' 610 W. MAIN ST.. ROCKAWAY, NEW JERSEY 07866 
cnvino ^ 5C!£nc£; inc. 
^ ^ ^ - " ^ 
19 COPELAND RD.. DENVILLE. NEW JERSEY 07834 
^^'^yyy. 
(201)366^256 
f \ ~ s . ^ 
SDMS Document 
115531 
Apr II 1 7 , 1 9 8 6 
M r . C h a r I e s D o I an 
U S E P A , 
E R R D 
26 F e d e r a l 
P l a z a 
R o o m 7 4 7 , S I C B 
N e w Y o r k , N Y 
1 0 2 7 8 
R e : 
I s l a n d C h e m i c a l 
C o m p a n Y . U . S . v i r g i n 
I s l a n d s 
D e a r M r . D o l a n : 
As per o u r t e l e p h o n e 
c o n v e r s a t i o n , I am s e n d i n g the e n c l o s e d 
I n f o r m a t i o n 
c o n c e r n i n g 
E n v i r o - S c i e n c e s , I n c . w o r k at the 
I s l a n d 
C h e m i c a l 
C o m p a n y 
s i t e in S t . C r o i x , U . S . V . l . 
I t r u s t 
t h a t 
t h i s 
p a c k a g e will b e h e l p f u l in y o u r u n d e r s t a n d i n g of the a c t i v i t i e s 
w h i c h 
h a v e o c c u r r e d o n the s i t e d u r i n g the p r i o r o n e a n d o n e - h a l f 
y e a r s . 
A S w e d i s c u s s e d , I w i s h to m e e t w i t h y o u c o n c e r n i n g 
t h i s m a t t e r . If 
p o s s i b l e , I w o u l d p r e f e r to s c h e d u l e 
t h i s m e e t i n g for T h u r s d a y 
mor n 1 ng , A p r i I 24 t h . 
If y o u h a v e a n y q u e s t i o n s , c o n t a c t m e at 2 0 1 / 3 6 6 - 6 2 5 6 . 
V e r y 
t r u l y y o u r s . 
E N V I R O - S C I E N C E S , I N C . 
^ 
izq (^7rJ^-nc/' y^Ol 
A l a n L. K y I e s , P h . D . 
V i c e 
P r e s i d e n t 
A L K / p o 
( A K - 8 6 1 4 3 ) 
E n c l o s u r e s : 
P r o j e c t 
S u m m a r y w i t h 
a t t a c h m e n t s 
c c : ; R . M i I o s 
F. Cur t i s 
R . W i l l i s 
1 . Ar s h e n 
S E N T V I A F E D E R A L 
E X P R E S S O N 4 / 1 7 / 8 6 . 
100086 
P r o l e c t 
S u m m g r y 
for 
I s l a n d C h e m i c a l 
C o m p a p y . 
Inc.. 
( B e r l e x ) S t . C r o l y . V i r g i n 
I s l a n d s 
•
^ 
I n c l u d e d h e r e i n 
Is a s u c c i n c t 
s u m m a r y 
for the e n v i r o n m e n t a l 
c l e a n u p 
of 
I s l a n d C h e m i c a l 
C o m p a n y 
( I C C ) , S t . C r o i x , V i r g i n 
I s l a n d s . 
D o c u m e n t a t i o n 
for all a c t i v i t i e s a r e 
I n c l u d e d as a t t a c h m e n t s . 
E n v i r o - S c i e n c e s , 
Inc. i n i t i a t e d a s i t e e v a l u a t i o n 
In S e p t e m b e r , 
1 9 8 4 
a n d c o n t i n u e d 
the 
I n v e s t i g a t i o n 
Into O c t o b e r . 
C o n t a m i n a t i o n 
w a s 
f o u n d at s e v e r a l 
l o c a t i o n s a n d a p r e l i m i n a r y 
c l e a n u p p l a n 
w a s 
d e v e l o p e d 
and d e l i v e r e d 
to M r . C o n r a d S i m o n , U S E P A R e g i o n 
1 1 , N e w 
Y o r k d u r i n g D e c e m b e r , 1 9 8 4 . 
( S e e A t t a c h m e n t A ) . 
M r . S i m o n a s s i g n e d M r . R o b e r t H a r r i s as the p r o j e c t o f f i c e r . 
A f t e r 
n u m e r o u s t e l e p h o n e d i s c u s s i o n s a n d 
I n f o r m a t i o n r e q u e s t s by M r . 
H a r r i s , an a d d e n d u m to the o r i g i n a l 
r e p o r t w a s s u b m i t t e d 
in A p r i l , 
1 9 8 5 
(At t a c h m e n t B ) . 
F o l l o w - u p c o n v e r s a t i o n s w i t h M r . H a r r i s 
i n d i c a t e d 
that the 
p r o p o s e d 
p r o g r a m w a s s a t i s f a c t o r y . 
I r e q u e s t e d 
a letter of a p p r o v a l 
f r o m 
h i m ; 
h o w e v e r , he s t a t e d that the U S E P A w o u l d not 
issue a l e t t e r . 
He did 
s t a t e 
that 
I s h o u l d send h i m a l e t t e r s t a t i n g our 
intent 
to 
c l e a n u p 
(At t a c h m e n t C ) . 
D u r i n g 
the a p p r o v a l 
p e r i o d , M r . H a r r i s r e q u e s t e d c o p i e s of 
h a z a r d o u s 
w a s t e m a n i f e s t s 
for m a t e r i a l s s e n t 
f r o m the f a c i l i t y by ICC in 1 9 8 2 
( A t t a c h m e n t 
D ) . 
B e t w e e n J u n e and A u g u s t , 1 9 8 5 s e v e r a l 
t a s k s 
w e r e 
p e r f o r m e d 
at the ICC s i t e . 
T a s k s p e r f o r m e d 
by d a t e s are 
summarizisd 
be I o w : 
1 . 
J u n e 6 - 1 5 . 
1 9 8 5 
T o l u e n e C o n t a m i n a t i o n 
f O r v e r ) 
S o i l 
from e i g h t 
(8) of a t o t a l 
of 14 d r u m s of 
t o l u e n e - c o n t a m i n a t e d 
soil w a s put on d r y i n g t r a y s and p l a c e d 
in 
the d r y i n g o v e n . 
T e m p e r a t u r e 
r e a c h e d 
a p p r o x i m a t e l y 
42 d e g r e e s C 
a n d c o n t i n u e d 
to i n c r e a s e as m o i s t u r e w a s 
l o s t . 
T w o 
( 2 ) 
2 0 - g a i l o n p i a s t i c - I i n e d 
p a p e r b a r r e l s w h i c h w e r e o n e - h a l f 
full 
of 
s o i l 
and w a t e r w e r e p l a c e d 
in the d r y e r 
intact 
in an a t t e m p t 
to 
e v a p o r a t e 
the w a t e r b e f o r e p l a c i n g 
the soil o n t r a y s . 
E x h a u s t 
f r o m the v e n t w a s m o n i t o r e d w i t h a F l a m e 
I o n i z a t i o n D e c t o r 
( F I D ) 
for e m i s s i o n of T o l u e n e . 
P y r i d i n e C o n t a m i n a t i o n 
( L a b o r a t o r y 
P i t ) 
All 
liquid w a s t e to the 
l a b o r a t o r y 
pit w a s r e r o u t e d ; 
n o n - c o n t a c t 
c o o l i n g w a t e r 
to the gut a n d 
l a b o r a t o r y 
r i n s e w a t e r 
to a 
s t a i n l e s s steel c o n t a i n e r . 
All 
l a b o r a t o r y w a s t e s 
( r e a g e n t s , 
s o l v e n t s , e t c . ) w e r e c o l l e c t e d 
in 5 5 - g a l l o n d r u m s a l o n g 
w i t h 
f i r s t and s e c o n d 
r i n s e s . 
100087 
P o r t a b l e 
t o i l e t s w e r e p r o v i d e d 
to r e p l a c e 
the o f f i c e 
f a c i l i t i e s 
s i n c e 
it w a s s u s p e c t e d 
t h a t the s e p t i c 
t a n k m i g h t 
be 
In the 
I a b o r a t o r y 
p i t . 
C o n c r e t e w a s b r o k e n 
In an a r e a o u t l i n e d 
by t e s t h o l e s 
w h i c h 
e x h i b i t e d 
h i g h p p m e m i s s i o n s d u r i n g a b o r i n g p r o g r a m 
In O c t o b e r , 
1 9 8 4 . 
S o i l w a s e x c a v a t e d 
and p l a c e d 
a r o u n d 
t h e o p e n e d p i t . 
The 
s i d e w a l l s a n d f l o o r of t h e e x c a v a t i o n 
w e r e e x a m i n e d w i t h 
the FID 
for o r g a n i c e m i s s i o n s . 
R e a d i n g s a l o n g 
t w o s i d e w a l l s w e r e 
In the 
7 0 0 - 9 0 0 p p m r a n g e . 
T h e s e w a l l s w e r e e x c a v a t e d 
a n d 
r e c h e c k e d . 
F i n a l l y , a pit w a s e x c a v a t e d w h i c h d i d n o t e l u c i d a t e 
a p p m 
r e a d i n g o n the F I D . 
T h i s pit m e a s u r e s 
3 0 x 3 0 f e e t a n d 9 feet 
d e e p . 
E x c a v a t i o n 
r e v e a l e d 
t h a t a p r e v i o u s o w n e r 
laid m a c a d a m o v e r 
the 
e n t i r e a r e a a b o u t 
t w o ( 2 ) feet b e l o w t h e p r e s e n t 
level of 
the 
c o n c r e t e . 
A later o w n e r 
c o v e r e d 
t h e m a c a d a m w i t h a b o u t o n e 
and 
o n e - h a l f 
f e e t of s o i l 
a n d p o u r e d c o n c r e t e 
to t h e p r e s e n t 
l e v e l . 
T h e 
l a b o r a t o r y w a s t e s 
f l o w e d 
into a p i t w h i c h w a s a b o u t 8-9 
feet 
d e e p . 
T h e b o t t o m 
t h r e e 
( 3 ) feet w e r e f i l l e d w i t h c o b b l e . 
W h e n 
l i q u i d f i l l e d 
the p i t , 
it w o u l d 
f l o w 
i n t o a f o u r 
( 4 ) inch 
P V C 
p i p e and d r a i n to a n o t h e r 
c o b b I e - f 1 1 1 e d 
pit n e a r 
the r e a r 
f e n c e . 
T h i s pit w a s 
i n v e s t i g a t e d 
d u r i n g O c t o b e r 
( s e e p r o g r e s s 
r e p o r t ) . 
D r a i n 
L i n e s 
T w o ( 2 ) s t o r m d r a i n 
l i n e s w e r e e x c a v a t e d 
to r e p l a c e 
the 
e x i s t i n g 
l i n e s w h i c h w e r e d e t e r i o r a t e d 
and c a v i n g 
in at 
s e v e r a l 
l o c a t i o n s . 
B o t h 
l i n e s w e r e c o n s t r u c t e d 
of 5 5 - g a l l o n d r u m s 
w h i c h 
w e r e w e l d e d . 
E x c a v a t i o n 
r e v e a l e d o n e 
line c o n t a i n e d 
a s l u d g y 
m a t e r i a l 
w i t h an o i l y 
t e x t u r e . 
T h i s m a t e r i a l 
w a s c o l l e c t e d 
and 
p l a c e d 
in 5 5 - g a M o n , o p e n 
top d r u m s 
( 1 3 t o t a l ) a n d s t o r e d 
u n t i l 
a n a l y s i s 
I n d i c a t e d 
the c o n s t i t u e n t s . 
D r u m s f r o m 
the d r a i n 
line 
w e r e p l a c e d 
in a c o n t a i n e r 
for 
later d i s p o s a l . 
N o s l u d g e or 
r e s i d u e w a s p r e s e n t 
in t h e s e c o n d d r a i n 
l i n e . 
T h e b a r r e l s 
from 
t h i s 
line w e r e p l a c e d 
in a c o n t a i n e r 
for 
later 
d i s p o s a l . 
O n e 
line w a s r e p l a c e d w i t h 
10 inch P V C 
p i p e . 
T h e e x c a v a t i o n and r e p l a c e m e n t of e a c h 
line w a s d i s c u s s e d 
w i t h 
P u b l i c W o r k s as to the n e e d for an " E a r t h C h a n g e " p e r m i t . 
A f t e r 
r e v i e w and 
i n s p e c t i o n , P u b l i c W o r k s d i d n o t r e q u i r e a p e r m i t 
for 
rep i a c e m e n t . 
P r o c e s s 
Pit 
• 
D u r i n g t h i s f i e l d v i s i t 
( J u n e 6 - 1 5 ) 
s a m p l e s w e r e t a k e n 
f r o m 
v a r i o u s a r e a s and s e n t 
to s t a t e s i d e 
l a b o r a t o r i e s 
for 
a n a l y s i s . 
T h e s e 
l a b o r a t o r i e s a r e 
i n d u s t r i a l 
C o r r o s i o n M a n a g e m e n t , 
Inc. 
( I C M ) , R a n d o l p h , N e w J e r s e y and Y o r k L a b o r a t o r i e s , 
I n c . 
( Y o r k ) , 
M o n r o e , C o n n e c t i c u t . 
D u p l i c a t e s of m o s t 
s a m p l e s w e r e s e n t 
to 
e a c h 
l a b o r a t o r y as a q u a l i t y c o n t r o l , p r o c e d u r e . 
100088 
T h e 
f o l l o w i n g 
s a m p l e s 
w e r e 
t a k e n 
L o c a t 1 o n 
T y,ii.e. 
NP. 
A n a .1 y s I s 
D r y e r 
S o i 1 
L a b o r a t o r y 
P i t 
S o i l 
D r a i n L 1 n e s 
P r o c e s s P i t 
1 I - J u n e 
31 - J u l y 3 
L i q u i d 
2 
So 
S 1 u d g e 
9 
T o l u e n e 
P y r 1 d I n e 
V o lat 1 le 
O r g a n i c s 
V o I at i I e 
O r g a n 1 c s 
P r i o r i t y 
P o l l u t a n t s 
P l u s 
4 0 
C o m m e n t s 
T w o ( 2 ) s a m p l e s 
to 
e a c h 
l a b o r a t o r y 
F o u r ( 4 ) s a m p i e s to 
e a c h 
l a b o r a t o r y 
I CM on 1y 
T w o ( 2 ) s a m p les to 
e a c h 
l a b o r a t o r y 
I CM on 1y ; alt 
s a m p l e s 
c o m p o s i t e d 
to o n e 
s a m p l e 
T h e s i t e w a s r e v i s i t e d a n d s o i l 
s a m p l e s w e r e t a k e n f r o m 
the 
d r y e r 
( 4 ) and the l a b o r a t o r y pit 
( 8 ) . 
T h e s a m p l e s w e r e 
d i v i d e d 
e v e n l y b e t w e e n the 
l a b o r a t o r i e s . 
T h e r e m a i n i n g six 
( 6 ) 
b a r r e l s 
of t o l u e n e - c o n t a m i n a t e d 
s o i l w a s 
l o a d e d o n t o t r a y s and p l a c e d 
in 
t h e d r y e r . 
In a d d i t i o n , 
l i q u i d s a m p l e s from the p r o c e s s 
pit 
w e r e t a k e n for P r i o r i t y P o l l u t a n t s p l u s 4 0 a n a l y s i s . 
H o w e v e r , 
t h e y w e r e 
lost 
in s h i p m e n t 
and h a d 
to be r e t a k e n at a 
l a t e r 
d a t e . 
I I I - J u l y 16 - 19 
T h e s i t e w a s r e v i s i t e d a n d f o u r 
( 4 ) s a m p l e s e a c h 
w e r e 
t h e d r y e r and the l a b o r a t o r y p i t . 
T w o ( 2 ) s a m p l e s of 
s e n t 
to e a c h 
l a b o r a t o r y . 
P r i o r i t y 
P o l l u t a n t s p l u s 
4 0 
s a m p l e s w e r e r e t a k e n f r o m the p r o c e s s 
p i t . 
IV - A u g u s t 
6 - 9 
t a k e n 
f r o m 
e a c h 
w e r e 
w a t e r 
A d d i t i o n a l 
c o n d u c t e d . 
s a m p l i n g of t h e 
l a b o r a t o r y pit and d r y e r 
w a s 
A n a l y t i c a l 
s h e e t s for the f i r s t 
t h r e e ( 3 ) s i t e s a m p l i n g p e r i o d s 
a r e 
in A t t a c h m e n t 
E w h i c h w a s a r e q u e s t of C o n s e r v a t i o n and 
C u l t u r a l 
A f f a i r s . 
A n a l y t i c a l 
s h e e t s for the A u g u s t v i s i t 
a r e 
in A t t a c h m e n t 
F. 
Nu.T.erous s a m p l e s b e t w e e n J u n e and A u g u s t w e r e d u p l i c a t e d and s e n t 
to 
a n o t h e r 
l a b o r a t o r y , Y o r k L a b o r a t o r i e s D i v i s i o n . 
T h e s e r e s u l t s a r e 
in 
A t t a c h m e n t G. 
100089 
D u r i n g S e p t e m b e r , the s i t e w a s v i s i t e d and s a m p l e s of all 
w a s t e 
s t r e a m s 
( c o n t a m i n a t e d 
a r e a s ) w e r e c o l l e c t e d 
for s h i p m e n t 
to C h e m i c a l 
W a s t e M a n a g e m e n t . 
T h i s d a t a 
Is r e q u i r e d by them b e f o r e they 
can 
a c c e p t w a s t e s for d i s p o s a l . 
T h e m a t e r i a l 
p r o f i l e s h e e t s for 
e a c h 
w a s t e s t r e a m a r e l n A t t a c h m e n t H . 
O n S e p t e m b e r 
1 7 , the s i t e w a s v i s i t e d by M r . L o u i s D i g u a r d i a , 
U S E P A 
R e g i o n 
1 1 . 
He c o l l e c t e d s a m p l e s and d i s c u s s e d 
the s i t e 
a c t i v i t i e s 
w i t h M r . R a y m o n d 
H a y s . 
A f t e r C h e m i c a l 
W a s t e M a n a g e m e n t 
a c c e p t e d 
the w a s t e s t r e a m s 
for 
d i s p o s a l , the s i t e w a s v i s i t e d d u r i n g e a r l y O c t o b e r 
to d r u m all 
m a t e r i a l s 
for s h i p m e n t and d i s p o s a l . 
A t t e m p t s w e r e m a d e to 
d i s p o s e 
of w a s h e d d r u m s 
locally t h r o u g h a v e r b a l 
r e q u e s t 
to A u s t i n 
M c o r e h e a d . 
He s u g g e s t e d 
1 call U S E P A R e g i o n 
ll. 
T h e a n s w e r 
from 
R e g i o n 
II w a s to send a l e t t e r . 
A c t i o n t i m e w o u l d h a v e b e e n 
2-3 
w e e k s . 
T h i s w a s not p u r s u e d d u e to c o s t s . 
tn a d d i t i o n , as per 
the 
r e q u e s t 
of M r . Bob M i l o s 
( B e r l e x ) , p e r m i s s i o n w a s s o u g h t by 
letter 
( h a n d w r i t t e n , A t t a c h m e n t 
I) to e v a p o r a t e , p r o c e s s pit w a t e r 
i n s t e a d 
of s h i p p i n g o f f 
Isiand. 
M r . M o o r e h e a d 
r e s p o n d e d 
to the 
letter 
v e r b a l l y 
that t h i s w o u l d r e q u i r e c o n s i d e r a b l e 
time for a p p r o v a l . 
At 
t h i s s a m e t i m e , 192 d r u m s of h a z a r d o u s w a s t e w e r e 
p a c k e d , 
a n i m a n i f e s t e d 
to C h e m i c a l 
W a s t e M a n a g e m e n t 
for 
d i s p o s a l 
( A t t a c h m e n t J ) . 
o a d e d 
For U . S . C u s t o m s to r e l e a s e the d r u m s h i p m e n t 
in L a k e C h a r l e s , 
L o u i s i a n a 
a letter with s u p p o r t i v e d o c u m e n t s w a s s e n t to M r . Carl 
B e c n e l l 
( A t t a c h m e n t K ) , c u s t o m s b r o k e r 
r e t a i n e d by 
ICC. 
On N o v e m b e r 6, r e s u l t s of the s a m p l i n g by the U S E P A 
( L o u i s 
D i g u a r d i a ) 
w a s r e q u e s t e d 
( A t t a c h m e n t 
L ) . 
At t h i s d a t e (April 
1 6 , 1 9 8 6 ) the 
r e p o r t 
is not 
a v a i l a b l e . 
A f t e r 
a m e e t i n g with B e r l e x 
In W a y n e , 
it w a s d e c i d e d that 
I r e t u r n 
to 
t h e s i t e and s a m p l e the gut for v o l a t i l e o r g a n i c s and 
m e t a l s 
( A t t a c h m e n t M ) . 
A n a l y s e s 
I n d i c a t e the p r e s e n c e of heavy m e t a l s at 
s e v e r a l 
l o c a t i o n s . 
A s u b s e q u e n t 
EP Tox test 
i n d i c a t e s that 
the 
l e a c h a b l e 
f r a c t i o n 
is well b e l o w U S E P A s t a n d a r d s ( d a t a s h e e t 
not 
a v a i l a b l e 
for t h i s s u b m i s s i o n ) . 
In a d d i t i o n , v o l a t i l e o r g a n i c s 
w e r e 
n o t 
d e t e c t e d . 
It w a s d e c i d e d 
that 
I r e t u r n on M a r c h 
13 to take s p l i t s a m p l e s 
w i t h 
U S H P A R e g i o n 
11 p e r s o n n e l . 
T h e r e s u l t s of t h i s s a m p l i n g are not 
a v a i l a b l e at t h i s t i m e . 
C o r r e s p o n d e n c e 
c o n c e r n i n g 
the e x t e n t of s i t e c l e a n u p was f o r w a r d e d 
to 
M r . S i m o n , U S E P A ( A t t a c h m e n t N ) . 
( A K - 8 6 1 3 4 ) 
100090 
ATTACHMENT A 
i 
100091 
PROGRESS 
Kti'UKX 
ISLAND 
C.HE.'^.ICAL 
COMPANY, 
I N C . 
(BERLEX) 
S T . 
C R O I X , 
VIRGIN 
ISLAN'DS 
ATTACHMENT 
/ 7^1^ yc ^^^-
'I 
/ 
Env iro-Scie.Tces , Inc. 
19 Ccpeland Read 
Denville, Nev Jersey G7o5-
(201} 366-6256 
December, 1?S4 
100092 
:.*:TRODUCTICN 
as contracted by Berlex Laboratories, 
nmental study cf their Island 
Erviro-Sciences/ Inc. (ESI) w 
I.'".c. (Eerlex) to ccncuct an envirc 
^ __ 
_ 
Chemical Company, Inc. (ICC) facility in St. Croix, Virain 
Islands. Eerlex sold the facility to Virgin Island Chemical 
Ccnpany, Inc. (VICC) in September, 1984. Under the contractual 
agreement between Eerlex and VICC, ESI is responsible for 
certifying that the facility is environmentally clean and free of 
chemical contamination. 
The following discussion is a summary of the ESI site 
investigations and their results-
SITE HISTORY 
Eerlex accuired the nine year old facility in St. Croix when it 
purchased Cooper Laboratories (Cooper) in 196G. At the time 
purchase the facility was in a non-operational mode. Both C 
of 
oope: 
of the 
_.id the original owner were in the pharmaceuticals area __ 
chemical industry. Exact manufacturing processes used by the 
original owner cannot be documented at this time. Cooper produced 
Neither owner was fully operational during this time. 
c u i n i d i n e 
:iped the f a c i l i t y 
and o p e r a t e d 
for about two of 
i t s 
sf o w n e r s h i p . 
The f a c i l i t y 
produced 
p r i m a r i l y 
. r , . . . 
^ . . i 
r . i 
r . r . 
T Z l - . . . - ^ A . . ^ . . i r . . . . 
. . . . . . 
. 3 . . - . . . . . . • . • ; . . . . . ^ ^ 
. . U ... . . 
. . U . 
E e r l e x 
revam 
f o u r 
y e a r s o 
cuinidine from quinine 
rethodolocies used produced a 
.rethods used elsewhere in the industry. 
^ 
than a year prior to purchase by vicC 
Production was drsccntinued 
more expensj.ve product than newer 
Th! plant did 
fcr more 
when the 
ew< 
not operate 
SITE EVALUATION 
.".r. Irving Cohen of ESI initiated the evaluation program on 
September 11, 1984 and was replaced by Dr. Alan Kyles on September 
13. The initial phase continued through S<rptember 20, 19S4. A 
second phase was undertaken frcm October 22 through October 31, 
1584. 
T.he entire property was walked and scrutinized for visible surface 
contamination. A backhoe was utilized to open trenches in areas 
where contamination might be expected. Most trenches were 
excavated to a depth of six feet. A portable Flame Ionization 
Detector (FID) was used to sense volatile organic compounds on the 
ground surface and faces of open trenches. (The FID has a 
detection range of 1 to 1,000 ppm.) As the program progressed a 
drilling rig capable cf boring concrete and split-spoon sampling 
fcr soil was broucht to t-he site. 
100093 
Scil samples were taken from all trenched areas showing volatile 
crganic contamination and from bore holes at various depths. All 
trenches were backfilled after investigations were completed. 
Trench and boring locations are shown in Figures 1 and 2. 
RESULTS 
The site evaluation procedures detected four areas of 
ccntamination. These are: 
1) along trench number 4, under concrete slab number 3; 
2) between tanks numbered 8 and 9; 
3) along trench number 9: and 
4) under the concrete surfaced loading dock. 
The contaminated area located along trench 4 is shown in Figure 3. 
T.he contaminant had a distinct odcr of toluene and exceeded a 280 
ppr. reading on the FID. However, gas chromatography sample 
a.-.alysis (Sample numbers S4 through S4-4 ) did not detect the 
presence of toluene or indicated levels of <0.2 ppm. These 
analyses were conducted by two separate Eerlex laboratories. (See 
Appendices A and E, respectively.) The time lag between sample 
ta.^ing and analysis (3 weeks) may account for the difference 
between field readings and laboratory analytical results. 
A three- tc four-foot wide section was removed from slab 3 to 
determine the extent of contamination. 
Inspection with the FID 
i.ndicated that contamination was limited to this area and does not 
extend or penetrate the soil under slabs 2 and 4. Depth of 
cc.ntamination was restricted to the first two to three feet of 
scil. 
All contaminated soil (approximately 4 cubic yards) was placed in 
55 gallon drums and stored in the warehouse for eventual disposal. 
The pit was backfilled with clean soil. 
T.-.e entire area between and in front cf Tanks 8 and 9 was 
ccntaminated with toluene which escaped frcm Tank 8 during 
cleaning. Laboratory analysis indicated that Tank 8 contained a 
1.4 percent solution of toluene and water and the surrounding soil 
ar.d gravel mixture contained 694 ppm of toluene. (See Appendix A, 
Samples Tank 8 and Tank 6-1.) 
Due to rain the prior evening and 
i-pending for later in the day, the area was cleaned. Soil and 
gravel was removed down to a depth of about one foot. At this 
depth a hard clay layer is present. All material including water 
was placed in 55 gallon arums and removed to the warehouse fcr 
later disposal. Sample analysis of the clay soil indicated the 
absence of toluene (see Appendix E, Sample Tank 8-2). 
100094 
When opening trench 9 behin 
was broken (Figure 2 ) . Imm 
pyridine and the FID record 
broken pipe was probed. Th 
usage. Surface water settl 
280 ppm. Further excavatio 
the fence containing stones 
emissions from the pit appr 
discontinued for about 4 we 
Surface samples (Figure 2) 
drains to the dry river bed 
nunbers D-1 through D-5; se 
were absent of pyridine: ho 
pps), D-2 (507 ppm) and D-5 
a quinine sulfate were pres 
pyridine odcr was prevalent 
period. 
d the loading dock, a 
ediate odor indicated 
ed in excess of 1,000 
is pipe was dry, indie 
ing in the open cut ha 
n and line tracing lea 
and covered with tin 
cached 800 ppm. Furth 
eks until the return v 
were taken in the erod 
and the excavated tre 
e Appendix A ) . Sample 
wever, pyridine was pr 
(3,014 ppm). Quinidi 
ent in these samples, 
during the excavation 
4-inch PVC line 
the presence of 
ppm when the 
ating no recent 
d a reading of 
d to a pit near 
sheeting. Vapor 
er excavation was 
isit in October, 
ed trench which 
nch (sample 
s D-3 and D-4 
esent in D-1 (920 
ne gluconate and 
also. A strong 
and sampling 
Upon the return visit in October the pyridine odor was not 
noticeable. Probing the pit and PVC pipe did not elicit a 
response on the FID. The pit was excavated without detection of 
organic vapors especially pyridine. 
The presence of pyridine in the above discussed area lead to 
additional investigations; either the drain line was broken under 
t.he concrete, or another source of pyridine contamination was 
present. Discussions with personnel who have been at the facility 
fcr a number of years revealed the past history for the loading 
deck area. Originally, laboratory drains exited from the building 
and wastes flowed directly to an open pit. Occassionally, during 
the rainy season the pit would fill with water and overflow by a 
swale to the dry river bed beyond the fence. Later, the pit was 
filled and the area concreted for use as a loading dock. It was 
uncertain how the laboratory drain was rerouted to the pit near 
t.he fence. 
A total of 40 borings were made in the loading dock area: 22 
curing September and 18 during October. Most borings were at 
least 6-feet deep with a few Ibeing 8-feet deep. Table 1 shows t.he 
FID readings for all samples taken during September. Soil texture 
indicates that contaminants are confined to sandy-clay material 
which was apparently used for fill. Samples taken from the dense 
clay below the sand were relatively free of contamination. 
100095 
t h e s i d e 
w a l l s 
A p p a r e n t l y e x p o s u r e 
t o 
a i r 
T h e r a p i d 
v o l a t i l i t y 
i s 
shown w i t h 
d a t a 
i n T a b l e 
2 . 
FID 
r e a d i n g s 
f o r 
t h e 
b o r e 
h o l e s 
i n S e p t e m b e r 
show r a t h e r 
h i g h 
c o n c e n t r a t i o n s . 
Upon r e t u r n i n g 
i n O c t o b e r 
n o n e of 
t h e s e 
h o l e s e x h i b i t e d 
v o l a t i l e s 
u s i n g 
t h e 
F I D . 
P r o b i n g 
t h e 
b o r e 
h o l e 
a n d 
l o o s i n g 
w o u l d 
r e s u l t 
i n a s m a l l 
FID r e s p o n s e . 
A p p a r e n t l y 
^ 
a l l o w s 
f o r 
o x i d a t i o n 
o r e s c a p e 
of 
t h e 
c o n t a m i n a n t s . 
T h e a d d i t i o n a l 
b o r i n g s 
made 
i n O c t o b e r 
f u r t h e r 
d e l i n e a t e d 
t h e 
c o n t a m i n a t i o n 
and p r o v i d e d 
i n f o r m a t i o n 
on t h e l a b o r a t o r y 
d r a i n 
r o u t i n g 
u n d e r 
t h e 
c o n c r e t e . 
I d e a s 
w e r e 
c o n f i r m e d 
u s i n g 
f l u o r e s c e i n 
d y e . 
