ 
''RITY POLLUTANT VOLATILE ORGANI--
LABORATORY ID #14116 
LAB # 53366 
NALYSIS 
PARAMETER 
Chloromethane 
Bromomethane 
Vinyl Chloride 
Chloroethane 
Methylene Chloride 
1,1-Oichloroethene 
1,1-Dichloroethane 
Trans-l ,2-Dichloroethene 
Chloroform 
1,2-Dichloroethane 
1,1,1-Trichloroethane 
Carbon Tetrachloride 
Bromodichloromethane 
1,2-Oichloropropane 
Trans-l ,3-Oichloropropene --• 
Trichloroethene 
Dibromochloromethane 
1,1,2-Trichloroethane -• 
Benzene 
cis-V,3-0ichloropropene 
2-Chloroethylvinylether 
Bromoform 
Tetrachloroethene 
1,1,2,2-Tetrachloroethane — 
Toluene 
Chlorobenzene 
Ethylbenzene 
Total Xylenes 
*Dichlorobenzenes noc analyzed under chis method 
CLIENT: ENVIRO SCIENCES - I s l a n d Che---; , 1 
o - . . .; 
SAMPLE SOURCE 0 8 5 - 2 5 5 - E S I 
GC/MS Method 
6 2 4 * 
T i e r 
I I 
D e l i v e r a b l e s 
RESULT 
ugAs 
U 
JJ 
_ _ . « . M « . ^ . . _ _ _ ^ . . 
TT 
. . — — — .— ».» — — * . * . . _ 
TT 
„ 
,.,3 
'.„• 
., 
^ 
L 
— / —. 
3 . a a 
, 
"~~ 
" " 
u . 
u 
L 
~ " ~ 
]j 
u 
- - - - - - - - - - - - - - - - 
^ 
u 
. - - - - - - . _ . _ - - . . - 
u 
. _ - 
y 
- - — - - - - _ _ - - - - _ _ - 
jj 
- - - - - - - - - - - - - - - - 
y 
— — — — — — — — — — — — — — — — 
TT 
- - - - - - - - - - - - - - - - 
\J 
— — — — — — — — — — — — — — — — 
TT 
— — — — — — — — — — — — — — — — 
TT 
— — — — — — — — — — — — — — — — 
TT 
- - - - - - - - - - - - - - - - 
u 
. — — — — — — — — — — — — — — — — 
7T 
. - - - - - - - . - - - - - - - - 
n 
METHOD 
BLANK 
ug/kg 
IJ 
U 
'A 
: . 2.., 
w 
z 
i j 
7 . 3 J 
U 
;• 
TT 
:: 
:T 
U 
TJ 
U 
2 . 0 J 
u 
U 
U 
U 
u 
4 . 9 J 
U 
U 
U 
MDL 
" n 
• 0 
^ ' j 
• ~ 
• 
10 
IG 
. 
,-v 
10 
10 
10 
10 
10 
10 
10 
10 
•-' 10 
10 
10 
10 
10 
10 
10 
10 
10 
Analyzed by GC/MS Mechod 62; 
301718 
C H A I N OF C L ' S T C D Y 
lAO-^Ozz-' 
' • i i ^ i ^ w ^ 
3 6 6 - 5 2 5 5 
m0amm>m^m 
Send Reo.ort 
T o : '• y ^ ^ y 
y./Ay 
y<Ay 
' i l l a t i o n : 
m o l i n g S e r i e s : 
y ^ y - y 
/ / C y y f 
SamolerCs) 
N a m e : 
2 1 5.-;a ture: 
/ ^ £ V / y<k/yc^ 
^ . . / 
m o l e iGenti f ica tion 
S a m o l i n g 
L o c a t i o n 
P o i n t 
S a m o l i n g 
Gate 
S a m o l i n g 
T i m e 
S a m o l e 
Type 
C o m ; 
Grao 
A n a l y s i s 
R eouirec 
- y - y . y / - ^ - ^ . 
(Aiy. y z 
/^y/k/jz I ^ y ^ 
> 
<r^ 
' - - ^ ^ C 2 
A^yr- Z^-y 
yy 
y-zS'-
cS 
/ 
.y-
y y 
cc 
X 
cy. 
N o . C ! 
C c . - : a i n e r s 
y 
y 
A^ 
-y-^s^-yzr 
'y-s-r-yr 
y.yiyk/^ 
y y - y y 
y 
^y 
y y<: 
^ y c 
1 ^' c ^ 
1 ^ V$. z^ 
e i i n o u i s n e o 
3 y : 
( S i g n . ] 
A N A L V S I S 
PEOUIRED 
out c o o e in p r o o e r 
c o l u m n ] 
P r i o r i t y 
pollutant+-"iO: 
P a t r o i e u m 
h y d r o c a r o o n s : 
V o l a t i l e o r g a n i c s CGC]: 
V o l a t i l e o r g a n i c s CGC/MS]: 
C y a n i d e s : 
1 
F 
COOE 
0 1 
°Sr 
^ j ^ 
(o>^ 
QS 
_ 
_ 
A N A L Y S I S 
N i c k e l : 
C . l r o m i u m : 
A r s a n i c r 
CoDDsr: 
L a a d : 
M e r c u r y : 
A n t i m o n y : 
CODE 
06 
07 
08 
09 
10 
11 
12 
A N A L Y S I S 
Z i n c : 
C a d m i u m : 
S a l a n i u m : 
S i l v e r : 
B a r i u m : 
1 COO: 
B O D : 
COQ£ 
13 
14-
IS 
16 
17 
18 
19 
ANALYSIS 
TSS: 
TCS: 
pH: 
P C 3 : 
Otner: 
CSoacify) 
c-z^ j 1 
20 
2.1 
22 
1 
23 
24. 
,01719 
C H A I N OF 
C U S T O D Y 
yk.^ - k y 
7 
•jir« ^ 
-csi-vc^ \ nc. 
• 6 2 5 5 . 
s t a l l a t i o n : 
/ T ^ r : ; ^ ^ 
y/A''-<Zyy/Cy/.^ A Z 
/ A y ^ y ) 
(- — - _ y 
i m o l i n g S e r i e s : 
C / V 7 
/ y C y y 
i m o i e 
I d e n t i f i c a t i o n 
- : 7 - ^ r y y A r 
^.r-.yr2-yfZy 
r..''z:>r3-y^.T 
•:---'-r-2r<-<sy 
y.r- yrr-r^sr 
) 
S a m o l i n g 
L o c a t i o n 
P o i n t 
yyyy 
1 
^ ; ^ , y y 
S a m o l i n g 
Gate 
y ^ yyyy.f/A 
/ y 
y y - y ^ c 
yr^ 
y -
y r ^ 
y y -
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^ e l i n q u i s n e o 
3 y : 
( S i g n . ] 
Send R e o j r t 
T o : 
y / ^ 
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N a m e : 
i S . g r a f j r e : 
/z^^z^ y y^ycci^ 
S a m p l i n g 
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/ y y / j y 
A:yy...-. ... 
y-sc.:....., 
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y * y t 
y y / 
y ^ ^ 
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— 
1 
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— 
) 
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CSign.] 
C a t e / T i m e 
T e linQui s n e o ' 3y:^>iS,ign.] 
| R e c a i v e d 
By: 
( S i g n . ] 
i C a • e / ' T i m e 
^;7/;c./-^ 
R e i i n a u i s n e c 
To L a o o r a t o r y Sy: 
( S i g n . ) 
R e c e i v e d For L a o o r a t o r y 3 y : 
( S i g n . ] 
l a t e / T i m e 
M e i n o o 
Ot 
R e l i n c u i s n m e n t : 
N a m e Ot 
L a o o r a t o r y : 
A N A L Y S I S 
REOUIREO 
CODE 
( c u t c o o e 
in p r o o e r 
c o l u m n ] 
P r i o r i t y p o l l u t a n t 4-40: 
0 1 
P e t r o l e u m h y d r o c a r o o n s : 
02 
V o l a t i l e o r g a n i c s (GC]: 
03 
V o l a t i l e o r g a n i c s ( G C / M S ] : 
04 
C y a n i d e s : 
QS 
A N A L Y S I S 
COCE 
I 
A N A L ' ^ S I S 
N i c k e l : 
C J i r o m i u m : 
A r s e n i c r 
C o o o e r 
L e a d : 
M e r c u r y : 
A n t i m o n y : 
06 
07 
08 
09 
IQ 
1 1 
12 
Zinc: 
Cadmium: 
S a l a n i u m : 
S i l v e r : 
B a r i u m : 
C O O : 
B O O ; 
CCCE 
13 
14 
I S 
16 
17 
18 
19 
A N A L ' 
TSS: 
T C S : 
p H : 
P C S : 
O t n a r : 
( S o a c i f y l 
y^<r^- y^p.rrcL. Oy.f^ 
20 
2 1 
22 
2 Z _ 
" 2 4 " ; 
301720 
o 
-J 
to 
:ei'i 
INDUSTRIAL 
CORROSION 
MANAGEMEhrr 
INCORPORATED 
K'JOCP C e r t i f i e d Drir.king Wa I er/WcS I ewal er 
Laboratory 
10 /('I'll 16 
RtPCjRT DATE :_.. Hay 2, . l'Jli6 _^ 
LAB i' 
_ 5r)62 
'^1^'E''"'": 
ENVIRO _SGIENCES_INC^=J:ilimci.Chcoilcal.l'rn.1er.t_ — 
SAKPLE SOURCE: 
085-251::ESI 
SAMPLE DATE:„ 3/1.3/86 
SAhPLED OY: 
Al_!<yleH 
AT LAB DATE: 
:i/17/06 
ACID 
EXTRACTABLES 
PRIORITY 
POLLUTANTS 
+ hO 
_b y.-G C./.M S -LI Q. P £ £ K S 
ACID EXTRACTABLES PRIORITY POLLUTANTS + 10 Peaks 
2-chlorophfcnoI 
'2-ni t j-ophenol - - 
- -
phenol 
2,'i,-dimethyIphenol 
2 , * » , - d i c h l o r o p h e n o ! 
pentachlorophenol 
2,'l-dinl t rophenol 
'(.S-dinl 1 r c - o - c r e s o l 
— 
'l-nl t rophenol 
- 
- -
2 , ' t , 6 - t r l c h l o r o p h e n o l 
- -
k-ch)oro-'i melhyl 
phenol 
_33ni)_ 
33011 
_ 3 3 0 i r 
_33QfL 
_330!L 
.165niJ_ 
i^SOiL 
_330ll_ 
_33QIL. 
S'.IKItOCATE UI'.(:OVI-.l<rES 
2 - l ' l iii)r|)liciui I 
P h e n o L-(I5 
2, /(, 6-Tr Ihroiiioplicnr)] 
Ali^'^ 
S O . b X 
5 0 . U 
All r e s u l c s are r e p o r t e d In ug/l<g(ppl)) dry weight 
b a s i s . 
INDUSTRIAL 
CORROSION hAKAGCHENT, 
INC 
.''''yl yW.'^. 
. / l . f V i IIU 
RSL: dlh • 
L T - l e s s 
T h a n 
ND'h'ot Pet ec ted 
Pri'i Idcnt 
rC 
LO 
O 
H 
to 
to 
• I I 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
ni; »D.'n If. UNDD.Prt. wrw j|RSf» a m ?c- sutuo 
l.'JDLP C c i t i f i t - d D r i n k i n g Wa t er/Wa s t ewa I er 
Laboratory 
ID /f Mi 1 16 
REPORT DATE:. Miiy 2,._|'J(!f). 
LAB (i'__531(>J 
. 
CL I ENT:_|^Hyj|{n_SCIENCES_INC..-r-Ialand.Chem lr.il l-Prn.|er.L_... 
SAKPLE SOURCE: 
n85-252-EST 
SAKPLE DATE:_3Zl2/56 
SAhPLED BY: _ . 
.A.,_ Kyles. 
AT LAB DATE: 
.3/1 7/1! fi. 
ACID 
EXTRACTABLES 
PRIORITY 
POLLUTANTS + 'i 0 
_b.Y._GC7.H5,-LlO_PEAKS 
_AClD_E>(TRACTABLES_PR!ORITY_POLl,yTANTS 
2 - c h l o r o p h e n o l 
- 
_330U 
2-ni t rophenol 
- - 
_33QU 
. 
phenol - 
_33QIJ_ 
2 , ' l , - d i m e t h y l p h e n o l 
- - _330ll 
2 , ' i , - d l c h l o r o p h e n o l 
_330IJ__ 
p e n t a c h l o r o p h e n o l 
- 
J650n 
2 , J j - d i n l t r o p h e n o l 
- 
.16501J 
i t i f i - d i n l i r c - o - c r e s o l 
- 
- 
J^SOU 
^i-nl t r o p h e n o l 
- - .1650IJ_ 
2 , ' « , 6 - t r i c h l o r o p h e n o l 
- 
_ 3 3 n u _ 
^i-chloro-j methyl phenol 
_ 3 3 Q U _ 
All results are reported In iig/kg(ppb) dry weight bnsls. 
KSL: 
L T = L e s s 
T h a n 
ND=Not 
D e t e c t e d 
S'.lKKnnATEJUjCnVEUT E.S 
2-l''lii(iroph(!n()l 
9fl. 5% 
I'lien()l-d5 
7R.8Z 
2,'!i , 6 - T r Ibromoiilicnol 
90.6% 
INDUSTRIAL 
CORROSION MANAGEMENT, 
INC 
R l c » i a t d 
S . 