A p p a r e n t l y 
t h e 
l a b o r a t o r y w a s t e s 
flow 
i n t o 
a 
p i t 
f i l l e d 
w i t h 
s t o n e 
n e a r 
b o r i n g s 
20 and 
20A. 
Once t h e 
p i t 
f i l l s , 
l i q u i d 
o v e r f l o w s 
t o a " t a n k " 
n e a r 
b o r i n g 
1 6 . 
T h i s 
" t a n k " 
maybe 
t h e 
s e p t i c 
t a n k w h i c h s e r v i c e s 
r e s t r o o m s 
i n 
t h e o f f i c e 
p o r t i o n 
of 
t.he 
f a c i l i t y . 
Once t h i s 
f i l l s 
t h e n 
f l o w 
c o n t i n u e s 
o u t 
t o 
t h e 
p i t 
n e a r 
t h e 
f e n c e . 
S a m p l e s w e r e 
s e l e c t e d 
from 
t h e s e 
new b o r i n g s and 
i m m e d i a t e l y 
a n a l y z e d . 
The r e s u l t s 
a r e 
p r e s e n t e d 
i n 
Appendix 
D. 
A n a l y s e s 
s h o w s 
t h e 
p r e s e n c e 
of a t 
l e a s t 
690 p p b 
t o l u e n e : 
4 3 , 0 0 0 
ppb 
p y r i d i n e : 
6 4 , 0 0 0 d i p h e n y l 
m e t h a n o n e : 
a n d 600 t o t a l 
x y l e n e . 
A d d i t i o n a l 
m a t e r i a l s 
were 
p r e s e n t 
a t 
l o w e r 
c o n c e n t r a t i o n s . 
O i l 
e n d 
g r e a s e 
a n a l y s i s 
i n d i c a t e d 
c o n c e n t r a t i o n s 
up t o 1,500 
ppm. 
PROPOSED CLEANUP PROCEDURES 
ESI 
i s 
p r o p o s i n g 
t o c l e a n 
t h e 
c o n t a m i n a t e d 
s o i l 
on s i t e 
i n s t e a d 
of 
s o i l 
r e m o v e d 
t o a c e r t i f i e d 
l a n d f i l l 
w h i c h 
i s p r o b a b l y 
l o c a t e d 
on 
t h e 
m a i n l a n d . 
We h a v e c o n s i d e r e d 
n u m e r o u s a l t e r n a t i v e s 
i n c l u d i n g 
c n - i s l a n d 
i n c i n e r a t i o n 
a t 
t h e 
H e s s 
R e f i n e r y . 
O n - s i t e 
d e c o n t a m i n a t i o n 
a p p e a r s 
n o t 
o n l y 
f e a s i b l e 
b u t c o s t 
e f f e c t i v e . 
100096 
The contaminated 
been cleaned up a 
drums. ESI propo 
equipment and ove 
emptied onto pans 
temperature tolue 
contaminated soil 
it to the site, 
site for soil dec 
temporary air emi 
areas around Tank 8 and at the end of slab 3 have 
nd the material is stored on site in 55 gallon 
s e s to decontaminate the soil using air drying 
ns on site. Drummed-contaminated soil would be 
and placed in the ovens. By raising the 
ne can be evaporated leaving non-toluene 
This soil would be analyzed before returning 
VICC officers will allow the use of equipment on 
ontamination. ESI will probably require a 
ssion permit from the EPA. 
ESI proposes to treat the contaminated area behind the loading 
dock while the soil is in place. This method will involve the 
following sequence: 
1) All laboratory waste flows will be rerouted to a self 
contained unit thus preventing new contaminants and 
liquid from entering the area. 
2) Portable toilets will be available to prevent the 
discharge of wastes and water to the area. 
3) A shelter will be constructed over the area to prevent 
rainfall and runoff from entering the area. 
4) All overlying concrete will be removed to expose the 
contaminated soil, laboratory drains, p:t, and septic 
tank. 
5) A berm will be constructed around the -e.^posed soil 
to prevent inflow of water from rainfal.'.. 
These preliminary steps will allow for vaporization of volatile 
r.aterials to the atmosphere- 
Periodically, the soil will be 
turned using a backhoe to expose underlying soii; layers. Samples 
will be taken every 4-5 days to determine the rate of volatile 
release and confirm the success of the methodology employed. 
Discussions with Dr. Medhat Reiser of Nepara, Inc. (914-782-8171) 
indicate that pyridine will disappear upon exposure to air. He 
stated that although it is on the hazardous materials list it is 
biodegradeable in about 21 days if exposed to air and not in 
contact with water. The above precautions and methodology should 
allow for the biodegradation of pyridine. Also, other volatiles 
should disappear using this method. 
If this method is successful, 
the area will be rehabilitated to its prior condition. Acceptable 
ir.ethods for laboratory waste and septic discharges will be 
incorporated in the new design. 
ESI realizes that this method of treatment will require a 
temporary air emissions permit. Also, a tempor.3ry discharge 
permit maybe required if unexpected heavy rainfall should flood 
the pit area. Both permits will be requested from the EPA prior 
to initiation of the treatment method. 
100097 
ESI held a meeting with Mr. Alfred Williams and Mr. Austin 
Mcorehead of the Department of Conservation and Cultural Affairs, 
St. Croix (809-773-0565). The contents of this report were 
discussed in its entirety and they consider the proposed methods 
tc be suitable for the situation at the facility. They suggested 
that all work be coordinated through EPA Region II. 
100098 
TABLE 1 
FID READINGS (ppm) FOR ISLAND CHEMICAL COMPANY (BERLEX) -1/ 
Boring 
No . 
1 Foot 
Dent h 
3 Feet 
Deoth 
4 Feet 
D e o t h • 
6 Feet 
D e o t h 
8 Fee: 
Deoc h 
1 
2 
3 
U 
5 
6 
7 
8 
9 
10 
1 1 
12 
13 
\i* 
15 
16 
17 
18 
19* 
2 0 * * 
2 1 * * * 
22 
B 
B 
B 
B 
10 
0 
1 10 
55 
60 
90 
200 
0 
0 
10 
100 
100 
10 
45 
30 
20 
300 
110 
15 
10 
10 
0 
30 
150 
110 
10 
10 
0 
0 
0 
100 
80 
10 
35 
10 
65 
200 
n / a 
15 
10 
0 
0 
110 
30 
110 
10 
10 
0 
0 
25 
100 
80 
10 
40 
30 
X 
100 
n/a 
10 
10 
10 
0 
20 
15 
10 
160 
10 
55 
0 
10 
20 
140 
45 
10 
300 
40 
80 
X 
SP 
120 
0 
0 
40 
10 
80 
45 
210 
45 
20 
0 
10 
20 
250 
100 
20 
3 00 
20 
45 
X 
SP 
310 
35 
10 
60 
0 
15 
200 
150 
15 
0 
10 
30 
10 
90 
60 
0 
110 
30 
45 
X 
SP 
100 
30 
20 
10 
45 
100 
45 
80 
0 
0 
0 
10 
40 
100 
65 
10 
320 
10 
40 
S? 
130 
0 
20 
0 
25 
120 
15 
60 
0 
0 
0 
0 
10 
15 
100 
100 
15 
160 
10 
15 
20 
SP 
15 
10 
40 
90 
10 
45 
0 
0 
0 
0 
10 
20 
300 
100 
40 
200 
10 
45 
15 
SP 
lOOC 680 
0 
0 
30 
40 
0 
10 
0 
0 
25 
25 
0 
10 
0 
0 
150 
55 
0 
10 
15 
B 
10 
10 
10 
\_l Sanpled during September. 
* X = No Sample 
**SP = Septic Pit 
***At the 4 Feet Depth, Letter B should read 1000 plus 
100099 
TABLE 2 
FID READING FOR BORINGS 
Dm 
Borina 
1 
2 
3 
4 
5 
6 
7 
8 
9 
10 
11 
12 
13 
14 
15 
16 
17 
18 
19 
20 
21 
22 
60 
35 
40 
270 
40 
550 
0 
0 
350 
200 
280 
240 
1000+ 
110 
110 
130 
750 
650 
45 
100100 
TABLE 3 
Inventory Items which have been at 
ISLAND CHEMICAL COMP.^Y. INC. (BERLEX) 
Quinine Sulfate 
Quinidinone 
Quinidine Base 
Quinidine Gluconate 
Quinacr 
Quinine Bisulfate 
THF (tetrahydrofuran) 
Toluene 
Pyridine (Karl Fisher Reagent) 
Isopropanol 
Sodium Chloride 
Ethyl Alcohol 
Benzvlphenone 
Chloroform 
Methylene Chloride 
Cinchona Bark 
20% Dibah in Toluene 
Sodium Hydroxide (caustic soda) 
pellets and solution 
Gluccno-A -Lactone 
Liquid Ammonia 
Muriatic Acid 
Sulfate Acid 
Sodium Hypochlori"te Solution 
So'iium Bicarbonate 
Magnesium Sulfate 
Flourenone 
Potassium-t-Butoxide 
Acetone 
Calcium Hypochloride (H-T-H) 
Tetaric Acid 
Variquat 
Acetic Acid 
Soda Ash 
Gluconofin 
Carbon Black 
Kenite 7C0 
Potassium lodo Platinate 
Butylated Hydroxy Toluene 
Ethylene Glycol 
Methanol 
Charcoal 
Castor Wax 
100101 
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100102 
DRY RIVER BED 
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FIGURE 2 
BORING LOCATIONS 
SCALE : f 
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WAREHOUSE 
2IA 
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LABORATORY 
DRAIN \ \ 
LOADING DOCK 
> 
o 
21 
> 
o 
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FENCE 
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FIGURE 3 
v/yyyyyyy/yyy.i^ 
BACK FILLED 
TRENCH 
CONTAMINATION 
AREA 
100104 
FiGURE 
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P R C ^ ' ' . £ S FOR FID READINGS 
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BORING NUMBER 
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1 
X I SEE FIGURZ 3 
100105 
FIGURE 5 
PROFILE LOCATIONS 
WAREHOUSE 
C 
11 
B 
° i o 
12 
.18. 
19 
LOADING 
15 
13 
16 
17 
A' 
' 2 1 
LABORATORY 
DRAIN^ 
•20 
22 
DOCK 
100106 
APPENDIX A 
100107 
tCM/tOLI r K . 
To: 
From: 
Date: 
Subject: 
f i i v ^ 
\
»
i 
II,. 
Laboratories Inc. 
Memorandum 
J. Beck 
D.W. McKennon 
October 15, 1984 
ISLAND CHEMICAL ENVIRONMENTAL SAMPLES 
On 9/17/84, we received several samples from Irv Cohen of Enviro Sciences Inc. 
for analysis for various organic components. 
We agreed to examine the samples for volatile organics via GC techniques, 
and then for nonvolatile organics like quinidine using HPLC techniques. 
Our investigation is complete, and data is attached. 
DISCUSSION 
I. GC ANALYSIS 
Quantitable amounts of toluene were found in samples T8-1 and Tank-8. 
Also, quantitable amounts of pyridine were found in samples D-1, D-2, 
and D-5. 
Qualitatively, the chromatograms were examined for additional peaks. 
Samples S4-2, D-5, T8-1, and T8-2 contain an unknown peak eluting 
between the pyridine and toluene peak. Tank-8 had an unidentifiable 
peak which eluted shortly after toluene. 
II. HPLC 
Quantitable amounts of quinidine and/or quinine were found in D-1, 
D-2, D-5, T8-1, Tank-8, Tank-4, and Tank-9. 
Qualitatively, the HPLC chromatograms in many cases have some unidentified 
early eluting peaks which are not related to quinidine, quinine, or 
any of the other cinchona alkaloids. 
DEPOSITION OF SAMPLES 
On October 10, 1984, all samples were given to Al Kyles who is a 
representative of Enviro Sciences Inc. 
Note: Due to the extreme rush to analyze these samples, limited, 
precautions were taken to protect either GC or LC columns. Total 
replacement cost for columns is approximately $960. 
^MZZZZ^-^i^z^^ 
100108 
D.W. McKennon 
DWM/hms 
Attachment 
cc: R, 
R. 
R. 
Willis 
Wohl 
Milos 
I.-Cohen/Enviro Sciences Inc 
G.C. ANALYSTS* 
SAMPLE 
IDENTIFICATION 
S4-1 
S4-2 
S4-3 
S4-4 
S4-surface 
D-1 
D-2 
D-3 
D-4 
D-5 
-8-1 
TS-2 
Tank-
Tank-
Tank-
Tank-
•8 
-4 
-9 
-7 
^4 Sample 
^•4-High Cone. 
TOLUENE 
N/D 
N/D 
N/D 
N/D 
N/D 
N/D 
N/D 
N/D 
N/D 
N/D 
694 ppm 
N/D 
13,880 ppm 
-
-
-
-
-
PYRIDINE 
N/D 
N/D 
N/D 
N/D 
N/D 
920 ppm 
507 ppm 
N/D 
N/D 
3014 ppm 
N/D 
N/D 
N/D 
-
-
-
-
-
L . C . ANALYSIS** 
VTTnrvr 
Q U I N I N E 
SULFATE 
QUINIDINE 
GLUCONATE 
N/D 
N/D 
N/D 
N/D 
N/D 
452 ppm 
96 ppm 
N/D 
N/D 
170 ppm 
274 ppm 
47 ppm 
4050 ppm 
8227 ppm 
N/D 
N/D 
N/D 
N/D 
N/D 
N/D 
N/D 
N/D 
N/D 
82 ppm 
N/D 
N/D 
N/D 
N/D 
101 ppm 
N/D 
1521 ppm 
2594 ppm 
354 ppm 
N/D 
N/D 
N/D 
N/D = None Detected 
*G.C. Reference Bk. 83-9, pp. 75-79, EGO 
•^L.C. Reference Bk. 83-11, pp. 22-30, MSM 
100109 
APPENDIX B 
100110 
liiiniy 
*Linumm0anomiimiii' / 
Laboratories Inc. 
To: 
W. C. Lumma 
From: 
R. A . Wohl 
Date: 
October 22, 1984 
Subject: 
Soil Samoles from Island Chemical Comoanv 
Memorandum 
cc: 
A. Kyles/Enviro Scie.nces 
D. W. McKennon* 
R. Milos* 
A. Rudzik* 
Enclosed please find our Analytical Report (G. Rudd to 
W. B. Caldwell, dated October 19, 1984) on the three soil 
samples S4-1, 1' H-22 and 3' H-21. These three soil samples, 
originating from Island Chemical Company were received from 
A. Kyles of Enviro Sciences, Inc. on Oct. 12, 1984. 
Wohl 
RAW:cj 
E n c l o s u r e * 
100111 
• \ « — 
y 
I -
Laboratories Inc. 
Memorandum 
To: Dr. W. B. Caldwell 
cc: W. Lumr.a 
R. Wohl 
From: G. Rudd 
Date: October 19, 1984 
Suojsct; Analysis of Soil Samples from Island Chemical by 
- Headsoace•Gas - Chromatography 
Three soil samples received 10/15/84 from the Island 
Chemical site were examined by headspace gas chromatography 
for the prese.nce of toluene and pyridine. T.he results 
are listed in the table below. Chromatograms of the 
three samples are attached. The large pea.ks observed 
at t.he beginning of each chromatographic run are artifacts 
of the headsoace experiment. 
Samole 
S4-1 
H-22 1 
K-21 3 
A 
B 
Toluene, ppm 
<0.2 
none detected-^ 
none detected 
Pyridine, ocm 
<C0.2 
none detected 
1.2 
(1) Limit of detection ca^. 0.1 ppm 
Quantitation was performed by standard addition (Ippm) 
to the sample and comparison to the unspi.ked si=..^ple. 
Chromatography Conditions 
A. Toluene 
Column: 6' x 2mm glass packed with 80/100 Carbooack C/ 
0.1% SP-1000 
Te.Tiperatures: Injector - 250°C Detector - 275^C 
Oven - 1 min (§ 100°C; 200°C & 16°C/min 
Carrier: 
Nitroge.n, 22 ml/min 
Detector: 
FID 
B. Pyridine 
Column: 4' x 2mm glass packed wit.h. 60/80 Carbopack 3/ 
4% Carbowax 20.M/0.8% KOK 
100112 
-2-
Temperatures: Injector - 250°C Detector - 275°C 
Oven - 130°C isothermal 
Carrier: Helium, 30 ml/min 
Decector: FID 
Assav Procedure 
5.0 grams of sample were placed in a 50 ml serum bottle that 
was sealed with a Teflon lined septtun. The sealed serum 
bcttle containing the sam^ple was equilibrated at 90°C for 
1-1.5 hours. With a previously heated gas tight syringe, 0.5 ml 
of t.he headspace volume from the serxim bottle was withdrawn 
a.-.d quickly injected into the gas chromatograph. 
McMeal, T. and Breder, C.V., JAOAC, 65, 184-187 (1982). 
Xc zebook Reference 
GI-l-1-143-146 
G, I. Rudd 
100113 
" -iHnuimiH. 
S 
•Cl. 
• • 
'•ill. 
• i l i i - l l ' 
'.y-K 
-i..uiimitiinutMmitmimii' 
To: 
From: 
Date: 
Subject: 
o 
o 
o 
UJ 
a 
•X. 
Laboratories Inc. 
- 3 
-
Memorandum 
i:.:? _ 
SIX>A of- 
r^ifi^pttci. 
f^^i 
/ . l 6 ^iDfr\ 
<r>.CS. 
1C.S9 
10.e« . 
10.5: 
RT in minutes 
SAMPLE: l.lSFrM SPIK INJECTED AT 18:47:15 CN OCT 17. 1984 
Heth: STD39 
Ra>r, R2£c47 
Prcc: P3S247 
o 
03 
Ol 
C-
(Q 
C 
UJ 
o 
o 
(j)' i 2'*"" 
I.'i. 
Ctz^rritr • /V/^ ^ Z ' 2 ^ fW^rM.n 
RT in Blnutss 
SAMPLE: S4-i*2 
Heth: ST033 
INJECTED AT 19:21:42 ON OCT 17. 1SS4 
Ra»r. 
flaS249 
Proc: P2924g 
1 0 0 1 1 4 
. ^ ^ • • ^ 
-••nitimimtj 
..tMnummjTm.'1/mniMfi 
To: 
From: 
Date: 
Subject: 
CM 
a 
o 
C-
fO 
o 
ca 
o 
UJ 
n 
^ Laboratories Inc. 
-H " 
io.:iL 
Memorandum 
'5'CC^ C<- rstix.i.'spKiL 
T r Z Z T ' ^ 3 3 /'.'•'£» 
(ff 'f- 2.1^'^ 'A-
4.:0 
RT in minutes 
SAMPLE; 3'B H21*2 
INJECTED AT 19:08:50 CN OCT 17. 1SB4 
Meth: STD29 
Rax: R3£24a 
Ppoc: P2S24a 
ru 
O) 
c 
C 
Lu 
O 
o 
o 
s 
RT in minutes 
? 
CsiK/^.. 
•BbfiCXO CAThoauO. C/O. 1% fP-OCT i 
^ ' < 2rY\rv\ 1.4 
fZ'f) 
. 
Zo.n,o '• ^J•^ a.^ J2roL/rw>»> 
" 
j 
r ^ . . : 
d.;: 
SAMPLE: IA H-C2 
Heth: STD39 
INJECTED AT IB: 41: £5 ON OCT 17. 1984 
Raw: R3S242 . 
Proc: P29242 I 
100115 
^w^ 
* • ' • % 
• ^ ^ • • h ."SBiHI "ffmaiutm,. 
B 
'Stl.KU 
'I'nem.mwm.t^.ui'- 
L a b o r a t o r f e s Inc. 
- S ~ 
To: 
From: 
Date: 
Subject: 
cn 
c 
IO 
o cs 
UJ 
C3 
Memorandum 
3.7? _ 
3.:< _ 
B..:9L 
/ndiVvtf 
RT in minutes 
SAHPLL-
Hetn: GC42 
INJECTED AT 9: OB: 35 ON OCT 19. 1934 
Raw: R42aB7 
Proc: P42E57 
o 
rrj 
c 
o 
o 
a 
Z3 
3 . : : 
y 
5.."3 .. 
i ? . ; 
/J^c^'^'^ 
Zoo6 A£wc9^c£ S^'^fsitf S**-' 
(;^'kx~»n • Carho^ci. Blf^o 0^rszc>..^t 
i? v^n • iSo :! 
UA:>''^' 
dvi«'' 
,,.w> 
(< VP»") 
U 
( 
^ 
'/»p~) 
RT in minutes 
SAMPLE: 
Hetn: GC42 
L.S. 
INJECTED AT 8: 2B: 00 ON OCT 19. 1984 
Raw: R42EB2 
Proc: P42B52 
100116 
•itHmuiirj, 
.I'mifiy 
To: 
From; 
Date: 
Subject: 
Laboratories Inc. " ^ ' 
Memorandum 
o 
er} 
03 
(O 
o 
tn 
o 
c 
ID 
c 
LU 
C3 
O 
LU 
1:2 
•.:.9T 
9.2< 
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l ' « 2 r . « 
Co.r'oofs.itcy.t h f o 
^arfca-xf 
2 0 / ^ / : .'S-fa 
t.0>^ 
.r: 
:.a: 
RT in minutes 
SAMPLE: 
Heth: EC42 
INJECTED AT 
8: 41: 40 ON OCT 19. 1934 
Ra>r. R42S53 
Proc: P42a53 
' . ? 
TOr-^ J o . ^ ^ <:<?H 
100117 
RT in minutes 
SAMPLE: 
Het.h: GC42 
INJECTED AT 
8: 47: 45 ON OCT 19. 1934 
Raw: 
fl42E64 
Proc: P^2=54 
APPENDIX C 
100118 
( (AT'yy/^^^j 
\^*0^0e0e^>^ 
1% COPEL»*0 RO.. DEMVllXE. N€W JERSEY 07834 
CHAIN OF CUSTODY RECORD 
I n s t a l l a t i o n : ^ ^ c c < /&SS, ^ ^ ^ , 
.Zr<.yA/o ^rv€yrt/ez<. da. . ^ c . 
JlZ ^^a^J( l///fs/^ /Zc»fOS 
S u r v e y 
N o . : 
r-l a 
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• 
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a 
V3 : c 
/s 
^'£ 
rs 
S t a t i o n 
L o c a t i o n 
2<s 
<tr 
/s 
<I><S 2 / 
R e l i n q u i s h e d 
b y : 
( S i g n . ) 
R e l i n q u i s h e d 
b y : 
( S i g n . ) 
R e . : . i n q u i s h e d 
b y : 
( S i g n . ) 
R e l i n q u i s h e d 
b y : 
( S i g n . ) 
D i s p a t c h e d 
b y : 
( S i g n . ) 
D a t e / T i m e 
.Method of 
S h i p m e n t : 
S a m p l e r s : 
( S i g n a t u r e ) 
D a t e 
yr-yfJrfir' 
// 
// 
// 
Time 
Sample 
Type 
Uomp . 
R e c e i v e d 
b y : 
( S i g n . ) 
R e c e i v e d 
b y : 
( S i g n . ) 
R e c e i v e d 
b y : 
( S i g n . ) 
R e c ' d 
by 
L a b o r a t o r y 
f o r 
f i e l d 
a n a l y s i s 
( S i g n . ) 
-IK 
"x L a b o r a t o r y 
A 
c ^ ^ 
G r a b 
X 
/ 
/ 
/ 
No. of 
Contalnere 
/ 
/ 
/ 
/ 
D a t e / T i m e 
D a t e / T i m e 
D a t e / T i n e 
D a t e / T i m e 
D a t e / T i m e 
100119 
; ; - t 
MFAOSPACF 
Ai •i'lVZA^'^ arr'.Ki'.; uanr/oaBteoater iabori ^rv 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
ns? m m lo RANOOIPH NF^T jt RSIT 07869 701 SB* 0330 
V O L A T I L E 
O R G . ^ M C S BV PURGE AKD TR,^P 
GC/MS 
Compounde d e t e c t e d i n p a r t e per m i l l i o n 
( m i l i g v a m a / k i l o g v a m s jOry Wgt.Basis 
SAMPLE SOURCE: ENVIRO SCIENCES 
SAMPLE ID: i' B Mole #20 
Kcport Dale: Ociobcr 9. '08't 
Lab. * 
}h(>2k 
SAMPLE DATE: 
Sept. 18-19, 198'< 
TAKE.X BV: Alan l.Kvler 
-AT LAB DATE 
9/27/8«» 
O 
O 
NJ 
O 
CHLOROMETHANE 
BROMOMETHANE 
DICHLORODIFLUOROMETHANE 
VI.WL CHLORIDE 
CHLOROETHA.NE 
METHVLE.NE CHLORIDE 
ACETO.VE 
T N I C I I L O R O F L U O R O M E T H A . X E . , 
1 ,]-D1CHL0R0ETHVLE.\E 
1 ,1-D1CHL0R0ETHA.\E 
t-1.2-DlCHL0R0ETHVLE\E. 
CHLOROFOR.M 
FKEO.N 115 
, 
1,2-DICHLOROETHANE 
t-BUTVL METHVL ETHER... 
1 ,1 ,1-TR]CHL0R0ETHANE.. 
CARBON TETRACHLORIDE... 
BROMODICHLOROMETHANE... 
1,2-DICHLOROPROPANE 
c-1,3-DICHLOROPROPENE 
t-l,5-DICHLOROPR0PENE 
TCE (TRICHLOROETHYLENE).. 
DlBRO^IOCHL01'.CMETiLANE 
BENZENE 
DlISOPROPYL ETHER 
Z-CHLOROETHVLVINVL ETHER. 
HEXANE 
BROMOFOR.M 
1,1,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHVLENE) 
HEPTANE 
TOLUENE 
.. 
CHLOROBENZENE 
•. 
ETHYLBENZENE 
0. 16 
For the above listed volatile pollutants, nothing detected at O.Olppmsensitivity level 
X Other peaks detected. Fluorethyne ^ 0. *» 5 ; 2-me t hy I propano 1 0.20; pentane O.OI; 
LT = Less than, GT=Greater than, ND=Not detected 
'•'NOTE: Possibly from plastic bag 
H E A D S P A C E 
-'•:'l •i']^.\'A^° driKkiy; ujiev/waetejater Labora. 
y 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
us? ROUit 10 RANDOLPH. NC* jCRSfT 07869 ?oi 58.0330 
V O L A T I L E 
O R G A N I C S 
BV PURGE AND TR.AP 
GC/MS 
Compounds d e t e c t e d in p a r t e per m i l l i o n 
(miligrams/kilograma )Ory Wgt.Basis 
S.AMPLE SOURCE: ENVIRO SCIENCES 
SAMPLE ID: i, • Q nole H ^ 
Report Date: October 9, 198'« 
Lab. n 3'«625 
S.AMPLE DATE: 
Sept. 18-19, 198'* 
TAKEN BV: Alan L.Kyler 
AT LAB DATE 
9/27/8'« 
I-* 
o 
o 
lO 
CHLOROMETHANE 
BR0M0.^1ETHANE 
DICHLORODIFLUOROMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
TRICHLOROFLUORO.NIE THANE. 
1,1-DICHLOROETHYLENE... 
1,1-DICHLOROETHANE 
t-l,2-DICHL0R0ETHVLENE. 
CHL0ROFOR.M 
FREON 115 
1,2-DICHLOROETHANE 
t-BUTVL METHVL ETHER... 
1,1,1-TRICHLOROETHANE.. 
CARBON TETRACHLORIDE 
BROMODICHLOROMETHANE... 
1 ,2-DICHLOROPROPANE 
c-1,5-DICHLOROPROPENE 
t-l,5-DICHL0R0PR0PENE 
TCE (TRICHLOROETHYLENE).. 
DI EROMOCHLOP.OMETH.ANE 
BENZENE 
DIISOPROPYL ETHER 
2-CHLOROETHVLVINVL ETHER. 
HEXANE 
BRO.MOFOR.M 
, 
1,1,2,2-TETRACHLOROETHANE 
PCE (TETR.ACHLOROETHVLENE) 
HEPTANE 
TOLUENE 
CHLOROBENZENE.. . .: 
ETHYLBENZENE 
J^ 
For the above listed volatile pollutants, notlung detected at 0. 01 ppnsensi t ivity level 
_X 
Other peaks detected. 
Fluorethyne •'0.38; 2-methyl propanol 0.16 
LT = Less than, GT^Gieater than, ND=Not detected 
••'•NOTE: Possibly from plastic bag 
'"t'i -i1\\'A^° criKKv.: ii3ier/waeteoater Labot^, ,y 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
' 1'^^?5P^CE_ 
lU-port Date: 
October 9, 198'« 
INCORPORATED 
Lab. n 3,^626 
us? ROUU )0 RM-ooiPH NfW JCRSIY 07S69 701S84 0330 
V O L A T I L E 
ORGANICS 
BV PURGE AND TR.AP 
GC/MS 
Compounde d e t e c t e d 
i n p a r t e 
p e r m i l l i o n fmt Zigrama/ki iograma )Ory Wgt .Basi s 
S.AMPLE S O U R C E : ENVIRO SCIENCES 
SAMPLE ID: 
3- D-Mole 
I M 
SAMPLE D A T E : 
S e p t . 18-19. 198'< 
TAKEN BY: Alan L.Kyler 
AT LAB DATE: 
9/27/B'( 
O 
O 
to 
to 
CHLOROMETHANE 
BROMOMETHANE 
DICHLORODIFLUOROMETHANE 
\INYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
TR1CHLOROFLUOR0.^1ETHANE. , 
1,1-DICHLOROETHYLENE 
1,1-DICHLOROETHANE 
t-l,2-DICHLOROETHYLENE., 
CHLOROFOR.M 
FREON 115 
1,2-DICHLOROETHANE 
t-BUTVL METHYL ETHER 
1,1,1-TRICHLOROETHANE. . , 
CARBON TETRACHLORIDE 
BROMODICHLOROMETH.ANE. . . 
1 .2-DICH LOROPROPANE 
c-l,5-DICHL0R0PR0PENE 
t-l,5-DICIiL0R0PR0PENE 
TCE (TRICHLOROETHYLENE).. 
DIBROMOCHLOROMETHANE 
BENZENE 
DIISOPROPYL ETHER 
2-CHLOROETHYLVINVL ETHER. 
HEXANE 
BROMOFOR.M 
1,1,2,2-TETRACHLOROETHANE 
PCE (TETR.ACHLOROETHVLENE) 
HEPTANE 
TOLUENE 
CHLOROBENZENE 
; 
ETHYLBENZENE 
J< 
For the above listed volatile p o l l u t a n t s , notliing detected at O.Olppmsensitivity level 
J( 
Otlier peaks d e t e c t e d , f i nnrp.i hynp, ''< Q . l l : 2-methyl 
propanol 0.16 
LT = Less t h a n , G T = G i e a t e r than, ND=Not detected 
ANOTE: 
Possibly from plastic bag 
^ 
w-r..:^- . e m : tea ^irn.rut.: uater/uaetewater Labor jru 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
' l-'^^?^?^^^- 
Report Date: 
October 9, 198't 
INCORPORATED 
Lab. i ^ken 
ns? ROUU 10 RANDOiPH NfW jfRSfY o?B69 ?oi 584 0330 
V O L A T I L E 
O R G A N I C S 
BV PURGE 
AND T R A P 
G C / M S 
Compounds d e t e c t e d in p a r t s per m i l l i o n 
(miligrame/kilograms)Ory Vgt.iasi 
S.AMPLE SOURCE: ENVIRO SCIENCES 
SAMPLE ID: /^ . Q Hole 21 
SAMPLE DATE: 
Sept. 18-19, 198'* 
TAKEN BY: Alan L.Kyler 
AT LAB DATE: 
9/2 7/8'< 
H 
o 
o 
to 
LO 
CHLOROMETHANE 
BROMOMETHANE 
DICHLORODIFLUOROMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
MEniYLENE CHLORIDE 
, 
ACETONE 
TRICHLOROFLUOROMETHANE. , 
1,1-DICHLOROETHYLENE 
I,1-DICHLOROETHANE 
t-l,2-DICHLOROETHYLENE., 
CHLOROFOR.M 
FREON 115 
1,2-DICHLOROETHANE 
, 
t-BUTVL METHYL ETHER 
1 ,1 ,1-TRICllLOROETHANE. . , 
CARBON TETRACHLORIDE 
BRO.^IODICHLOROMETH.ANE. . . 