P r e s i d e n t 
n 
INDUSTRIAL 
CORROSION 
MANAGEMEfJT 
INCORPORATED 
o 
l-« 
to 
NJDLP C f c f t i f i t d O i i n k i i u j Wa t er/Was t ewa I er 
I a b o r a i o r y 
ID /M'i I 16 
REPORT DATE:.M.iy. 2, 
!0)i6 
LAB H yVUi'i 
•^l-IENT: 
EHVIRQ.SGIENCES_INC.-.-_Ibland.Chemica I-Prnject.. 
SAKPLE SOURCE :_85rl52-ESI 
; 
SAMPLE DATE: 
3/J3/86 
SAMPLED BY: 
A^,..I<ylea 
AT LAB DATE :._.;_ 3/!.7/fj6. 
ACID 
EXTRACTABIES 
PRIORITY 
POLLUTANTS 
+ kO 
_bY._CC7M5.t:l.Q_P.[£KS 
ACID EXTRACTABLES PRIORITY POLLUTANTS + 10 Peaks 
2-chlorophenol - 
--
2-nitrophenol 
phenol 
2,'*,-dimethylphenol 
2,'i,-dichlorophenol 
pentachlorophenol -
2,'l-dini t rophenol 
V 6 - d i n l t r o - c - c r e s o l 
— 
^-nitrophenol 
2,'<,6-tr Ichlorophenol --
•t-chloro-B melhyl phenol 
33011 
330U 
33011 
330IJ 
330U 
_ 16.5 nil-
J65n!J_ 
J65Ql!_ 
165QU_ 
_J3QU_ 
__33QIL_ 
All results are reported in ng/kg(ppb) dry weight basis. 
R?L:dlh • 
LT = Le SS T h a n 
KD^Uot Detected 
.SIlHIiOCATl-: RECOVERIES 
2-I''l iioi'opheni) I 
Phenol (15 
All. 
52% 
2,/i, 6-Tr IbromoplienoL 
38^ 
OTIjER COMPOUNDS DI'TECTEI) APPROXTMATE CONnENTR_ATTONS 
Unknown liydroc.irlion peaks t o t a l l i n g 26 
7,700 
INDUSTRIAL 
CORROSION MANAGEMENT, 
INC 
Ul^Ci^^'^/[y/l/^^^i. 
H / r h i i f d 
S. 
I^LVJiic 
Presitltnt 
u 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
l i ; ; I.D.1I IC RtKHJ.IV. xfVi JlRSfl b U H 
?0- i l K i ' . U 
to o 
M 
to 
1 ^ 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID /f I'll 16 
REPORT DATE:... M')y 
' I L A ^ M . 
LAB ff 53365 
CL I ENT:_ENyiRO_SCIENCES_INC._r-Is land. Cliemical.Project 
SAMPLE SOURCE :__085-254-ESI 
SAMPLE DATE:_3/.13Z86 
S A K P I ED BY:, 
A._Kylea. 
. _ A T 
LAB D A T l : 
•)/!V/(!6_ 
ACID 
EXTRACTABIES 
P R I O R I T Y 
P O L L U T A N T S 
+ ^i 0 
_ b y _ _ G C y M S t ; I Q_PE£KS 
_ 
__ 
ACID EXTRACTABLES 
PRIORITY 
POLLUTANTS t 
10 Peaks 
2-chlorophenol 
2-nitrophenol 
phenol 
- ' 
2,'(.-dimethylphenol 
2,'4,-dichlorophenol 
pentachlorophenol 
2,'j-dini t rophenol 
'f.S-dinl t ro-o-cresol 
'j-nl I rophenol 
2 , ' i , 6 ' ' ' ' i c h l o r o p h e n o l 
- -
It-chloro-B methyl 
phenol 
33011 
l30ir 
33011 
_33Q!L 
_330U_ 
.1650LL 
.i65QU_ 
i6501L 
.I65QU_ 
! J } 3 Q I L 
S'.IRIIOCATE KECOVEKTES 
J3Q1L 
All results are reported in ug/kg(ppb) dry weight basis, 
2-El imroplioiii) I 
Pheiiol-(l5 
2 , /|, 6-Tr lbr(iiiiii|>lii:no1 
_^1 
51 
52 
8% 
5% 
INDUSTRIAL C O R R O S I O N M A N A G E M E N T , INC 
Richard S. / i v/ffe 
RSL: (ill, • 
L T = L e s s 
Than 
ND=Not Detected 
I'res Idem, 
\ '\ 
ih 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
l.'JDLP Certified Drinking Water/Wastewater 
laboratory ID /Tl'il 16 
RIPORT DATE:.. May. 2,_I'Jfi6_ 
LAB l/_^r\M 
CLIENT:_ENVIRQ_SQlENGEa_JNG.-_--l3land.Clieralcal..l'i-o.)ect, 
SAMPLE SOURCE : 085^255:iEST 
SAMPLE DATE:_3,n3/86 
SAMPLED BY: 
.A.;_Kyles._ 
.AT LAO DATE : _ J / ! 7 / f ] 6 _ 
ACID 
EXTRACTABLES 
PRIORITY 
POLLUTANTS 
+ 'i 0 
_byi._GcyMSi_|.Q..P.EAKS 
ACID EXTRACTABLES PRIORITY POLLUTANTS + 10 Peaks 
2-chlorophenoI 
2-nitrophenol 
phenol 
2,'i,-dimethyl phenol 
2 , ' ) , - d l c h l o r o p h c n o l 
pentachlorophenol 
2,'t-dini I rophenol 
A , 6 - d i n l t r o - o - c r e s o l 
it-nl t rophenol 
2,*(,6-tr Ichlorophenol 
--
l|-chloro-3 methyl 
phenol 
_330!!_ 
33011 
_33Ql!_ 
-_33QLL 
_33QU_ 
_1650li_ 
_[650ll_ 
J 6 5 0 t J _ 
_i65Qli_ 
330ll_ 
33011 
All results are reported in ug/kg(ppb) dry weight basis 
.SUR KOC ATE RECOVERIES 
2-El iiropluMio 1 
IMieiH)l-(l5 
2, ' i , 6-Tr I Uniniophennl 
98.2Z 
96.57. 
INDUSTRIAL CORROSION M A N A G E M E N T , INC 
u> 
o 
M 
to 
( J l 
I 
RSL: (llll • 
. L T = L e s s 
T h a n 
h'D=Not 
D e t e c t e d 
_ £^'^.y'^A/iAy'.-
Rlch^rd S. 
\ k \ \ k 
President A^ 
r 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROUt£ 10, SANOOLPH. .NEW JE.=?S£Y 07859 20l-5a4-033Q 
CL1£NT: 
ENVIRO SCIINCES 
INC. - 
I s l a r . d 
CheT-.icaL 
P r o - J e r t 
NJD£.= C e r t i f i e d 
D r i n k i n g 
W a t e r / 
Wascewacer Laboracop/ 
10 ^ U l l S 
REPORT DAT^: 
Mav 2. 
1986 
LAB I 
53363 
SAMPLE SOURCE: 
OS5-2f2-ESI 
SAMPLE DATE: 
3/L3/36 
SAMPLED 3Y: 
Kvles 
.AT LAB DATE:. 
BASE/NEUT-RAL E.XTRACTA8LES PRIORITY POLLUTANTS •*- kQ 
bv 
GC/MS 
+ 15 PEAKS 
Pa ra.T.ecer 
aceneohc^iene 
acer.acncny 1 e.'^.e 
anchracene 
. benzidine 
benzo (a)an cr.racene 
benzo{a) py rep.e 
3 , i4-ben2of lucran chene 
benzo (gi^ I ) pery 1 ene 
benra(!<.) f l u o r a n t h e n e 
bis(2-chlorQechoxy)mechane 
b i s ( 2 - c h I o r o e t h y i ) e t h e r 
bi s ( 2 - c h 1 o r o i s o p r o p y l ) e t h e i 
b ! s ( 2 - e t h y i h e x y l ) p h t n a l a c e 
i4-bromopheny I phenyl 
e t h e r 
butyibenzy! 
p h t h a l a t e 
2 - c h l o r o n a p h t h a l e n e 
ii-chl oropheny I phenyl 
e t h e r 
chrysene 
d ibenzo(a ,h)anthrace.ne 
1 , 2 - d i c h l o r o b e n z e n e 
1 ,3-cii chl orooenzene 
1 , i^-d ichl orobenzene 
3,3-d ichlorobenz i d i n e . 
Resul r 
--r\\t 
'^^!(1r• 
',01! 
.Resul t 
Pa rameter 
-:;0U 
diethyl phthalate 
Z'ZZ'Z 
dimetnyl phthalate 
;.;.QU 
di-n-butyl phthalate 
'-.LlZ'l 
2,'4-d i n i t rotol uene 
'-QU 
2,6-dinitrotoluene 
J J O U 
di-n-octyl phthalate 
j.^ou 
1 ,2-di pheny I hydraz ine(as azobenzene)- ; A^n; 
330L' 
fluoranthene, 
-^-ni 
3~Grj 
fluore.n'e 
330U 
hexachlorobenzene 
330L' 
hexachlorobutadiene 
320;.' 
hexachlorocyclopentadiene 
330L' 
hexachloroethane r 
• 
33QL' 
_ indeno(l ,2,3"Cd)pyrene 
330U 
isophorone 
• 
33Q(j 
naphthalene 
• 
330U 
nitrobenzene 
330U 
N-nitrosodimethyiamine 
33QU 
N-nitrosodi-n-propylamine 
330U 
N-ni trosodi phenylami ne 
330U 
phenanthrene 
330U 
pyrene 
660L' 
I ,2,^-trichlorobenzene 
Of 
-;TOr-
ni-
TTHi' 
nt' 
33C'J 
330U 
330U 
33 OU 
330U 
3 30U 
SURROGATES 
LT=Less Than 
ND=Not Detected 
d5-Nitrobenzene - 84.0% 
2-Fluorob:i.phenyl -L13.0% 
it-Terohenyi-dU 
-123.IZ 
APPROXIMATE CONCENTRATION 
OTHER COMPOUNDS DETECTED 
All resulcs are reporced in ug/kg(ppb)dry weighc basis. 
INDUSTRIAL CORXOSION MANAGEMENT, INC. 
y y u ^ 
Stichard S. ;^v4rna 
Presidnec. 
RST.:H1h 
301726 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROUfi IQ. RANOQL.''H. .N£W llRSlI 073S3 
201 534.03;a 
CLIENT: 
ENVIRO SCIENCES INC. - I s l a n d Chenical Prr'-'ec-
NJOEP C e r t i f i t o 
D r i n k i n g 
' J a z t r / 
Wastewater 
L a b o r a t o r y 
ID 
;?U116 
REPORT DATE: 
Mav 2. 
1986 
LAS i 
53564 
SAMPLE SOURCE: 
85-252-ESI 
SAMPLE GATE: 
3 / 1 3 / 8 5 
SAMPLED 
3Y: 
A. Kvles 
.AT LAB DATE:. -: /' ZO 
BASE/NEUTRAL EXTRACTABLES PRIORITY POLLUTANTS ^ kC 
by GC/.'-,S 
+ 15 PEAKS 
Pa rameter 
aceneohthene 
ace-ac".:.-5y 1 ena 
anznrccene 
b e n z i d i n e 
• 
b e n z o ( a ) a n t h r a c e n e 
b e n z o ( a ) p y r e n e 
3 , ^ - b e n z o f l u o r a n t h e n e 
benzo(ghi)pery1ene 
benzo(k.) f l u o r a n t h e n e 
b i s (2-ch 1 oroethc.xy )methane 
- — -
b i s ( 2 - c h l o r o e t h y 1 ) e t h e r 
bi s ( 2 - c h l o r o i s o p r o p y l ) e t h e r 
b i s ( 2 - e t h y l h e x y 1 ) p h t h a 1 a t e 
4-bromopheny1 phenyl 
e t h e r 
b u t y l b e n z y l 
p h t h a l a t e 
2 - c h l o r o n a p h t h a l e n e 
4-chIoropheny1 
phenyl e t h e r 
chrysene 
d ibenzo(a,h)anthracene 
1,2-dichlorobenzene 
I ,3-dichlorobenzene 
1 ,4-dichlorobenzene 
3 ,3-dichlorobenz idine 
Result 
Pa rameter 
;30V 
diethyl phthalate 
] '-.'j'Z 
dimethyl phtnalate 
3 3 0U 
di-n-butyl pnthaiate 
1c;2U 
2,4-dinitrotoluene 
;30U 
2,6-dinitrotoluene 
3 J OL' 
di-n-octyl phthalate 
330U 
1,2-dipheny1hyarazine(as azobenzene)' 
33QL' 
fluoranthene 
3 30r 
fluorene 
330U 
hexachlorobenzene 
330U 
hexachlorobutadiene 
3 30L' 
hexachlorocyclopentadiene 
330U 
hexachloroethane 
330L' 
indeno(l ,2,3-cd)pyi'ene 
330L' 
isophorone 
3 30U 
naphthalene 
• 
330U 
nitrobenzene 
330U 
N-nitrosodimethyiamine 
330U 
N-nitrosodi-n-propylamine 
3301' 
N-ni crosodiphenylamine 
33QU 
phenanthrene 
330U 
pyrene 
6 6 ou 
1,2,^-trichlorobenzene 
Resu! : 
LT=Less Than 
N D = N G C Dececced 
SURROGATES 
nzene - 37Z 
phenyl- 70% 
dl4 - 58% 
d5-N i trobe 
2-r 1 uorob.i 
4-Terpheny 
nc 
^ n I • 
APPROXIMATE CONCENTRATION 
OTHER COMPOUNDS DETECTED 
All resulcs are reporced in ug/k.g(?pb)dry weighc basis 
^.nv 
T!(VI 
--.rw 
•>. tor-
Tin" 
-l-!0" 
rjoi 
330U 
330U 
330U 
330L' 
230U 
# 
INDUSTRIAL C0R;510SI0N MJ^LNAGEMENT, INC. 
ifi chard S . Le 
Presidnec 
y 
RSL:dlh 
301727 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 SOUlc 10. SANOOlPH. N£W )£,SS£Y 07369 
201-534-02;D 
CLIENT: 
EN^.'IRO SCIENCES INC. - Island Che'n-ical Pro^ecr 
NJDE? Certifiea Drinking Water/ 
Wastewater Laboratory ID ,^14116 
REPORT DATP: M.qv 2. '.9g6 
LAB a 
53365 
. 