1 ,2-DICIILOROPROPANE 
c-1,5-DICHLOROPROPENE 
t-l,5-DlCHLOROPROPENE 
TCE (TRICHLOROETHYLENE).. 
DIBROMOCHLOROMETHANE 
BENZENE 
DIISOPROPYL ETHER 
2-CIILOROETHYLVINVL 
ETHER. 
HEXANE 
BROMOFOR.M 
1,1,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE) 
HEPTANE 
TOLUENE 
CHLOROBENZENE 
; 
ETHYLBENZENE 
For the above listed volatile pollutants, noiinng detected at o.Olppm sensi t ivi ty level. 
_X Otlier peaks detected, fluorethyne- 0.06; 2-methyl propanol 0.^)7. 2-me t hy I - I-hep t ene 0.21; 
pyr I d I ne 0.02 
\ 
LT = Less than, GT=Creater than, ND=Not detected. 
NOTE :-''Pos s i b 1 y from plastic bag. 
APPENDIX D 
100124 
November 12, 1984 
30850-145 
ENVIRO-SCIENCES, INC. 
19 Copeland Road 
Denville, New Jersey 
07834 
Artention: Mr. Irv Cohen 
PURPOSE 
Nine (9) soil samples were submitted to York Laboratories for 
determination of toluene and pyridine on a quantitative basis. 
0~her compounds found in the samples were also indentified and 
are reported on a semi-quantitative basis. 
The samples were 
also analyzed for oil and grease. 
METHODOLOGIES 
The 
samples were analyzed 
for toluene using 
the dynamic 
headspace 
Gas 
Chromatograph/Mass 
Spectrometry 
method 
in 
accordance with Chemical Analysis of Sediments and Elutriate 
Testing, EPA 1979. 
A Tekmar Model LSC-3 Purge and Trap 
iiiterfaced 
with an HP 5995C GC/MS/DS were used ' for the 
analysis. 
Tbe samples were analyzed for pyridine and oil and grease in 
accordance with EPA/CE-81-1 Procedures for Handling and Chemi-
cal Analysis of Sediments and Water Samples, May 1981. 
An HP 
5S95C GC/MS/DS was used for the pyridine analysis. 
RESULTS 
The results are listed in the following tables. 
Prepared by: 
"") C ^ - J ^^ S|^.,^ 
Gail 0. Sprio 
Senior. Chemist 
Approved by 
GDS/JCC/mz 
CJhilet'X;htemist 
100125 
YWC. INC • 2C0 Mof ,rc- 'ni-ior-- - ^'|••"•• -
TABLE 1 
ENVIRO-SCIENCES, INC. 
TOLUENE AND PYRIDINE RESULTS 
Sample 
Identification 
20 Septic 
20 A-2' 
21 A-2' 
21 A-4' 
25 - 2' 
27 - 2' 
32 - 2' 
35 - 4' 
36 - 2' 
(Auger) 
Toluene 
ug/kg (pDb) 
540 
690 
15 
43 
210 
16 
15 
8 
7 
Pyridi ne 
ug/kg rppb) 
<1,000 
<1 ,000 
<1,000 
<1,000 
13,000 
26,000 
43 ,000 
<1 .000 
<1,000 
100126 
i'vC" 
Sample 
Identification 
20 Septic (Auger) 
20 A - 2' 
21 A - 2 
21 A - 4 
2 5 - 2 
2 7 - 2 ' 
3 2 - 2 ' 
35 - 4' 
36 - 2' 
TABLE 2 
ENVIRO-SCIENCES, INC. 
Compounds Found 
1 ,1-methylene bis-benzene 
diphenyl methanone 
methylene chloride 
chloroform 
benzene 
methylene chloride 
chloroform 
benzene 
ethyl benzene 
total xylenes 
methylene chloride 
chloroform 
trichloroethylene 
benzene 
tetrachloroethylene 
ethyl benzene 
methylene chloride 
chloroform 
benzene 
methylene choride 
chloroform 
benzene 
methylene chloride 
chloroform 
benzene 
methylene chloride 
chloroform 
1,1,1-trichloroethane 
benzene 
methylene chloride 
chloroform 
1,1 ,1-trichloroethane 
benzene 
methylene chloride 
chloroform 
benzene 
C o n c e n t r a t i o n * 
8,400 
64,000 
<5 
12 
<5 
<5 
5 
<5 
68 
600 
<5 
<5 
<5 
<5 
<5 
7 
<5 
<5 
<5 
<5 
5 
<5 
<5 
19 
<5 
<5 
<5 
<5 
<5 
<5 
13 
11 
<5 
<5 
<5 
<5 
1.5) 
0.5) 
2 . 3 ) 
0.9) 
2.4) 
3.8) 
0.8) 
0.6) 
0.9) 
2 . 2 ) 
2 . 6 ) 
0 . 4 ) 
1.7) 
0.4) 
2 . 2 ) 
0.6) 
4 . 4 ) 
4 . 2 ) 
0 . 8 ) 
0 . 8 ) 
2 . 4 ) 
0 . 4 ) 
1.6) 
1-4) 
0.2) 
• R e s u l t s 
a r e r e p o r t e d on a s e m i - q u a n t i t a t i v e 
b a s i s . 
1 0 0 1 2 7 
wc,INC • 2r,r, r/,.-,'rr.r 
ATTACHMENT 
B 
100128 
ATTACHMENT B 
nnno m sasfKis mc. 
19 COPELAND RO.. DENVILLE. NEW JERSEY 07834 
(201)366-6256 
Mr. Robert Harris 
USEPA Region II 
26 Federal Plaza 
New York, NY 10007 
Dear Mr. Harris: 
Enclosed is the addendum to the progress report submitted to Mr. Conrad Simon 
In December. I hope that the information therein will answer the questions 
and concerns expressed by you during our numerous telephone conversations. 
Please review this information as soon as you can. If you have any question, 
please contact me at 201-366-6256. 
I sincerely appreciate your help during the past several months. 
Very truly yours, 
ENVIRO-SCIENCES, INC. 
Alan Kyles, Ph.D. 
Vice President 
AK/po 
Enclosure 
100129 
^I^J)»W¥0 
5Ct£nC£5irK. 
^ ^ V ^ ^ W 
19 COPELAND RD.. DENVILLE. NEW JERSEY 07834 
^ % % ' m N ^ 
(201) 366-6256 
A p r i l 2, 1985 
Mr. Conrad Simon 
USEPA Region II 
26 Federal Plaza 
New York. NY 10007 
Reference: Island Chemical Company, Inc.. St. Croix Virgin Islands 
Dear Mr. Simon: 
Er.closed is an addendum to the progress report submitted to you In December 
for Island Chemical Company, Inc. (Berlex), St. Croix, Virgin Islands. 
E-viro Sciences, Inc. (ESI) has prepared this addendum as the result of numerous 
telephone conversations with Mr. Robert Harris of your office. The enclosure 
addresses questions which were raised by Mr. Harris in his efforts to fully 
u-derstand ESI's efforts to cleanup toluene and pyridine spills at the facility. 
It is our hope that the addendum will help your staff to grant ESI the necessary 
permits to pursue the cleanup in an orderly and timely manner. 
If you have any questions concerning the addendum or desire a meeting with 
ESI, please contact me immediately. 
'«" 
Very truly yours, 
ENVIRO-SCIENCES, INC. 
<Z^-^yZ/p^^' 
Alan L. Kyles, Ph.D. 
Vice President 
ALK/po 
Enclosure 
cc: 
Mr. Robert Harris, USEPA Region II 
Mr. Robert Milos, Berlex 
Mr. Frank Curtis, Berlex 
100130 
1 
3 
3 
3 
1 
3 
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f 
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i 
ADDENDUM TO 
PROGRESS REPORT 
ISLAND CHEMICAL COMP.'iNY. INC. (BERLEX) 
ST. CROIX. VIRGIN ISLANDS 
Enviro-Sciences, Inc. 
19 Copeland Road 
Denville, New Jersey 07834 
(201) 
366-6256 
A p r i l A, 1985 
100131 
V W > 3 d l KdACUi 
1---V 
ADDENDUM 
PROGRESS REPORT 
U-J---.: 
Islanc3 Chemical Comoanv, • Inc. ( Berlex ) 
m 
n 
St.Croix, Virain Islands 
Prcaress Report Summary 
BackaroDnc3' Information 
-
* 
— 
— 
— 
• 
• 
- 
• 
- 
— 
Tl^.e facility is located on the island's south side and near the west 
e.nd (Figure 1) at Latitucae 17 42*26" and Longitude 64 47*25". 
It is 
situated approximately 6.1 miles equidistant from the two major towns: 
Frederiksted to the west and Christiansted to the east. Facility 
access is via Route 66 which traverses the island east and west. As 
seen in Figure 2, it is about 0-5 miles north of Alexander Hamilton 
Airport. 
Elevation is approximately 40 feet mean sea level- An intermittant 
stream which originates near the north side of the island and empties 
i.nto the Caribbean Sea on the south side borders the north side of the 
property. Flow occurs generally during the wet season (September 
through December) and only during heavy runoff (Table 1 ) . The lower 
portion of the drainage lying beyond the facility is flowing and is 
utilized aa sewage outfall 
Wind direction is frora the east and southeast (trade winds) with 
velocities ranging from 5-15 miles per hour. 
Closest residences are located about 0.1 miles east of and upwind of 
the facility. 
As shown in Figure 3, the facility is situated on soils of the Coamo 
Series. These are gently sloping, well drained soils which occur as 
alluvial fans and terraces. They formed in sediments derived from 
volcanic and limestone rocks- They range in texture frora clay to 
sand. The upper layer is typically grayish-brown clay loam which is 
uncferlain by numerous layers of yellowish-brown clay and clay loam. 
Permeability is slow to moderate, and the shrink-swell potential is 
100132 
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f 
a 
moderate. These soils are commonly associated with San Anton, Glynn 
and Fraternidad soils. 
potable water for distribution is supplied from both ground water (30 
percent) and desalted water (70 percent). 
However, the island is very 
dependent on storage (cisterns) to cope with water demands. Most 
private dwellings have their own roof/cistern systems for water 
supply- 
There are eight major well fields on St. Croix and they are 
located as shown in Figure 4. The quality is generally poor due to 
mineralization and oil contamination from pump lubrication. These 
contaminants are often pumped into the supply system. 
The location of the three closest well fields in relation to the 
facility are shown in Figure 5. The three fields contain 14 of the 37 
total well field wells. 
Field•Study Results 
The original field investigation detected contamination in four 
locations (Figure 6 ) : 
1) along trench number 4, under concrete slab number 3; 
2) between tanks numbered 8 and 9; 
3) along trench number 9: and 
4) under the concrete surfaced loading dock. 
Analysis indicated that areas 1 and 2 above were primarily 
ccntaminated with toluene. As stated earlier, the toluene 
ccntaminated areas were cleaned and the contaminated soil placed in 
drums (25) and stored in the facility's warehouse. The pyridine 
contamination is still in place. 
Based upon analytical results (see Progress Report) the pounds of 
contamination were calculated as follows: 
Scil•in"Drums 
3 
a 
I 
1 
Contamination•Concentration 
10,000 ppm 
1,000 ppm 
x 
X 
Soil•(Tons) 
4.5 Tons = 99 lbs. 
9.0 Tons =19;81bs; 
Soil Under Concrete-Pad ( 60-x'35-=-f oof area) 
Ccntamination Concentration 
9000 ppb 
3C0 ppb 
CleanuD Procedures 
X 
X 
Soil (Tons) 
6,000 tons = 119 lbs. Pyridine 
6,000 tons = 
4 lbs. Toluene 
! 
ESI proposes to clean the contaminated soil using the following 
100133 
1 
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1 
I 
I 
1 
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1 
methodology: 
Toluene contaminated soil will be placed on trays in a dryer which is 
at the facility. The location is shown in Figure 7. Prior to 
beginning the drying operation, calculations will be made using the 
and stack diameter to insure 
During the handling of contaminated soil, protective clothing and an 
appropriate breathing apparatus will be used by all personnel (t.he 
breat.hing apparatus used is discussed later). 
The pyridine contaminated area will require rerouting existing 
laboratory discharges to a self-contained unit (probably 250-500 
gallon stainless steel vessel) and providing portable toilets in place 
of existing restroom facilities. These changes will eliminate sources 
of water which are presently entering the contaminated area and would 
prevent the degradation of pyridine. 
The pyridine contaminated area will be prepared as follows: 
1. A structure will be built over the area which will be exposed 
to prevent soil saturation from rainfall. 
2. The concrete will be cut and removed using a backhoe. 
The concrete will be hauled to a landfill, or used to 
stabilize the bank along the dry river bed. The 
Department of Public Works will be contacted for 
permission to do the latter. 
3. The soil will be tilled using a backhoe at 2 - 3 day 
intervals. Soil turning will allow exposure of the 
contaminated soil to ambient air-
The release of pyridine and minor amounts of toluene to the ambient 
air cannot be controlled. However, the interval between the soil 
turning can be lengthened to decrease the release rate. 
100134 
«-o-««,«c 
Samples will be taken at the beginning of the cleanup operation and 
continue at weekly intervals until acceptable pyridine contamination 
levels are reached. It is expected that this level will approach a 
very low level rather quickly, since half-life is about seven days-
During all phases of cleanup, workers will be provided protective 
clothing and a breathing apparatus. 
As mentioned earlier, sampling will occur on a weekly basis beginning 
when the area is fully exposed. Samples will be taken at 3 to 4 
locations from three different levels: surface, mid-depth and bottom. 
In addition, one sample will be taken from the clay layer underlaying 
the contaminated area. All samples will be sent state-side to a 
certified laboratory for analysis. 
When the pyridine level has decreased to zero or an acceptable level, 
the area will be restored and resurfaced according to the owner's 
requirements. The existing septic system will be used as is, replaced 
in Che same location or relocated elsewhere on the property. All 
laboratory effluent will be containerized until plans are made by the 
owner for disposal. Disposal procedures under consideration include 
sewerage, pretreatment and sewerage, or disposal in accordance with 
St. Croix Island authoratative guidelines. 
Safety Procedures 
To ensure the health of all personnel involved in the cleanup 
procedures, disposable protective clothing, including shoe coverings 
and hats will be provided. The breathing apparatus will be NIOSH 
approved masks with filters for organic vapors, acid gases and dust. 
The Scott part numbers and descriptions are listed below: 
Respirator (half face) 
Cartridge 
Dust Filter 
Dust Filter Holder 
TC-23C-174 
642-OA 
642-F 
642-FR 
Monitoring 
The program will be monitored by weekly sampling and analysis. 
Samples will be taken by ESI personnel or qualified persons presently 
cn site. 
Proiect Timina 
The cleanup of pyridine using the above described degradation 
procedures requires that water is prevented from entering the exposed 
area. 
This will be facilitated by rerouting of laboratory effluent, 
supplying portable toilets, and construction of an overhead shelter. 
This concept is further enhanced by conducting cleanup operations 
during May and June when rainfall is minimal. It is expected that the 
pyridine contamination can be cleaned in 30 - 45 days. The drying of 
100135 
Kunajnc 
We would appreciate your timely review of this request and a 
determination as to the disposal location of each item listed 
above. I will contact you next week as to your progress. If you 
have any question, please call me collect at 919/499-5182. 
Very truly yours/ 
ENVIRO-SCIENCES, INC. 
'X iZkzy 
Alan L. Kyles, PhD. 
Vice President 
AK/po 
(AK-8 5225) 
cc: Mr. Greg Rhymers 
Dept. Conservation & Cultural Affairs 
P.O. Box 4399 
S t . 
T h o m a s , 
U . S . V . l . 
00801 
100136 
• 
I.KDUSTRIAL 
CORROSION 
MANAGEMENT 
!NC0RPCPJ2,TED 
1152 ROUTE ;C. .RANDOLPH, NEW JERSEY 07869 '201 53<03;0 
m 
L 
CLIENT: ENVIRO SCIENCES. INC 
SAMPLE SOURCE: ICC (BERLEX). PKOJECT 
!iata Sheet 1 
NJD.EP Cartified Drinking Water/ 
Wastewater Laboratory ID i*14116 
REPORT DATE: August 15.1985 
LAB If 
42882 
SAMPLE ID: Drain Line Ifl 
SA."^LE DATE: 6/7/85 
SAMJ-'LED SY: 
A. Kyles 
SOIL SAMPLE 
LABORATORY ANALYSIS 
REPORT 
AT LAB DATE: 
6/18/85 
Idencificacion of Black Soil; 
Paranecer 
Result 
ienzene 
Ethylbenzene 
M-Xylene 
' 
0,?-Xylene 
0.10 
0.25 
0.33 
0.27 
Sample has "Toluene like or solvent odor. 
UNKNCU-N PE.-UCS 
?..T. 6.89 ac 40 mg/kg 
R.I.30.81 -c 2 mg/kg 
All results reported in mg/kg. 
Ve thank you for this opportunity to serve you. If you have any questions, 
please do not hesitate co call. 
nroUSTRLAL CORROSION MANAGEMENT, INC. 
ET/jmg 
•cl. 
^^pLess Than 
Edwin Tichenor 
Vice President 
100137 
M 
O 
O 
W 
00 
:ffl 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
\M1 IWUII 10. MMOMID. WW XKU.10'MI 101 M« 0)10 
CLIENT; 
ENVIRO SCIENCE - ICC (Berlex) 
NJDEP Certified Drinlcing Uater/Wastewat4^P^ 
Laboratory ID IIUIS 
SOIL SAMPLE 
REPORT DATE; July 31. 1985 
LAB f /|?861 
SAMPLE ID; Drain Line SI 
SAMPLE DATE: 
blllQb 
SAMPLED BY; 
A. Kyles 
VOLATILE ORGANICS BY PURGE AND TRAP 
By GC 
BTX/HEADSPACE 
^AT LAB DATE; 
8/18/85 
Compounds detected In parts per million (ml 11 igrams/lcilograms) dry weight basis. 
CHLOROMETHANE 
• 
BROMOMETHANE 
• 
VINYL CHLORIDE 
-
CHLOROETHANE 
• 
METHYLENE CHLORIDE 
ACETONE 
• 
1,1-DICHLOROETHYLENE -
1,1-DICHLOROETHANE **-• 
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER -• 
1,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE -• 
BROMODICHLOROMETHANE -• 
1,2-DICHLOROPROPANE ---
1,240 
M! 
68 
10 
"^Compounds co-elute (could be either material) 
LT«Less Than, GT-Greater Than 
dwb-Dry Weight Basis. 
X-Not Detected 
rC-1,3-DICHL0R0PR0PENE 
t-I,3-DICHL0ROPR0PENE 
— 
TCE (TRICHLOROETHYLENE) 
X_ 
^rl,l,2-TRICHLOROETHANE 
^DIBROMOCHLOROMETHANE 
BENZENE 
X_ 
DiISOPROPYL ETHER 
X 
2-CHLOROETHYLViNYL ETHER 
X_ 
BROMOFORM 
X_ 
1,1,2,2-TETRACHLOROETHANE 
X_ 
PCE (TETRACHLOROETHYLENE 
X. 
TOLUENE 
CHLOROBENZENE 
ETHYLBENZENE 
-
M-XYLENE 
• 
*rO-XYLENE 
P-XYLENE 
5.600 
**Tetrahydrofuran ( Phosgene also elute at this 
point. Numerical results are calculated for 
I,l-Dichloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of: 
_X 
^Unknown peaks detected (retention time,estImated amount); Xylenes 
16; 10 unknown hydrocarbon peaks ranging 
from 2 to 10 tng/kg. 
_ _ _ _ _ _ ^ 
NOTE;Compound Identification Is based upon retention time matches with specific known standards. Confirmation 
of anaiysis using GC/MS is required to positively identify any material and/or amount detected. 
11 
rt 
Dl 
n 
n 
n 
in Tichcftor, Vice Presf^Jm^ 
H 
O 
O 
l-» 
OJ 
vo 
Pi 
INDUSTRIAL 
CORROSION 
SOIL SAMPLE 
MANAGEMENT 
L'j 1 I I INCORPORATED 
))•>> KMU to MNtXHnt. WW JIHUT OrMI NI U4<I}N 
CLIENT; 
ENVIRO SCIENCE 
ICC (Berlex) 
NJDEP Certified Drinking Water/Wastewal 
Laboratory ID IUII6 
REPORT DATE; 
July 31.1985 
LAB I /.2889 
_ _ _ _ ^ 
SAMPLE ID: 
Dryer 
SAMPLE DATE: 
6/14/85 
SAMPLED BY: 
A. Kylea 
VOLATILE ORGANICS BY PURGE AND TRAP 
By GC 
BTX/HEADSPACE 
_AT LAB DATE; 
6/18/85 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis. 
CHLOROMETHANE 
BROMOMETHANE 
• 
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
1,1-DICHLOROETHYLENE -
1 ,1-DICHLOROETHANE **-• 
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER --
1,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE --
BROMODICHLOROMETHANE -
1,2-DICHLOROPROPANE ---
*[ c-l,3-DICHL0R0PR0PENE 
t-l,3-DICHL0R0PR0PENE "' 
TCE (TRICHLOROETHYLENE)-
^,I,1,2-TRICHLOROETHANE 
„ 
^DI BROMOCHLOROMETHANE 
"' 
' " ' 
— 
4.0 
340 
4.2 
^Compounds co-elute (could be either material) 
LT-Less Than, GT-Greater Than 
dwb-Dry Weight Basis. X-Not Detected 
BENZENE 
• 
DlISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER • 
BROMOFORM --T 
1,1,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE • 
TOLUENE 
• 
CHLOROBENZENE 
ETHYLBENZENE 
M-XYLENE 
*rO-XYLENE 
P-XYLENE 
6.6 
A. 000 
16.1 
ILL 
15.1 
A^Tetrahydrofuran & Phosgene also elute at this 
point. Numerical results are calculated for 
I,1-Dlchloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of; 1 mg/kg dwb. 
Unknown peaks detected (retention t ime,est imated amount): 
• 
NOTE:Compound identification Is based upon retention time matches with specific known standards. Confirmation 
of analysis using GC/HS Is required to positively identify any material and/or amount detected. 
INDUSJ 
J? 
rf 
m 
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u> 
(-> 
o 
o 
l - » 
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i 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
lit; Rouif 10. lUNoarH wA j(HS(r oiut nuti-oix 
NJDEP Certified Drinking Water/Uastewater 
Laboratory ID n h W d 
REPORT OATE:_ 
LAB H i^'il'^1 
AuniMt n.l9H5 
CLIENT: CNVIRO SCIENCES,INC. - ICC (BERLEX) PROJECT 
SAMPLE DATE: 
7/1/85 
SAMPLED BY: 
Enviro Sciences 
SAMPLE ID; Dryer 
AT LAB DATE: 
7/11/85 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CHROMATOGRAPHY/ HEADSPACE 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis 
CHLOROMETHANE 
BROMOMETHANE 
, 
VINYL CHLORIDE 
• 
CHLOROETHANE 
• 
METHYLENE CHLORIDE 
ACETONE 
• 
1 ,1-DICHLOROETHYLENE -• 
1,1-DICHLOROETHANE ** • 
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
1 ,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER --
1 ,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE --
BROMODICHLOROMETHANE --
M 
*[ 
1,2-DICHLOROPROPANE 
c-1 ,3-DICHLOROPROPENE 
t-l,3-DICHLOROPROPENE 
TCE (TRICHLOROETHYLENE) --
1,1,2-TRICHLOROETHANE 
DIBROMOCHLOROMETHANE 
BENZENE 
DlISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER -
BROMOFORM 
1,1,2,2-TETRACHLOROETHANE • 
PCE ( TETRACHLOROETHYLENE) 
TOLUENE 
• 
CHLOROBENZENE 
• 
ETHYLBENZENE 
• 
JL 
sua 
JL 
••Compounds co-elute (could be either material) 
LT"Les5 Than 
dwb«Dry Weight Basis. 
GT=Greater Than X-Not Detected 
**Tetrahydrofuran & Phosgene also elute at this 
point. Numerical results are caluclated for 
1,l-Dichloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 
mg/kg dwb. 
n 
If 
_X 
Unknown peaks detected (retention time, estimated amount) 
numerous other hydrocarbon peaks, 0.02 to 0.1 mn/kg 
NOTE: Compound identification is based upon retention time 
matches with specific known standards. Confirmation 
of analysis using GC/MS is required to positively 
EJ/ 
identify any material and/or amount detected. 
INDUSTRIAL CORROSION MGMT.,INC. 
r. Vice President 
H 
O 
O 
M 
M 
u 
INDUSTRIAL 
CORROSION . 
MANAGEMENT 
INCORPORATED 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID n k W S 
i M K U n tc. IWNOOini. WW XRSET 071(9 20l!l4-0)]0 
REPORT OATE; 
LAB # 
August 13.1985 
A3752 
Dryer 
CLIENT; ENVIRO SCIENCES,INC. - ICC (BERLEX) PROJECT 
SAMPLE ID; 
SAMPLE DATE: 
7/1/85 
SAMPLED BY: 
Enviro Sciences 
^AT LAB DATE; 
7/11/85 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CHROMATOGRAPHY/HEADSPACE 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis 
CHLOROMETHANE 
BROMOMETHANE-
VINYL CHLORIDE 
• 
CHLOROETHANE 
• 
METHYLENE CHLORIDE 
ACETONE 
• 
1,1-DICHLOROETHYLENE -
1,1-DICHLOROETHANE ** • 
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER --
1,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE — 
BROMODICHLOROMETHANE --
.2.JL 
*( 
*I 
1,2-DICHLOROPROPANE 
c-l,3-DlCHL0R0PR0PENE 
t-i ,3-DICHLOROPROPENE 
TCE (TRICHLOROETHYLENE) — 
1,1,2-TRICHLOROETHANE 
DIBROMOCHLOROMETHANE 
BENZENE 
DlISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER -
BROMOFORM 
• 
1,1,2,2-TETRACHLOROETHANE • 
PCE ( TETRACHLOROETHYLENE)-
TOLUENE 
• 
CHLOROBENZENE 
-
ETHYLBENZENE 
• 
JLui. 
••'Compounds co-elute (could be either material) 
LT-Less Than 
dwb-Dry Weight Basis. 
GT-Greater Than X-Not Detected 
Ai^Tetrahydrofuran & Phosgene also elute at this 
point. Numerical results are caluclated for 
1,l-Dichloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 
J( 
Unknown peaks detected (retention time, estimated amount) 34.07 g 15 mg/kg 
mg/kg dwb. 
NOTE; Compound identification is based upon retention time 
matches with specific known standards. Confirmation 
of analysis using GC/MS is required to positively 
EJ/ 
identify any material and/or amount detected. 
INDUSTRIAL CORROSION MGMT.,iNC. 
n 
n 
rt 
/in Tichenor, Vice President 
• 
toluene ladened soils will be ongoing during this time period. 
Summarv 
Over 6,000 tons (estimated) of soil has to be cleansed of about 245 
pounds of hazardous materials (125 lbs- of toluene; 120 lbs. of 
pyridine). ESI proposes to clean the soil on site since proper 
equipment is available, the materials are conducive to on site 
cleanup, and the total amount is rather small (245 lbs.). Release of 
these materials to ambient air will not have an adverse effect on 
nearby residence (0.1 miles away) since the release rate will be low, 
5 - 15 mile per hour winds are normally present, and nearby residents 
are upwind from the facility. Safety precautions will be employed 
during all phases of the operation. 
It is the contention of Berlex and ESI that the above described 
cleanup procedures are the most cost effective and efficient methods 
which can be utilzed. 
Literature Sources Consulted 
Black, Crow, and Eidsness, Inc. 1976. A Water Management Plan for St, 
Croix, U.S. Virgin Islands. Project No. 540-72-51. 
Department of Conservation and Cultural Affairs. 1983. 
Comprehensive Water Resources Management Plan for the 
U.S. Virgin Islands. 
Environmental Research and Technology, Inc. 1984. 
The Land Treatability of Appendix VIII Constituents Present 
in Petroleum Industry Wastes. API Publication 4379. 
Washington, D.C. 
1983. Land Treatment 
Practices in the Petroleum Industry. American Petroleum 
Institute, Washington, D.C. 
Soil Conservation Service. 1970. Soil Survey: Virgin Islands of the 
United States. USDA. Washington, D.C. 
100142 
TABLE I 
TE.MPERATURE AND PRECIPITATION 
[Data from Alexander Hamilton Field, St. Croix] 
3 
1 
3 
a 
a 
Month 
January 
February 
March 
. April 
1 May 
' June 
July 
August 
September--
October 
November 
December 
Year 
Temperature 
Average 
daily 
maximum 
•F. 
83 
83 
84 
86 
86 
88 
88 
89 
88 
88 
86 
84 
86 
Average 
daily 
minimusi 
"F. 
70 
70 
-1 
73 
74 
76 
76 
76 
75 
75 
73 
72 
73 
Average 
maximum 
... 
r . 
86 
36 
66 
88 
89 
90 
90 
91 
91 
90 
89 
j87 
92 
Average 
minimum 
•F. 
65 
66 
66 
68 
70 
71 
71 
72 
71 
70 
68 
^67 
Precipitation 
Average 
total 
In. 
2.23 
2.19 
1.73 
2.83 
4.31 
3.10 
3.51 
4.58 
6.65 
5.45 
4.65 
3.34 
44.57 
One year in 10 will have--
Less than--
In. 
0.50 
.44 
.40 
.55 
.60 
.58 
.80 
1.20 
2.20 
1.60 
1.20 
1.00 
34.00 
More than--
In. 
7.2 
5.8 
4.6 
7.6 
8.2 
6.0 
6.6 
8.8 
11.0 
10.2 
9.0 
8.6 
53.8 
Average number of 
days with more 
than one-tenth 
of an inch of 
rainfall 
5 
6 . 
4 
6 
8 
9 
8 
9 
10 
8 
9 
9 
91 
Average annual highest 
temperature. 
Average annual lowest ternperature. 
100143 
FIGURE 1 
FACILITY LOCATION MAP 
5.000 10.000 
FEET 
FACILITY 
LOCATION 
H 
O 
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SOURCE: 
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WATER 
RESOURCES 
MANAGEMENT 
P L A N FOR THE UNITED 
STATES VIRGIN I S L A N D S . 
1983. 
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SCALE 
100149 
CONCRETE 
PADDING 
V 
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SCALE 
100150 
ATTACHMENT 
100151 
ATTACHMENT C 
.;iRo • KicncEJ inc. 
%<^W<^|^%« 19 COPEUVND RD., DENVILLE. NEW JERSEY 07834 
^ ^ ^ ^ ^ ^ 
(201)366-6256 
Mav 
1 5 , 
1985 
Mr. Robert Harris 
U.S.E.P.A. 
Region II 
26 Federal Plaza 
NY, NY 
10007 
Re : Island Chemical Co. (Berlex) St. Croix, U.S.V.l. 
Dear Mr. Harris: 
A" 
As per our telephone communication on May 9, 1985, 
Enviro-Sciences, Inc. (ESI) will begin the cleanup of pyridine and 
toluene contamination at Island Chemica^l Co., U.S.V.l. This 
cleanup will commence on June 6 and be conducted as described in 
documents submitted to you in December, 1984 (Progress Report 
Island Chemical Company, Inc. St. Croix Virgin Islands) and April 
4 ;Addendum to Progress Report...). 
I r.ave briefed Mr. Carlos O'Neal in San Juan as to our plans and 
will forward to him the above documents. In addition, these same 
Gccuments will be sent to Mr. Austin Moorhead of the Conservation 
and Cultural Affairs office in St. Croix. 
ESI will take all samples which will be sent with a chain of 
c'jstody to independent laboratories stateside for analysis. All 
samples will be handled in accordance with U.S. Department of 
Agriculture permits which are in the possession of the 
laboratories. ESI will adhere to the restrictions of the permits 
when shipping soil samples. 
Attempts will be made to isolate all contamination (especially 
pyridine odor) to the site. If odor is excessive after concrete 
re:noval , release of contamination from the exposed area will be 
daripened using plastic sheeting. However, ESI does not think that 
excessive odor release will be a problem. 
100152 
ATTACHMENT D 
100153 
AITACHMENT 
D 
^cnvmoBlKicnaiinc. 
^ M ^ S ^ y W 19 COPELAND RD., DENVILLE. NEW JERSEY 07834 
(201)366^256 
May 7 , 
1985 
Mr. Robert Harris 
U.S.E.P.A. 
Region II 
Room 1000 
26 Federal Plaza 
New York, NY 10007 
Reference; Island Chemical Co., St. Croix, U.S.V.l. 
Dear Mr. Harris: 
Enclosed is information concerning the manifesting of hazardous 
material at Island Chemical Co. when operations ceased end prior 
to its sale by Berlex to Virgin Island Chemical Co. Included are 
eight (8) manifests. 
In addition, there is an explanation as to why activities at the 
facility would classify it as a small generator. 
We are anticipating a meeting in the immediate future with USEPA 
staff members to discuss this project. 
If you have any questions, call me at 201-366-6256. 
Very truly yours, 
EKVIRO-SCIENCES, INC. 
Alan L. Kyle's, Ph.D. 
Vice President 
ALK/po 
(AK-8531) 
Enclosure 
cc: Mr. Robert Milos 
r/-
Mr. Frank Curtis 
^ 
Ray Willis, Ph.D. 
100154 
I a p p r e c i a t e your continual a t t e n t i o n to t h i s project over the 
past months and w i l l keep you informed as to our progress. 
Very t r u l y yours, 
ENVIRO-SCIENCES, INC. 
^ • < ^ 
; 
Alan L. Kyles, Ph.D. 
Vice President 
ALK/po (AK-8554) 
cc: 
Bob Milos 
Frank Curtis 
Ray Willes, PhD. 
100155 
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INDUSTRIAL 
CORROSION 
SOIL SAMPLE 
MANAGEMEf/T 
INCORPORATED 
IIW IWtni 10 MMXHFH. MIW JUUT OfMI K l M4«l)0 
CLIENT: 
ENVIRO SCIENCE 
ICC (Berlex) 
NJDEP Certified Drinking WaterA/aslewate 
Laboratory ID l l \ k \ \ e 
REPORT DATE; 
July 31.1985 
LAB / 
/*2H89 
__ SAMPLE ID; 
Dryer 
SAMPLE DATE; 
6/1A/85 
SAMPLED BY: 
A. Kylea 
VOLATILE ORGANICS BY PURGE ANO TRAP 
By GC 
'BTX/HEADSPACE 
_AT LAB DATE; 
6/18/85 
m 
H 
o 
o 
H 
Compounds detected In parts per million (milligrams/kilograms) dry weight basis. 
CHLOROMETHANE 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
1,1-DICHLOROETHYLENE -
1,1-DICHLOROETHANE **--
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
1 ,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER -
1 ,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE -
BROMODICHLOROMETHANE --
1,2-DICHLOROPROPANE 
— 
*[ 
c-l,3-DICHL0R0PR0PENE 
t-l,3-DlCHL0R0PR0PENE ' 
TCE (TRICHLOROETHYLENE) 
^f1,1,2-TRICHLOROETHANE 
„ 
'DIBROMOCHLOROMETHANE 
' 
A.O 
340 
A.2 
^Compounds co-elute (could be either material). 
LT-Less Than, GT-Greater Than 
dwb-Dry Weight Basis. X-Not Detected 
BENZENE 
DlISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER -
BROMOFORM --T 
1,1,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE -
TOLUENE 
CHLOROBENZENE 
ETHYLBENZENE 
M-XYLENE 
*r O-XYLENE 
, 
P-XYLENE 
6,6 
A. 000 
16.1 
ALd. 
15.1 
**Tetrahydrofuran & Phosgene also elute at this 
point. Numerical results are calculated for 
I,l-Dichloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of; 1 mR/kR dwb. 
Unknown peaks detected (retention time,estImated amount); 
NOTE:Compound identification Is based upon retention time matches with specific known standards. Confirmation 
of analysis using GC/MS Is required to positively Identify any material and/or amount detected. 
INDUS! 
rf 
n 
Rrm~^ 
l\ 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
lli2M)UI£ 10. RANOO.N. N(* JiAS(r07M> 20l'il4-0]]0 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID /?U116 
REPORT DATE:_ 
LAB # 437A7 
Aui'.u.st 15.1985 
CLIENT: CNVIRO SCIENCES.INC. - ICC (BERLEX) PROJECT 
SAMPLE ID; Dryer 
SAMPLE DATE: 
7/1/85 
SAMPLED BY: 
Enviro Sciences 
AT LAB DATE; 
7/11/85 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CHROMATOGRAPHY / HEADSPACE 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis 
CHLOROMETHANE 
BROMOMETHANE- 
, 
VINYL CHLORIDE 
CHLOROETHANE 
• 
METHYLENE CHLORIDE 
ACETONE — — 
• 
1,1-DICHLOROETHYLENE -
1,1-DICHLOROETHANE ** • 
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
I,2-DICHLOROETHANE 
;-BUTYL METHYL ETHER -
1,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE --
BROMODICHLOROMETHANE --
X 
i. 
X_ 
1,2-DICHLOROPROPANE 
. 
^,c-1,3-DICHLOROPROPENE 
' 
't-l,3-DICHLOROPROPENE 
TCE (TRICHLOROETHYLENE) 
^ 
^rl,l,2-TRICHLOROETHANE 
'DIBROMOCHLOROMETHANE 
^ 
BENZENE 
DIISOPROPYL ETHER 
' 
2-CHLOROETHYLVINYL ETHER 
" 
BROMOFORM 
" 
1,1,2,2-TETRACHLOROETHANE 
" 
PCE ( TETRACHLOROETHYLENE) 
" 
TOLUENE 
" 
CHLOROBENZENE 
' 
ETHYLBENZENE 
' 
K. 
X 
HJil 
••'Compounds co-elute (could be either material). 
LT-Less Than 
dwb-Dry Weight Basis. 
GT-Greater Than X»Not Detected 
**Tetrahydrofuran & Phosgene also elute at this 
point. Numerical results are caluclated for 
1,l-Dichloroethane only. 
KO 
rH 
O 
O 
H 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 
mg/kg dwb. 
_X 
Unknov^/n peaks detected (retention time, estimated amount) 
numerous other hydrocarbon peaks, 0.02 to 0.1 wf./kg. 
ID 
m 
rr 
NOTE: Compound identification is based upon retention time 
matches with specific known standards. Confirmation 
of analysis using GC/MS is required to positively 
£-^/ 
identify any material and/or amount detected. 
INDUSTRIAL CORROSION MGMT.,INC. 
Cdwin Tichenor, Vice President 
01 
:i;'i'i 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
lib? win( IC. KAWxuftt. m w x K i i otitt loi-stt-oijo 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID /^'i'tllS 
REPORT DATE:_ 
LAB 
ff 
A3752 
August 15.1985 
CLIENT; ENVIRO SCIENCES,INC. - ICC (BERLEX) PROJECT 
SAMPLE DATE: 
7/1/85 
SAMPLED BY: 
Enviro Sciences 
SAMPLE ID: 
Dryer 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CHROMATOGRAPHY/ HEADSPACE 
AT LAB DATE; 
7/11/85 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis 
CHLOROMETHANE 
BROMOMETHANE 
VINYL CHLORIDE 
• 
CHLOROETHANE 
• 
METHYLENE CHLORIDE — • 
ACETONE 
• 
I,1-DICHLOROETHYLENE -
1,1-DICHLOROETHANE ** -
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
JL 
X 
XJL 
X 
X 
1,2-DICHLOROETHANE --• 
t-BUTYL METHYL ETHER -
1.1,1-TRICHLOROETHANE 
CARBON TETRACHLORIDE -
BROMODICHLOROMETHANE -
X 
1,2-DJCHLOROPROPANE 
^,c-l,3-DICHL0R0PR0PENE 
4-1 ,3-DICHLOROPROPENE 
TCE (TRICHLOROETHYLENE) --
^e1,1,2-TRICHLOROETHANE 
'oIBROMOCHLOROMETHANE 
BENZENE 
DIISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER -
BROMOFORM 
1,1,2,2-TETRACHLOROETHANE • 
PCE ( TETRACHLOROETHYLENE)' 
TOLUENE 
• 
CHLOROBENZENE 
• 
ETHYLBENZENE 
• 
J . ^ 
•'•Compounds co-elute (could be either material) 
LT-Less Than 
dwb-Dry Weight Basis. 
GT-Greater Than X-Not Detected 
**Tetrahydrofuran & Phosgene also elute at this 
point. Numerical results are caluclated for 
1, l-Dichloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 
J5 
Unknown peaks detected (retention time, estimated amount) 34.07 g 15 mg/kg 
mg/kg dwb. 
NOTE; Compound identification is based upon retention time 
matches with specific known standards. Confirmation 
of analysis using GC/MS is required to positively 
ET/ 
^^entify any material and/or amount detected. 
INDUSTRIAL CORROSION MGMT.,INC. 
. 
3w.n Tichenor, Vice President 
IT) 
vo 
H 
o 
o 
H 
:y 
n 
n 
rt 
tn 
>j'i 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1)2 MMII .0. MNOOIPH. WM J(U(T 071(9 201 il4«lH 
CLIENT: ENVIRO SCIENCES,INC. - ICC (BERLEX) PROJECT 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID jCI'<ll6 
REPORT DATE: 
August 15.1985 
LAB # 
AA629 
SAMPLE ID: 
Dryer 
SAMPLE DATE: 
7/17/S5 
SAMPLED BY: 
Enviro Sciences 
AT LAB DATE: 
7/25/85 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CHROMATOGRAPHY / HEADSPACE 
Compounds detected In parts per million (milligrams/kilograms) dry weight basis 
CHLOROMETHANE 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
I , I-DICHLOROETHYLENE 
--
I ,1-DICHLOROETHANE * * • 
t - l ,2-DICHLOROETHYLENE 
X 
CHLOROFORM 
I ,2-DICHLOROETHANE ---
t-BUTYL METHYL ETHER • 
1,1,1-TRICHLOROETHANE 
CARBON TETRACHLORIDE -
BROMODICHLOROMETHANE -
X 
X 
X 
X 
1.2 
X 
X 
X 
X 
X 
X 
X 
X 
X 
*i 
" I 
* I 
1,2-DICHLOROPROPANE 
c-1,3-DICHLOROPROPENE 
t-l,3-DICHLOROPROPENE 
TCE (TRICHLOROETHYLENE) --
I,1,2-TRICHLOROETHANE 
DIBROMOCHLOROMETHANE 
BENZENE 
DIISOPROPYL ETHER 
• 
2-CHLOROETHYLVINYL ETHER -• 
BROMOFORM 
• 
1,1,2,2-TETRACHLOROETHANE • 
PCE ( TETRACHLOROETHYLENE) 
TOLUENE 
• 
CHLOROBENZENE 
• 
ETHYLBENZENE 
• 
0.07 
0.36 
"Compounds co-elute (could be either material) 
LT-Less Than 
dwb-Dry Weight Basis. 
GT-Greater Than X-Not Detected 
**Tetrahydrofuran S Phosgene also elute at this 
point. Numerical results are caluclated for 
1,l-Dichloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 
mg/kg dwb. 
^Unknown peaks detected (retention time, estimated amount) numerous other hydrocarbon peaks O.OI to 1 ms/kg 
vo — 
vo 
H — 
o 
o 
t-t 
— 
O i 
NOTE; Compound identification Is based upon retention time 
matches with specific known standards. Confirmation 
of analysis using CC/MS is required to positively 
EX/ 
identify any material and/or amount detected. 
INDUSTRIAL CORROSION MGMT.,INC. 
t 
r, Vice President 
INDUSTRIAL 
CORROSION sI^LE 
MANAGEMENT 
INCORPORATED 
i t a 
Sheet 7 
NJDEP C e r t i f i e d 
D r i n k i n g 
W a t e r / 
W a s t e w a t e r 
L a b o r a t o r y 
ID # l ' 4 l l 6 
REPORT DATF: 
J u l v 3 1 . 1985 
LAB » 
^2886 & ^2887-COMPOSITE 
1152 ROlHE 10. RANDOLPH. NEW JERSEY 07869 
201 584 0330 
CLIENT; 
ENVIRO SCIENCES 
SAMPLE SOURCE:. 
SAMPLE DATE: 
6 / 1 A / 8 5 
ICC (Berlex) 
SAh'.PLED BY: 
A . K y l e s 
AT LAB DATE: 
6/18/85 
PRIORITY POLLUTANT VOLATILE ORGANICS + AO 
by 
GC/MS 
t 
15 
PEAKS 
Pararrieter 
R e s u l t 
P a r a m e t e r 
R e s u l t 
a c r o l e i n * 
a c r y l o n i t r l l e * 
benzene 
b r o o o f o r m 
c a r b o n 
t e t r a c h l o r i d e 
c h l o r o b e n z e n e 
c h l o r o d ibrcxTKjmethane 
c h l o r e t h a n e 
2 - c h l o r o e t h y l v i n y l 
e t h e r 
c h l o r o f o r m 
d l c h l o r o b r o m o m e t h a n e 
1 , 1 - d i c h l o r o e t h a n e 
1 , 2 - d i c h l o r o e t h a n e 
1 , 1 - d i c h l o r o e t h y 1 e n e 
_Z2IL 
1,2-dichloropropane 
1,3-dichloropropylene 
ethylbenzene 
methyl bromide 
methyl chloride 
methylene chloride 
1 ,1 ,2,2-tetrachloroethane • 
tetrachloroethylene 
toluene 
•,----
1 ,2-trans-dichloroethylene 
1 ,1,1-trichloroethane 
1,I,2-trichIoroethane 
trichloroethylene 
vinyl chloride 
Results reported in mg/kg (ppm), dry weight basis. 
*Detection Limit 
LT-Le5s than 
X=Not detected 
100 ppm 
OTHER COMPOUNDS DETECTED 
APPROXIMATE 
CONCENTRATIONS 
125 
1.560 
benryl acetate — 
22 
chloromethyl benzene 
1430 
l-chloro-2-methyl benzene 
40 
ET/jmg 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
dwlnV \Ar^<?r> 
EdwinVTichen'cvc 
Vice President 
100167 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1152 ROOTE 10. RANDOLPH. NEW JERSEY 07869 
201 5M 0330 
CLIFNT: 
ENVIRO SCIENCE 
" ^ t a Sheet 8 
NJDEP Cert 
led D r i n k i n g Water/ 
WasLewate.- Laboratory 
ID #1^116 
REPORT DATE: July 31, 1985 
LAB I 
42886 & 42887 COMPOSITE 
SOIL SAMPLE 
SAMPLE SOURCE; 
ICC (Berlex) 
SAMPLE DATE: 
ft/U/fiS 
SAHPLFD BY: A. Kvles 
.AT LAB DATF.; 
6/18/fi5 
PESTICIDE 6 PCB EXTRACTABLES 
PRIORITY POLLUTANTS + kO 
• 
by GC/MS 
Pa rameter 
Result 
Aldrin 
LT 2-
a-BHC 
LT 2 
b-BHC 
LT 2 
d-BHC 
- 
LT 2 
S-BHC 
- 
LT 2 
C.hlordane 
LT 12 
'»,^'-DDD 
LT 3 
ij.^'-DDE 
LT 3 
i^.A'-ODT 
- - 
LT 3 
O i e l d r l n 
LT 3 
E.-idosulfan I 
L T 3 
Endosulfan 
II 
LT 3 
Endosulfan Sulfate 
LT 3 
E.-idrin 
LT 3 
Endrin Aldehyde 
LT 3 
Heptachlor 
LT 3 
Heptachlor Epoxide 
LT 3 
Tcxaphene 
• 
LT 12 
PCB-10'16 - - — 
— 
LT 45 
PCB-1221 
- 
LT 45 
P^B-^232 
- 
LT45 
PCB-12A2 
LT 45 
P^B-12A8 
- 
- 
- 
LT 4-7 
PCB-125A 
LT 45 
PCB-1260 
LT 45 
All 
r e s u l t s are reported in mg/kg (ppm), dry weight b a s i s . 
INDUSTRIAL CORROSION MGMT, 
Edw i V*^ T i ch^xior 
— 
/ , 
E T / j m g 
V i c e P r e s i d e n t 
/ d ^ 
L T » L e s s 
Than 
X=Not 
D e t e c t e d 
100168 
INC 
INDUSJ. ..AL 
CORROSION ^°'^ ' ^ ^ ^ 
ti.ivKf (,«•'I I 1 • 
' u r m k l i x ) M.wr.r/ 
Data Sheet 9 
Wastewater 
L. 
. l a t o r y 
ID #14116 
MANAGEMENT 
INCORPORATED 
nS2 R0U1E 10. RANDOLPH. NEW JERSEY 07869 
201 5«4 0330 
CL I ENT: 
ENVIRO SCIENCES 
REPORT DATE: 
Julv 31,1985 
LAB # 
42886 & 42887-COMPOSITE 
SAMPLE SOURCE; ICC (Berlex) 
SAMPLE DATC; 6/14/85 
SAMPLED BY: 
A.Kyles 
.AT LAB DATE; 
6/13/85 
BASE/NEUTRAL EXTRACTABLES PRIORITY POLLUTANTS + ««0 
by GC/MS 
•» 15 PEAKS 
Parameter 
Result 
acenephthene 
X 
acenaphthylcne 
X 
anthracene 
• 
X 
benzidine 
X 
benzo (a)anthracene 
X 
ben2o(a)pyrcne 
X 
S.'l-benzof lucranthene 
X 
benzo(ghl)perylene 
X 
benzo(k)fluoranthene 
X 
bls(2-chloroethoxy)methane 
X 
b l s ( 2 - c h l o r o e t h y l ) e t h e r 
X 
bl s ( 2 - c h l o r o l s o p r o p y l ) e t h e r 
X 
b l 5 ( 2 - e t h y l h e x y l ) p h t h a l a t e 
X 
'»-bror>ophenyl phenyl ether 
X 
b u t y l benzyl phthalate 
X 
2-ch1 oronaphthalene 
X 
*»-chl orophenyl phenyl ether 
X 
chrysene. 
X 
dlbe.izo(a,h)anthracene 
X 
1,2-dIchlorobenzene 
X 
1,3-dlchlorobenzene 
X 
1 ,l»-d Ichlorobenzene 
X 
' 3,3-dichlorobenzIdlne 
. 
X 
Parameter 
Result 
diethyl phthalate 
dimethyl phthalate 
dl-n-butyl phthalate 
2,'»-dln i tro to luene 
2,6-d ini trotoluene 
di-n-octyl phthalate 
1,2-dI phenyl hydrazine(as azobenjene)' 
fluoran thene 
fluorene 
hexachlorobenzene 
hexachlorobuladlene 
• 
hexachtorocyclopentadiene 
--
hexachloroethane 
lndeno(l,2,3-cd)pyrcne 
isophorone 
naphtha Icne 
ni trobenzene 
N-ni trosodlmcthylamine 
N-nltrosodi-n-propylamine 
N-ni trosodiphenyl aminc 
phenanthrene 
pyrene 
1 ,2,'<-trIchlorobenzene 
A 
- _ X 
None of the above listed Priority Pollutants detected at a sensitivity level of 
450 ng/kg (ppm) dry weight basis. ** . 
LT-Less Than 
X=Not Detected 
**Large dilution necessary due to high concentration of benzyl acetate. 
APPROXIMATE CONCENTRATION 
OTHER COMPOUNDS DETECTED 
benzyl acetate — 
,/Se/r^ benzene methanol 
_ 
170,000 
15,000 
l,l'-[oxybi8 (inethylene) 
bis Jbenzene 
Chloromethyl benzene 
diphenyl methanone — 
9H-fluorene-9-one 
— 
4,400 
30,000 
4,000 
All results reported in mg/kg (ppm), dry weight basis. 
E T / - - f 
3,000 
100169 
INDUSTRIAL CORROSION MGMT.,INC. 
INDUSTRIAL 
CORROSION 
fAAHAGEMEKT 
L ' J I 1 I INCORPORATED 
IDIMUIIIO.MMKIirHWWJIRMTO/IM H I U 4 01N 
NJDEP C e r t i f i e d Drinking Water/Wastewa 
Laboratory ID #I<<I16 
arer 
SOIL SAMPLE 
REPORT nATP; 
July 3 1 . 1965 
LAB I 
A2886 & 42887 COMPOSITE 
CLIENT: 
ENVIRO SCIENCE.^ 
SAMPLE SOURCE; 
ip.r. rRprl.v^ 
SAMPLE DATE: 
6/14/»S 
SAMPLED BY: 
A 
yyi^g 
AT LAB DATE; 
6/lS/fl5 
ACID 
EXTRACTABLES 
PRIORITY 
POLLUTANTS + kO 
bv qC/MS-H 10 PEAKS 
O 
O 
M 
-J 
O 
ACID EXTRACTABLES PRIORITY POLLUTANTS + 1 0 Peaks 
2-chlorophenol 
2-nitrophenol 
phenol 
2,'<,-dimethylphenol 
2,'<,-dichlorophenol 
pentachlorophenol 
2,'i-dlnl trophenol 
'•,6-dlnl tro-o-cresol 
— 
'•-ni trophenol 
2,'»,6-trichlorophenol --
'•-chloro-3 methyl phenol 
OTHER COMPOUNDS DETECTED APPROXIMATE CONCENTRATIONS 
X 
None of the above listed Priority Pollutants detected 
at a aenistivity level of 450 mg/kg (ppm) dry weight basia 
No other Phenolic compounds detected at a sensitivit} 
of 500 mg/kg (ppm) dry weight basis. ** 
INDUSTRIAL CORROSION MANAGEMENT, INC 
** Large dilution necessary due to high concentration 
of benzyl acetate. 
ET/jmg 
LT-Less Than 
X-Not Detected 
Edwifr- Tich 
Vice President 
rt 
tu 
n 
n 
rt 
ca Sheet Ll 
INDUSTRIAL 
CORROSION 
„ 
MANAGEMENT 
INCORPORATED 
lis? RWJll 10. RANOOIPH. NEW XRStT 0;tl£9 
?0l M< 0 IVI 
n IFMT. 
ENVIRO SCIENCES 
SOIL SAMPLE 
NJDEP Ceriified Drinking Water 
Wjslewater Laboratory ID #14116 
REPORT DATE: Julv 31. 1985 
LAB # 42886 & 42887 Composite 
SAMPLE SOURCE: ICC (Berlex) 
SAIPLE DATE L_1ZAAZ85___ SAMPLED BY: A. Kyles 
AT LAB DATE:6/18/85 
— - ^ 
PRIORITY POLLUTANTS-H 40 
TOXIC POLLUTANTS: Metals, Cyanide and Total Phenols 
PARAMETER 
Tot a 
Tota 
Tota 
Tota 
Tota 
Tota 
Tcta 
Tota 
Tcta 
Tcta 
Tcta 
Tota 
Tcta 
Tota 
Tcta 
Antimony -
Arsenic --
Be ryI Ii um 
Cadmium --
Chromium -
Copper 
— 
Lead -- — • 
Mercury -• 
Nickel --• 
Selenium • 
S iIver — 
ThaI Ii um • 
Zinc 
RESULT 
LT 118. 
40.0 
LT 
2.87 
22.8 
592 
327 
688 
2.73 
134 
LT 
1.08 
LT 
7.48 
LT 66.2 
3.594 
Cyan ide 
Phenol -
ZL.^U 
9^01 
All 
r e s u l t s are reported in mg/kg (ppm)', dry weight b a s i s . 
We thank you for this opportunity to serve you. 
If you have any q u e s t i o n s , 
please 
do not h e s i t a t e to c a l l . 
Very truly yours, 
INDUSTRIAL CORROSION MGMT., INC. 
ET/jmg 
LT=Less Than 
X=Not Detected 
dwin TicheWor 
— 
/ 6^ 
Edwin TicheWo 
Vice President 
100171 
;>ata ineet L^ 
INDUS Ml AL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Cc.tified Drinking Water/ 
Wastewater Laboratory ID #14116 
REPORT DATE: August 15.1985 
LAB # 44418 
1152 ROUTE 10, RANDOLPH, NEW JERSEY 07869 
2QI 584 0330 
CLIENT: 
ENVIRO SCIENCES. INC. 
SAMPLE SOURCE: 
ICC (BERLEXI PROJECT 
SAMPLE ID; St.Croix 
SAMPLE DATE: -w^wova- 
SAMPLED BY: 
Al Kyles 
.AT LAB DATE: 
TI22J%5 
WATER 
Parameter 
PRIORITY POLLUTANT VOLATILE ORGANICS 
by GC/MS 
acrolein* 
acrylonitrile* 
benzene 
brornoform 
carbon t e t r a c h l o r i d e 
chlorobenzene 
chlorodibromomethane 
chlorethane 
2-chloroethy1vinyl 
ether 
chloroform 
dichlorobromomethane 
I , I - d i c h l o r o e t h a n e 
I ,2-dIchloroethane 
1 ,1-dichloroethylene 
Result 
0.04 
Parameter 
I,2-dichloropropane 
I,3-dichloropropylene 
ethylbenzene 
methyl bromide 
methyl chloride 
methylene chloride 
I,1,2,2-tetrachloroethane -
tetrachloroethylene 
toluene 
I,2-trans-dichloroethylene 
I,1,I-trichloroethane 
I,I,2-trichloroethane 
trichloroethylene 
vinyl chloride 
-
Results reported in mg/l (ppm). Detection limit 0.001 mg/l (ppm) 
Resui t 
.Q.3g 
JL 
*Detection Limit: Q.l mg/i 
E T / j m g 
I N D U S T R I A L 
C O R R O S I O N 
M G M T . , I N C 
J 
Edwin 
T i c h e n o r 
V i c e 
P r e s i d e n t 
LT=Less Than 
X=Not Detected 
100172 
INDUS'i..iAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
..V.UUI ».<.i Lll I tz- 
II idKing wa L t r/ Wa stewater 
Laboratory 10 ,116 
Data Sheet 13 
REPORT DATE: 
August 15.1985 
LAB » 
^^^^8 
; 
1152 ROUTE 10. RANDOLPH, NEW JERSEY 07869 
201 584-0330 
CL I FMTf 
FNVTi;n 
< ; r T E N r E S . 
I N C . 
SAMPLE cniiRrP- 
ICC(BERIEX) 
; 
St. Croix 
SAMPLE nATg: 
u n l r — - 
<;AMPI FD BY: 
A l Kyles 
AT LAB OATE: 
/9y/^d<ryr'jyi— 
WATER 
PESTICIDE & PCB EXTRACTABLES 
PRIORITY POLLUTANTS 
, 
by GC/h? 
Parameter 
Result 
Aldrln 
- 
- 
LT 0.01 
a-BHC 
LT 0.01 
b-BHC 
LT 0.01 
d-BHC : 
LT 0.01 
g-BHC 
— 
- LT 0.01 
Chlordane 
- 
LT 0.02 
4,i*'-DDD 
LT 0.01 
1*,4'-DDE 
- 
LT 0.01 
1»,'»'-DDT 
LT 0.01 
Dieldrin 
LT 0.01 
Endosulfan I 
- 
LT 0.01 
Endosulfan II 
LT 0.01 
Endosulfan Sulfate 
- 
— LT 0.01 
Endrin 
- 
LT 0.01 
Endrin Aldehyde 
- 
- 
LT 0.01 
Heptachlor 
- ^ 
- 
LT O.OI 
Heptachlor Epoxide 
LT 0.01 
Toxaphene 
- 
LT 0.02 
PCB-I 016 
- 
LT 0.01 
PCB-1221 
- 
-— LT 0.01 
PCB-1232 
- 
LT 0.01 
PCB-1 2^*2 
- 
LT 0.01 
PCB-12'»8 
- 
LT 0.01 
PCB-125A 
- 
- 
LT 0.01 
PCB-1260 
- 
LT 0.01 
A l l 
r e s u l t s reported in mg/l (ppm). 
INDUSJRIAL^CJia&i)SI/ 
Edwin 
T i c h e n o r 
ET/jmg 
Vice 
P r e s i d e n t 
LT=Less 
t h a n 
X=Not 
d e t e c t e d 
7/22/85 
MGMT. , INC 
100173 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
i l » ; ROUTE 10. MNOOlfN, NEW JUSEr tJU9 » l M4-03M 
CLIENT: 
ENVIRO SCIENCES, INC, 
NJDEP C e r t i f i e d Drinking Water/Wastewater 
Laboratory ID #11«I16 
REPORT DATE: 
August 15,1985 
LAB # 
44418 
l-« 
o 
o 
l-» 
•J 
1^. 