SAMPLE SOURCE: -035-254-E5I 
SAMPLE DATE: 
5/15/86 
SAMPLED BY: 
A^ Kvles 
.AT LAS DATE:. 
le cer 
ocenesntnene 
ace.^.asn-ny 1 ene 
anc.Tracene 
ben2 id ine 
. 
b e n z o ( a ) a n t h r a c e n e 
benzo (a) py re.ne 
3 , 4 - b e n z o f l u o r a n t h e n e 
b e n z o ( g h i ) p e r y i e n e 
b e n z o ( k ) f l u o r a n t h e n e 
b i s ( 2 - c h l o r o e t h o x y ) n e t h a n e 
b i s ( 2 - c h l o r o e t h y 1 ) e t h e r 
—. 
b i s ( 2 - c h l o r o i s o p r o p y l ) e t h e r 
b i s ( 2 - e c h y l h e x y 1 ) p h c h a l a c e 
4-brcmophenyI 
phenyl echer 
butylbenzyl 
p h t h a l a t e : 
2 - c h l o r o n a p h t n a 1 e n e 
4-chlorophenY1 
phenyl 
e t h e r 
chrysene 
dibenzo(a,h)anthracene 
• 1,2-dichlorobenzene 
1,3-aichlorooenzene 
1 ,4-dichlorobenzene 
3,3-dichlorobenzidine 
BASE/NE'JTRAL EXTRACTABLES PRIORITY POLLUTANTS -r 40 
by GC/MS 
f 15 PEAKS 
Resulc 
Parameter 
3'C'L' 
diethyl phthalate 
.-3Of 
dimethyl phtnalate 
3 30L' 
di-n-butyl phthalate 
1-52U 
2,4-dinicrocoluene 
3 3GU 
2,6-ainitrotoluene 
3 30L' 
di-n-occyl phtnaiace 
330'j 
I ,2-di pheny I hydraz i ne(as azooenzene)' 
3 3G'j 
fluoranthene 
33QU 
fluorene 
330U 
hexachlorobenzene 
330U 
hexachlorobutadiene 
• 
330U 
hexachlorocyclopentadiene 
3 30U 
hexachloroethane 
330U 
indeno(l,2,3-cd)pyrene 
330U 
"isophorone 
330U 
naphthalene 
330U 
nitrobenzene 
330U 
N-nitrosodimethylamine 
330U 
N-nitrosodi-n-propylamine 
330U 
N-nitrosodiphenylamine 
3 30U 
phenanthrene 
330U 
pyrene 
iboOU 
1 , 2 , 4 - t r i c h l o r o b e n z e n e 
• o r -
nnr-
- O i : 
' 0 " 
10" 
: - > 0 r -
•:o,'-
T - n i ' 
'.Of 
33QU 
330U 
:0U 
330U 
3 30U 
SURROGATES 
LT=Less Than 
ND=Noc Dececced 
d5-Nitrobenzene 
- 37% 
2-Fluorobiiiphenyl - 69.7% 
4-TerDhenyl-dl4 
- 72.1% 
APPROXIMATE CONCENTRATION 
OTHER COMPOUNDS DETECTED 
A l l r e s u l c s a r e r e p o r c e d in ug/itgCppb) -dry weighc b a s i s . 
INDUSTS.IAL CORROSION MJ^NAGEMENT, I.NC 
Ri<fhard S. L/ev%e 
P r e s i d n e c 
RSL:dlh 
301728 
INDUSTHIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 .'?OUr£ 10. RANOCL.=H. ,V£W JERSEY Q7S69 
201-:3-t-0230 
CLIENT: 
EN'/IRO SCIEI^rCES INC. - I s l a n d Che:?.ical Pr?-!-
NJOEP C e r t i f . 
D r i n k i n g 
Wacer/ 
Wascewace.'- L a b o r a c o r / 
I0 f'I 4 1 1 £ 
K 
REPORT DATE: Mav 2. [ORn 
LAB # 
53366 
SAMPLE SOURCE: 085-255-ESI 
SAMPLE DATE: 5/15/56 
SAMPLED BY: 
A. Kvles 
.AT LAB DATE:. 
BASE/NEUTRAL EXTRACTABLES PRIORITY POLLUTANTS -r 40 
bv 
GC/MS 
+ 15 PEAKS 
:3GL 
3 50L" 
O Z -
Parameter 
Resul t 
aceneohthene 
3 30L' 
ac e.'^ a cn cny 1 e.".e 
_ 
anthracene 
_ 
benzidine 
_j 
b e n z o ( a ) a n t h r a c e n e 
•- _ 
b e n z o ( a ) p y r e n e 
_ 
3 , 4-benzof1uoranthene 
_ 
b e n z o ( g h i ) p e r y 1 e n e 
_ 
b e n z o ( k ) f l u o r a n t h e n e 
_ 
b i s (2-chloroethoxY)methane 
_ 
b i s ( 2 - c h l o r o e t h y 1 ) e c h e r 
_ 
bi 5 ( 2 - c h l o r o i s o p r o p y l ) e c h e i 
_ 
b i s ( 2 - e t h y l h e x y l ) p h t h a l a t e 
~ 
4-bromopheny1 phenyl 
e t h e r 
butylbenzyl 
p h c h a l a c e 
_ 
• 2 - c h l o r o n a p h t h a l e n e 
_ 
4-ch1oropheny1 
phenyl 
e t h e r 
c h r y s e n e 
_ 
d i b e n z o ( a , h ) a n t h r a c e n e 
1 , 2 - d i c h i o r o b e n z e n e 
1 , 3 - d i c h l o r o b e n z e n e 
1 , 4 - d i c h l o r o b e n z e n e 
3 , 3 - d i c h l o r o b e n z i d i n e 
Paramete.-
R e s u l c 
y y 
330U 
5 50U 
33QL' 
330U 
350U 
330U 
_120U_ 
?50u 
330U 
330U 
330U 
330U 
330U 
350U 
330U 
330U 
660U 
diethyl phthalate 
--
dimethyl phthalate 
di-n-butyl phthalate 
2,4-dini trotoluene 
2,6-dini trotoluene 
di-n-octyl phthalate 
1,2-diphenyihydrazine(as azobenzene)' 
fluoranthene 
fluorene 
hexachlorobenzene 
hexachlorobutad iene 
hexachlorocyclopentadiene 
hexachloroethane -' 
• 
indeno(l,2,3-cd)pyrene 
i sophorone 
naphtha 1ene 
ni trobenzene 
N-ni trosodimethyiamine 
N-n i trosod i-n-propylami ne 
N-ni trosod iphenylamine 
phenanthrene 
pyrene 
' 
1 ,2,4-trichlorobenzene 
-.r:-
.-,-\r 
_2-lQiL 
J2Q1 
T;ni; 
3~,nr-
"'Or.-
~-.0r: 
3 5QU 
5JOU 
33QU 
5 30U 
3 3QU 
350U 
LT=Less Than 
ND=Noc Dececced 
SURROGATES 
d5-Ni trobenzene 
2-r ] uorob^ipheny I ] no surrogaces added 
4-Terpheny1-dl 4 
APPROXIMATE CONCENTRATION 
OTHER COMPOUNDS DETECTED 
All resulcs are reporced in ug/kg(ppb"*dry weighc basis. 
RSL:dlh 
INDUSTRIAL CORROSION MJI^NAGEMENT, INC. 
^ . ^ ^ ^ % r ^ 
Ridhard S 
Presidnec 
/ 
301729 
CHAIN OF CUSTODY 
yz'k 
.1 
%^ •••«••• 
3 6 6 - 6 2 5 5 
S e n c Reoflrt To: Z^z^^7%^J 
. ^ i l a i 
i m o l i n g S e r i e s : 
y ^ y y 
> - / / ^ ^ X r 
SamolerCs) 
Name: 
I i. 1 g.-; a [ u r = ; 
•tfty. 
Z-Ty^-y 
<ZMJ.. 
i m a l e icenti f ica rion i S a m c l i n g 
Location 
Point 
S a m o l i n g 
C a ; e 
S a m o l i n g 
T i m e 
S a m o l e T y p e 
j A n a l y s i s 
R e c u i r e c 
Com: 
Grao 
No. Cf 
Containers 
^ -y./r/-yrzrr 
yyr-,(ZZ-/ 
/3AfAy.AC 
A-Zro 
y . t 
'•r-zz-y.- yriziz 
y y y (^-3 
A-sC 
yzz 
yr-y-c 
e i i n a u i s n e a 
Sy: CSign.] 
R e c e i v e a 3y: CSign.] 
!a t e / T i m e 
' < y - ^ r ^ ~ 
y y 
•-.^-.yzry- y ^ . ' S ' 
y A y 
y ^ y 
y r y : 
y r -
\ 
'y 
r y 
S- cc 
\ 
S-^c 
-
•K 
V 
• 
— 
• 
• " • 
y z 
1 
zy 
i 
/ 
1 
/ 
. 
1 
1 
! 
1 
_ - . , _ . 
, 
l e u ncuisnt 
(fSigo^ 
R e c e i v e d - By: 
CSign.) 
(}yL ^•rOt^uTcG y 
"2 a te/Tifna 
/ y. i ••// J^i: 
/^. y 
l e i i n c u i s n e c To Laoaraflory By: CSign.} 
Received For L a o o r a t o r y 3y: CSign.] 
; a I e / T i m e 
.Aetnoa Of 
Relincuisnment: 
Name 01 L a o o r a t o r y : 
A N A L Y S I S 
R £ O U I ? = 0 
put c o c a 
in p r o o e r 
c a i u m n ] 
Priority pollutant+'<iO: 
Petroleum hyarocaroons: 
Volatile organics CGC]: 
Volatile organics CGC/MS]: 
, C y a n i a e s : 
CCCE I ANALYSIS 
COCg I ANALYSIS 
. CCCE 
01 
02 
03 
04 
OS 
Nickel: 
C f i r o m i u m : 
A r s e n i c r 
C o o o e r : 
L e a d : 
M e r c u r y : 
A n t i m o n y : 
06 
07 
08 
09 
10 
1 1 
12 
Zinc: 
Cadmium: 
Selenium: 
S i l v e r : 
Barium: 
COO: 
B O O ; 
13 
14-
15 
16 
17 
18 
19 
ANAL'^SiS 
TSS: 
TDS: 
p H : 
PCS: 
Otnar: 
CSoecify} 
C C C S 
20 
2 1 
24 
301730 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
U52 SCur£ iO. SANCCL=M. NEW ;£.RS£'f 07359 
2 Q I ; S . ; - G ; 3 0 
NJDE? Carcified Dri.-iking Wacar/Vastavaca; 
Laboracory ID;/ L4LI6 
REPORT D.^TE: in—'i i6 loa-
LAB i* 53562 
CLIZNT: EN\"RO SCIENCES - Island Checiical Proiecc 
SAMPLZ SOURCZ: 085-25I-ESI 
SAMPLE DATE: March 13. 1986 
TAKZN BY: A. Kvlgs 
AT LA3 DATZ: y.^r:h 
MATRIX: 
Soil 
' G9;; 
?C3 ANALYSIS 
'.2choc 605 bv G2.S Chronaco^raohv vich Zlaccron Ca-ci 
?.\RAMZTZR 
RESULT 
SPIKE 
DUP SPIKE 
RPD 
DETZCTICN' LIMITS 
Arochlor L016 
Arochlor 1221 
Arochlor 1232 
Arochlor 12^*2 
Arochlor 1243 
Arochlor 1254 
Arochlor 1260 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
X 
X 
X 
X 
X 
X 
X 
X 
X 
All resulcs are raporced in csg/kg(ppm) dry weighc basis. 
If you should have any quescions, please do noc hesicace co call. 
DBC SURROGATZ RZCOVERIZS; 
Blank: 
*^Tt 
Saciole: 39% 
Spike: 
*** 
Spike Dup:*** 
0. 1 
0. 
0. 1 
0. • 
0.1 
RSL: dlh 
ND=Noc Dececcion 
RPD-Relacive Percenc Difference 
INDUSTRIAL CORROSION MANAGEMENT. INC. 
Richard S. iievi-£e 
Presidenc A 
PCBEC0125 
PCBECW/S150 
SOITBI 
# 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
U52 ROUTE 10. SANOQLOH. NEW JE.'SEY 07869 
20l-5a4-03:0 
NJDE? Carcified Drinking Wacer/Vascevac 
Laboracory IBit 14116 
RZPORT DATE: .-Voril 16. 19g'^_ 
LAB it 53363 
CLIZNT: ENVIRO SCIZNCZS - Island Cheaical Proiecc 
SAMPLZ SOURCZ: 0S3-252-ZSI 
SAMPLZ DATZ: March L3. 1986 
TAKZN BY: A. Kvles 
AT LAB DATE: March I~. I?S-
MATRIX: Soil 
' 
, 
?C3 .VN.ALYSIS 
Mechcd 608 bv Gas Chromacoaraahv wich Zleccron Caocire 
P.--RAMZTZR 
Arochlor 1016 
Arochlor 1221 
Arochlor 1232 
Arochlor 1242 
Arochlor 1243 
Arochlor 1254 
Arochlor 1260 
RZSULT 
ND 
DUP SPIKZ 
ND 
ND 
ND 
ND 
RPD 
J L . 
DZTZCriCN LIMITS 
ND 
_s_ 
ND 
JL 
_S_ 
0. • 
1 
n 
n 
0 
0 
Q 
, . 
• 
. 
-, 
All resulcs are reporced in ng/kg(ppni) dry weighc basis. 
If you should have any quescions, please do noc hesicace co call. 
DBC SURROGATZ RZCOVERIZS: 
Blank.: *** 
Sample: 61!: 
Splka: *** 
Spike Dup: *** 
INDUSTRIAL CORROSION MANAGEMZNT, INC. 
Richard S. Liv2^ne 
Presidenc / 
RSL: dlh 
ND=»Noc Dececcion 
RPD-Relacive Percenc Difference 
PC3EC0125 
PC3ECW/S150 
301732 
# 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDE? Cercified Drinking Wacdr/Vascavacer 
Laboracory IDii* 14116 
REPORT DATE: April 16. 1985 
L A B ;/ 
"^-s-sfii • 
1152 SCUTE 10. RANCCL'H, NEW JE.RSEY 07369 
201-!S4-03;0 
CLIENT: E^TVIRG SCIZNCZS - Island Cheir.ical Proiecc 
SAM-PLZ SOURCZ: 85-255-;SI 
S.\M?LZ DATZ: March 13. 1986 
MAT RIX: Soil 
T.^<ZN 3Y: A. Kvlas 
AT LAB DATZ: March 17. 1986 
PCB ANALYSIS 
Me'ihod 608 bv Gas Chrocacozraohv wich Zleccron Cascura 
P.ARAMZTZR 
Arochlor 1016 
Arochlor 1221 
Arochlor 1232 
Arochlor 1242 
Arochlor 1248 
Arochlor 1254 
Arochlor 1260 
RZSULT 
ND 
SPIK 
DUP SPIKZ 
JSL 
ND 
Jffi. 
ND 
ND 
ND 
RPD 
X 
X 
X 
X 
X 
X 
X 
DETZCTICN LIMITS 
; n 
1 _ Q 
i.O 
1 
:-\ 
: :-. 
•i 
n 
1 
n 
All resulcs are reporced in mg/kgCppm) dry weighc basis. 
If you should have any quescions, please do noc hesicace co call. 
DBC SURROGATE RECOVERIES: 
Blank: *** 
Saaple: L08" 
Spike: *** 
Spike Dup:*** 
INDUSTRIAL CO 
N MANAGZMJINT, INC. 
Rf chard S. I^viiie 
Presid 
ard S. Le\ 
idenc 
C 
RSL:dlh 
ND=»Noc Dececcion 
RPD=Relacive Percenc Difference 
PCBEC0125 
PC3ECW/S150 
301733 
7 1 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
115; ROUTE 10, ,RA,NCGL.=H. ,N£W JERSEY Q7859 
: 0 1 : 3 4 - 0 2 ; Q 
NJDE? Carcified Drinking Wacer/Wasc-vac; 
Laboracory IDi/ 14116 
REPORT DATE: 
Aoril 16. 193^ 
LAB it 
53365 
CLIZNT: ZNVIRO SCIZ:-;CZS - Island Chemical Proiecc 
S.AMPLZ SOURCZ: 085-254-ESI 
SAMPLZ DATE: March 13. 1985 
TAKZN SY: A. Kvles 
AT LAB DATZ: March '•'. :9z~ 
MJ^TRIX: Sell 
PCB .ANALYSIS 
Mechod 60S bv Gas Chromacozraahv wich Electron Caocura 
PAR.AMZTZR 
Arochlor 1016 
Arochlor 1221 
Arochlor 1232 
Arochlor 1242 
Arochlor 1248 
Arochlor 1254 
Arochlor 1260 
RZSULl 
ND 
SPIKZ 
DUP SPIKZ 
ND 
ND 
X 
ND 
ND 
X 
ND 
ND 
X 
RPD 
X 
X 
X 
X 
X 
X 
X 
DEI EC" " O N 
: - • U T TS 
A 
; 
0.5 
0.5 
0.5 
0.5 
0.5 
0.5 
All resulcs are reporced in ng/kg(pptn) dry weighc basis. 
If you should have any quescions, please do noc hesicace co call. 
DBC SURROGATE RECOVERIES: 
Blank: *** 
Sample: 60% 
Spike: *** 
Spike Dup: *** 
INDUSTRIAL CORROSION MANAGEMENT, INC 
i 
R^fchard S. L§r/±tf^ 
P r e s i d e n 
S . 
LarV] 
RSL: dlh 
ND=»Noc Dececcion 
RPD»Reiacive Percenc 
D i f f e r e n c e 
PCBEC0125 
PCBECW/S150 
301734 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROUTE 10. RANDOLPH. NEW ,'E.RSEY 07363 
201-534.03;o 
NJDE? Carcified Drinki.Tg Wacsr/Vasce-. 
Laboracory ID!/ 14116 
REPORT DATE: ..•^oril 15. 1986 
LAB it 
53366 
•a Car 
CLIZNT: ENVIRO SCIENCES - Island Chenical Project 
SAMJ'LE SOURCE: 085-255-ESI 
S.AMPLE DATE:v=--- i "! iQS6 
MJilRIX: Sell 
" 
TAKZN BY: A. KVI QC 
AT LAB DATE: \<, 
?C3 ANALYSIS 
Mechod 608 bv Gas Chroaacoeraohv wich Electron Caocurs 
PA.RAMETZR 
Arochlor 1016 
Arochlor 1221 
Arochlor 1232 
Arochlor 1242 
Arochlor 1243 
Arochlor 1254 
Arochlor 1260 
RZ3UL" 
ND 
ND 
SPIKZ 
X 
DUP SPIKE 
ND 
ND 
ND 
ND 
ND 
X 
RPD 
X 
X 
X 
X 
X 
X 
X 
DETEC: ^ICN 
0. 
0. 
0. 
0. 
0. 
0. 
0 
i . 
_ 
: 
-* 
• \ 
; 
; 
; 
- V T TS 
All resulcs are reporced in nig/kg(ppa) dry weighc basis. 
If you should have any quescions, please do noc hesicace co call. 
DBC SURROGATE RECOVERIES: 
Blank: *** 
Sample: 70% 
Spike: *** 
Spike Dup: *** 
RSL: d l h 
ND=Noc Dececcion 
RPD"Relacive Percenc 
D i f f e r e n c e 
INDUSTRIAL CORROSION MANAGEMJINT, INC. 
y -
chard S. leoqi^ne 
Richard S. I 
Presidenc / 
PCBEC0125 
PCBECW/S150 
301735 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDE? Carcified Drinking Wacec'Vascevace: 
Laboracory ID;/ 14116 
REPORT DATE: Aoril 16. 19S6 
LAB if 
--,-!ST 
1152 ROUTE 10. RAN001..=H. NEW JERSEY 07869 
201-53-J-03;o 
CL I.::NT: E^rv'IRO SCIZNCZS - Isl.a.r.r' Cher.ical Proiecc 
__^ 
SAMJ'LE SOURCE: 085-256-ZSI 
. 
SAMJ'LE DATZ:M.^.---.. I-. :OS6 
TAKZN 5Y: A. Kvles 
^ AT LAB DATZ: March 1~. l-~f-
M_AIRIX: varar 
PZSTICIDE & PCB ANALYSIS-PRIORITY POLLUTANTS 
Suicabia for Compliance Tescing by Mechod 608 
Gas_Chrcn:acosrat3hv wich Electron Caocure 
P.ARA^-IZTZR 
RZSULT 
SPIKZ 
DUP SPIKZ 
RPD 
DZTZCTION LIM: 
Aldrin 
yp 
x 
x 
x 
O.Q2 
a-3K.C 
\T) 
X 
X 
X 
0.02 
b-BHC 
NTP 
X 
X 
X 
0 Q2 
d-3KC 
N^ 
X 
X 
_i_ 
0.02 
g-BHC (Lindane) 
vrp 
x 
x 
x 
0.Q2 
Chlordane 
^ 
x 
X 
X 
Q. 5 
p,p'-TDE(DDD) 
ND 
X 
X 
^ X 
0.2 
p,p'-DDE 
ND 
X 
X 
X 
Q.04 
p,p'-DDT 
ND 
X 
X 
• 
_X_ 
0.2 
Di^drin 
ND 
X 
X 
X 
0.04 
Endosulfan 1 
>n3 
X 
X 
X 
0.04 
Endosulfan 2 
^ 
X 
X 
X 
0.04 
Endosulfan sulfaca 
NP 
X 
x 
X 
0. 1 
. Endrin 
NP 
X 
X 
X 
0.04 
Endrin aldehyde 
NTD 
X 
X 
X 
0.2 
Hepcachlor 
ND 
X 
X 
X 
0.02 
Heptachlor epoxide 
ND 
X 
X 
X 
0..1 
Toxaphene. 
ND 
X 
X 
X 
0.5 
Arochlor 1016 
ND 
X 
X 
X 
1.0 
Arochlor 1221 
ND 
X 
X 
X 
1.0 
Arochlor 1232 
: 
ND 
X 
X 
X 
1.0 
Arochlor 1242 
ND 
X 
X 
X 
I. Q 
.A^rochlor 1248 
— 
ND 
X 
X 
X 
1.0 
Arochlor 1254 
. ND 
X 
X 
X 
I.O 
Arochlor 1260 
ND 
X 
X 
X 
1-0 
All resulcs are reporced in ug/l(ppb). 
If you should have any quescions, please do noc hesicace Co call. 
DBC SURROGATE RECOVERIES: 
Blank:*** 
Sample: 145% 
Spike:*** 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
Spike Dup: *** 
1/ J f 
JjA 
pMnsT^jA^i 
RSL:dlh 
Ric?nard S. LaViGe('/Presidenc 
ND-Noc Dececced 
/ 
RPD-Relacive Percenc Difference 
~ ^ - „ _ ^ 
INDUS MIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROUTE 10. RANOOLPH. NEW JERSEY 07869 
201-534-0330 
NJOE? Cerci; 
j Drinking Water/ 
Wascewacer Laboracory 10 .^l^^llS 
-L) 
REPORT DATE: 
.Aorll 74, 
l o a ^ 
LAS a 
53367 
CLIENT: 
^^TX7T?.0 SCIZNCZS INC. - Island Che-.ic.^l P-n^°cr 
SAMPLE SOURCE: 
085-256-ESI 
SAMPLE DATE: -3/15/36 
SA^.PLED BY; 
A. Kvlas 
AT LAB DATE:. - / ' - / c S 
Paramecer 
acrolein* 
aery 1 cn i c r i 1 e" 
benzene 
bromoform 
carbon cecrachI oride 
chlorobenzene 
chlorodibrcmomechane 
chlorechane 
2-chloroechylVinyl ether 
chloroform 
dichlorobromomethane 
1 , 1-dichloroethane 
1 ,2-dichloroechane 
1 ,1-dichloroechylene 
PRIORITY POLLUTANT VOLATILE ORGANICS + i*0 
by G C / M S + 15 P E A K S 
Dececcion limic 10 ug/l(ppb) 
Resul t 
jnL 
:SL 
ZZL 
JiL-
ND_ 
:nL 
_2L 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
Paramecer 
1 , 2-dichloropropane 
1,3-dichloropropy1ene 
ethylbenzene 
methyl bromide 
methyl chloride 
methylene chloride 
1,1,2,2-tetrachloroethane -
tetrachloroethylene 
toluene 
1 , 2-'trans-d ichl oroethy 1 ene 
1 ,1,1-trichloroethane 
1 ,1,2-trichloroethane 
crichloroechyiene 
vinyl chloride 
Resu i 
:iiL 
ND 
Jffi_ 
ND 
ND 
.ND 
JS-
•ND 
*Dececcion Limic 
LT=Less than 
ND»Noc Dececced 
IOOO ug/lCoob). 
OTHER COMPOUNDS DETECTED 
APPROXIMATE 
CONCENTRATIONS 
SURROGATZ RECOVERIES 
1,2-dichloroechane d4 - 104% 
dS toluene 
- 
99% 
BFB 
- 
96Z 
95%(spike) 
99%(spike) 
103%(soike) 
98%(spike duplicace) 
98%(spika duplicace) 
93%(spike duplicace) 
INDUSTRIAL CO 
RSL:dlh 
Richard S 
Presidenc 
301737 
:--A 
i 
I 
i 
1 
1. 