SAMPLE SOURCE; 
SAMPLE D A T E L 
ICC (BERLEX) PROJECT 
unknown-' 
/^y^^yyftJ&— 
SAMPLED BY: 
Al 
BASE/NEUTRAL 
Parameter 
Result 
acenaphthene 
X 
acenaphthylene 
X 
anthracene 
• 
X 
benzidine 
X 
benzo(a)anthracene 
X 
ben2o(a)pyrene 
X 
3 .'i-benzof luoranthene 
X 
ben2o(ghl)perylene 
X 
benzo(k)fluoranthene 
X 
bis(2-chloroethoxy)methane 
X 
bis (2-chIoroethyl)ether 
X 
bis (2-chloroisopropyI)ether 
X 
bis(2-ethyihexyl)phthalate 
X 
4-bromophenyI phenyl ether 
X 
butylbenzyl phthalate 
X 
2-chloronaphthalene 
X 
4-chlorophenyl phenyl ether 
X 
chrysene 
X 
diben2o(a,h)anthracene 
X 
I ,2-dlchlorobenzene 
X 
I ,3-dichlorobenzene 
X 
I ,'4-dlchlorobenzehe 
X 
3,3-d'chloroben2ldlne 
X 
None of the above Priority Pollutants detected 
**Other compounds see Addendum I 
LT-Less Than 
X-Not Detected 
C T / I mr* 
SAMPLE ID: ST. Croix 
Kyles 
AT LAB DATE: 
7/22/85 
EXTRACTABLES PRIORITY POLLUTANTS 
bv GC/MS 
Parameter 
diethyl phthalate 
dimethyl phthalate 
di-n-butyl phthalate 
-; 
2,4-dinitrotoluene 
2 ,6-dini trotoluene 
di-n-octyl phthalate 
I,2-diphenylhydrazine (as azobenzene) 
fluoranthene 
fluorene 
---
hexachlorobenzene 
" 
hexachIorobutad iene 
hexachlorocyclopen tadiene 
hexachloroethane 
indeno(l,2,3-cd)pyrene 
i sophorone 
naphthalene 
n i t robenzene 
N-n11 rosod imethy I amIne 
N-ni trosod i-n-propyI amine 
N-ni t rosodI phenyl amine 
phenanthrene 
pyrene 
1,2,'•-tr Ichlorobenzene 
at a sensitivity level of 0.03 mg/l (ppm) 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
Result 
rr 
0) 
n 
n 
rt 
Edwin Tichenor 
Vice President 
''CI 
'Hta Sheet If 
NJDEP Certified Drinking Water/ 
Wastewater Laboratory ID ii'14116 
REPORT DATE; August 15,1985 
LAB H 44418 
CLIENT: 
ENVIRO SCIENCES, INC. 
SAMPLE SOURCE; 
ICC (Berlex) 
SAMPLE ID: St. Croix 
SAMPLE DATE; wkriuwir 
SAMPLED BY: 
Al. Kyles 
AT LAB DATE; 
y9yZZZEZyys~~ 
BASE/NEUTRAL EXTRACTABLES PRIORITY POLLUTANTS 
ADDENDUM I 
_0THER_C0MP01JNDS DETECTED 
by~Gc7MS~ ~ 
Parameter 
Result 
7/22/85 
benzaldehyde 
chloromethyl benzene 
benzene methanol 
phenyl acetate 
diphenyl methane 
1-1'-[oxybis(methylene]bis benzene 
All results are reported in mg/l (ppm). 
3.0 
0.3 
24.0 
26.0 
0.4 
0.4 
We thank you for this opportunity to serve you. If you have any questions, 
please do not hesitate to call. 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
ET/jmg 
end. 
LT=Less Than 
Edwin Tictfenor 
Vice President 
100175 
Jata Sheet 16 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
11S2 ROUTE 10, RANDOLPH, NEW JERSEY 07869 
201 584-0330 
NJDEP Certified Drinking Water/ 
Wastewater Laboratory ID #14116 
REPORT DATE: 
August 15.1085 
LAB # 
44418 
CLIENT: 
ENVIRO SCIENCES. INC. 
SAMPLE SOURCE 
ICC (BERLEX) PROJECT 
ST. Croix 
SAMPLE DATE: 
unKuuwir SAMPLED BY: 
Al Kvles 
y9J7rcy/9crr^ 
AT LAB DATE: 
ACID EXTRACTABLES 
PRIORITY POLLUTANTS bv GC/MS 
l l l H ^ ' ^ 
WATER 
Parameter 
Result 
2-chlorophenol 
X 
2-nitrophenol 
X 
phenol 
X 
2,4-dimethylphenol 
X 
2,i4-dichlorophenol 
X 
2, i( ,6-trichlorophenol 
X 
pentachlorophenol 
X 
2 ,i<-din i trophenol 
X 
A.^-dinitro-o-cresol 
X 
'•-n i trophenol 
X 
'4-chloro-3 methyl phenol 
X 
None of the above P r i o r i t y P o l l u t a n t s detected at a s e n s i t i v i t y level of 0.01 mg/l (pp: 
OTEZR PEAKS DETECTED: 
benzoic acid (? 3 mg/l 
INDUSTRIAL CORROSION 
MGMT.,INC 
ET:j mg 
LT=Less Than 
X^Not Detected 
ZZZE^ 
Edwin 
T i c h e n o r 
V i c e 
P r e s i d e n t 
100176 
jata Sheet 17 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
u s ? RLvll 10. RANOOlPH, NtW JERSEY 07S69 
201 W4 OI"«l 
CL1ENT: 
ENVIRO SCIENCES INC. 
NJDEP Certified Drinking Water 
Wastewater Laboratory ID #14116 
REPORT DATE: 
A»yn«;t 15.1985 
LAB I 
44418 
SA.-.PLE SOURCE-^ 
SA.-.PLE DATE: 
ICC (BERLEX) PROJECT 
SAIQ'LE ID: 
St. Croix 
• uitknumr* <;AMPI rn BY: 
Al Kyles 
y^jZrc^/rp/j— 
PRIORITY 
POLLUTANTS 
AT LAB DATE: 
7/22/85 
TCXIC POLLUTANTS: 
PAt^AMETER 
Metals, Cyanide and Total Phenols 
Tota 
Tota 
Tota 
Tota 
Tota 
Tota 
Tota 
Tota 
Tota 
Tota 
Tota 
Tota 
Tota 
Tota 
Tota 
All 
Antimony -
Arsenic --
Beryl Iium 
Cadmium -• 
Chromium • 
Copper 
Lead -----
Mercury -• 
Nickel --• 
Selenium • 
S iIver — 
Thai 1ium ' 
Zinc 
Cyan i de 
Phenol • 
WATER SAMPLE 
RESULT 
LT 
LT 
LT 
],T 
0. 
0-
fi-
0. 
0. 
0 
0 
n 
0 
0 
0 
0 
4 
0 
0 
m6 
005 
013 
003 
027 
JJ.3 
nn 
nm 
080 
Jlil5 
sm 
SOS 
85 
053 
061 
results are reported in ng/l (ppm). 
We thank you for this opportunity to serve you. 
do -lot hesitate to call. 
If you have any questions, please 
Very truly yours, 
INDUSTRIAL CORROSION MGMT., INC. 
L. 
E T / > q 
LT=Less Than 
X=Sot Detected 
Edwin Tichenor 
Vice President 
100177 
1» COPtLANO TO.. DEMVILLt NEW JERSCT 07a>4 
CHAIN OP CUSTODY RECORD 
I n s t a l l a t i o n : 
ICC (Berlex) 
S u r v e y 
N o . : 
S a m p l e r s : 
( S i g n a t u r e ) 
(ULtXyU^t^. *>fc^jZo> 
o. 
B 
«o c 
Vi Z 
S t a t i o n 
L o c a t i o n 
Date 
Analysis 
Time 
Sample 
Type 
Comp 
G r a b 
vr 
u 
c 
«»-l 
- r i 
o n 
u 
• c 
o o 
2 
U 
Drain Line 
^ t Z l ^ S ' l 
Toluene 
6/8/85 
Identify the contents bf^the black soil 
sample.] 
2 
3 
4 
5 
6 
Laboratory P i t 
^ ^ S ^ P 3 
Pyridine 
6/14/85 
Laboratory Pit-duplicate ^ ^ ^ VGA /^(^/, 6/14/85 
Time limit may have expired, if so do not run.] 
7 7 7 F S 
Plt--diinHe3re niniHd^ P r l n r i t v Pollutants 6/14/8! 
y: 
Pit-duplicate (liquid) Priority Pollutantb 6/14/85 4m 
^F^mrs 
Pit-Interface(liquid/sludge)\ 
combine and 
run 
6/14/85 
T A T F T 
i p r i o r i t y 
Pit-3ludge 
v a f g ^ 
-^ p o l l u t a n 
u t a n t s 
6/14/85 /pyo 
X 
[* One container has a white lump, segregate 
^ 
it and an; lyze for qulnid ne. ] 
Drver 
Relinquished by: (Sign.) 
CC- ifs 'A^^f'f 
Toluene 
6/14/85 
Relinquished by: (Sign.) 
R e c e i v e d 
by:. ( S i g n . ) 
JZLi / 
R e c e i v e d 
b ^ : 
( S i g n . ) 
D a t e / T i m e 
D a t e / T i m e 
r e l i n q u i s h e d 
b y : 
( S i g n . ) 
R e c e i v e d 
by: 
( S i g n . ) D a t e / T i m e 
R e l i n c m i s h e d 
by 
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f i e l d 
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( S i g n . ) 
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D a t e / T i m e 
^7i'^s' /x'/.r 
Dispatched by: (Sl/^n.) 
Date/Tlra^ Rec'd for Laboratory 
by: 
D a t e / T i m e 
.Method of 
S h i p m e n t : 
Express Air Freight 
/ T L 
ClcAAEtAy^ 
1 0 0 1 7 8 
LAB NO. 42885 
Pit duplicate (liquid),Priority Pollutants +40 
(Process Pit) 
Samples not analyzed because sample volume too small. 
100179 
I t COPtLANO TO., DEMVnOJL MEW JEWCY 07»M 
CHAIN OP CUSTODY RECORD 
'3f^^ 
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(^1-^ 
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Date/Time 
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• 
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Rec'd by Laboratory 
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V 
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V 
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Date /Time 
Date/Time 
D a t e / T i m e 
D a t e / T i m e 
D a t e / T i m e 
Method of Ship^nenXi, 
y 
, / ^ 
/ 
^ 
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100180 
CHAIM OP CUSTODY RECORD 
I t CJDflUMO TO, O e f V U l . NEW J C W l OTtM 
I n . t . l U t l o n : 
^
^ 
;
^
^ 
Survay Mo.: 
^ ^ i c ^ 9 
^ 4 0 ^ 3 c 
-<A-<^62I 
CO 
Station Location 
Samplers: (Slgnatur*) 
/)/e</€y2, (^7a'y('^^<yzA) 
/^S^/^ / Z / " J a ^ T ^ ^ c J / ^ / ^ / l y x ^ ) 
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Rirlinqulahed by:, ( S i g n . ) 
Rezlinquished by: (Sign//) 
Relinquished by: 
(Sign.) 
Relinquished by: 
( S i g n . ) 
"X 
> ^ 
/ 
^ 
Received by: (Sign. ) 
fZZ Ji 
^-i~Lcyr^-'.-.-<-!JL^ 
Received by: CSlgn. ) 
Dat«/TiB* 
Received by: (Sign. ) 
Dispatched by: 
(Sign.) 
Date/Tim* 
Rec'd by Laboratory 
for field 
analysis 
(Sign.) 
Dat«/TiiBa 
Data/Time 
Date/Tim* 
Rec'd for Laboratory 
by: 
Dattt/Tima 
Method of Shipment 
cZziyuc^ zZ^/oC /^^^ly^ay/y' 
100181 
anwio S Ksncsi nc 
CHAIN OP CUSTODY RECORD 
I t C O m > M O TO.. O e M L L I k M n r JEMKY OTVM 
i^/g 
In.t.llation: 
y ^ ^ 
^ / f < r 
Survey No.: 
• 
a 
S ' 
« c 
Vi 2 
• 
Station Location 
/Z^y/^y/y/^^y//?*;/! -A- ^ ^ 
/"^^-^^^^ /<y^ A4/C<^ 
RelAnquished by: (Sign.) 
Relinquished by: (Sign.) / 
Kelinquiahed by: (Sign.) 
Relinquished by: (Sign.) 
Dispatched by: (Sign.) 
Date/Time 
Samplers: (Signature) 
Date 
/^yf! 
/ 
• 
Time 
^ 2 cc 
Sample Typoj 
Comp. 
Received by: (Sign.) 
Received by: J Sign.) 
Received by: (Sign.) 
Rec'd by Laboratory 
for field analyais 
(Sign.) 
Rec'd for Laboratory 
by: 
-tirab 
V 
No. of 
Containeri 
<y. 
Date/Time 
Date/Time 
Date/Time 
Date/Time 
Date/Time 
Method of Shipment: 
^ 
y / 
100182 
ATTACHMENT 
100183 
u^ T 
&i till 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
iis?nuuiE 10.RANOGLPii.Niv.'jEnsEr07669 
roistt-oajo 
NJDEP Ceiiificd Drinking Water/Wastewater 
Laboratory 10^14116 
REPORT DATE: 
Septeml.cr 12.1985 
LAB 
45362 
CLIENT: 
ENVIRO SCIENCE - ICC RERLEX PROJECT 
SAMPLE ID: 
Lab Pit //5965 
SAMPLE DATE: August 7, 1985 
SAMPLED BY: 
Enviro Science 
AT LAB DATE: 
August 9. 1985 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CHROMATOGRAPHY/ HEADSPACE 
CHLOROMETHANE.. 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE ---
ACETONE 
1,1-DICHLOROETHYLENE -
I ,1-DICHLOROETHANE *^ 
t-I ,2-niCHLOROETHYLENE 
CHLOROFORM 
1 ,2-OICHLOROETHANE ---
t-BUTYL METHYL ETHER -
1 ,1 ,1-TRlCHLOROETHANE 
CARBON TETRACHLORIDE -
BROMODICHLOROMETHANE -
Compounds detected in parts per million (milligrams/kilograms) dry weight basis 
- 
X 
X 
X 
X 
X 
0. 32 
X 
0. 
0. 
02 
02 
X 
X 
X 
X 
X 
X 
M 
1,2-DICHLOROPROPANE 
c-1,3-DICHLOROPROPENE 
t-I,3-OICHLOROPROPENE'" 
TCE (TRICHLOROETHYLENE) 
1,1 ,2-TRICHLOROETHANE 
DIBROMOCHLOROMETHANE 
BENZENE 
DIISOPROPYL ETHER --- 
• 
2-CHLOROETHYLVINYL ETHER -• 
BROMOFORM 
• 
1,1 ,2,2-TETRACHLOROETHANE • 
PCE ( TETRACHLOROETHYLENE)-
TOLUENE 
• 
CHLOROBENZENE 
ETHYLBENZENE 
• 
0.34 
0.08 
0.01 
"Compounds co-elute (could be either material) 
LT=Less Than 
dwb=Dry Weight Basis. 
GT=Greater Than X=Not Detected 
••'••"Tetrahydrofuran £ Phosgene also elute at this 
point. Numerical results are caluclated for 
1,1-Dichloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 
0.01 
mg/kg dwb. 
H 
o 
o 
H 
00 
(1^ 
JJ Unknown peaks detected (retention time, estimated amount) Xylenes approx 0.06 mg/kg dwb 
NOTE: Compound identification is based upon retention time 
matches with specific known standards. Confirmation 
of analysis using GC/MS is required to positively 
identify any material end/or amount detected. 
;:SI.: 
INDUSTRIAL CORROSION MANAGEMENT, INC. 
zMyZjl^ 
'iJichard 
SyLevi'he/P 
lii chard S./Levi'he/President 
> 
o 
H 
ni 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
1157HOurt l i WNDOLPli, Nf* Jt«5tro?<69 ?0I 58<-O330 
NJDEP C e r t i f i e d Drinking Water/Wastewater 
Laboratory ID H k W i , 
REPORT DATE: 
September 12.1985 
LAB ff 
45363 
CLIENT: 
ENVIRO SCIENCE - ICC BERLEX PROJECT 
SAMPLE ID: 
Lab P i t 
//5966 
SAMPLE DATE: 
Aufiust 
7, 
1985 
SAMPLED BY: 
E n v i r o 
Science 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CHROMATOGRAPHY/ HEADSPACE 
AT LAB DATE: 
August 9 . 
1985 
CHLOROMETHANE 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
HETHYLENE CHLORIDE - — 
ACETONE 
- -
1,1-DICHLOROETHYLENE 
-
1 ,1-DICHLOROETHANE '^* 
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
I,2-DICHLOROETHANE 
- - -
t-BUTYL METHYL ETHER -
1 ,1,1-TRICHLOROETHANE 
CARBON TETRACHLORIDE 
-
BROMODICHLOROMETHANE 
-
Compounds d e t e c t e d 
in p a r t s 
per m i l l i o n 
( m i l l i g r a m s / k i l o g r a m s ) 
dry w e i g h t 
b a s i s 
X 
1,2-DICHLOROPROPANE 
-
X 
X 
X 
X 
0. 27 
X 
0. 
0, 
02 
01 
X 
X 
X 
X 
X 
X 
,rc-l,3-DICHLOROPROPENE 
"'t-l,3-DICHLOROPROPENE" 
M 
TCE (TRICHLOROETHYLENE) 
, 1 , 2 - T R I C H L 0 R 0 E T H A N E _ _ 
DI BROMOCHLOROMETHANE 
BENZENE 
DIISOPROPYL 
ETHER 
2-CHLOROETHYLVINYL 
ETHER -
BROMOFORM 
1,1,2,2-TETRACHLOROETHANE 
• 
PCE ( 
TETRACHLOROETHYLENE)' 
TOLUENE 
CHLOROBENZENE 
• 
ETHYLBENZENE 
JL 
A.OL 
X 
X . 
"Compounds co-elute (could be either material). 
LT=Less Than 
dwb=Dry Weight Basis. 
GT=Greater Than 
X=Not Detected 
••"^••'Tetrahydrofuran 6 Phosgene also elute at this 
point. 
Numerical results are caluclated for 
1,1-Dichloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 
mg/kg dwb. 
o 
Unknown peaks detected (retention time, estimated amount) 
M 
00 
tn 
NOTE: Compound i d e n t i f i c a t i o n is based upon r e t e n t i o n time 
matches w i t h s p e c i f i c known standards. Confirmation 
of analysis using GC/HS is required to p o s i t i v e l y 
i d e n t i f y any m a t e r i a l and/or amount d e t e c t e d . 
INIJUSTRIAL CORROSION HAf.'AGEMENT, INC. 
'ilichorci S ./Lev i-ne/Pres i d e n t 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
ll5?H0UIt 10. RfNOOini. NtW jenSCV 0»«69 30) 5»«-0330 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID n ^ \ 16 
REPORT OATE: 
.^e pi ember 12.1985 
LAB /f 
45364 
CLIENT: 
ENVIRO SCIENCE - ICC BERLEX PROJECT 
SAMPLE ID: Lab Pit //5967 
SAMPLE DATE: August 7, 1985 
SAMPLED BY: 
Enviro Science 
AT LAB DATE: August 9. 1985 
VOLATILE ORGANICS BY PURGE AND TRAP 
GAS CHROMATOGRAPHY/HEADSPACE 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis 
"Compounds co-elute (could be either material) 
LT=Less Than 
dwb=Dry Weight Basis. 
GT=Greater Than X=Not Detected 
X 
CHLOROMETHANE 
X 
BROMOMETHANE 
X 
VINYL CHLORIDE 
211 
CHLOROETHANE 
HETHYLENE CHLORIDE 
- 
— 
ACETONE 
I,1-DICHLOROETHYLENE --
1,1-DICHLOROETHANE AA 
t-l,2-DICHLOROETHYLENE 
-
CHLOROFORM 
- 
- 
--- 
- — 
1 ,2-DICHLOROETHANE 
-
t-BUTYL METHYL ETHER 
1 , I , 1-TRICHLOROETHANE 
-
CARBON TETRACHLORIDE 
BROMODICHLOROMETHANE -- 
--- 
--
0.23 
0.03 
0.11 
,2-DICHLOROPROPANE 
.,rc-l ,3-DICHLOROPROPENE 
"'t-l,3-DICHLOROPROPENE'" 
TCE (TRICHLOROETHYLENE) 
^rl,1,2-TRICHLOROETHANE 
"'0 IBROHOCHLOROMETHANE 
BENZENE 
DIISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER -
BROMOFORH 
1,1,2,2-TETRACHLOROETHANE • 
PCE ( TETRACHLOROETHYLENE)-
TOLUENE 
CHLOROBENZENE 
ETHYLBENZENE 
X 
X 
X 
0. 01 
X 
X 
X 
X 
X 
0. 05 
X 
0. 04 
••"^Tetrahydrofuran 6 Phosgene also elute at this 
point. Numerical results are caluclated for 
1,1-Dichloroethane only. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 
0.01 
mg/kg dwb. 
XUnknov;n peaks detected (retention time, estimated amount) 
o 
00 
-. 
o\ , 
NOTE: Compound identification Is based upon retention time 
matches with specific known standards. Confirmation 
of analysis using GC/HS is required to positively 
identify any material and/or amount detected. 
;.SL: 
Xylene —0.02 mg/kg dwb 
INDUSTRIAL CORROSION MANAGEMENT. INC. 
Kichard S ./Lev IT 
ine/President 
CHAIM Of CUSTODY RECORD 
V5-'J^V 
.'i-3<i J ^ ^ / 
/ .z:}co- V 
• 
-. 
• 
• 
i«cofCLAMOno.DefvmxNIWjcwr OTVM 
I t i . t a l U t i o n : 
/ ^ ^ 
j
^
.
^ 
Survey Mo.: 
a • « c 
CO a 
r-2.-3 
s-^L/ 
't\ 
S t a t i o n 
L o c a t i o n 
^ ^ / ( ^ < ^ 
//^^^y<>*^) 
/ ^ ^ 
( ^ r Z Z ^ d h o y ^ 
y^^/^yZ^ f/ZU^-aZZAic, 
/ 
i n q u i s h e d by: 
( S i g n . ) 
\^.A^^\t^.y\, c L ^ - 
/^ie\AX>\.>k-A^ 
K e i i n q u i a h e d 
by: 
( S i g n . ) | 
K e i i n q u i s h e d 
by: 
( S i g n . ) 
R e l i n q u i a h e d 
by: 
( S i g n . ) 
D i a p a t c h e d b y : 
( S i g n . ) 
Date/Time 
Samplera: 
( S i g n a t u r e ) 
(y 
Date 
7^^1^ 
// 
Time 
' y^.'Arry 
tZP.yx?^ 
^ • * % V r f 
Sample 
Type 
Comp. G r a b 
^ 
\ 
\ 
• 
Received by: 
( S i g n . ) 
Received 
by:(j(Sign.) 
Received by: ( S i g n . ) 
Rec'd by Laboratory 
for f i e l d 
a n a l y a i s 
( S i g n . ) 
Rec'd for 
L a b o r a t o r y 
by: 
1 
No. of 
Container! 
/ 
z 
^ 
D a t e / T i m e 
D a t e / T i m e 
D a t e / T i m e 
D a t e / T i m e 
D a t e / T i m e 
Method of Shipment: 
^ ^ 
1 0 0 1 8 7 
ATTACHMENT G 
100188 
YORK LABORATORIES DIVISION 
ATTACHMENT G 
/^.f-^ 
CERTIFIED REPORT TRANSMIHAL 
REPORT NUMBER 
3 0 8 5 0 - 1 4 5 
DATE_ 
November 12, 19 8 4 
CLIE.NT 
Enviro-Sciences, Inc-
19 Copeland Road 
Denville, New Jersey 
07834 
AHENTION ]ZZ^ 
Ir^j Cohen 
• 
The above referenced report is enclosed. Copies of this report and supporting dctc 
will be retained in our files in tfie event ttiey are required for future reference. 
If ttiere are any questions conceming ttiis report, please do not hesitate to contact us 
Any samples subnnitted to our Laboratory will be retained for a maximum of sixty (60] 
days from receipt of this report, unless other arrangemenrs are desired. 
Naturally, cs in the pest, our staft will be pleased to quote on any future requirements 
you may have. 'n addition to the sen/ice provided, we also offer the following: 
Hazardous Waste Analyses 
Product Evcluction'R&.D 
Water and Wastewater Analyses 
Air and Process Gcs Analyses 
Industrial Hygiene Surveys 
fvletallurgical Analyses 
fvlicrobiologicci Analyses 
Mass Spectrometry Services 
ruly Y o u j s ' / ^ 
Robert Q. Bradley 
Vice President 
C. .NC. 
100189 
November 12, 1984 
30850-145 
ENVIRO-SCIENCES, INC. 
19 Copeland Road 
Denville, New Jersey 
07834 
Attention: Mr. Irv Cohen 
PURPOSE 
Nine (9) soil samples were submitted to York Laboratories for 
determination of toluene and pyridine on a quantitative basis. 
Other compounds found in the samples were also indentified and 
are reported on a semi-quantitative basis. 
The samples were 
also analyzed for oil and grease. 
METHODOLOGIES 
The 
samples were analyzed 
for toluene using 
the dynamic 
headspace 
Gas 
Chromatograph/Mass 
Spectrometry 
method 
in 
accordance with Chemical Analysis of Sediments and Elutriate 
Testing, EPA 1979. 
A Tekmar Model LSC-3 Purge and Trap 
interfaced 
with 
an HP 5995C GC/MS/DS were used 
for the 
analysis. 
The samples were analyzed for pyridine and oil and grease in 
accordance with EPA/CE-81-1 Procedures for Handling and Chemi-
cal Analysis of Sediments and Water Samples, May 1981. 
An HP 
5995C GC/MS/DS was used for the pyridine analysis. 
RESULTS 
The results are listed in the following tables. 
Prepared by 
.ZJl^ 
Gail D. Sprio 
Senior, Chemist 
oenxor v..neraisx A 
Approved by: 
U/>/^^../ C • IAAJ.UZC' 
J^ejzitey C. Curran 
Ghiigt'X:hleraist 
^ 
GDS/JCC/mz 
100190 
TABLE 1 
ENVIRO-SCIENCES, INC. 
TOLUENE AND PYRIDINE RESULTS 
Sample 
Identification 
20 Septic 
20 A-2' 
21 A-2' 
21 A-4' 
25 - 2' 
27 - 2' 
32 - 2' 
35 - 4' 
36 - 2' 
(Auger) 
Toluene 
ug/kg (pob) 
540 
690 
15 
43 
210 
16 
15 
8 
7 
Pyridine 
ug/kg (ppb) 
<1,000 
<1 ,000 
<1 ,000 
<1 ,000 
13,000 
26,000 
43 ,000 
<1 ,000 
<1,000 
100191 
Samole Identification 
20 Septic (Auger) 
20 A - 2' 
21 A - 2 
21 A - 4 
2 5 - 2 
- 2' 
3 2 - 2 
35 - 4' 
35 - 2' 
TABLE 2. 
ENVIRO-SCIENCES. INC. 
Compounds Found 
1,1-raethylene bis-benzene 
diphenyl methanone 
methylene chloride 
chloroform 
benzene 
methylene chloride 
chloroform 
benzene 
ethyl benzene 
total xylenes 
methylene chloride 
chloroform 
trichloroethylene 
benzene 
tetrachloroethylene 
ethyl benzene 
methylene chloride 
chloroform 
benzene 
methylene choride 
chloroform 
benzene 
methylene chloride 
chloroform 
benzene 
methylene chloride 
chloroform 
1,1, l-trichloroethane 
benzene 
methylene chloride 
chloroform 
1 ,1 , l-trichloroethane 
benzene 
methylene chloride 
chloroform 
benzene 
Concentration* 
8,400 
64 ,000 
<5 
12 
<5 
<5 
5 
<5 
68 
600 
<5 
<5 
<5 
<5 
<5 
7 
<5 
<5 
<5 
<5 
5 
<5 
<5 
19 
<5 
<5 
<5 
<5 
<5 
<5 
13 
11 
<5 
<5 
<5 
<5 
1.5) 
0.5) 
2.3) 
0.9) 
4) 
3) 
S) 
6) 
9) 
2.2) 
2.6) 
0.4) 
1-7) 
0.4) 
2.2) 
0.6) 
4.4) 
4.2) 
0.8) 
0.8) 
2.4) 
0.4) 
1.6) 
1.4) 
0.2) 
^Results are reported on a semi-quantitative basis 
100192 
TABLE 3 
ENVIRO-SCIENCES, INC. 
OIL AND GREASE RESULTS 
Oil And Grease 
Sample Identification 
mg/kg (ppm) 
20 Septic (Auger) 
20 A - 2' 
21 A - 2' 
21 A - 4' 
2 5 - 2 ' 
2 7 - 2 ' 
3 2 - 2 ' 
35 - 4' 
36 - 2' 
241 
566 
1 ,500 
27.9 
89.6 
137 
50.6 
39 .5 
965 
100193 
YORK LABORATORIES DIVISION 
(^yy/rr^ 
CERTIFIED REPORT TRANSMIHAL 
REPORT NUMBER 
30850-1195 
DATE 
Septe:nber 25, 
1985 
CUENT 
E n v i r o s c i e n c e s , 
I n c . 
19 Copeland Road 
D e n v i l l e , NJ 
07834 
ATTENTION 
Dr. A. Kyles 
The above referenced report is enclosed. Copies of this report and supoorting data 
will be retained in our files in the event they are required for future reference. 
If there are any questions conceming this report, please do not hesitate to contact u i 
Any samples submitted to our Laboraton/ will be retained for a maximum of sixty (60) 
days from receipt otthis report, unless other arrangements are desired. 
Naturally, cs in the past, our staff will be pleased to quote on any future requirements 
you may have. In addition to the service provided, we also offer the following: 
Hazardous Waste Analyses 
Product Evaluation/R&D 
Water and Wastewater Analyses 
Air and Process Gas Analyses 
Industrial Hygiene Surveys 
Metallurgical Analyses 
Microbiological Analyses 
Moss Spectrometry Services 
V^y Truly Yourv/' 
Robert Q. Bradley . 
Vice President 
^ 
100194 
,c.-.-ce 
;;.^6 • :ViC.' 
September 25, 1985 
30850-1195 
ENVIROSCIENCES, INC. 
19 Copeland Road 
Denville, New Jersey 07834 
Attention: Dr. A. Kyles 
PURPOSE AND RESULTS 
Eight (8) soil samples were submitted to York Laboratories for 
analysis. The samples were prepared and analyzed in accordance 
with Procedures for Handling and Chemical Analysis of Sediment 
and Water Samples, EPA/CE-Sf-I. 
The results are reported in the following Tables. 
Prepared by; ZII^xv^x^^-^-6^ 
Daniel F. Ott 
Laboratory Manager 
Approved by: ^ i J o , u., C ^ - (z/U<y,^ 
•J^fr^y/C. Curran 
/Cftikf Chemist 
D?0/JCC/md 
100195 
TABLE 1 
30850-1195 
ENVIROSCIENCES, INC. 
Sample Identification 
Toluene, ug/kg 
Drainline #1, 6/7/85 4 p.m. 
140,000 
Drainline #2, 6/7/85 4 p.m. 
310,000 
Dryer SI, 6/14/85 10 a.m. 
1,500,000 
Dryer #2, 6/14/85 10 a.m. 
150,000 
100196 
Y'.VC. !\'C. • 2ZZ McP'CS T^.TCi'<e • ••Acr.rce. Cznr.zrzr.es. C6^6£ •i2Z2'; 2z'-^z3. 
TABLE 2 
30850-1195 
ENVIROSCIENCES, INC. 
Sample Identification 
Pyridine, ug/kg 
Lab Pit #1, 6/14/85 
3,900 
Lab Pit #2, 6/14/85 
<150 
Lab Pit #3, 6/14/85 
510 
Lab Pit #4, 6/14/85 
180 
100197 
>VC. '->^IC. • 222 */'c.~'c-? '^rrz.'<e • Mc^rce. 2zr.r.ecz.z'z: C;6-c; • !2-3' 26'-—53 
YORK LABORATORIES DIVISJON 
'/zyrr 
CERTIFIED REPORT TRANSMIHAL 
REPORT NUMBER 
30850-1283 
DATE 
September 2 5 . 1985 
CLIENT 
E n v i r o s c i e n c e s , 
I n c . 