. 
I., 
i. 
to 
o 
r-» 
- J 
U> 
00 
:^:i'i 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
IISIROUTl 10. RAMDOim NCWJfRSEr OMit 
lOISeiOllO 
NJOEP Ceriified Drinking Water/Waslewaler 
Laboidtory ID #l'il 16 
REPORT 0ATE:.Ai>rLl_24,_L9ft6_ 
LAB // .53!(.7_._ 
CLIENT; ENVTRO SCTENCES TNC. - Island Chemical Project 
SAMPLE SOURCE: Ofl5-256-EST 
SAMPLE DATE: March »3. i9fl6SAMPLED BY: 
A. 
Kyles 
AT LAD OATE: Marcli 17, 
1986 
ACID 
EXTRACTABLES 
P R I O R I T Y 
POLLUTANTS 
+ 'lO 
_biL_G C7Jii±_l.Q_P. E A K S 
ACID EXTRACTABIES PRIORITY POLLUTANTS + 10 Peaks 
2-chlorophenol 
2-nitrophenol 
phenol 
2,'),-dimethylphenol 
2,'(,-dlchlorophenol 
pentachlorophenol 
Z.'j-dinI t rophenol -
't,6-dinl t ro-o-cresol 
— 
^-nitrophenol 
2 , ' t , 6 - t r l c h l o r o p h e n o l 
- -
'i-chloro-B methyl 
phenol 
_loy_ 
1011 
IQIL 
I oil 
JDU_ 
M\L 
JQiL 
JQIL 
_LQIL 
I oil 
JillRKOCATI' KKCOVF.Uir.S 
2-FI iioroplieni) I 
Phenol-(l5 
2 , 4 , 6 - ' r r i l)roiii()|iliun(>l 
5 2 . 1 % 
21 .OZ 
67.9% 
OTIII'lt COMPOIIND.S DETI'm'ED APPROXTMATE CnNr.F.NTUATTONS 
Unknown llydroc/irhon Peak 
5. ft 
INDUSTRIAL C O R R O S I O N M A N A G E M E N T , INC 
RSL:dlli 
R i c h a r d S./I.uv ini; 
I'res iilfciu 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
11S2 aouI£ 10. RANDOLPH. .'i£W lEaStf 07863 2i:i-5i4..o;;o 
CLIE.MT: ZNVIRO SCIEMCES IMC. - I s l a n d Cher.ical 
Pro-iect 
NJOE? C e r t i f . - 0 
Drinking Uacer/ 
Wastewater Laboratory 
10 ;?! 1*116 
REPORT OATE: Aoril 24. 
iggr, 
LAB < / _ _ l l ] i I 
<;AMP[F SOURCE: 08;-25n-rsT 
<;AHPI F DATE: j/l 3/S6 
SAhP LED 3Y: 
A. Kvioc 
AT lAa OATE: 3/17/ 
BASE/NEUTRAL EXTRACTABLES PRIORITY POLLUTANTS + ^40 
bv 
GC/.'-.S 
+ 15 PEAKS 
Pararr^eter 
aceneoht.~.ene 
::Ce.naG."ic."y i e.ne 
-in-nracene 
. 
' \ 
benzova)pyrene 
•
^
1 
"
1 
j,-f-oen2or[ucrancriene 
/ 
I 
• 
\ 
. 
\ 
_ 
_ 
b i s (2-c.hloroethoxy)methane -
bis(2-chloroethyl)ether 
bi s(2-cnloroi sopropyl)ether-
bls(2-ethylhexyl)phchalate -
i4-bromoDheny 1 phenyl echer -
outyiDencyi pntnaijte 
z-c.-1 oronapncna 1 ene 
it-chl oropheny 1 phenyl ether 
, 
cnrysene 
• 
0 1 den20 la , n ^ an t.-raCe-ne 
, . , . , , 
, 
1,2-d1ch1orobenzene --------
•
.
_
.
,
. 
1,3-d Icniorobenzene 
1
1 
J . 
- 1 
L-
1.H-d1cnlorobenzene 
3 ,3"d 1 cn 1 orobe.nz 1 a 1 ne 
LT=Less Than 
.ND=Noc Decaccad 
Result 
_., 
'. CL 
lOU 
- -T 
— — 
^j 
, _ 
;0U 
IGU 
lOU 
I OU 
LOU 
lOU 
iOU 
- - - 
-1 n r 
IOU 
_ 
IOU 
_ 
'.ou 
IOU 
lOU 
lOU 
lOL 
-
IOU 
_ 
10b 
20U 
SURROGAT 
d5-Nitrobe 
2-r 1 uorob.i. 
'^-Terpheny 
Parameter 
di-n-butyl phthalate 
di-n-occyi phthalate 
1 ,2-diphenylhydrazine(as azobenzene) 
fluorene - - - - — 
hexachIorocyclopentadiene 
inaenoii,z,j-ca^pyrene 
1sopnorone -------------—---— 
napn t.na i ene 
N-n 1 trosod ifr.etny 1 ami ne 
N-n1trosoo i -n-propyiamine - - - — - - — 
N-n i t rosod i phenyl ami ne -------------
phenanthrene 
pyrene 
1,^,H-tr1ch1orobenzene 
—-----
ES 
nzene 
- 6.3Z 
phenyl - 59.7% 
l-dU 
- 91.8% 
APPROXIMATE CONCENTRATION 
OTHER COMPOUNDS DETECTED 
36 
Resu! : 
! .irr 
:0U 
50L-
I ni-
- 
2 . i J 
5 on 
'01' 
IOU 
1 nu 
^ IOU 
• ou 
- ,. 1 n r' 
I n n 
- 
1 nif 
- 
1 Of 
1 
^ ) ^ ' . 
IQU 
LOU 
IOU 
IOU 
IOU 
• ~ 
IUU 
RSL:dlh 
INDUSTRIAL CORROSION MANAGEMENT, UC. 
Richard S. Kevi^'e 
President / 
.01-739 
Zn 
CORROSION 
MANAGEMENT 
INCORPORATED 
1I5J KOurE '.O. RAHOCUM. .IEW :iJI&ct 37183 
2ai.5j4.0JM 
NJDE? Carcif: • Dri.ikir.g Vatar. 
Laboracory ID .14116 
REPORT DAIE: 
Mav 2. 19S6 
"•io ..evacar 
LA3 It 
53367 
PRIORITY POLLUT.ANT 
L.\30.RAT0RY AMALYSIS 
CLIENT: --rZ^.^O SCIEMCES 
SAxHPLE SOURCE: Island Chsr-.lcal 
SAxMPLE ID: 
OS5-25o-;SI 
UNITS; -g/l^oo-' 
SAMPLE DATE: March 13. •. ;
c
; 
SAMPLED BY: 
A 1 Kvlas 
AT LAB DATE: March 17. -,« — .-
MATRIX: 
vatar 
(This report Lav~ concains boch che original sample resulc and che duplicate result.) 
j 
Arsenic 
' 
aervlli-n 
! 
Cadmiun 
' 
Chromium 
! 
Coooer 
' 
Laad 
) 
Mercurv 
Nickel • 
Selenium 
Silver 
Thallium 
Zinc 
Phenol 
Cvanide 
1 
';.007 ! 
LT O.OOL 
LT 0.001 i 
0.002 
0.007 
0.005 
0.0005 
LT 0.006 
0.019 
0.004 
LT 0.014 
0.022 
LT 0.005 
0.007 
r- nn^ ' 
0. OQ 1 
0.001 
0.002 
0.007 
0.005 
LT 
0.0007 
0.006 
0.029 
LT 
O.OOi 
O.OU 
0.027 
X 
0.008 
17^: 
i 
NC 
i 
NC 
i 
NC 
NC 
! 
NC 
17% 
1 
• NC 
42% 
NC 
NC 
20% 
X 
13% 
:75!: 
NC 
NC 
NC 
NC 
NC 
i55% 
NC 
;33% 
NC 
NC 
t20% 
X 
= 20% 
-^--
; T 
LT 
LT 
:LT 
LT 
LT 
LT 
LT 
LT 
LT 
LT 
LT 
LT 
0.0C2 '-
O.QCl ! 
0.OC 1 ! 
0.001 i 
0.001 1 
0.002 ! 
0.0005 i 
0.006 
0.005 i 
0.001 i 
0.014 i 
0.001 i 
0.005 ! 
0.007 i 
--
'T 
T^--
T -> 
:.. 
— i 
^ I 
•_-2 
-_-
-_-
«i. 
r_-
LT 
-_-
0.002 I 
0.001 i 
0.001 
0.001 
0.001 i 
0.002 1 
0.0005 
0.006 
0.005 
0.001 
0.014 1 
0.001 
0.005 
0.007 
1 
1 
1 
1 
1 
NC = Non-calcuabie RPD due co vaiueCs) less chan dececcion limic. 
dwb =» Dry Weighc Basis 
X » Noc Analyzed 
LT =• Lass Than 
INDUSTRIAL CORROSION MANAGEME.NT, INC. 
RPD =» Relacive percenc difference. 
RSL/dlh 
itichard 
S./tev'f'ne 
Presidenc 
Ai^'^*-^ 
301740 
^ ) 
C H A I N OF C L / S T O D Y 
jiTic :m xi^tOii ;nc. 
%^^ w — 
3 6 6 - 6 2 5 5 
Sena Reopr; To: 
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I l l a t i o n : 
^ S c r ^ a ^vsV./^.-«c^ 
C^. ( Z T i / i L ) 
. m a l i n g S a r i e s : 
y ^ / y 
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i i n a i e I c e n t i ( i c a tion 
S a m s l i ng-
L o c a t i o n 
P o i n t 
S a m c I i n q 
Cate 
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coyctz. 
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R e c e i v e a 8 y : CSign.] 
'w a t e / T i m e 
R e c e i v e d 8 y ; ( S i g n . ) 
C a t e / I I .Tl e 
lAJilJA'^ 
I '•:/•'. I < y 
nei'incuisneo To Laooratory 3y: (Sign.3 
Receivea Far Laooratory ay: CSign.} 
Cate/Time 
iMetnod Qt 
Relinauisnment: 
Nama 01 Laooratory: 
I 
A N A L Y S I S 
R g Q U I P g P 
iCout c a a e 
in p r o o e r 
c o l u m n } 
P r i o r i t y pollutant+-<iO: 
Petroleum 
h y a r o c a r o o n s : 
I 
V o l a t i l e o r g a n i c s CGC}: 
V o l a t i l e o r g a n i c s CGC/MS}: 
, C y a n i d e s : 
COC£ 1 
<^P 
02 
1 
03 
1 
/ ! & 
05 
1 
A.^4ALYSIS 
N i c k e l : 
C h r o m i u m : 
A r s a n i c r 
C o o o e r : 
L e a d : 
M e r c u r y : 
A n t i m o n y : 
C C O E 1 
06 
07 
OS 
09 
10 
n 
12 
A N A L Y S I S 
Zinc: 
C a d m i u m : 
S e l e n i u m : 
S i l v e r : 
1 
B a r i u m : 
1 COO: 
B O O : 
CCC = 
13 
14-
I S 
16 
17 
18 
19 
A N A L •' s ; S 
T S S ; 
T D S : 
p H : 
PCS: 
Otner: 
CSoecify} 
C C C ^ 
20 
2 1 
2 * 
301741 
tMtkl' 
Berlox . ^ ^ r a t o r l e a 
St. Croix, Virgin lalanda 
ik 
tiaitJi 
••^4-4.3 
> . ^ i 
L__i.l 
C.::J 
l^t^uixl 1 ^ ^ : : 
-.3 
VID980651095 
Table 2 - Results of Organic Analyais- Organic Compounda Detected 
Compound name 
Sample location/Sample > 
VGA 
Xylene 
Chloroform 
Gut Back-
ground* 
1085251 
Lab waste 
pit seep 
#085252 
Drainage 
pit disch. 
1085253 
470 
Lab waste 
pit il 1 
•085254 
huh waste 
pit # 2 
#085255 
On-site 
well (ug/l) 
#085256 
130 
NVOA 
Butyl benzyl phthalate 
Dl-n-octyl phthalate 
1,4 dichlorobenzene 
1/2 dichlorobenzene 
Napthalene 
Flourene 
Phenanthrene 
Bis(2-ethylhexyl)phthalate 
Aliphatic 6 aromatic 
hydrocarbons 
1000 
17000 
9000 
7700 
870 
2900 
2100 
2000 
2400 
M 
4900 
3200 
2K 
3.9 
280 
PCB 
PCB-1016 
PCB-1221 
PCB-1232 
PCB-1242 
PCB-1248 
PCB-1254 
PCB-1260 
to 
O 
-J 
to 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
lOOOK 
1000K 
1000K 
lOOOK 
1000K 
1000K 
1000K 
100 OK 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
1000K 
lOOOK 
IK 
IK 
IK 
IK 
IK 
IK 
IK 
•All values in ug/kg except where otherwise stated. 
K " Actual value known to be less than value given. 
M =• Presence of material verified but not quantified. 
Blank space means compound was not detected in samr»l <» x"»"»--» 
I 
t. 
Berl^'^^ boratorles 
St. CroiX, Virgin Islands 
I: , t ,i I A •;, I t 
Table 3 - Results, of Metals Scan Analysis 
Compound name 
Sample location/Bample I 
*A11 values in mg/kg except where otherwise stated. 
J - Estimated value. 
H •• Presence of material verified but not quantified. 
Blank space means compound waa not detected in sample analysis. 
to 
o 
'iN 
VID980651095 
Silver 
Arsenic 
Beryllium 
Cadmium 
Chromium 
Copper 
Mercury 
Lead 
Nickel 
Antimony 
Selenium 
Thallium 
Zinc 
Gut Back-
ground* 
•085251 
2J 
10 
40 
19 
IJ 
100 
Lab waste 
pit seep 
1085252 
U 
7J 
22 
45 
20 J 
10 
63 
Drainage 
pit disch. 
#085253 
0.8J 
8J 
52 
52 
30J • 
32 
IJ -
360 -
Lab waste 
pit 1 1 
#085254 
0.8J 
7J 
27 
55 
25 
8.4 
O.BJ 
80 
Lab waste 
pit # 2 
#085255 
2J 
7J 
26 
58 
27 
O.BJ 
79 
On-site 
well (ug/l) 
•085256 
2J 
5J 
3 J 
7J 
8J 
0.6J 
3J • 
20J 
• 
\ . 
•J 
i{:k 
to 
\ 
! 
b.'-.z'"! 
:m t(fl(: vt crdiir 
l|>lll: 
«}-tiei-oi 
•;«i(Pll« OAtf: 11711 
im cm no.: is'ij m 
VOIAIIUS 
Simie 10 no. 
Irillic Report No. 
i l J l f i i 
•mils 
: ilulion rjclor, 
PetcenI Koiiture 
.
* 
SITE INSPECTION SA 
^-RESULTS 
«8/0j/')| 
1 
I 
I 
1 
1 
I 
Mil 
4 
flnfwmn 
:irM,w),n!V|.i ow: 
Vl.-i CW1IPUV1?5CII< 
VI250«5 
VI25CW6 
VI2S-SC0I VlJS-StOJ V125-StOJ VI2S-StO«(OVIJ5-S£OS VI25-SID4 VI25-S1IIIS/ VI25-S2 
VI25-5i 
VI25-Si 
VI25-|I|I(I 
Bf.lOI 
UAUt 
1 
1 
u.. o: 
w-llll 
O ' l 
1 
1 
BUOl 
ii;)iiR 
ICIO< 
UAHI) 
lltjli 
1 
1 
ICIOS 
VUII) 
ug/l 
t 
1 
IGlOi 
UAKR 
ug/l 
1 
(ClO» 
s ( i ) i « r n i 
ug/kg 
1 
V 
ICllO 
SCDIntHI 
ug/kg 
1 
1 
JJ 
BGlll 
:(Dtn(Ht 
ug/kg 
t 
1 
(J 
ICU2 
SCDIACKI 
ug/kg 
1 
1 
J< 
IGlll 
StOIMHI 
ug/kg 
t 
X 
11 
I U U 
SCOIKCMI 
ug/kg 
1 
1 
IUU 
soil 
ug/kg 
t 
1 
l i 
ICIH 
SOU 
ug/kg 
1 
1 
U 
K l I S 
SOU 
ug/kg 
1 
1 
11 
IC12J 
SOU 
ug/kg 
1 
1 
9 
1(118 
VAUR 
ug/l 
., 
'.hloroielbane 
Iroioiethint 
vinri Chloride 
Lhloroelhine 
itthirlenc (hloriije 
icdont 
iirboii Disulfide 
.l-Dichloroelhene 
,I-Oi(li|oroelhi(\e 
iiflt-l.?-Dichloroellient 
i<ll 
hloroloii 
/ 
.2-Dich|oroeliiin( 
lirlinoAi 
.I.MrlcMoroelhint 
irbon leltichloride 
inyl (celile 
oiodifhloroietlijne 
7-OicMoiooropine 
fl,J-Dichloropropen< 
ichleioelhene 
broiochloroielhine 
1,2-lriclilorectlijne 
niene 
iM-I.J-Oichloropiooer.t 
iioloii 
lelhifl-2-Pe(iliiio/ie 
leiincne 
richloroelhene 
uene 
,2,;-letricliloroethir.e 
orobtnrene 
flbemene 
rem 
met (totill 
(J: 
<k ipicc • ceipound inily.ti) U i twi 
M l delected 
(oepound found in lib i\in> ,'. ai|| 
tiipje, indjcilei potiitle tiotiiii 
blinl conliilnillon 
eitiiiled vtlue 
eiliiiled vilue, coepound presiM 
keloi CROl but ibe>c lOi 
I 
inilriil did nol pisi ( M OA/OC 
'reiMPliti evidence ol the pitttncc 
ll li>e iileriil 
inilfSis nol required 
tion lieili elevited il Dilution 
r >l ind/oi parceni eoisluri .01 
12 
i 
IS t liO 
It t 
210 I 
t 
J 
to o 
\ •, 
TO 
(D 
< 
XT 
O 
o 
o 
ro 
1 
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t—• 
o 
H - • 
o 
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1/1 
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\ ' [ 
\ 
i 
I 
I 
^IK U M : VI CHlnlCAl 
IOU: 
O2-9I01-0* 
CUNPIIW DAIt: 
J/28/91 
(PA CASf NO.: 
I595J U B . 
i . II n •ri n 1 -^ n '1 fTn n 
SITE INSPECTION SAMPLING RBBUbTS 
(cont'd) 
.:onPucHfn 
to o 
\^ 
~J 
* > • 
cn 
VOIAIIKS 
iiiplt ID Ro. 
Irjltic Repoit Ho. 
Hatrix 
Unili 
Dilution fjclor 
I'trcent Noislure 
CMotoietliine 
lioioitlhine 
Vin/I Chloride 
thloroethine 
nelhylent CMoride 
"Tfcelone 
Cirbon bitullide 
l,l-Dich)oroilbifle 
1,1-OicMoroelbine 
lrini-l,2-DicMoiotlhent i .UII 
Chlorolori 
1.2-DlcMofoel)iinc 
2-lulinont 
l.l.l-lricMoroelhine 
C.rbon lelrichloride 
'~ifinrl Aceljle 
IroiodicMoroeelhjne 
l,2-Diih)oropropine 
cis-l,]-DicMotopr3pene 
_l;ichloroelbene 
MbroiocbloroieU.jne 
l,l,2-lricliloro(lbint 
lenrene 
Irent-I.J'Ditliloroproper.t 
iroiolore 
""l-llelhirl-J-Penljnone 
J-Neiinjne 
letricMoiottbene 
toluene 
^1,1,2,2-tetrjcMoroelhjnt 
(Morostniene 
(Ibylbeniene 
Slyrene 
ryler.es I I O I J I ) 
VI2b-RII(2 
VI2S-I8HI 
ICI 19 
IGi:2 
WAUR 
WAHR 
ug/l 
u g / l 
I 
I 
l>i"l|'. 
ilini spirt • (lapovino «nil|.(0 k : u : 
nol »teclid 
I • toepouna lounc ',i n t t l i ' i »• . i . : , 
H i t . t , .noKJiti point.t t ' : ; j [ . i 
blank coAliiinition 
f • cslliilid vilue 
J • estitiled «)lut. coepot.ni: pteicM 
belo. CROl bill ibovc IDl 
I • intlysil did nol piii (PI 0«/0f 
« • Pitsunplive evidence ol Die pretintt 
ol Ihe laleiiil 
>l - tnilyiii Ml reouired 
Nitcllon l i i i l i eleviled il Dilution 
ticior >\ tat/at H'teni Miiiuie >C\ 
pa c
n> ^
< 
I
I tilt l... 
IDPI: 
t: 
i n CASt KO 
^ ^ i : t 
• 
\ 
i 
I 
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SITE INSPECTIO..^riPLING RESULTS 
(cont'd) 
n n#^> 
I 
I 
5tH|-V0IAI|l(5 
Saiple ID Ro. 
Iridic Report Ho 
nilrii 
Units 
Dilution faclot/tPt i . \ i i u t i , i • 
Percent Hoisture 
Phenol 
bisl2-ChloroeIhynelb;i 
I-Chlciophenol 
I.J-Oichlo'obenitne 
. 
l.l-Dichlorobeniene 
Itniyl alcohol 
l.2-0icMorobtni(nr 
2-Helhylphenol 
bisl2-Chloroi50trooy!l?ltff 
l-Helhylphencl 
R-Rilroso-di-n-dijtooyliiiie 
lle>achloro(than( 
Kiliobenient 
Isophorone 
J-mirophenol 
J.l-Diielhylohenol 
Itntoic acid 
bis(2-Chloroetho«i lie Ihji.i 
2,1-Dichlorophenol 
l,2.(-lrichloroben;(ne 
Kiphtbiline 
t-Chloroinillne 
Heiachlorobutidiene 
4-Chlcro-J-lltthy|phfnol 
2-llethylnaphlhalfne 
Keiachlorocycloi'cnljdiene 
I.l.i-lrichlorophenel 
2,4,5-lricMoiophenol 
2-Chloronaphlhalene 
__7-llitrojniIine 
Diitthylphlhalale 
Aceniphthylenf 
7,i-Dinitrolo|jene 
J-Hitroaniline 
_jlcenipMhent 
2,<-Dinltrooh(nol 
Mlilrophenol 
Dibtnioluran 
J,l-Dlnltrplolu«ne 
Jiethylphlhilite 
l-Chlorophenylphenyl elh/i 
fluorene 
4-Kilioinllint 
l.4-0lnllro-2-»elhyl;hfril 
jt-niliosodiphenylaeine 
«-lroiothenylphtnyl t\»f 
Heaachlorobeniene 
to 
o 
H-* 
-J 
i r i C J i n s 
(tlOl 
HdtP 
u;/l 
1 
irscu; 
fcio: 
UAKD 
iig. I 
1 
J 
vL'V'.Kiiouvirs-wi 
m O J 
BC104 
VAHR 
VAUfl 
ug/l 
ug/l 
1 
1 
V125-;ilS 
IGIOS 
MAKR 
ug/l 
1 
KR 
KR 
KR 
KR 
NR 
KR 
KR 
MR 
HR 
HR 
NR 
HR 
HR 
HR 
HI 
NR 
KR 
KR 
NR 
HR 
KR 
NR 
KR 
HR 
NR 
NR 
HR 
NR 
NR 
HD 
HR 
NR 
IIR 
KR 
IIR 
HR 
Hf) 
IIR 
NR 
NR 
HR 
HR 
IIR 
•IR 
KR 
Nl 
HP 
V I 2 5 - ( ; W 
tUOi 
mn . 
ug/l 
. . . . y . . . . . 
VI25-5t01 
8(lQf 
SIDUIINI 
ug/kg 
1 
1 
27 
R 
;-. 
VI25-5fD2 
ICI 10 
SlDinCNI 
ug/Vg 
t 
1 
JJ 
R 
-
VI25S(DJ 
BClll 
SCDIKIKI 
ug/kg 
1 
1 
<J 
VI25-StOI(tVI2S-SfOS 
BGII2 
SlflMtm 
ug/kg 
1 
J« 
R 
6«n 
SIDinCNI 
ug/kg 
1 
1 
19 
UO ( 
Vi:5-5JD4 
BCIK 
SEDimNI 
ug/kg 
4 
42 
V I ? S - 5 l ( « / VI2S-52 
BCIIJ 
SOU 
ug/kg 
1 
1 
R 
CCII4 
SOU 
ug/kg 
1 
1 
l i 
R 
VI25-SJ 
ICI IS 
SOU 
ug/kg 
1 
1 
It 
VI25-C4 
icirj 
sou 
ug/kg 
1 
1 
9 
VI2SaiKI 
BCtIt 
VAHR 
ug/l 
1 
. 1 
If: 
», 
I'A 
$ r t »A1f: 
» 
IDDI: 
0:-«ICIO< 
SAnriiKC M i t : 
i ; : ( 
fPA CASf NO.: 
n i J : 
H i : 
i.y 
L ..] L..J 
L J L_J LiAB^«i:.../ i' j' 
SITE INSPECTION .^^LINGi.RESULTS 
(cont'd) 
:fii'.' i!:ii 
I 
1 I 
t 
I 
t 
I 
] 
I 
I 
stni-toiAiiirs 
Saiol! ID No. 
I r a l f i c Pepoil No. 
Ilatrii 
Units 
Dilution faclor/crc ''\i >.-. 