19 Copeland Road 
D e n v i l l e , NJ 
07834 
ATTENTION 
Dr. A. Kvles 
The above referenced report is enclosed. Copies of this report and supporting date 
will be retained in our tiles in the event they are required for future reference. 
If there are any questions conceming this report, please do not hesitate to contact us. 
Any samples submitted to our Laboratory will be retained for a maximum of sixty (60) 
days from receipt of this report, unless other arrangements are desired. 
Naturally, c% in the past, our staff will be pleased to quote on any future requirements 
you may have. In addition to the service provided, we also offer the following: 
Hazordous Waste Analyses 
Product Evaluatioa'R&.D 
Water end Wastewater Analyses 
Air and Process Gas Analyses 
Industrial Hygiene Surveys 
Metallurgical Analyses 
Microbiological Analyses 
Mass SpectTometr/ Services 
Robert Q. Bradley 
Vice President 
/ 
100198 
r.vr 
Mc-rce rw.-rc:.;3 • ^icrrce. Cc: 
September 25, 1985 
30850-1283 
ENVIROSCIENCES, INC. 
19 Copeland Road 
Denville, New Jersey 
07834 
Attention: Dr. A. Kyles 
PURPOSE AND RESULTS 
Six (6) soil samples were submitted to York Laboratories for 
analysis. The samples were prepared and analyzed in accordance 
with Procedures for Handling and Chem.ical Analysis of Sediment 
and Water Samples, EPA/CE-81-1. 
The results are reported in the following Tables. 
'repared by; ^^^.y,^' ^ - t : Z ^ 
Daniel F. Ott 
Laboratory Manager 
Acoroved bv 
C. Curran 
hemist 
DFO/JCC/md 
100199 
T.VC. :NJC • z r : Mcr-ca :'jrT.-z: 
••/crrce. 
:nr.:?c 
TABLE 1 
3 0 8 5 0 - 1 2 8 3 
ENVIROSCIENCES, 
INC. 
Sample I d e n t i f i c a t i o n 
T o l u e n e , 
ug/kg 
5434 - D r y e r , 
7 / 1 / 8 5 
7,700 
5435 - D r y e r , 
7 / 1 / 8 5 
920 
100200 
•.VC, :.''JC. • 2C3 ''/ic."ro3 Tc.rc:/e • 'Vlcnrce. Cc-r,ecr:c-: Cd-ic; • '22;'. 25'-—;£i 
TABLE 2 
30850-1283 
ENVIROSCIENCES, INC. 
Sample Identification 
Pyridine, ug/kg 
5436 - Lab Pit, #1, 7/1/85 
1,100 
5437 - Lab Pit, #2, 7/1/85 
3,400 
5438 - Lab Pit, #3, 7/1/85 
<150 
5439 - Lab Pit, #4, 7/1/85 
<150 
100201 
n v c . :NC. • 22C .Mcrrce 'u.-Ci^e • !'Azr.rzs. Czrr.Bczz-s: 06Ui5 • •22;', 2i'--^£3 
YORK LABORATORIES DIVISJON 
7Z7zrj-
CERTIFIED REPORT TRANSMIHAL 
REPORT NUMBER 
30850-13^3 
DATE 
September 26, 1985 
• 
CL'ENT 
AHENTION 
Envirosciences, Inc. 
19 Copeland Road 
Denville, NJ 0783A 
Dr. A. Kvles 
The above referenced report is enclosed. Copies of this recort and supporting data 
will be retained in our files in ihe event they ore required fcr future reference. 
If there are any questions conceming this report, please do not hesitate to contact us. 
Any samples submitted to our Laboraton/ will be retained fcr a maximum of sixty (60) 
days from receipt of this report, unless other arrangements cre desired. 
Naturally, as in the past, our staff will be pleased to quote on any future requirements 
you may have. In addition to the service provided, we also offer the following: 
Hazardous Waste Analyses 
Product EvaluatiorvR&D 
Vv'ater and Wastewater Analyses 
Air and Process Gas Analyses 
Industrial Hygiene Surveys 
Metallurgical Analyses 
Microbiological Analyses 
Mass Spectrometry Services 
Very Truly Yoi 
Robert Q. Bradley 
Vice President 
100202 
•^vvc. : N C .-"JC '-A-
: e 
•.•W.T.C:J<^ 
September 26, 1985 
30850-1343 
ENVIROSCIENCES, INC. 
19 Copeland Road 
Denville, New Jersey 
07834 
Attention: Dr. A. Kyles 
PURPOSE AND RESULTS 
Four (4) soil samples were submitted to York Laboratories for 
analysis. The samples were prepared and analyzed in accordance 
with Procedures for Handling and Chemical Analysis of Sediment 
and Water Samples , EP.A/CE-8 1-1 . 
The results are reported in the following Tables. 
Prepared by: —^^U. ..> r-cSH 
Daniel F. Ott 
Laboratory Manager 
Approved by: Q - y ^ ^ 
C-- 
( , / U ^ ^ . 
yjffk-p^ fZ. Curran 
/^'hA^r Chemist 
DFO/JCC/md 
"X/ 
100203 
TABLE 1 
30850-1343 
ENVIROSCIENCES, INC. 
Sample Identification 
Toluene, ug/kg 
5753 - Dryer 
600 
5754 - Drver 
660 
100204 
/'.VC. :.NC. • 222 r/cr.,'ce Tu.—.ciiee-Mc,".rce. Ccr;r.ec:;c'jt 26^:63 •1,2031 261-^-^53 
TABLE 2 
30850-1343 
ENVTROSCIENCES, INC. 
Sample Identification 
5751 - Lab Pit #2 
5752 - Lab Pit #1 
P y r i d i n e , 
uc/kg 
<150 
<150 
100205 
'V.'C. INC. •222.Mcr,rc 
j.T-.cike • v.orrce, C; 
JT 06^65-'2231 261-0453 
YORK LABORATORIES DIVISJON 
W.'f^ 
CERTIFIED REPORT TRANSMITTAL 
REPORT NUMBER 
30850-14AA 
DATE. 
September 25, 1985 
CUENT 
Envirosciences, Inc. 
19 Copeland Road 
Denville, NJ 0783A 
AnENTION 
Dr. A. Kvles 
The above referenced report is enclosed. Copies of this report and supporting data 
will be retained in our files in the event they are required for future reference. 
If there are any questions concerning this report, please do not hesitaie to contact us. 
Any samples submitted to our Laboratory will be retained for a maximum of sixty (60) 
days from receipt of this report, unless other arrangements are desired. 
Naturally, as in the past, our staff will be pleased to quote on any future requirements 
you may have. In addition to the service provided, we also offer the following: 
Hazardous Waste Analyses 
Product Evcluation/R&D 
Water and Wastewater Analyses 
Air and Process Gas Analyses 
Industrial Hygiene Sun/eys 
Metallurgical Analyses 
Microbiological Analyses 
Mass Spectrometry Sen/ices 
Roberto. Bradley 
Vice President 
^V/C.. 
' 2C2 N'tCT-'cs 'w.T.ci-^3 • "'icrrcs. Ccrr.s-cTicui Ji—o'j • 
100206 
September 25, 1985 
30850-1444 
ENVIROSCIENCES, INC. 
19 Copeland Road 
Denville, New Jersey 
07834 
A-ttention: Dr. A. Kyles 
PURPOSE AND RESULTS 
Five (5) soil samples were submitted to York Laboratories for 
analysis. 
The samples were prepared and analyzed in accord-
ance with Procedures for Handling and Chemical Analysis of 
Sediment and Water Samples, EPA/CE-81-1. 
The results are reported in the following Tables. 
Prepared by: 
....j P' c x ^ 
Daniel F. Oct 
Laboratory Manager 
.^y.:i C - (yCc^^y,. 
^proved by; v^,^^/.-.. v_ - -.^c^v./., 
^fifrey* C. Curran 
:hemist 
CFO/JCC/md 
100207 
'^•VC. i.NC. • 222 i'vic.Tce "u.T'.CKa • Mcrrcs. CcrnecT;c'_t Zt~tZ • '^O;' 261-—ici 
TABLE 1 
30850-1444 
ENVIROSCIENCES, INC. 
Sample Identification 
Toluene, ug/kg 
ICC Berlex, 8/7/85 1:00 
360 
100208 
",VC. ;MC. • 222 Mcr.rce Turoike • -V.cr.rce, Ccr,nec:;cuT C i ^ i ; • i222-, 26V^c = 
TABLE 2 
30850-1444 
ENVIROSCIENCES, INC. 
Sample Identification 
Pyridine, ug/kg 
ICC Berlex - Lab Pit, 8/7/85 12:00 
2,700 
ICC Berlex - Lab Pit, 8/7/85 12:00 
<150 
100209 
'•''.VC. ' C. • 222 V'cr^'cs TL.'.'HC--'? •-'vicr'c^ O—~'^?CT;c'j.'Ci«c£ "'2221 Z-i-*—--53 
TABLE 3 
30850-1444 
ENVIROSCIENCES, INC. 
VOLATILE PRIORITY POLLUTANTS 
All results reported in ug/l. 
Sample Identification 
Compound 
chloromethane 
bromomethane 
vinyl chloride 
chloroethane 
methylene chloride 
trichlorofluoromethane 
acrolein 
acrylonitrile 
1,1-dichloroethene 
",1-dichloroethane 
trans-1,2-dichloroethene 
chloroform 
* ,2-dichloroethane 
"•4,1,1 -trichloroethane 
carbon tetrachloride 
bromodichloromethane 
2-chloroethylvinyl ether 
',2-dichloropropane 
trans-1,3-dichloropropene 
trichloroethylene 
benzene 
cis-1,2-dichloropropene 
c ibromochloromethane 
*,1,2-trichloroethane 
bromoform 
tetrachloroethylene 
', , 1 ,2-2-tetrachloroethane 
toluene 
chlorobenzene 
erhyl benzene 
ICC B e r l e x 
Lab 
P i t 
8 / 7 / 8 5 
3:00 
<10 
<10 
<10 
<10 
<10 
<10 
<100 
<100 
<10 
<10 
<10 
<10 
<1G 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
22 
<10 
<10 
ICC 
B e r l e x 
Lab 
P i t 
8 / 7 / 8 5 
3:00 
<10 
<10 
<10 
<10 
<10 
<10 
<100 
<100 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
21 
<10 
<10 
ICC 
B e r l e x 
Lab 
P i t 
8 / 7 / 8 5 3:00 
<10 
<10 
<10 
<10 
<10 
<10 
<100 
<100 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
<10 
360 
<10 
<10 
100210 
'.^VC..^JC.•222 Mc 
_rrc.'<s • 'V^cr'cs. Ccr.r.ectlcjT 26—63 • '222". 2i1-«i'i£r. 
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. f - o 
p f t M r : c p 
u s EPA ID Number 
27 
form Aop.evffl QMB ^o ^QCW 0404 dp.let 7 31 
22.^aj« 
' " ' o " " a i i o n in me snaoeo areas 
1$ n o i requireo t>y f o o e r a l 
L Stale Mantleil Oocumsnt 
Numoar 
CWMA 
J y 4 3 ^ 3 / 
M.State Ganeisioi's ID 
" 
N. Slate Trantponar't ID 
0 . Trarttooner'i. Phone 
P. State Trantponer't 10 
U.Trantponer't 
^ ' l o " ^ 7 1 P _ / l ' ? O C ' 5 / l O 
28 US DOT Description (Including Proper Shipping Nome. Haiard Class, a n d ID Numberi 
Profile Numtier y ^ L S ' 2 ) < ? / 6 £ ' Z J ~ ' ^ ^ 
29. Containers 
Type 
^ 
30 
Total 
Quantity 
J l . 
Unit 
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Watte No.' 
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CWM Profile Number 
CWM Profile Number 
CWM Profile Number 
h. 
CWM Profile Number 
CWM Profile Number 
S. A6C.;.cnal Descriotions for Materials LijtetJ Above 
fA<r. 
/<•<(- Vn-( ^ ' ^ F^-
Ttfr«grw>ri'— 
32. S: 
TZy. 7y^^^ 
'i^izy^jS:,^^^ 
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b. 
c. 
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t i y . _ , 
, 
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33. T r e n i c o n e r 
Acknovvfe<3gemenI of Receipt of Materials 
3^ 
Date 
Printe<:/Typ«d 
Nerne 
i^r7".r. u TiuubpuiL inc" 
-au:: 
- & ^ ^ U i 
Month Day Year 
1 t o l 1 ? ! « <
34. Tf»ns;>onef " ^ 
AgknowleOgement or Receipt o< Meionals 
Printei3/Typ*d Name 
/-> 
/ 
/ 
Simiature 
' j ^ ^ 
Date 
Month Day Year 
35. Oiacfeoancy Irxlicstion Space 
rx%^ 
100221 
nAZ.A.iUUU5VVASTL IVlAN!^tb! 
^ ^ 
(As Required By The Alabama Department of Environmental Management) 
^l«4k« print or rvp* 
f f o r m designed for use on ehie 117-pitch) lype^^rner } 
f o r m Approvet) OMB f^o iOOO-OaOa t i o i r t i 7 31 86 
UNIFORM 
HAZARDOUS 
WASTE MANIFEST 
M a n i i a i t 
1. Oenoiaior s US fcPA 10 So 
/ • / ' ^ • 9'ff' c<^ • / , I a.9 ir]j^°tWi>'*-l. 
2. Page 1 
of X 
intormaiion in tne snaoeP 
areas 
I t n o t r e q u i r e d b y F e o e r a i 
law 
~3. 
{jeneraior s .Sarr^e ano Mamng Aooia&s 
ZZZsiS*J.C ^r/CyJfC^^ Cf^i^Ol^t^ 
4, 
Generators Phone ( Z d / ) ^ f d ^ ^ ^ O O 
T r a i l e r 
Number 
RTMZ 251880 
A Stata Manitast Oocumani 
Numoar 
.-CWMA-.. 243031 
S. S u i a 
{janaraior a 10 
. . ' . " • • ' ' . • • • 
. - 
• . -
Iransponer 1 Comoany 
Name 
6. 
US EPA 10 Numoar 
C S u i a ..Tranapooar a IO 
0 . Tranaponar'a 
f t K m a 
/ . 
i r a n t p o n a r ^ Company 
Nama 
y. 
Uesignaiaa 
Facility Nama anC \stl9 A d O r a u ~ ~ 
C H E M I C A L W A S T E M A N A G E M E N T , I N C . 
E m e l l e F a c j i i t y 
A l a o a m a H i T i m a y 17 at Mile M a r k e r 1 6 3 
Emelle. A l a b a m a 3 5 4 5 9 
T 
USiPfi 10 Numoar 
E. SiBia Tranaponat > IO 
J^^li£lfj£i£_lf_!.li*i£I2-l£. 
f. Tranaportar'a 
Phona 
ia 
u s EPA 10 Number 
C S i a i a 
Faciiitya 10 
) A | L| D| 0| 0 , 0 , 6 ) 2 , 2 | 4 ) 6 | 4 
H. Faciiny'a 
Piyjna 
205/652-9721 
1 1 . u s OOT 0«scription (Including Proper Shipping N%m». H a t a r d Clata. antI ID N u n ^ a r l 
12. Coniainars 
No. 
I Type 
13. 
Total 
Quantity 
14. 
Unit I 
W t / V o l 
'• 
\ . • • 
Wane No. 
»• yysZr^yyrZco^ ^-^ycjy/i, yyi^u/y^ yycs^Toccriyyrz:. ^yZry</^t^/^ 
CWM Profile Number /<?i>?.2J 
V S 6 d 2 . . M L / ^ I I I I 
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^ / C r ^ ~ ^ 
y-ryJ 9 y y 9 
CWM Prodlc Number/^^^ t / / 4 ^ 4 ^ 
1 Ij mm I I I I 
t 
C W M Profile N u m b e r 
A<lailional 
^^escnptiora for M s t e n a l i 
Listed Above 
^ 
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K. Hendling Cooes for Wastes Ljsiea Above 
<y&] 
.OS I 
15. Special nervciing 
Instructions and Additional 
Inlormaiion 
D. dpeciai narvcnno 
instructions ano Aociiionai 
i r i o r m a n o n 
^ 
/ g- y 
^ 
//c. i ^ Z y . / , y y d ^ z t ^ K ^ 2 Z u < ^ . y/uy/^y^. ^ ^ . . ^ ^ y ^ y ^ r y r ^ . y ^ ^ , ^ ^ ^ 
1 6. G E N E R A T O R ' S C E R T I F I C A T I O N : I nereoy ceciare inai tne contents of mis consignment are fully ana accurately oescriPeO above by 
proper srtipping name aT\t are classified, packed, marked, and labeled, and ara m all respects in proper condition for transport by highway 
iccordir>g t o applicable international and national government regulations. 
Unless I a m a small quantity generator w h o has been exempted by statute or regulation Irom the duty to make a wasie m i m m u a i i o n 
cemfication 
under Stc-.ion 3002(bl of RCRA. I also cenify that I have a program m place to reduce the volume and toxicity of waste generated to the degree I 
have d e t e r m i n e d to be economically practicable and I have selected the method of treatment, storage, or disposal curreritiy available to me which 
m:nimi2es t ^ e present ana futur'e threat to h u m a n health and the environment 
P t i m a c / T y r ^ 
Name 
•.t'tft^^ Name 
y i - i ^ y. yZy/yt 
" ^ ^ ^ z ^ f f ^ 
M o n t h 
Day Yaar 
\ / yP\/ C \ 0 t S ' ' 
T 
17.Transponar 1 Acknowieogement of Receipt of Materials 
R 
_ frifited<;Tvae<: 
N j m e 
0 N e a l e s Trai 
Tt 
.ransport Inc 
Signature 
(L- m /Q^ 
M o n t h 
Day Year 
' 1! nl 17 ^ "s 
IS.Trensponer 2 Acj^nowleogement of Receipt of Materials 
rr;*Med/Typ«< 
Name 
y / 
/^ocyiy 
yytyyy^yy 
S i g n ^ u r * 
/^'yyyrdoc. 
yzyy / y y ] 
/ I 
L ' 
M o n t h 
Day Year 
1 /-:^x^i^s 
13.Discrepancy indication Space 
/ 
^ /^y5 
100222 
S.Facility O w r * r or Operator: Certification of receipt of haiaroous materials coverail by this maii<lest e i c e ^ as noted in Item 19 
:rei!l 
PTimoQ/Typ«c 
Name 
Signature 
Jti:=. 
M o n t h 
Day Year 
A i2^gi3i?<5'i 
iPAPtKH, 8700-22 ,'flev. 4-86) Previous edition ..Obsolete. 
STATE OF ALABAMA ( M u ^ Accompony Shipment) 
J / U ^ J I ^ Q 
u 
. 
I F n r m aesipneo f p r m e pr- H . t t (12 o . t c M t y r e w t i t e r I 
^ " * ' • > " " ' ^ ^ - ^ ^ 
— 
^ 
2 1 . ! . e n c , a . o . 
s U S e P A l b N O 
" D M FORM HAZARDOUS 
^ 
WASTE M A N I F ^ ^ . 
(Continuatioc^rte^l! 
M a n l i e s t 
• D o c u m e n t N o 
y r /) 9 ffo 6 s^/to <ps\ 
r o r m Aoo'n»»0 O M B No rO>J 0 4 0 * E»D"e» 7 3 
I S . ^ a g e 
i n l o r m a i i o n i n t h e s n a o e o aree 
is 
n o i r e o u i r e d 
Oy 
F e o e r ^ 
l a w 
Zc/z, 
2 3 G e n e r a t o r ' s N o m a 
T r a i l e r Ntx-nber 
RTMZ 251880 
5 4 T r a n t p o n a r 
C o m p a n y 
N a m e 
- ; p - m ? ^ W » « « r / 
J ' p m p a n y 
N a m e 
r-'-r^f:^, o/\Mr:rB 
25^; 
u s E P A ID N u m b e r 
yycfiZ? g c S O J 9 9 7 
2 7 . 
u s E P A ID N u m o e r 
L. S t a t e 
M a n i f e s t 
O o c u m e n i 
N u m o a r 
- CWMA 
Jy4'^<^s/ 
M . S l a t e 
G a n e r a i o r £ ID 
\ . S t a t e 
T r a n t p o n a r ' t 
ID 
0 . T r a n t p o n a r ' t . 
P h o n a 
P. S t a t e 
T r a n t p o n a r ' t 
ID 
U . T r a n t p o n e r ' t 
P ^ o n a T T 
p _ £ | ' 2 0 C 9 / i C 
2 8 U S D O T D e s c r i p t i o n ( I n c l u d i n g P r o p e r S h i p p i n g N a m e . H a i e r d Class, a n d I D N u m b e r ) 
2 9 . C o n t a i n e r s 
P r o f i l e N u m b e r / J C c ^ A ^ < f / S ^ i 
0 / C y ^ - ^ ^ ^ J V ^ J [ Z y S 
^ 
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. . . C W M p r o f i l e N u m t s e i y ^ ^ y ) 
9 ^ 6 0 9 — 
3 0 
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O u a n i i i y 
3 1 
U n i t 
U M A W 
R. 
• -
W a t t e No.-
• y - i - f . . 
C W M Profile Numtaer 
C W M P r o f i l e N u m t i e r 
, , V : . 
~ZZZ:J':. 
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h. 
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C W M P r o f i l e N u m t j e r 
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. 
• . ' . ' - • ^ - « ' -
S . 
A d c j i t i o n a l D e s c r i p t i o n s for Materials Listed A b o v e 
-//a,*^ / y* 
f ^ ' ^ f t i C C 
) T . H e n d l i n g Codes f o r Wastes Listed A b o v e . 
a . 
d . 
. - B - 
-'—•"• 
i ^ ^ - t - ^ - y i - j i ^ 
< ^ - ^ j ^ y / 
r Z y ^ / j i E y -
e. 
h;..'. 
3 2 . S o f c c e — r t a n d l i n g I n s t r u c t i o n s a n d A e a i t i o " B i 
' - ^ y r - ^ a f n n 
AJf^Hdr^ 
\ ^ ' ' r i ^ ^ ( / L ^ . ^yj^^-y^^^^yu^Zi^y^ -'/yyz>y-yyp^y2A.c^y4' 
^y^J^o^yyi^-Mty d?^ y^y<^ . yZyLZatr^>*'^^/^ 
3 3 . T r e n a o o n e r 
A c k n o w l e d g e m e n t 
of Receipt of 
M a t e r i a l s 
Date 
P r i n t n i / T y p o d 
N a m e 
p^o—: . ^ l "" ..ii.'.nnr! inr" 
S i g n a t u r e 
i g n a t u r e i 
gry: 
m -A^^A. 
M o n i h D a y 
Yeer 
I, 
A I I 7|R = 
fi 
3 4 . T r a n t p o n e r ' ^ 
A e f c n o w l e < ^ e m e n t 
or Receipt of 
M a t e r i a l s 
I . 
^''^ 
T / ^ y T ^ E)oAo<j..i-^l^\m':^yZEm 
M o n t h D a y 
Year 
0-1 ^ If/" 
3 5 . D i a c r e - p a n c Y I n d i c a t i o n S p a c e 
rxTT-
100223 
^ ^ ^ / 
(As Required By The Alabama Department of Environmental Management) 
f-ieasa print or tvp« 
(Form designed for usa on elite 112-pitchl typemrriier.) 
<i" 
U N I F O R M HAZARDOUS 
W A S T E MANIFEST 
f o r m Approved OMB No 20O0-0tO4 Ctpires 7 31-86 
1. Generator s US EPA 10 No. 
Maniiest 
t^i / 1^ I ^ i f l o i g if^ ^ 1^1 P I T I /^°&V''h'*^ 
oeneratc-' s Name and Mailing 
Aodress 
JZZrce-'t* C/^i/v^cBc coy>t,^A/c/ 
£>co y ^ y ^ ^ y r r ^ ^ " ^ ^ 
e7a-x> 
4. 
Generator t 
Phone ( ^ O / 
) 6 9 d - ^ / O O 
6, 
Iranspor-.t--"! 
Company 
Name 
7 y ^ S * t U / S Q X f - . 
g ' ^ C / g . . . 
/ . 
iranspor-.6/ 2 Company 
Name 
T7fS/c^/i. /(»7/«/*/</e' rAa*iyyo^rjjwf~ 
T r a i l e r Number 
TMTZ 680365 
u s EPA 10 Number 
\P\i&\Z>\9\9\o\i,\^\<i.\S'\79 
8. 
US EPA ID Numper 
| / > ^ | 2 > | ^ | g 1^71 gig \<i.\S'\7\9 
2. Page ) 
of Z . 
(niormaiion m (n« snaoec 
i r t a 
IS n o t 
r e g u > r « d 
b y 
F e d e r a l 
law 
A. Siaia 
Manifest 
Document 
Numoer 
CWMA 
243032 
8. Stata Ganaraior's ID 
C. State T r a n t p o n e r ' t 10 
0 . Transponar t 
Phone 
£. State Trantponet t 10 
F. Transponer's 
Phone < - / / ( / . ' / I C - \ — i U U 
9. 
b a s i g r u i e c 
Faciiiry Name and Site 
Address 
C H E M I C A L W A S T E M A N A G E M E N T . I N C . 
E m e l l e 
F a n l i t y 
A l a b a m a —:ighv«ay 17 at Mile M a r k e r 1 6 3 
Ernelle, A ataama 3 5 4 5 9 
10. 
US EPA 10 Numoer 
G. State Facility t ID 
, A , L| D, 0| 0 | 0 | 6 | 2 | 
2 | 4 | 6 | 
H. FaciliTy's 
Phone 
205/652-9721 
1 1 . u s DOT Description (Including Proper Shipping Name. H a i a r d Class, a n d ID Number I 
yyS-&yj/Z/)CcyJ ur9/rz, Z/po/y) yycs(7hcr/e»i y ^ ^ z i ^ 
12. Comamers 
No. 
Type 
13. 
Total 
Quantity 
14. 
Unit 
Wt/Vo 
I. 
Waste No. 
- T -
^/€^'<r y//?9y/9 
C W M Profile Utitntset y ^ y ^ ^ 
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I ^ y : 
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d . 
C W M Profile N u m b e r 
I 
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I 
I I I 
Aoainor.£. 
Descriptions tor Matenals 
Listed Above 
~ 
/ r i : , . y * a ^ rya*<y / o y -yU/Zejxc e^ruyi ^^^^^c^^* 
/ / 6 ' y^^M-erj^^^lZy ^ o ' y tTyi^o^acti^, yi,cu^A<Zy^ r^^^^Tf^^.^ 
y / c ' yU4^»ia,3 C r v T ! ^ yaoK^tey y^/<^«».<*^r^/'«<nny e v / / ^ ^ ^ 
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I n c T r • ir-v m n r 
s n M 
a r t H i ? m r \ a l 
I r A A r m 9 * • A n 
* 
K. Handling Codes for Wastes Listed Above 
,.De< 
d. 
IS. 
Special 
—.andiing 
Instructions and Additional 
Irtormation 
/ / a . ^k<«*«:<t uyZcij .yyu^<m> Tio/LcjiZ/yuiCy «5<*/^><s«i*i-''^>r»«<L.^lZt^ y ^ Cuyy9fy9 
15. G E N E R A T O R ' S CERTIFICATION: I nereoy declare mat tne contents ot tnis consignment are tully ano accurately described apove by 
proper s.-:sping name ano are classified, packed, marked, and lat)€led. and are in all respects in proper condition for t r a n s p o n by hignway 
a c c o r d i r ^ t o applicable international artd national government regulations. 
Unless : a m a small quantity generator w h o has been exempted by statute or regulation from ihe duty to make a waste minimization 
cenificetion 
under S e c t i o n 3002(b) of RCRA. I also cenify lhat I have a program in place to reduce the volume and toxicity of waste generated to the degree I 
hava c e t e r m i n e d to be economically practicable and I have selected the method of treatment, 
storage, or disposal currently available to me »*hich 
m i n i m c » 3 i n e present and future threat to human health and the environment 
7 
Pnniefl. . v p e d 
Name 
y^-oiAy y yyyyid 
Signatun Z ^ ; ^ ' ^ 
Month 
Day 
Year 
\ / r ? \ / \ y y . S ' 
T 
17.Tr»nspc.—sr 
1 Acknowieogement of Receipt of Materials 
R 
A 
N 
S 
V 
Priniec, " vpsd Name 
~ 
Oneale s Transport Inc 
Norton 1 . M. Burt 
Signature 
i 
•y^ e . - m 
-A..^lr . ^ • 
Month 
Day 
Year 
18.Tr»nsoc-^»r 
2 Acknowledgemen;^ of Receipt of Materials 
Pri;>»ec. ~ vped 
Name 
7 
y 
tjnaxtuy , 
/ 
. 
^ 
Month 
Day 
Year 
zy ^ys 
19.0iScrec.a''.CY Indication Space 
/ 
P ^ 2 0 . F a C i l i t y 
Crwner or Operator; Cenrfication of receipt of hazardous materials ca'vered by tlyiymaTtifa^t except as noted in Item 19. 
^ 
Nam* 
I f 
.'. 
J Z- / 
• 
Prinie<i. 
fT>ed 
N a n i e ^ 
^ClS-
Signatijre 
Month 
Day 
Yeer 
E P A F o r m e 7 0 C ^ 2 i (Rev. 4 - 8 5 ) Previous edition is obsolete. 
S T A T E 
D P A l A R A ^ / . A /
M
. • c + ^ A . r - r o m r ^ n n v 
. « ; h i t D m e n t ) 
i . ^ 
^
, 
^ 
100224 
Pi»»»« pr.ot or NT» 
(Form designed for use on elite ( i S o n c n ) tvpewr.ter I 
UNIFORM HAZARDOUS 
WASTE MANIFEST 
(Continuation Sheet) 
2 1. Generator s US c ?A iD No" 
Mannest 
• Document No 
y r /) 9 / 0 ^ s-y a 9 s \ X C Q o S 
f p i n Aoofo»ea 0>^a No 7000 0404 E.D.rrs : 31 86 
« 
23.Generator s Name 
.Z2x.P^^ (Z^^ry'tisc Ca^^-vy 
T r a i l e r Number 
Sots /^y>^'^''rtu> ^dS£ 
gyc7o 
"^^^ 680365 
24. Transporter Q C o m p a n y 
Natrta 
/?5/i/£~C/if 
yy/irraA/M/fO,*, 
26. T>aneaeRei '\ 
Compgny 
Narrsw, 
25. 
US EPAIO Numoer 
27. 
US EPA ID Numoer 
fsTage 
iniof rr^aiion .n tne snaoeo a.eas 
IS not 
required 
by 
Federal 
law 
L. State Manifest 
Document 
Number 
CWMA y ^ S D e / 
U.Slate Generators lO 
N. State Transponar s ID 
0. Trantportat t 
Pf>on6 
P. Stata Ttaniporter $ lO 
28. US DOT Description (Including Proper Shipping Name. Haiard Class, a n d ID Number, 
« 
^^y^fe/pi(>£M f//:iry;r. yypc//y] yyay/7oc:/a^^^j^m^^jmj^) 
CWM Profile Number y^zzT^-^^AA 
29. Coma 
No. 