Percent Moisture 
: n : s - i . v i . i K 
; 
BciC'; 
• 
WflIP 
! ug.'t 
; 
1 
I:5-CM: 
BC102 
NAUR 
ug/l 
1 
7i:scu;iouvir5-CK4 
ICIOJ 
UAUR 
ug/t 
1 
BG104 
UAUR 
ug/l 
1 
V125CK5 
8C10S 
NAUR 
ug/l 
1 
VI25-CK6 
80106 
NAUR 
ug/l 
1 
VI2;-SfDI 
ICI 09 
StOIKfKI 
ug/kg 
1 
21 
VI25-5[D2 
BCIIO 
StDlhlHI 
ug/kj 
) 
JJ 
V1?S-SI0J 
I G l l l 
SlDlntNI 
ug/kg 
1 
4J 
VI25-S(D4IDVI2SS(D5 
IGII2 
SlDlniKI 
ug/kg 
1 
Jl 
ecin 
StOlnCHI 
ug/kg 
1 
1 
19 
VI25-S(D6 
BGII6 
SIDIPfHI 
ug/kg 
4 
42 
V i r S S I I h S / VI25-52 
8CIIJ 
SOU 
ug/kg 
1 
1 
16 
B C l l l 
SOU 
ug'kg 
1 
1 
16 
VI2S-S: 
8GUS 
SOU 
ug/kg 
1 
1 
It 
vi;s-S6 
8C12I 
sou 
ug/kg 
1 
1 
9 
VI2S-RIHI 
I G l l l 
NAUR 
u g / l 
1 
1 
Penlachlorochenol 
Phenanthrene 
Anthracene 
Di-n-bulybhthalilc 
fluoranthsne 
Pyrene 
lutylbeniylphlhiUle 
J,J'-Dichloroben(iJir> 
leniolalanlhracene 
Chrysene 
blsl2-Elhylhe>yllphli.al<lf 
DI-n-oclylphlhalate 
lentolblMuoranlhene 
lentolUlluMinlhi-ne 
leniolaloyrene 
l n d e n o l l . ? . J - c d l p i f n f 
D i b e n r l a . h l a n t h r a c c n e 
leniolg.h.iloerylent 
KOUS: 
Hank space - conpount i n j | y ; e l h i 
b'll 
not detected 
I • coipound found In la:< tiUnV i ; veil js 
staple, indicale; oc i s l M e / i rr-sjlle 
blank contaainallon 
[ - eslinaled v i l u ; 
J • cstitaled v a l u i . (oroi.-il 
F V E I I 
belov (ROl but abo.f : M 
R - analysis did nol pi-f t ' - 
i ' t -
H • Presuirli>e f/id:i''.» .1 ihf : i i n . : ! 
of the a i l e i i a l 
KR • j n a l y i s njt I»T.' i ; ! 
Deletlion l i o i l s e l f . i l 
I i ! IT. 
' i n 
Fatloi 
I »nd.oi p c ' . ' i ' I.- 'U.t. 
'.-' 
NR 
HR 
KR 
KR 
HR 
HR 
KR 
HR 
KR 
HR 
KR 
KR 
NR 
KR 
NR 
KR 
KR 
KR 
10 ( 
R 
J 
R 
J 
J 
J 
J 
R 
R 
R 
22C0 [ 
R 
R 
R 
R 
R 
R 
R 
0 0 
o 
M 
•J 
m 
Krt|': 
iza 
SIfl lAI 
UU: { 
rAHPllft OAII: 2.'.V'-| 
fPA CASf NO : tS«!; 1 
L.ij • LlJ izZs 
y 
As! m , m ' y j LJ 
SITE INSPECTION^IPLING RESULTS 
(cont'd) 
n_n.._an_n«i 
_ i ^ . 
i _ . 
i"-)rri' if-c 
sfHi-vmAiiic 
Saeole ID No. 
Iralfic Report Ho. 
Nalrii 
Units 
Dilution racloi/i'.Pf rir.'..j,-i ' i l 
Percent noislure 
fhenol 
bis(2-Chloroelhyl!tlh'i 
}-Chloioph(noi 
I.J-Oichlcrobtnieie 
l.<-Dichloioben;rnF 
leniyl 
alcohol 
l.I-Dichlriohentene 
J-helhylphenol 
bisl2-CMorDisopiopy|telh( 
4-Helhylphinol 
N - K i l r o s o d i - n - d i M W i l i m i f 
Heaachloroelhane 
Kllrobentene 
Isophorone 
2-KilropSenol 
2,4-Diielhylphenol 
lenjoic 
acid 
bts(i-Chlo'ottho<ylirll.i'e 
2,4-Dichloripnenol 
l,2,4-lricMo(Obenirii. 
Kaphthilene 
4-Chloraaniline 
llMachlorobutaJien. 
4-CMoro-J-Nelhylohfiol 
I-ltelhylnaphlhalen' 
HeiachlorocyclopentaJitn; 
t . l . i ' l r i t h l o r o p h e n o l 
?,4.5-fiicMorothe>ol 
l-Chloronaphlba'.enr 
2-Nilroaniline 
Di>ethylthlhalal( 
Acenaphthvlene 
2.6-Oinitioliluene 
J-Nitroaniline 
Aceniphthtnr 
2,4-Pinilroph'nol 
4-Hitropheno: 
Dibenroturan 
2.4-Dinilrotoluff." 
Diethylphthalate 
4-Chloro(hen/|-|<h'n, I M'.i' 
lluoiene 
4'Hilioaniline 
4.t-Dinilr6-7-inlh»tihf'ol 
K-niliosodiphenylaai i; 
a-lroaoohtnylphenvl | i u > 
Heiathlrrobfi.'t'e 
K!;S -•[M: 
B t l . ' 
KA°(; 
ug'l 
OJ 
o 
H 
-J 
00 
V U ' . U l ' . l 
Bct:.-
KillR 
jg'l 
K.A 
1/A 
HR 
KF 
| : R 
IR 
KR 
NR 
KR 
NR 
KR 
KF 
NR 
NR 
NR 
NR 
NR 
tm 
NR 
NR 
N l 
KR 
NR 
KR 
NR 
VR 
HP 
NR 
KR 
NR 
NR 
KR 
IIR 
Nf 
HR 
KF 
HR 
Kr 
K l 
tn 
HP 
IIR 
HR 
»R 
K l 
'IR 
VB 
IP 
i... 
uu 
IDDI: 
SAKPIINI 
)H CNIMICAl 
l-OI 
2/28/91 
tP» CASI NO.: I59JJ lAI: CCNPUCHtN 
1 i I L..^, 
I i i i I i I ] [• i: r \ m \ r 1 
SITE INSPECTION „^^.^LIN6 RESULTS 
(cont'd) 
pfsriciDfs 
Silpit ID Ho. 
traltic Report No. 
Nilrli 
Units 
Dilution Faclor/CPC Cleanup IT) 
Percent Hoisture 
lIphi-tHC 
bela-IHC 
deUa-IHC 
gaiaa-IHC (lindane) 
Keptichlor 
Aldrin 
Heptachlor epoaida 
(ndosullin 1 
Dieldrin 
4,4'-00( 
Codrin 
(ndosulfan 11 
4,4"-DDD 
(ndoiullaA sulfate 
«.l'-ODI 
tiethoiychlor 
(ndrin ketone 
ilphi-Chloidine 
gaiia-Chlordant 
loiaphe'ne 
AtocUi-1016 
ltr6clor-l221 
*roclor-l2J2 
«roclor-IJ4J 
; 
Arocloi-nil 
; 
«roclor-l2SI 
', 
«roclor-12iQ 
', 
;*I25-RIN; 
: 8GII9 
1 NAUR 
: ug/l 
1 
[ 
virsimi 
tCl22 
UMIR 
ug/l 
N/A 
N/A 
NR 
NR 
HR 
KR 
NR 
KR 
HR 
NR 
NR 
NR 
KR 
NR 
NR 
HR 
NR 
KR 
RR 
HR 
NR 
KR 
HR 
NR 
H) 
HR 
NR 
HR 
HR 
to 
o 
-J 
HOKS: 
lUnk ipict - coipound enilyiid for but 
not diticled 
I - coepound found in lib bliiik as veil as 
stipla, indicates possible/probable 
blink conliAinitioA 
( - estiiated value 
J - estiiated value, coipound present 
biloK CIQI but above IDl 
I • analyiii did nol pats ( M OA/QC 
I - Presuiptive evidence of the presence 
ol the taterial 
analyiii nol required 
Detection liaill elevated if Dilution 
FiCtor )l and/or percent toisluie >0\ 
nil 
\-. 
FT) t
< 
O •
y\m\ 
H m i U DAI.. ./2I/9I 
m m i HO.: IS)]) 
U l HAHE: SItHNEfl 
IHOICAHtCS 
Seiple ID lo. 
Trifflc leport Ko. 
Iitrli 
Unttt 
Dilution Fictor 
i » 1 1-1 y i-L/w.' ' * 
SITE INSPECTION SAfi. uiNG RESULTS 
(cont'd) 
# 
1 i. ) i 1 
1 i 
\- 
i 
VI2S-GNIINS/KSDI 
NBFIOI 
HUP 
ug.'l 
VI25-C1(2 
HBril02 
NIIER 
ug/l 
V125-C»1(DUP1 
NBFAOJ 
HAKI 
ug/l 
«I2S-CH 
KBFA04 
•AIEI 
ug/l 
VIIS-GVS 
KBFtOS 
lAUH 
U9/1 
yi2i-Q«l 
NBFA06 
I t U R 
ug/L 
VliS-StOI 
NSFAOl 
SEDIHERI 
ig/kg 
VI25-St02 
HIFAIO 
SEDINEHI 
•l/kg 
»12S-SE01 
NBFtll 
SEOIHEHI 
ug/kg 
»12S-S(0IIDUP) 
KBFAI2 
SEDINEHI 
•g/kg 
V125-SED5 
HeFAII 
SEOIHEHI 
•9/kg 
y|2S-SEOI 
KBFtll 
SEDINEHI 
•g/kg 
y|2S-SI|NS/NSDl 
KIFAU 
SOU 
• 9 / k | 
9125-SJ 
NIFAU 
. SOU 
i | / k | 
»I25-S1 
MFtIS 
SOU 
•|/k| 
lluilnua 
Intlkony 
kriinic 
l i r l u i 
i i r r l l l u i 
Cidilui 
CiUlui 
Oiroilui 
Cobilt 
Copper 
Iron 
leid 
Xi|ieelui 
Hin|ineee 
KifCiirif 
llcMI 
rotiiiiui 
tileniui 
Silver 
lodlui 
I l i i l l l g i 
riaidiiii 
Ilic 
WUS: 
llink ipici - coipound inilyiid for but 
AOt ditictid 
( • i i t i i i t i d vilue 
J • u t i l l t e d Tilui. coipound present 
belov CIDl but ibove 101 
i - i n i l y i l i did nol piss (PA OA/QC 
l l - i n i l M i t not riouired 
J 
J 
eiioo 
J 
.121 E 
f (M.I 
4|S00 
J 
^c» ( 
J 
J 
J 
iUOO 
i 
J 
L>:>4 
4^100 
.31] 
J 
J 
14100 
J 
J 
fltit.l 
Sl(SOO 
.400 
i 
J 
12^00 
i 
i 
<.>''3.» 
itlaoo 
c ) l f . l 
J 
J 
J 
iibo 
J 
i 
0OJ.1 
40^00 
r J O t . l t 
J 
J 
r/ioo 
J 
" C .» 
t l 00 
J 
" " Q . n ! 
J 
5M' 
tsioo 
J 
90.3 
45100 
II.I I 
14.f 
41.4 
2SI00 
IS.I 
fllO 
954 
10.1 ( 
J 
oSO.3 I 
i 
J 
a f . c n . i 
53.9 E 
32400 
J 
3.2 E 
115 
14900 
l i . 3 E 
23.1 
10.5 
35100 
f.5 
lOiOO 
1320 
13.1 I 
1490 
(2.1 
13.5 E 
30100 
J 
4.1 E 
I t l 
J 
19900 
W . I E 
24.1 
12 
39200 
I.i 
I IIOO 
IIOO 
14.1 E 
itOO E 
Jl^doo E 
Jfl/oO E' 
590^00 ( 
5 ) 2 ^ E 
Ij/oOO E 
J 
IMO E 
J 
13.2 
12.3 E 
33(00 
3.8 E 
122 
12100 
11.8 E 
25.4 
il.t 
31100 
I.t 
I IIOO 
1430 
15.2 E 
IIOO 
1150 E 
ei.i 
IJ.I E 
9400 
10100 
21.1 E 
J 
I E 
5.5 E 
48.1 
35.1 
51200 
5/,I E 
13.1 
31/ 
113000 
4tt 
4140 
925 
41,1 E 
4.5 
42IQO 
110 E 
tf.3 
lOi 
121000 
- 
Ill 
5000 
1120 
49.1 E 
J 
J 
J 
1500 E 
irio E 
13100 
101 
11100 
I I . I E 
13.4 
si.r 
21500 
t 
M30 
135 
10.) E 
l l i o 
14.J 
142 E 
21)00 
21000 
J 
l . l E 
l . l E 
131 
1)1 
11)00 
D.i ( 
11.1 
II.I 
44101 
n . j 
)I00 
lose 
11.1 E 
11)0 
11.1 
31) E 
1)100 
4) E 
21.1 
)1.) 
11)00 
311 
)420 
91) 
31.1 ( 
1)20 
13.5 
312 E 
U> 
O 
O 
\\ 
01/21/91 
H 
SIU fAnr; 
/I (N(n|('.'. 
• 
IDDI: 
0:''<I0|-C4 
• 
fUnPllllG DAU: 
2 / : ; ' ' l 
• 
[PA u s t NO.: 
1 ! 1 : J U I : 
: ' n f ' i ! ( f < 
• 
tini'VOlAIIKS 
• 
Siaole ID >lo. 
• 
I r a l f i c Repo-I Ko. 
• 
Kalriit 
1 
Unit! 
1 
Dilutio.i faclor/crr C l n . u r 
n . 
1 
Percent iloisluie 
1 
Pentachlorophenol 
1 
Pheninlhrei^e 
1 
Anthracene 
Di-n-butylphlhalate 
Fluoranthene 
Pyrene 
lutylbeniylohlhjIalF 
J.J'-Dichlorob*niidine 
leniolalanlhracene 
Chrysene 
b i s l } - n h y ) h e i ' y n p h l . j l . . i ( 
Di-n-octylphlhalale 
leniolbllluorarlhenr 
bentolkUluoranthere 
lentolalpyrene 
lndenoll,;.3cdloyiei.e 
Oib'ent|a,hlanlhtac(i>e 
len(o|g,h,i)oerylen( 
; 
HOKS: 
Blank space • coapouid aial';e': Jo- tut 
not delecUd 
1 - coipound fruno in lal blani >• mW 
i : 
saaple. inditales r o i s i M t / i . i p : a t l f 
blank contaiination 
[ • estiialed value 
) • estiiated value. (o>noun< o t t i n . l 
beloM CROl but atovF I U 
R • analysis lid nol p n ! EP-I OA.'i': 
H - Presuapli/e evi'ltnc' i-l He ; . ! i n { ( 
of Ihe a a t e r i i l 
HR - analysis nol 
i f o i i i * J 
Detection l i a i l s e l e v i l ' l i l t'lluH.-r. 
facloi >l and'or pe'trnl a j i s l m ; 
K 
• I . - ' I N : vi:5-uiM 
BCir- 
BCl.T 
KAUP 
NAUR 
ug/l 
ug/l 
1 
N/A 
N/A 
NR 
NR 
HR 
KR 
HR 
NR 
KR 
NR 
NR 
NR 
N^ 
NF 
IIR 
KR 
NR 
NF 
KR 
NR 
i/\BLE ! 
SITE INSPECTION SAMPLING RESULTS 
(cont'd) 
to o 
-J 
vn 
' ^ 'I \ ] ) j 
M i l 
I 
ri/)i' 
r I ' ! .• i 
I i' { #1 
V 
> 
• :i 
;• 1 r 
DIE HAHE: V] CNEHICU 
IDOI: ei-)iei-04 
tAKPlIlt DUE: 1/21/91 
EPA CASE 10.: 15133 
U l IIHE: SIIHHEI 
TABLE 1 
SITE INSPECTION SAMPLING RESULTS 
(cont'd) 
IIOIMIICS 
tuple ID Ho. 
Iriffic Report Ho. 
Hitrli 
Uilti 
Dlltllon fictor 
Aluiliiiii 
litliony 
Ariiiiic 
l i r l u i 
I i r r l l l u i 
Cidalu* • 
CilcUi 
Chroilai 
Cobilt 
Copper 
Irta 
(lid 
lifaeilui 
Riniiniia 
Rerciry 
lickel 
rotiiiiui 
lllver 
lodlea 
l l i i l l l i i 
Yinidin 
line 
; VI25-58 
; KBIA22 
SOU 
: 
«9/k9 
: 
I92P0 
: 
J 
11) 
• 
IIOOO 
20 ( 
19.5 
• 
43.1 
. 
25100 
9.9 
5M0 
IPIP 
10.3 f 
2500 
J 
81.9 
U . l ( 
VI25-RIHI 
VI25-RIH2 
KBFAII 
K8FAt9 
NAUR 
NAUR 
ug/l 
ug/l 
J 
J 
J 
J 
J 
'^•223 [ 
J 
O . ' ^ l . l 
J 
J 
i 
J 
0.21 E 
J 
J 
. 
J 
J 
J 
9125-IIUI 
I/A 
H/A 
U|/l 
III 
HI 
HI 
HI 
XI 
XI 
HI 
HI 
HI 
XI 
HI 
XI 
XI 
XI 
HI 
HI 
HH 
HI • 
HI 
HI 
HI 
Nl 
Kl 
XOIES: 
Hint ipitt - coipound inily;ed lor but 
•ot detected 
E - iitliited vilui 
J - iitlaitid yelue, conpound oresent 
bilON CROl but ibove IDl 
I - inilrili did not piss (PA QA'OC 
HI - inil|iiii not reouired 
to o 
M 
Ul 
;o t
(t> I
< 
O 
Appendix N 
Figures Showing Previous Sampling Locations 
\WORK\2423l\02\WORKPLA.N.REP 
HARDING LAWSON ASSOCIATES 
301753 
Figure 10 
ICC Plot Plan: 
Trenches 
T r e n c h e s 
1-12 
301754 
> 
/i 
> 
I 
to 
o 
M 
vJ 
UT 
Ul 
ony RIVER eeo 
' aOnitIO LOCATIONS 
0 
«' 
• • ' 
[ = € = : y = y 
9 c « l « 
WAREHOUSE 
Figure 9 
ICC Laboratory Pil 
U a b o r a l o r y 
P U 
4 " 
P V C 
L i n o 
:((i) ---.-rrr 
4 " 
P V C 
L i n e 
LOAOINC DOCK 
/ t 
- / i 
fHvina sciCHCes. w c 
Cll.Ill 
! t £ 
l>i*w»» Ity . . . n . . O J I » . . _ - " 
tu.uvl (ly ll*f ('<>• 
l u i i l 
'-i^tt.ttl. 
i n . . . . 
m 
"1 
1 
St. Croix, VI 
DPYING OVEN 
- toluene contaminated soil 
v m 80651095 
1 
1 
y 
Right 
Side 
(North Side) 
NORIH 
( Tcp View ) 
c3oor 
Coirosite soil sarrple frcm crying oven 
° 
1087001 - l e f t side (south side) 
° 
#087002 - right side (north side) 
- 1 
1 
I 
I , 
J 
- • 
— 
door 
Ijsft 
Side 
(South Side) 
( Not to Scale ) 
* Each rectangle represents one bin containing 
a stack of twenty trays. 
Figure 4 - Sarple location Map - Drying Oven 
jse-ft 
3 0 1 7 5 6 
^ 
^,,,ftr ^ - ' ' ^ ^^'*""
Berlex Laboratories 
St. Croix, VI 
VID 80651095 
LAB WASTE DRAIJiAGE AREA 
- pyridine contaminated soil 
Building 
® 
® 
® 
• 
® 
® 
® 
• 
® 
® 
(foimer loading dock area) 
-
— I 
^ 
NORTH 
• 
^ ) 
- Sanple locations for conposite 
Soil sanple frt^n north side of the lab Waste Drainage Area 
" Surface - #087003 
" Subsurface - #087004 
Soil sample fron south side of the lab Waste Drainage Area 
" Surface,- #087005 
» Subsurface - #087006 
( Not to Scale ) 
Figure 5 - Sanple Location Map - Lab Waste Drainage Area 
301757 
irc/ri. 
r^ff-r t t ^ Q r 
t u t r i x Iy,-t^tt.\. 
Figure 3 
flap qt .sarrpiincj_points 
1 
:3 
J 
• a 
•I 
•a 
i 
*i 
O^S-SSS 
CD 
OD 
CD 
CD 
OD 
CD 
CD 
LAB..; 
'•^' IST 
^ - - 7 L 
•«4-rt-«>..«r 
« . * « C*«wiCAl. h.OT fvwe 
M 
MC 
tJ^ 
PW 
M 
•-•—* 
X = Sanpiing point 
• 
= Production %^ell 
301758 
K o t t n c - a 1 , 
^ C H I7.l1fl<- 
5«^t«- t*C*Tl*rv^ 
CHEMICAL, ST. CROIX, U.S.V.l 
cnRprTr=f ATirvM 
Appendix O 
Compendium of Groundv^^ater Data 
\WORK\24231\02\WORiCPLAN.REP 
HARDING LAWSON ASSOCIATES 
301760 
n\ 
DATE: 
JECT: 
FROM: 
TO: 
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY 
OCT 1 8 1990 
REGION II 
Virgin Island Chemical Co. (VIChem) - Well Water Data 
John Higgins, P.E., On-Scene Coordinator 
Response & Prevention Branch 
Sherrel Hemy, Remedial Project Manager 
Eastern New York/Caribbean Remedial Action Branch 
Please find attached the, "Compendium of Well Water Data Collected at the Virgin Island Chemical Co. 
by the USEPA (1986-1990)." Thank you for reviewing the draft version. As we agreed, I am sending this 
report to Ms. Yvette Canegatta of the Virgin Island Department bf Natural Resources. This repon will 
also be appended to the VIChem OSC Report 
I can be contacted at (FTS) 340-6194, should you have any questions regarding the removal action ar 
VIChem. 
Attachment 
cc: Yvette Canegatta, VIDPNR 
^ 
301761 
^\r-/^i*^»t tt r- f^r^t t 4 o^s^v 
4 ff^ in F \ 
COMPENDIUM OF WELL WATER DATA 
COLLECTED AT THE VIRGIN ISLAND CHEMICAL CO. BY THE USEPA 
(1986-19901 
FOREWORD 
The piirpose of this report is to summarize pertinent sampling data and information regarding the volatile 
organic, well water data coUected by the United States Envirormiental Protection Agency (EPA) during 
various sampling events at, and in the vicinity of the Virgin Island Chemical Co. (VIChem) Hazardous 
Waste Site in St Croix during and prior to the 1990 Superfund Removal Action. Summary repons of ezch 
of these sampling events are included in the VIChem Removal Action Site Files. 
A review of the data indicates that Chloroform was consistently the dominant contaminant during each 
of the sampling events. For this reason, Chloroform results are included herein and are plotted in the 
attached graph, "Chloroform Contamination in Well Water - Virgin Island Chemical Co. Site, St. Croix". 
Since the purpose of this repon is to merely assemble pertinent data, and not to interpret the data or 
make recommendations based on the data, all analyzed data, including qualified and rejected data, are 
included in this report. 
It should be pointed out that the Drinking Water Maximum Contaminant Level for total trihalomethanes 
is 100 ug/l (See 40 CFR §141.12) and the 1980 Federal Water Quality Criteria for Chloroform (as revised), 
based on a carcinogenicity of IO"*, is 5.70 ug/l for human exposure from contaminated water and fish. 
COMPENDIUM 
•j 
1. RCRA Enforcement (3/13/86) The Environmental Services Division (ESD) of Region 2 conducted a 
RCRA Enforcement Inspection of the VIChem facUity, then known as Berlex Laboratories, on March 13, 
.1986. The inspection included 3 soD samples taken from the intermittent stream, or "gut", on the site 
perimeter, 2 soil samples obtained from the laboratory water drainage pit, and one sample taken from Lhe 
production well in the northwest comer of the property. The results of the organic analysis from the 
production well indicated Chloroform contamination at a level of 130 ug/l. 
2. St. Croix Well Survey Phase I (3/7/88-3/10/88) The Response and Prevention Branch (RPB) conducted 
well sampling for volatile organic constituents at 21 locations in St. Croix, including four wells in the 
vicinity of the VIChem Site. The data was rejected by the Monitoring Management Branch (MMB) due 
to excessive holding times. Chloroform contamination was indicated in the October 25, 1988 repon. 'Si. 
Croix Well Survey", prepared by Weston - TAT, as shown below: 
Well Name 
- Fairplains #6 
Fairplains #9 
. VIPA #1 
VIPA #2 
Chlorofonn (ug/l) 
24 
75 &70 
11.5 
11.3 
3. St. Croix Well Survey Phase I (10/31/88-11/2/88) RPB resampled wells at eight locations, including 
four wells in the vicinity of the VIChem Site. Chloroform contamination was indicated as shown below: 
Well Name 
Fairplains #6 
Fairplains #9 
Fairplains #8 
VIPA #2 
Chloroform (ug/l)' 
35.9 
10.4 & 9.7 
12.4 
1.6U" 
"* Chloroform was not detected at the detection level of 1.6 ug/l. 
3 017 62 
4. VIChem Removal Action Phase I (1/17/90) During Phase I removal action activities at VIChem, three 
off-site wells and the on-site water tank were sampled for volatile organic contamination. Analytical 
services were provided by a private laboratory procured by the TAT. In addition to the routine QA/QC 
required for Level 2 Removal Program sampling, two performance evaluation samples and one blind 
duplicate sample were analyzed. TAT validated the data and, although QA/QC discrepansies were slight 
and few, the data was qualified as estimated. Once again, Chloroform was the most dominant compound 
in each sample; the data for this contaminant are shown below: 
Well Name 
Fairplains #6 
Fairplains #9 
Fairplains #8 
Water Tank 
Chlorofonn (ug/I) 
39.0 
25.0 
5.0 
23.9* 
* This is an average of Chloroform contamination in the three tank samples (Water tank sample = 23.9 
ug/l, Water tank drain sample = 22.7 ug/l. Water tank pump sample = 25.0 ug/l). 
5. VIChem Removal Action Phase I f6/25/90) During Phase II removal action activities at VIChem, four 
off-site wells were sampled and analyzed for volatile organic contaminants. When detected, Chlorofonn 
was the most dominant compound in each sample and in 3 out of 4 samples the only VOC detected. 
Analytical services were provided by the Contract Laboratory Program and the data was validated by MMB. 
The only data qualified was for a QA/QC sample for a single compound. The Chloroform data for this 
sampling event are shown below: 
Well Name 
Fairplains #6 
Fairplains #9 
' 
VIPA #1 
VIPA #2 
Chloroform (ug/l) 
11 
39 
2J* 
' 
5U* 
* An estimated value of 2 ug/l was reported. 
** Chloroform was not detected at the detection level of 5 ug/l. 
T** 
301763 
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Chloroform Contamination (ug/l) in fell Water 
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