Type 
U . T r a n t p o n a t t 
Phone:;; j 
^ ^ _ / j ^ q _ p ^ ^ 7 7 j t T 
inert I 
3 0 
| 3 1 . 1 
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f ^ / ^ ^
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CW\B Pfefill> • ' i i m h ( l f ^ < 7 f ^ V ? ^ ^ < g ^ ^ f ^ ^ . 
/ 
CWM Pro file Number 
/./\^/f 
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CWM Profile Number 
% 
CWM Profile Number 
CWM Profile Number 
CWM Profile Number 
/VA 
d/y 
vyf^ 
Total 
Quantity 
Unit 
R. 
Waste No. 
CWM Profile Number 
. Addmona. DesCTiptionsVor Materials Listed Above 
^ p 
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^ ^ ^ . . ^ ^ ^ ^ ^ ^ - . ^ ^ ^ t / j e K / ^ ^ s Z i Z ^ < ^ ^^'uJJeZ yuy0t^iy/yiya/,iy-\~ c 
T. Handling Codes for Wastes Listed A b o « 
a. 
d. 
g. 
e. 
h. 
f. 
i. 
onai Information 
32. Special Hjja^nnqlnstr 
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V 
33. Tran&c>on»r 
Acknowieogement 
of Receipi of 
Materials 
Date 
PTy\te<3.fIyp»d_ Name 
•& i . C u ^ l . 
G 
...L'di' 
ar: sport—me 
crzcr. C^M—Bur: 
Signatura 
j f 
Month Day 
Year 
r > , 
(
\ 
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I 
Date 
34. Trantpor.ar 
< Acknowledgement 
or Receipt of 
Materials 
P r i p » K l / T r p « d Name 
/ - \ 
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I Siigniiiure 
f l 
\ 
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DiaCrapartcY Indication Spaca 
S 
Month Day. 
Yeeu 
100225 
£ ? A F o r m 8 7 0 C - 2 2 A (3-84) 
STATE OF ALABAMA (Must Accomoanv Shioment) 
HAZAHDOiiS-WASYb MANIFEST 
(As Required By The Alabama Department of Environmental Management) 
l-lea^e onnt or tvo« 
iform designed for use on elite 112-piichl lypei^riter t 
f o r m A o p r o t e d O M B No 20CX) 0 * 3 4 e.p.tes 7-31 Sf 
# 
U N I F O R M HAZARDOUS 
W A S T E MANIFEST 
J. 
vjaneraicr s Nam« and •'•tauino Aooress 
XZrcs^'U C/<^£/»'COt, co/rsf^ti/r/ 
4. 
Ganaraior's Phone ( • S ^ / 
I ^ ^ ^ 
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b. 
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1. Ganaraior s US EPA 10 No. 
Mannest 
.Pocpr^j^n\ No 
i . Page ) 
of Z . 
inlormaiion m tne snaoeo areas 
IS not 
reouireo by Feoeral 
law 
Trailer Nunber 
TMTZ 680365 
7 ' ^ 5 4 J U ^<g>€(r- 
T T y y c . 
us EPA 10 NumtHir 
/. 
iransponer 2 Company Nama 
\P\£'l>^?' e\ gig I ^'ti.\£'\7'9 
A StBle Manileet Documani Number 
CWMA_243032 
6. State Car\araior'i lO 
C Slaia Transpoaar t ID 
0. Trantponer't Phona 
US EPA 10 Numoer 
rx-fftrcxA./»7/«>g/vc r«s*trye>jtr^jwe.' 
\P'^\Z)i9i0\O\^><f-s^^^\7\9 
•?! 
uiastgnatcj raciliiy Name ar<d Siie Address 
C H E M I C A L WASTE MANAGEMENT. INC. 
Emelle Facility 
Alabama Highway 17 at Mile Marker 163 
Emelle. Aabama 35459 
to. 
US EPA 10 Numoer 
1 A, L, D) 0, 0, 01 6 I 2 I 2| 4 I 6 1 4 
E. State Traruponer't 10 
F. Transponar I Pnona 
G. Stata Faaliryt 10 ^CAE'Lt^ZA-fqUX 
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H. Feciliry't Pnona 
205/652-9721 
11. u s OOT Description (Including Proper Shipping Name. Haiartl Class, end ID Number) 
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12. Conumars 
No. 
I Type 
. 13. 
Total 
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14. 
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Aaiitittrja. Deacriptions ior Materials Ijsied Apova 
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iructipns and AodHional Ir^orma 
K. Handling Codes for Wastes Listed Above 
! b.D0( 
^D3l Z 
d. 
15. Special r\andiing 
instructipns and Acdilional inoTmatton 
/ / a . Si^u**vcd. t4.AZz^ ,^<^uvc. yv yx.yyriny^ ^-^^y/..^yy^y^.. 
MJCA 
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16. GENERATOR'S CERTIFICATION: I hereby declare tnai tne contents o< this consignment are luiiy and accurately oescnbec aoove by 
proper sr.^ping name eno ar© classified, packed, marhec. ond labeled, and are m all respects in proper condition for transpon oy highway 
according :o applicable international and national government regulations. 
Unless I am a small quantity generator who has been exempted by statute or regulation from the duty to make a waste minimization cenification 
under Section 3002(b) of RCRA. 1 also certify that 1 have a program m piace to reduce the volume and toxicity of waste generated tp the degree I 
hava determined to be economically practicable and I have selected the method ol treatment, storage, or disposal currently available to me which 
mmimces tne present and future threat to human health ar\C tne environment 
PrimecyTyped Name 
y ^ ' P / y y / y y y £ i / 
Signatur 
^ ^ ^ ^ ^ c y ^ ; ^ ^ 
Month 
Day 
Year 
\ / i ? \ / y \ / r \ 
T 
17.Transoor-.e- 1 Acknowledgement of Receipt ol Materials 
R 
A 
N s 
A..d- i 
I 
T 
PrinteoTypjd Name 
.T 
O n e a l e s T r a n s o o r t I n c 
Norton C. M. Biirt 
Signaiuf« i 
Month 
Day 
Year 
h i n h i7ifi 'Si 
' 6.Tf»ns3or:«r 2 Acknowiedgemeoj^ ol Receioi ot Materials 
Ptipt^c^^.rz^a Name 
/ / 
M o n t h 
Day 
Year 
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/ / 
^
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20.FaciliT;r Crwmer or Operator: Certification of receipt of hazardous materials covered by iiyi/manilust excepi at noieo in Item 19. 
10022G 
Prin^a/T I'ped Name_ 
Month 
Day 
Year 
l / i Z j ^ ? i r : 3 " 
-..EPA Form 870C-22 (Rev. 4-86) Previous edition 1. Obsolete. 
< ; T A T P 
D ^ 
A l A R A \ / . A / ^ / r . c t ^ A r - ^ n m n n n v 
< ; h i n m e n t ) 
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U N I F O R M H A Z A R D O U S 
W A S T E M A N I F E S T 
fCor-:inuation Sheet) 
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I CTanTToIi 
d
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foi*!. Hooio.re OMB No 70OO Oarn E . O . ' H ' 3' 86 
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24. Tranaponer ^ C o m p a n y 
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^rtrnpary 
Namn 
26. T'»a»>f>onei 
25. 
US EPA ID Number 
X^i. z> 9 9 o 8 o 3 'Y'7 7 
•^AtinrR-
27. 
US EPA ID Numoer 
28. US DOT Deacription (Including Proper Shipping Name. Haiard Class, and ID Numberi 
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CWMProtileNum^T'T^^Z^igry^^-tJ 
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Intoir^aiion in ine shaoed areas 
IS not required by Foderai 
law 
C. State Manifest Oocuyn^nt 
Numoer 
CWMA 
M.Slate Generator's ID 
N. Slate Transponar s ID 
0. Trantponar't 
Pttone 
P. State Transponer's ID 
U. Transponar 1 Phone'2' 
29. Containers 
No 
I Type 
30. 
Total 
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CWM Profile Number 
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CWM Profile Number 
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CWM Profile Numt>er 
CWM Profile Number 
S. Additional DeicripttonsJor Materials Listed Above 
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T. Handling Codes for Wastes Listed Above 
a. 
d. 
g. 
b. 
e. 
h. 
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33. Tranaponer 
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Name 
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o,...-»• 
Signaiura 
^{yyit 
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Year I 
34. Tran»t>on»r 
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Prip««d/Trp*d 
Name 
/ - ~ \ 
' 
Z) 
I signjlture 
t ] \ 
<Zy / ] 
Date 
Dia£r»p«rwc-< Irtdicaiion Spaca 
^i 
Month Day., 
f t / i — 
100227 
?A Form 8700-22A (3-84) 
STATE OF A L A B A M A 
(Must Accomoanv Shioment) 
t-Xat 
- ^ 
HAZA,^UUUS WAS TL MAf^lFEbT 
(As Required By The Alabaina Department of Environmental Management) 
(Porrri aesignaa Por usa on ahta 112 pitch) typewriter ) 
^ 
f o r m A p p r o v a l OMB No 2 0 O 0 0 4 0 4 
e i p t r e i 7 31 86 
# 
UNIFORM HAZARDOUS 
V»'ASTE MANIFEST 
1. Generator s uS EPA 10 No 
Manirest 
u«n*.-a'.^' s .Name ana Mamng 
Aooress 
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T r a i l e r 
Number 
RTMZ;274676 
A Siaie Mannest Oocumam 
Numoar 
CWMA 
243033 
B. State Ganaraior's 10 
6. 
US EPA 10 Number 
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6 
US EPA ID Numper 
y. 
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hacitiiv 
Name and Site 
Aooress 
C H E . V l C A L W A S T E M A N A G E M E N T . I N C . 
E m e l l e 
- a c i l i t y 
Alaaarr-a H i ^ w a y 
17 at Mile M a r k e r 163 
ErT>e:!e. A . ' a b a m a 3 5 4 5 9 
10. 
US EPA 10 Numoer 
A , L| 
D, 0, 0 , 0 | 6 , 2 I 2] 4 | 
6 ) 4 
C Stata Tranaponer s 10 
O. Transponar'* 
Ptvina 
E. Slate Transooner s ID 
P. Transponer's 
Phone 
G. State FaciliTy's 10 
H, Pacilitv s Phona 
.205/652-9721 
1 1 . u s DOT Description /Including Proper Shipping Name. Hatard Class, and ID Number/ 
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12. Containers 
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13. 
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Descriptions 
lor 
Materials 
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K. Handling Cooes for Wastes Listed APove 
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15. Spec-^* 
—andiing 
instruciions 
and Aaainonai 
iriormaiion 
y/<^€'/^.yZ7:Zki 
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• ^ i . G E N ^ f i A ' T O R ' S C E R T I F I C A T I O N ; 1 hereDy oeciare xtsax the coniems oi inis consignmeni are :uiiy ano accurately oescnbeo at>ove by 
proper v*-c3ping name and ere clBSSifi«d, packed, marked, and labeted. and are m ad respects in proper condition lor transpon by highway 
• c c o r f i i r ^ to applicable international and national government regulations. 
Unless ' «rn a small guaniiry generatof 
who has been exempied by siaiuie or regulation from the duty lo make a waste m m i m i r a i i o n 
ceriiflcation 
unoer S e r t i o n 3002ib) o* RCSA. 1 also certify that I have a program rn place to reduce the volume and toxicity of waste generated to the degree i 
have Ce'.e—Ttinod to be economically practicable and I have selected the method ol treatment, storage, or disposal currently available to me 
whicn 
mrnimi2«^ r*ie present and future threat to human health and the environment. 
!l 
7 
Primec. 't-yan Name 
ycoAy y. /z/itT 
Signature 
'^a^^y^^k^r^ 
M o n t h 
Day 
Year 
\/yr>\yi\Q\F.r' 
T 
1 T.Transpcr-.e* 
1 Acttnov^iedgement 
of 
Receipt of 
Materials 
Prmtec.'~«ped 
Name 
O ' N e a l e 
s T r a n s o o r t 
I n c 
Nortcr. C .M. Burt 
Signature 
i 2 
itm 
A 
nicyvlcZ\ 
rl.. m. /Z}y>u yH. 
M o n t h 
Day 
Year 
I I ' O I I 
I 7 I 8 ' 5 
16.Transpor-.e- 
2 Acknowieogement 
of Receipt of 
Materieis 
ignaiuiE-^' f 
, 
y 
y 
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M o n t h 
Day 
Yeer 
Printec/"" *^«K3 
Name 
l^y . ^~^tra narrie 
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1S.Di»cfeo*.-«cv Indication Space 
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1 0 0 2 2 8 
X 
zD^Faeility C^wner 
or Operator: Cenification ol receipt of riazaroous materials coveced by this manifest enoepi as noted m item 
19 
PrimeOy/ 'vw^l 
Nama 
//:yyAey? 
/yE?7^c^ 
Sionature 
M o n t h 
Day 
Year 
i/i'2r^>.3iS'^ 
PA Fcrm 8700-22 (Rev. 4-86) Previous edition is opsoi.te. 
S T A T E 
O F A L A B A M A 
( A \ u S t A c C O m ^ O n y 
S h i p m e n t ) 
/ ^ / 
. y / ^ 
or rvTie 
(Porm designed for me on ene 11? oitcri) typewriter > 
21.Ciuner3lor t uS c r A iD ,Mo. 
UNIFORM HAZARDOUS 
WASTE MANIFEST 
'Continuation Sheet) 
Manifest 
Document No 
y / ^ 9 0 o 4 s- / o 9 s^Z'yoCi / 
r o " " 
»DD'0.ea O M 8 No JOOO 0«O« E ' D . ' H 7 3t 8 f 
;:.?a9e 
Z ' / Z 
iniorrnation in tne snadec areas 
1$ not required by f e d e r a l 
law 
23 Qtr>tti\ot \ Name 
. 
JTy^.o^Mi <Z^yyfy<!at. Ct^frf/>a<// 
Trailer Number 
S a o jC^/tey^/icO ^rOLD 
o'7tx7o 
RTMZ; 274676 
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L State 
Manifest Document 
Numt)er 
M. State Ganaraior'» ID 
' 
24. T r a n a p o r t e r ^ Company 
Heme 
26. Tranaponer i^ Comruuiy 
Name 
25. 
US EPA ID Number 
\r^r. a 9 0 t9 ff a 3 9 7 7 
N. State Transporters ID 
0. Transoonar't 
Phone 
/ 
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27. 
US EPA ID Number 
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p. State Transponar « ID 
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2S. US DOT Oescriplion (Including Proper Shipping Name. Haiard Class, end ID Numberi 
sPyy>i>-r^ , / l K ^ 9 y / f omivunitNumot, ^<^.^i<g^;,gBJ: 
/ y \ / > / f 
29. Containers 
No 
Type 
3D. 
Total 
'j}q-a59-62i!9 
Quantity 
WiytJci 
Unit 
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Waste No. 
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^us^<L fyU^£Ar€j~Al 
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CWM P'ofile Numoer 
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CWM Pro file Number 
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'yyi-yyp''-
CWrul Profile Number 
# 
CWM Profile Number 
CWM Profile Number 
CWM Profile Number 
CWM Profile Numoer 
S. Additiorvai Descriptions for Materials Listed Above 
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j T. Handling Codes for Wasters Listed Above 
{ 
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g. 
b. 
e. 
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c. 
f. 
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32. Soe^.j IlJ JJliiiy instructions and Additional Information 
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T 
33. Transponar 
Acknowledgement of Receipt of Materials 
Dale 
Signature \ 
^ 
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^^Tyzyz^/^^zm. JLJA^y^. 
^ ^ ^ n ^ r ^ 
tfajna 
—--- ^ ' 
nspn. -r T ac 
34. T r a n a p o n e r ^ 
Acknowledflement or Receipt of Materials 
l/Trt>^ 
Narne 
Month Day 
Year 
.\\ 
Q!I 7[R S 
T 
P^ftnad/Trffha 
Name ^ — 
, 
'•^y/rrht j / y / /C laucZ= 
'"t^/r.,,..///^ y ^ y ' 
Date 
Month Day 
Year 
- Diacrepar>CY Indication Spaca 
100229 
PA F o r m 8 7 0 0 - 2 2 A 
(3-84) 
C ; T A T F n p A l ARAA.AA 
^ M . i e t 
Ar-i-r^r 
cu:. 
.1. 
hAZA::UUUS"WAbii: 
>^ y-u y-^ 
^bbi 
l e print or tVD* 
' (As Required By The Alabama Department of Environmental Management) 
(Forrritletigned tor u s e o n e l i t e l H - p i i e h l i y p e r r r i i e r I 
f o r m Approved OMB No 30O0 0 a 0 4 Eioires 7 31 SB 
F 
U N I F O R M HAZARDOUS 
W A S T E MANIFEST 
J . 
u e n a r a t o r s Name ano Mamnq 
Aooress 
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£cyn/yy^ yyecy ^Ti/Uiy 
4 
G e n a r a t w s Phone ( ^ O / 
) 
£ 9 « -
a. 
I r a n s p c ' . e r 1 Company 
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(/| /'•/> I f i^.g 1^ .s-^r ,g If >r ^ ^ ^ f g ^ y / 
O^t^TIO 
^yoo 
T r a i l e r Number 
RTMZ;274676 
o '/%y^^£4T rK.utJCfi/C' ^ r m / u ^ 
I Name 
6. 
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8. 
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/ . 
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Company 
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T 
U e s i g n a i s o 
Facility Nama ano Sua Address 
10. 
US EPA ID Numoer 
C H E M I C A L W A S T E M A N A G E M E N T . I N C . 
E m e l l e 
F a c i l i t y 
A l a b a m a r-iighway 17 at Mile Marker 163 
Errielle. A l a b a m a 3 5 4 5 9 
[ A , L| D| 0 | 0 | Oj 6 | 2 I 2 | 4 | 
6 | 4 
2. Page I 
ol 
^ 
I n l o r m a i i o n m tne snaoeo 
areas 
IS n o t r e Q u i r a d by F e d e r a l 
taw 
A Stale Manifest 
D o c u m o n i 
Numper 
CWMA 
243033 
B. State Gertarator's ID 
C. State Transporter's ID 
0 . Transporter's 
Pnone 
E. S u i e 
Tratuponer's 10 
F. Transponer s Phone 
(j. Sieta Facility's ID 
M. Faeilriy's 
Pttona 
205/652-9721 
1 1 . u s DOT Description (Including Proper Shipping Name, H a i a r d Class, a n d ID Numbarl 
12. Containers 
No. I Type 
13. 
Total 
Quantiry 
14. 
Unit 
W t / V o 
1. 
Waste No. 
/ / ^ z yS'yeJXfe/j c*^r9sr£ J'ocyz> yiy£?s (7h<-^^''y^ f y c e r ^ ^ e ) 
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A o t u t i o r . ^ 
Descriptions 
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.^arerials Usted Above 
/ / i t . , y^ss M&d] / o ' / . Tocy/ytida ef^y/fciZASvij 
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A-*^^ T^oyr / o Y 7cU/t*tc. Ottyy. Cyr^fiTfrvfiyi 
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K. Handling Codes for Wastes Listed Atxive 
a.i/Bi 
c D B l 
bPsA • 
d. 
I s . Special 
—.anoling Instruaions and Adcitionai 
Information 
y i / < ^ £ ' y j Z / y k i 
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16. G E N E R A T O R ' S C E R T I F I C A T I O N ; I herebv oeciare tnai trie contents ol this consignment are lully ano accurately cescribeo above bv 
proper f r p p i n g name and are classified, pacired. mariied. and labeled, and are m all respeas m proper condition for transpon by hignway 
a c c o r d i r ^ t o applicable international and national government regulations. 
Unless •' a m a small quantiry generator wno has been exempted by statute pr regulation from the duty to make a waste minimization 
certification 
under S-ection 3002(b| of RCRA. I also cenify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I 
have d e t e r m i n e d to be economically practicable and I have selected the method of treatment, storage, or disposal currently available to me 
which 
m i n i m i r e s the present and future threat to human health and the environment. 
V 
P r i n t e c " y p e d 
Name 
/^coAy y . y / < € j -
'•^..iyy^y^ 
M o n t h 
Day 
Yea 
\/y>\n\-7\!A\ A 
17.Transoci-:er 1 Acknowledgement of Receipt of Materials 
Prmtec. "yped Name 
O'Neale s Transport Inc 
Nortor- C.M. Burt 
Signature 
i 2 
i ^ 
A 
M o n t h 
Day 
Year 
11 10 11'7 18^5 
18.7ransocr-:er 2 Acknowledgement of Receipt of Materials 
Prtrttjc. ~ y p e d 
Name 
iTi^c- 
.ypeu raamo 
, y 
-rV/yjrzziy yyyyjec/ 
SignatuiiE^';'^ 
» 
y / 
* 
M o n t h 
Day Year 
1 9 . D i * c r e c * ^ C Y Indication Space 
(j-yyy3 
ff 
20,FacilitY 
^Fwner or Operator'. Certification of receipt of haiardous materials coveted by this maiS'ifesi eioeot as noted in Item 
19. 
Primeo--- 
iT>«d 
Name 
/ - / : ^ y / i r s ^ 
/ ^ n > ^ c y 
% i . 
M o n t h 
Day Year 
EPA Form 87o^2i (Rev. 4-85) Previous edition IS Obsolete. 
STATE OF ALABAMA (A\ust Accom^Qny Shipment) 
u i l I J y 
100230 
':»t*m r-int or rvoa 
(Form desioned for use on e'ltf (IJoitch) typewriter i 
ferr" Aoo'o.pfl QMB No 2000 040a t ' c r s 7 2' P' 
t 
UNIFORM HAZARDOUS 
WASTE MANIFEST 
(Continuation Sheet) 
n .>3ooeraior s US lirA O No 
Man.lest 
n.r'age 
Document No 
d
urocumeni nts 
z o/Z 
iniorrnaiion in tne sn^OtC d'«ras 
L State Manifest Document Num&er 
CWMA 
Z^s^^y^ 
23.Generator s Name 
. 
ZTsc^^u} ^y^yyfrCot^ C^-rrpy:^/ 
Sd^o y'^i'£y^^(cy:> ^(JSZ) 
O 7tr?o 
cjyuyyy^y y / t ^ AZe/^y 
24.Transponet»..g Company Name 
y A * / g . £ 4 _ 
X ^ T'AOtl/cti/'XI^ 
26. Transporft-4 
Cornpany Name 
• TYPFr! 
V\'^\<yT^y 
..Trailer Number 
RTMZ; 
l l k b l h 
T'rc j!<}/-^9^ €./oo 
•5! 
u s EPA 10 Number 
L 
M.State Caneraior s ID 
N. State Transponer s ID 
\ r t. e> 9 S o 9 d> 3 9 7 7 
27. 
US EPA ID Numoer 
I n n nn7riT257n 
0. Transponer's Phone 
P. Stata Transponar s ID 
U. Transponer s Phon 
28. US OOT Description (Including Proper Shipping Nerne. Haiard Class, and ID Number, 
29.Containers 
No. 
Type 
30. 
Total 
Quantity 
i'3;LS-a?9-52^-!9 
Unit 
AWol 
R 
Waste No 
/ z ^ A^-f 
g ' / g / g g ^ < f 
y \ / y 9 f ^ y l S . 
«W(rt^rol,le Numoer / ^ ^ y l > i > / U y f - ^=>z^ J>/iy 
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CWM Profile Numoer y^tfy^zZ—^v-
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CWM Profile Number 
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CWM Profile Number 
CWIul Profile Number 
CWM Profile Number 
CWM Profile Number 
CWM Profile Number 
S. Additior-.ai DesCTiptions for Materials Listed Above 
^ 
ml -
'^^lZ^^xA=y^y^i-Tci^taycr. 
^^fu^ & / ^ ^ ^ ^ * ^ 
T. Handling Cooes for Wastes Listed Abov? 
a. 
d. 
g. 
h 
e. 
h. 
f. 
32. St>*til^i 11I..UIll-It) ihslructipns and Additional Information 
JZ-/C /^-^^''^fy^EryfTt! /ya, iZ y/^. /y^^jy ytz. yrytfyx£c/Cj> ^ y cyj/z/yy>y^ yy/cy:^ 
7 5 yey'^yTTf/^^, /='y^a^ rTZCyoyy ytC^?.=pfyy ^ ^ o c ^ r ^ r ^ 
y ^ ^ - y y y Z / y y y r y ^ p / ^ j — 
J I 33. Transponer 
Acknowledgement of Receipt o< Materials 
* I 
^ r ^ ^ ^ r j . ' r ; ^ 
Nerne 
J 
-<ivl.\ g - • ^ " ^ '^-r^rMz.r.cTr T n r 
P I 
v=- - - -,,- r> V 
•a..X^' 
° I 34.Trans{>orter-7^Acknowledaemenl or Receipt of Materials 
Sionature ) 
/ l y y ^ y ^ 'E.Tn. iSZZZc ^ 5 
Date 
Month Day 
' • tr 
I 1 n! 1 7I 1; ^ 
f 
i3. Diacreparkcy Indication Space 
~ 
— - ^ 
I 
Date 
I 
SiOT^turi 
* y y, 
y 
Z Z y E 
Month Day Y-ar 
Urf..a. /{f. 4.^.uW 
I / L l AJ • ^ 
i?A Form 8700-22A (3-84) 
< ; T A T P 
D P A I A R A K A A 
( M i K i t Ar 
, , 
Cklr.— ^ . - * . ! 
100231 
ATTACHMENT K 
100232 
ATTACHMENT K 
snviio Ki scisDc^ inc. 
19 C0P5LAND RD.. DENVILLE. NEW JERSEY 07834 ^ ^ ^ ^ ^ i ^ 
32 EAST 39 STREET. NEW YORK. NEW YORK 10016 
(201) 366-6256 ^ ^ ^ ^ » ^ ^ 
(212) 697-9450 
November 15, 1985 
Mr. Carl Becnell 
G, A. Becnell, Customs Brokers 
150 >iarine Street 
Lake Charles, Louisiana 70601 
Dear Mr. Becnell: 
As per a telephone request from Mr. Frank Curtis of Berlex Laboratories, Inc., 
I a=. sending the enclosed laboratory analytical sheets which describe the chemical 
consents of hazardous wastes which originated in St. Croix, USVI. 
It is my 
understanding that U. S. Customs will not release the material for shippment 
to Chemical Waste Management, Inc. in Alabama until they know the contents 
of the shippment. 
Below is a listing of data sheets and to which drums they are applicable. 
DATA SHEETS 
1 and 2 
3 - 6 
7 - 11 
12 - 17 
* 
CHEM. WASTE 
KA.NIFEST NO. 
ALA D 
ALA E 
ALA D 
ALA D 
ALA E 
48604 
68803 
48603 
48602 
68804 
M.^TERLA.L 
Soil 
Soil 
Sludge 
Water 
Pieces of 
Metal Drums 
NO, OF DRL-MS 
24 
15 
45 
94 
14 
* Pieces of washed drums which contained materials in items 1 and 2 above. 
I trust that this information will suffice for release of the material. 
If you 
have any questions, contact me at 919/499-5182 or 201/366-6256, 
Ver-^ truly yours, 
Ala- L. Kyles, '^hD, 
Vice President 
enclosures 
100233 
ATTACHMENT 
L 
100234 
ATTACHMENT L 
ic:£fK2i inc. 
Ci-LjVijXjnir 19 COPELAND RO.. DENVILLE. NEW JERSEY 07834 
^ ^ * * ^ ' " * ' 
(201)366-5256 
November 6, 1985 
Mr. Louis Diguardia 
DSEPA 
Environmental Services Division 
Woccbridce Avenue 
Edison, NJ 
08837 
Re: 
Island Chemical Comoanv, St. Crcix, U.S.V.l. 
Dear Mr. Diguardia: 
T.hrough the Freedom of Information Act, I am requesting a copy of 
the analytical results for samples taken by you on September 9, 
1985 at the Island Chemical Company site in St. Croix, U.S.V.l. 
Berlex Laboratories, Inc., the company responsible for site 
cleanup, wishes to finalize t.heir responsibilities to the new 
owner. Virgin Island Chemical Company. 
Your immediate response to this request would be appreciated. 
Very truly yours, 
ENVIRO-SCIENCES, INC. 
Alan L. Kyles, Ph.D. 
Vice President 
ALK/po 
(AK-85391) 
100235 
ATTACHMENT M 
100236 
ATTACHMENT .". 
Heavv .Metal Analvses For "Gut" Sarr.Dles 
Loca 
G-1 
G-2 
G-3 
G-4 
G-5 
G-6 
G-7 
G-8 
G-9 
G-10 
G-11 
tion 
1) 
2) 
3) 
3) 
4 ) 
Cadmium 
LT 0.24 
LT 0.2 3 
LT 0.2 2 
LT 0.2 2 
LT 0.2 3 
1.0 
2.4 
LT 0.23 
LT 0.2 3 
LT 0.30 
LT 0.5 4 
Chromium 
14.5 
16.4 
16.7 
12.0 
17.1 
46.4 
71.1 
20.4 
19.8 
30.6 
41.1 
CoDoer 
37.3 
38.3 
33.8 
25.3 
36.1 
40.0 
51.4 
32.8 
34.9 
62.7 
69.7 
Lead 
• 21.0 
22.0 
14.5 
13.2 
20.2 
32.9 
46.4 
19.4 
21.4 
16.5 
12.8 
Mercury 
LT 
LT 
LT 
LT 
LT 
LT 
LT 
LT 
LT 
LT 
LT 
0.092 
0.103 
0.101 
0.102 
0.105 
0.122 
0.121 
0.093 
0.113 
0.106 
0.194 
•Zinc 
63.1 
57.8 
129 
37.1 
57.2 
349 
861 
76.2 
75.7 
66.5 
871 
Volatile Organic Analyses 
All sa~ples appear to be clean (verbal from ICM 6 Mar, 4:00 p.m.) 
1) G-1: Background - above plant site. 
2) G-3: Just below Laboratory pit outlet to the gut. 
3) G-5 and G-7: At point of drain line discharge. 
4) G-11: Setting "basin" area in gut 250-300 feet beyond drainline 
discharge point. 
100237 
Q ^ / z -
100238 
: ,1 
1 i 
I i. ; 4 i 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
ns?i)ixiiti> «A«:)OL)^. NfWjiH^tr o/abs ?ui^a4.u.i.iu 
NJDEP Certified Drinking Vacer/Wastewace: 
Laboratory ID //14116 
REPORT DATE: 
March 5. 1986 
LAB If •52i63 
PRIORITY POLLUTANT 
LABORATORY A.N'ALYSIS 
CLIENT: ENVIRO SCIENCES INC 
SA.MPL 
SA.MPL 
UNITS 
SOURCE: Tsland Cheynical Co. 
ID: G-1 
SAMPLE DATE: February 19. 1986 
SAMPLED BY: 
Al.-^n Kvles 
!r.p/kg''ppm') dry weight basis 
AT LAB DATE: Fphru.-^ry 21. 1986 
MATRIX: S Q U 
NC = 2;on-calcuable RPD due to value(s) less than detection limit. 
dwb = Dry Weight Basis 
X = N"ct Analyzed 
LT = less Than 
INDUSTRIAL CORROSION MANAGEME.NT. INC. 
RPD = Relative percent difference. 
RSL/dlh 
(This report form contains 
Parameter 
Ant ir.env 
Arser.ic 
Bervllium 
Cac-.iu3i 
Chro-ium 
Coooar 
Lead 
Mercurv 
Nickel 
Selenium 
Silver 
Thallium 
Zinc 
Phenol 
Cvar.ice 
Sample 
Result 
X 
X 
X 
LT 0.24 
U.S 
37.3 
21.0 
LT 0.092 
X 
X 
X 
X 
63.1 
X 
X 
both the ori 
Sample 
Duplicate 
X 
X 
X 
LT 0.26 
17.9 
63.5 
25.7 
LT 0.093 
X 
X 
X 
X 
67.8 
X 
X 
ginal sample 
RPD 
X 
X 
X 
NC 
20% 
15% 
20% 
NC 
X 
X 
X 
X 
7% 
X 
X 
result and 
Control 
Limits 
X 
X 
X 
NC 
.20% 
.20% 
±20% 
NC 
X 
X 
X 
X 
120% 
X 
' 
X 
the duplicate result.) 
Minimum 
Detection 
Limit 
X 
X 
X 
LT 0.2-!. 
LT 0.22 
LT 0.62 
LT 1.3 
LT 0.092 
X 
X 
X 
X 
LT 2.28 
X 
X 
Method 
Blank 
Analysis 
X 
X 
X 
LT 0.24 
LT 0.22 
LT 0.62 
LT 1.3 
LT 0.092 
X 
X 
X 
X 
1.03 
X 
X 
' 
1 
1 
1 
1 
! 
! 
i 
1 
1 
RMenard S. 
L^vj 
P r e s i d e n t 
100239 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
iti^HouTE!: fANOOuv. KEwjeRSEr 07ttt :ai'M443w 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID <I14116 
REPORT DATE; March 5. 1986 
LAB It 52466 
PRIORITY POLLUTANT 
LABORATORY ANALYSIS 
CLIENT: ENVIRO SCIENCES. INC. 
SA.HPLE SOURCE: Island Chemical Co. 
SA.MPLE ID: G-2 
UNITS: mg/kg(pPTn) drv weight basis 
• SAMPLE DATE: February 19. 1986 
SAMPLED BY: Alan Kvles 
AT LAB DATE: February 21. 1986 
MATRIX: Soil 
Para-eter 
A.ntirrnv 
Arsenic 
Bervllium 
Cadni-m 
Chro-ium 
CoDoer 
Lead 
Mercurv 
Nickel 
Selenium 
Silver 
Thallium 
Zinc 
Phencl 
Cyanide 
Sample 
Result 
X 
X 
X 
LT 0.22 
16.4 
38.3 
22.C 
LT 0.103 
X 
X 
X 
X 
57.8 
X 
X 
Minimum 
Detection 
Limit 
X 
X 
X 
LT 0.23 
LT 0.21 
LT 0.59 
LT 1.3 
LT 0.103 
X 
X 
X 
X 
LT 2.1 
X 
X 
Method 
Blank 
Analvsis 
X 
X 
X 
LT 0.23 
LT 0.21 
LT 0.59 
LT 1.3 
LT 0.103 
1 
X 
X 
X 
1 
X 
0.97 
X 
X 
1 
dvb = Dry Weight Basis 
X * Net Analyzed 
LT » Less Than 
INDUSTRIAL CORROSION MANAGE.MENT, INC. 
RSL/clh 
100240 
95?hardS 
President 
yyyyy-
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
I I M WulE IC. MU1OCH.PH. NEW JERSEY 0>tb9 201'i>t44;)]u 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID tfl4116 
REPORT DATE: March 5. 1986 
LAB it 
52465 
CLIENT: ENVIRO SCIENCES, INC 
PRIORITY POLLUTANT 
LABORATORY ANALYSIS 
SA.MPLE 
SA.MPLE 
UNITS: 
SOURCE: Island Chemical Co. 
ID: 
G-3 
m^/ke(ppm) drv weight basis 
' SAMPLE DATE: February 19, 1986 
SAMPLED BY: 
Alan Kvles 
AT LAB DATE: February 21, 1986 
MATRIX: Soil 
dwb " Dry Weight Basis 
X « Not Analyzed 
LT » Less Than 
Parameter 
Antimony 
Arsenic 
Bervllium 
Cadr-ium 
Chromium 
Cooper 
Lead 
Mercurv 
Nickel 
Selenium 
Silver 
Thallium 
Zinc 
Phenol 
Cyanide 
Sample 
Result 
X 
X 
X 
LT 0.22 
16.7 
33.8 
14.5 
LT 0.101 
X 
X 
X 
X 
129 
X 
X 
Minimum 
Detection 
Limit 
X 
X 
X 
L"^ n.22 
LT 0.21 
LT 0.58 
LT l.-i 
^ T 0 1 r>i 
X 
X 
X 
X 
LT 2.1 
X 
X 
Method 
Blank 
Analysis 
1 
X 
X 
TT 0.22 
LT 0.21 
LT 0.58 
TT 1.^ 
1 
1T n ini 
1 
X 
i 
X 
X 
1 
X 
0.96 
X 
X 
INDUSTRIAL CORROSION MANAGEMENT,INC. 
RSL/dlh 
lievirie 
<. 
100241 
I^fchard S 
President 
' th I'I 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
nSIKWIE 10. *A«00l.PH. N£WJtRSE»0?t»li 7<>l-i>tt<l'iXi 
NJDEP Certified Drinking Water/Wastewate: 
Laboratory ID tfl4116 
REPORT DATE: M.qrch 5. 1986 
LAB II 52466 
PRIORITY POLLUTANT 
LABO.^MORY ANALYSIS 
CL IENT: FNVTRO SCIENCES INC. 
SAMPLE SOURCE; Island C: emical Co. 
SAMPLE ID: G-4 
UNITS: 
mg/ke(pom) drv weight basis 
• SA.MPLE DATE: February 19, 1986 
SAMPLED BY: 
Al^n Xv^^t, 
AT LAB DATE: Fehrii.nrv !> i . 1986 
MATRIX: Soil 
Parameter 
Antimony 
Arsenic 
Bervllium 
Cadmiur: 
Chromium 
Conner 
Lead 
Mercurv 
Nickel 
Selenium 
Silver 
Thallium 
Zinc 
Phenol 
Cvanlde 
Sample 
Result 
X 
X 
X 
LT 0.22 
12.0 
25.3 
13.2 
LT 0.102 
X 
X 
X 
X 
37.1 
X 
X 
r • — 
- ' 
— 
- 
a s — . 1 . 1 
Minimum 
Detection 
Limit 
X 
•X 
X 
LT 0.2 2 
IT 0.20 
LT 0.5 7 
LT 1.3 
LT 0.102 
X 
X 
X 
X 
LT 2.1 
X 
X 
^ 
Method 
Blank 
Analvsis 
X 
X 
X 
LT 0.22 
LT 0.20 
LT 0.57 
LT 1.3 
LT 0.102 
X 
X 
X 
X 
0.94 
X 
X 
dwb « Dry Weight Basis 
X - Not Analyzed 
LT - Less Than 
INDUSTRIAL CORROSION .MANAGE.MENT, INC. 
100242 
RSL/dlh 
lithard S. LeV: 
'resident 
/ 
• Si'i 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
iii;MiurE 10. fUNOOiPti. NEwxRStr o/ibt ni-iiH-orju 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID tfl4116 
REPORT DATE; March 5. 1986 
LAB II 52467 
PRIORITY POLLUTANT 
LABORATORY ANALYSIS 
CLIENT: ENVIRO SCIENCES INC. 
SAMPLE SOURCE; Island Che-^ical Co. 
SAMPLE ID: G-5 
' 
UNITS: 
mg/kg(ppm) drv weight basis 
' SAMPLE DATE: February 19, 1986 
SAMPLED BY: 
AT LAB DATE: 
Alan Kvlp.. 
Februarv 21. 1086 
MATRIX: So^l 
dwb » Dry Weight Basis 
X - Not Analyzed 
LT « Less Than 
Parameter 
Antimony 
Arsenic 
Bervllium 
Cadmium 
Chromium 
Copper 
Lead 
Mercurv 
Nickel 
Selenium 
Silver ' 
Thallium 
Zinc 
Phenol 
Cyanide 
Sample 
Result 
X 
X 
X 
LT 0.23 
17.1 
36. 1 
20.2 
LT 0.105 
X 
X 
X 
X 
57.2 
X 
X 
Minimum 
Detection 
Limit 
X 
X 
X 
LT 0.23 
LT 0.21 
LT 0.60 
LT 1,3 
LT 0.105 
X 
X 
X 
X 
LT 2.2 
X 
X 
Method 
Blank 
Analysis 
X 
X 
X 
LT 0.23 
LT 0.21 
LT 0.60 
LT 1.3 
LT 0.105 
X 
X 
X 
X 
0.98 
X 
X 
1 
RSL/dlh 
INDUSTRIAL CORROSION MANAGEMENT.INC. 
1 0 0 2 4 3 
lichard S./Le^<t-ne 
President C 
rii( 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
Wit MUIC IC. fW«iX>l.f>H. HlW JLfViir OltiH 
n\-SH-03M 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID tfl4116 
REPORT DATE: March 5. 1986 
LAB H_52AM 
PRIORITY POLLUTANT 
LABORATORY ANALYSIS 
CLIENT: ENVIRO SCIENCES INC. 
SAMPLE 
SAMPLE 
UNITS: 
SOURCE: 
ID: 
G-
Is 
-6 
mg/kgCripm") 
land 
dry 
Chemic£ 
weight 
ll Co. 
basis 
• SAMPLE DATE: February 19. 1986 
SAMPLED BY: Alan Kvles 
AT LAB DATE: Fehri'.T-" 21. 1QP6 
MATRIX: SQVI 
# 
dwb » Dry Weight Basis 
X » Not Analyzed 
LT - Less Than 
RSL/ dlh 
Parameter 
Antimonv 
Arsenic 
Bervllium 
Cadmium 
Chromium 
Copper 
Lead 
Mercurv 
Nickel 
Selenium 
Silver 
Thallium 
Zinc 
Phenol 
Cyanide 
Sample 
Result 
X 
X 
X 
1.0 
46. 6 
40.0 
32.9 
LT 0.122 
X 
X 
X 
X 
349 
X 
X 
Minimum 
Detection 
Limit 
X 
X 
X 
LT 0.28 
LT 0.25 
LT 0.71 
LT 1.6 
LT 0.122 
X 
X 
X 
X 
LT 2.6 
X 
X 
Method 
Blank 
Analysis 
X 
X 
X 
LT 0.28 
LT 0.25 
LT 0.71 
LT 1.6 
LT 0.122 
X 
X 
X 
X 
1.2 
X 
X 
INDUSTRIAL CORROSION MANAGELMENT, INC. 
100244 
Ri(ihard S 
President 
I.I 
i I 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID #14116 
I I M M X i U >0 k«> jOlPH. New JtH^LT U'B6t TOIMt-UjJU 
REPORT DATE: .March 5. 1986 
LAB It 52469 
PRIORITY POLLUTANT 
LABORATORY ANALYSIS 
CLIENT: ENVIRO SCIENCES INC. 
SA.MPLE DATE: February 19, 1986 
SA-MPLE SOURCE: Island Chemical Co. 
SA.MPLE ID: G-7 
SAMPLED BY: Alan Kvles 
AT LAB DATE:February 21. 1986 
UNITS: mg/kgrppm.-') H^v weipht basis 
MATRIX: Soil 
(This report form contains both the original sample result and the spike recovery.) 
Para-erer 
Antimcnv 
Arsenic 
Bervllium 
Cadiiiun 
Chromium 
Copper 
Lead 
.Me r cur-.' 
Nickel 
Seler.ium 
Silver 
Thallium 
Zinc 
Phenol 
Cyanide 
Sample 
Result 
X 
X 
X 
2.4 
71.1 
51.4 
. 46.4 
LT 0.121 
X 
X 
X 
X 
861 
X 
X 
Spike 
Added 
X 
X 
X 
1 
1 
1' 
1 
0.004 
X 
X 
X 
Y 
1 
X 
X 
Spiked 
Sample 
Result 
X 
X 
X 
1.13 
4.04 
2.89 
2.92 
1 0.0035 
i 
X 
1 
X 
i 
X 
i 
X 
': 
1.72 
' 
X 
i X 
X 
X 
X 
103% 
119% 
83% 
1 
1 106% 
1 88% 
! 
X 
X 
X 
! 
X 
103% 
1 
1 
X 
X 
Control 
Limits 
for %R 
75-125 Z 
75-125 % 
75-125 % 
75-125 2 
75-125 % 
75-125 % 
75-125 7. 
75-125 7. 
175-125 % 
I75-I25 7. 
175-125 % 
175-125 % 
I75-I25 7. 
175-125 7. 
b5-125 % 
Minimum 
Detection 
Limit 
X 
X 
X 
LT 0.28 
LT 0.25 
LT 0.72 
LT 1.5 
! LT 0.121 
1 
i 
X 
i 
X 
X 
! 
X 
•' LT 20.1 
i 
X 
i 
X 
i
l
i
! 
i 
1 
1 
1 
1 
j 
1 
1 
-^- 
' 
——' 
— 
Method 
Blank 
Analysis 
X 
X 
X 
LT 0.28 
LT 0.25 
LT 0.7 2 
LT 1.5 
LT 0.121 
X 
X 
X 
i 
i 
X 
1.17 
X 
i 
X 
%R = Percent Spike Recovery 
NR = .\'ot required. Standard addition performed. 
dwb » Dry Weight Basis 
X * Net Analyzed 
LT = less Than 
INDUSTRIAL CORROSION MANAGEMENT,INC. 
The spiked sample result is based on the soil 
/ 
rt 
in solution. It does not directly reflect the 
^1 
/ 
(J / ^ C 
100245 
final -g/kg dry weight basis result of the 
y / r - 
J A I Li 
sar-.pie. 
ALUiy^yiyJ hyiAyy^ 
^:i'i 
L 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
Mil HUUIE 10. S A M O O U ^ . MEW JEHSET U / S M 
2UI'&(<.UJ30 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID *14116 
REPORT DATE; March 5. 1986 
LAB if 524 70 
PRIORITY POLLUTANT 
LABORATORY ANALYSIS 
CLIENT: ENVIRO SCIENCES INC. 
SAMPLE SOURCE: Island ChcTnical Co. 
SA.MPLE ID: G-8 
UNITS: mg/kgCppm') drv weight basis 
' SAMPLE DATE; February 19. 1986 
SAMPLED BY: 
Alan Kyles 
AT LAB DATE: Feb'-u.Tv ''i. 1986 
MATRIX: Soil 
para-eter 
Antimony 
Arsenic 
Bervllium 
Cadriun 
Chror:ium 
Copper 
Lead 
Mercurv 
Nickel 
Selenium 
Silver 
Thallium 
Zinc 
Phencl 
Cvanide 
Sample 
Result 
X 
X 
X 
LT 0.23 
20.4 
32.8 
19.4 
LT 0.093 
X 
X 
X 
X 
76.2 
X 
X 
1 
Minimum 
Detection 
Limit 
X 
X 
X 
LT 0.23 
LT 0.21 
LT 0.60 
LT 1.3 
LT 0.093 
X 
X 
X 
X 
LT 0.4 4 
X 
V 
Method 
Blank 
Analysis 
X 
X 
X 
LT 0.23 
LT 0.21 
LT 0.60 
LT 1.3 
LT 0.093 
X 
X 
X 
X 
0.99 
X 
X 
dwb = Dry Weight Basis 
X " Net Analyzed 
LT » Less Than 
INDUSTRIAL CORROSION MANAGE-MENT, INC. 
RSL/dlh 
100246 
Ri6hard S. L^vin^ 
President 
K40n^ 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
Fi I. ^ • . 
INCORPORATED 
I I M OOUll 10. >IA*XK.PH. HEW JlRSlt OObB JOl >»»-UJJO 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID ^14116 
REPORT DATE; March 5. 1986 
LAB tl 52471 
PRIORITY POLLUTANT 
LABORATORY ANALYSIS 
CLIENT: ENVIRO SCIENCES INC. 
SA.HPLE 
SA-MPLE 
UNITS: 
SOURCE: 
ID: 
G-
7.2/k£( 
Isl 
-9 
?yn]. 
and 
d^^ 
Chemical Co. 
we .7ht hs'?-' t; 
"SAMPLE DATE; February 19. 1986 
SAMPLED BY: Alan Kvles 
AT LAB DATE: Fehrn?-^v 21 . 1986 
MATRIX; Soii 
dwb » Dry Weight Basis 
X " Not Analyzed 
LT - Less Than 
RSL/dlh 
Parameter 
Antimonv 
Arsenic 
Bervllium 
Cadmiun 
Chromiur: 
Copper 
Lead 
Mercurv 
Nickel 
Selenium 
Silver 
Thallium 
Zinc 
Phenol 
Cvanide 
Sample 
Result 
X 
X 
X 
LT 0.23 
19.8 
34.9 
21.4 
LT 0.113 
X 
X 
X 
X 
75.7 
X 
X 
Minimum 
Detection 
Limit 
' 
X 
X 
X 
LT 0.23 
LT 0.21 
LT 0.61 
LT 1.1 
LT 0.113 
X 
X 
Y 
X 
LT 0.44 
X 
X 
Method 
Blank 
Analvsis 
X 
X 
X 
LT 0.23 
LT 0.21 
LT 0.61 
LT 1.1 
LT 0.113 
X 
X 
X 
X 
0.99 
X 
X 
INDUSTRIAL CORROSION .MA.NAGE.MENT, INC. 
100247 
Ri^ard S. Lawine^ 
President 
m 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
pi L J t 1 
INCORPORATED 
IIMMXITE 10. fiA«r3C4.f>H. NEWJERSEr 0/tlia 
20l'ia4-03]0 
L 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID tfl4116 
REPORT DATE; M.arch 5, 1986 
LAB H 52472 
PRIORITY POLLUTANT 
LABORATORY ANALYSIS 
CLIE.NT: ENVIRO SCIKNCFS. INC. 
SAMPLE 
SA.MPLE 
UNITS; 
SOURCE 
ID: G-
: Is 
10 
-s/^?(rpni) 
land 
drv 
Chemical 
weight JL 
Co. 
?si? 
. SAMPLE DATE: February 19, 1986 
SAMPLED BY: 
Alan Kvles 
AT LAB DATE: Fehru.Tv 2' 
1986 
MATRIX; 
Sn--i 
Parameter 
Antimonv 
Arsenic 
Bervllium 
Cadciu-
Chromium 
Copper 
Lead 
Mercur-.-
Nickel 
Selenium 
Silver 
Thallium 
Zinc 
Phenol 
Cvanide 
Sample 
Result 
X 
X 
X 
LT 0.30 
30.6 
62.7 
16.5 
LT 0.106 
X 
X 
X 
X 
66. 5 
X 
X 
Minimum 
Detection 
Limit 
X 
X 
X 
LT 0.30 
LT 0.27 
LT 0.77 
LT 1.4 
LT 0.106 
X 
X 
X 
X 
LT 0.56 
X 
X 
Method 
Blank 
Analysis 
X 
X 
X 
LT 0.30 
LT 0.27 
LT 0.7 7 
LT 1.4 
LT 0.106 
X 
X 
X 
X 
1.3 
X 
X 
dwb « Dry Weight Basis 
X • Net Analyzed 
LT - Less Than 
INDUSTRIAL CORROSION MANAGEMENT,INC. 
RSL/dlh 
100248 
(A^2^^ 
f-,^ 
; INDUSTRIAL 
*' 
t 
i CORROSION 
MANAGEMENT 
INCORPORATED 
iib7Nuu:i lu iu>.«_™ NLW AKiir o/ubs yui sm u.i.u; 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID #14116 
REPORT DATE: March 5. 1986 
U\B It 52473 
PRIORITY POLLUTANT 
LABORATORY A.N'ALYSIS 
CLIE.NT: ENVIRO SCIENCES INC. 
SAMPLE 
SAMPLE 
UNITS: 
SOURCE: Island Chemical Co. 
ID: G-11 
m^/kg(ppm) drv weight basis 
' SAMPLE DATE: February 19, 1986 
SAMPLED BY: Alan Kvles 
AT LAB DATE: February 21, 1986 
MATRIX: Soil 
Parameter 
Antimonv 
Arsenic 
Bervllium 
Cadmiu-
Chromiur 
Copper 
Lead 
Mercurv 
Nickel 
Seleniu-
Silver 
Thalliu-
Zinc 
Phencl 
Cyanide 
Sample 
Result 
A 
X 
X 
LT 0.54 
41.1 
69.7 
12.8 
LT 0.194 
X 
X 
X 
X 
871 
X 
X 
Minimum 
Detection 
Limit 
X 
X 
X 
LT 0.54 
LT 0.49 
LT 1.4 
LT 2.5 
LT 0.194 
X 
X 
X 
X 
LT 5.1 
X 
X 
Method 
Blank 
Analvsis 
X 
X 
X 
LT 0.54 
LT 0.49 
LT 1.4 
LT 2.5 
LT 0.194 
X 
X 
X 
X 
2.3 
X 
X 
1 
i 
dwb = Iry Weight Basis 
X = Net Analyzed 
kLT = Less Than 
INDUSTRIAL CORROSION .MANAGEMENT, INC. 
100249 
RSL/dlh 
Vichard S. L^vi'i 
'resident / 
J L'J N I IN 
DUSTRIAL 
CORHOSION 
MANAGEMENT 
INCORPOnATED 
1152 ROUIE 10, HANOOLPll. NEW JCRSET 0rt69 201 S X OJJO 
O 
O 
Ul 
O 
NJDEP Certified Drinking Water/Wastewater 
Lahoralory ID n h \ \ f > 
REPORT DATE: March 10. 1986 
LAB ff 52A63 
Z 
CLIENT; ENVIRO SCIENCES. INC. - Island Chemical Company Prolect: 
SAMPLE ID: G-1 
, 
; 
SAMPLE DATE: February 19. 1986 SAMPLED BY: 
Alan Kvles 
^AT LAB DATE; Fchruarv 21. 1986 
VOLATILE ORGANICS BY PURGE AND TRAP 
; 
By GC/MS - HEADSPACE 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis, 
CHLOROMETHANE 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
---• 
METHYLENE CHLORIDE 
ACETONE 
1,1-DICHLOROETllYLENE -• 
1,1-DICHLOROETHANE 
t-I ,2-DICHLOROETHYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER --
1,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE --
BROMODICHLOROMETHANE --
-ND— 
-NIL-
-NIL-
-Nil— 
JJt 
NI) 
ND 
NI) 
NI) 
NI) 
Nl) 
NI) 
Nl) 
NI) 
1,2-DICHLOROPROPANE 
c-l,3-DICHL0R0PR0PENE 
t-l,3-DICHL0R0PR0PENE 
TCE 
(TRICHLOROETHYLENE)---
1,1,2-TRICHLOROETHANE 
DlBROMOCHLOROMETHANE 
BENZENE ---
DIISOPROPYL ETHER 
• 
2-CHLOROETHYLVINYL ETHER • 
BROMOFORH -
I,1,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE) 
TOLUENE 
CHLOROBENZENE -
ETHYLBENZENE -- 
-
ND 
ND 
ND 
_ N ! L 
U\L 
Nl) 
JUL 
JIIL 
JUL 
JJD 
JUL 
JilL 
Jin 
LT=Less Than, GT=Greater Than, ND=Not Detected 
dwb=Dry Weight Basis 
SURROGATE RECOVERIES; dj methylene chloride - 69Z 
d_ toluene - 125Z 
BFB 
- 13IZ 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0,02 mg/kg(ppm) dwb. 
Other compounds detected: 
' 
^ 
• I 
•-^-: 
INDllTlRlAL COB^OBION MANAGEMENT, INC. 
[ 
nil?1 RIAL COBl^^ION MAN; 
115 I'I 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCOnPOnATED 
n s ; ROUTE 10. RANOoini. KEW JERSEY 07ec9 ;oi s x 0330 
l-» 
O o 
to 
Ul 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID l l ] k \ \ f i 
REPORT DATE: March 10. 1986 
LAB # 
5246A 
CLIENT: ENVIRO SCIENCES INC. - Island Chemical Company Prolect 
SAMPLE DATE; Fcbrnnrv 19. 1986 SAMPLED BY; 
Aldn Kvles 
SAMPLE ID: G-2 
VOLATILE ORGANICS BY PURGE AND TRAP 
By GC/MS - HEADSPACE 
AT LAB DATE; February 21. 1986 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis, 
CHLOROMETHANE 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
1 ,1-DICHLOROETHYLENE -• 
1,1-DICHLOROfTHANE 
t - l ,2-DICHLOROETHYLENE 
CHLOROFORM 
1 ,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER - -
1,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE - -
BROMODICHLOROMETHANE - -
NIL 
n[L 
NIL 
NIL 
NIL 
NIL 
NIL 
NIL 
i\y 
NIL 
NU. 
NIL 
N 
NIL 
NIL 
1,2-DICHLOROPROPANE 
c-1 ,3-DICHLOROPROPENE 
t-l,3-DICHL0R0PR0PENE 
TCE 
(TRICHLOROETHYLENE)---
1,1,2-TRICHLOROETHANE 
DIBROMOCHLOROMETHANE 
BENZENE - 
-- 
• 
DIISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER • 
BROMOFORM 
1,1,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE) 
TOLUENE 
CHLOROBENZENE ---
ETHYLBENZENE 
JUL 
JIIL 
JIL 
— NIL 
IL 
HIL 
JUL 
IL 
JUL 
Nn_ 
NIL 
LT=Less T h a n , GT=Greater T h a n , 
ND^Not 
D e t e c t e d 
dwb=Dry Weight 
B a s i s 
SURROGATE RECOVERIES; 
dj methylene chloride - 6«Z 
tiene 
BFB - 126Z 
d 
toluene - ll<iZ 
X 
For the above l i s t e d Volatile P o l l u t a n t s , nothing detected at a s e n s i t i v i t y level of 0.02 mg/kg(ppm) dwb. 
Other compounds detected: 
_
^ 
'y 
' 
INDn^TIOAL COj^O^ON MANAGEMENT, INC. 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPOnATED 
l»2 ROUIE 10. RANKOIPII. NEW JdlSir 0/(69 201 Ae4 0330 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID l l \ k \ \ ( , 
REPORT DATE: March 10. 1986 
LAB # 
52465 
CLIENT; ENVIRO SCIENCES. INC. - Island Chemical Company Project 
SAMPLE ID: G-3 
SAMPLE DATE: February 19. 1986 SAMPLED BY: 
Alan Kyles 
_AT LAB DATE: February 21. 1986 
VOLATILE ORGANICS BY PURGE AND TRAP 
By GC/MS - HEADSPACE 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis. 
CHLOROMETHANE 
-• 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
1,1-DICHLOROETHYLENE --
1,1-DICHLOROETHANE 
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER --
1,1,1-TRICIILOROETHANE -
CARBON TETRACHLORIDE --
BROMODICHLOROMETHANE --
NI) 
NI) 
ND 
m 
Nl) 
ND 
ND 
JIQ. 
ND 
JilL 
JIIL 
JI!L 
Nl) 
JIIL 
JIIL 
1,2-DICHLOROPROPANE 
c-1,3-DICHLOROPROPENE 
t-l,3-DICHL0R0PR0PENE 
TCE (TRICHLOROETHYLENE)---
1,1,2-TRICHLOROETHANE 
DlBROMOCHLOROMETHANE 
• 
BENZENE 
- 
-
DlISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER -
BROMOFORM 
1,1,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE) 
TOLUENE 
CHLOROBENZENE 
ETHYLBENZENE 
JIIL 
JIIL 
JUL 
JIIL 
JIIL 
JIIL 
JIIL 
JUL 
JIIL 
JIIL 
JIIL 
Nl) 
LT=Less Than, GT=Greater Than, ND=Not Detected 
dwb=Dry Weight Basis 
SURROGATE RECOVERIES; dj methylene chloride - 98Z 
d_ toluene - 61Z 
BFB - 57Z 
o 
o 
tJl 
IO 
J. 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg(ppm) dwb. 
Other compounds detected: 
I 
CSION MANAGEMENT, INC. 
I ,..• (,,,• 
' \ < t 
, - • • l . l . 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCOnPORATED 
115? ROUIE to. RANDOlfH. NEW JERSEY 07«69 201 5B< 0330 
O 
O 
IO 
U l 
CO 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID n h W d 
't 
• 
.J. { -
REPORT DATE: March 10, 1986 ''v'^ ' • 
LAB H 52466 
' ':''-' ' 
CLIENT: ENVIRO SCIENCES. INC. - Island Chemical Company Prolect 
SAMPLE DATE: February 19. 1986 SAMPLED BY: 
Alan Kvles 
SAMPLE ID:_G-4 
VOLATILE ORGANICS BY PURGE AND TRAP 
By GC/MS - HEADSPACE 
_AT LAB DATE; February 21. 1986 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis. 
CHLOROMETHANE ---
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE ---
METHYLENE CHLORIDE 
ACETONE -
1,1-DICHLOROETHYLENE -• 
1,1-DICHLOROETHANE 
t-l ,2-DICHLOROETIIYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER --
1,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE -• 
BROMODICHLOROMETHANE --
-NO-
J l l l _ 
ND 
JIU 
_m 
J)U_ 
JIIL 
JIIL 
Jill 
Nl) 
NI) 
NI) 
Nl) 
1 ,2-DICHLOROPROPANE 
c-l,3-DICHL0R0PR0PENE 
t-l,3-DICHL0R0PR0PENE 
TCE (TRICHLOROETHYLENE)---
1 ,1,2-TRICIILOROETHANE 
D I BROMOCHLOROMETHANE 
BENZENE - - 
-• 
DIISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER -
BROMOFORM 
-
1,1,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE) 
TOLUENE 
CHLOROBENZENE --- 
--
ETHYLBENZENE 
ND 
ND 
ND 
Nl) 
ND 
ND 
ND 
ND 
NI) 
NO 
NO 
JUL 
ND 
ND 
ND 
SURROGATE RECOVERIES; dj methylene chloride - lOOZ 
LT=Less Than, GT=Greater Than, ND=Not Detected 
dwb=Dry Weight Basis 
cl_ toluene 
BFB - 63% 
70Z 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg(ppm) dwb, 
Other compounds detected: 
INDUSjrRLAL COKKpiON MANAGEMENT, INC. 
//y/Zjt<yA(H.ylAi'^ • 
'INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
l l j ; ROUIE to, RANDOLPH. NEW JERSEY a;a69 ; 0 I 584 0330 
NJDEP Certified Drinking WaterVWaslewater 
Laboratory ID #l'tn6 
t y 
' . ! • •! 
o 
o 
lO 
(Jl 
REPORT DATE; March 10, 1986 ••."'•' 
LAB # 52467 
CLIENT: ENVIRO SCIENCES. INC. - Island Chemical Company Project 
SAMPLE DATE; February 19. 1986 SAMPLED BY: 
Alan Kyles 
SAMPLE ID: 
G-5 
VOLATILE ORGANICS BY PURGE AND TRAP 
By 
GC/MS 
- 
HEADSPACE 
AT LAB DATE: 
February 2 1 . 1986 
•-'',- j : • 
Compounds detected in parts per mi 11 ion (mil 1igrams/kilograms) dry weight basis. 
CHLOROMETHANE 
BROMOMETHANE 
--
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
1,1-DICHLOROETHYLENE -• 
1,1-DICHLOROETHANE 
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER --
1,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE --
BROMODICHLOROMETHANE --
ND 
ND 
JUL 
ND 
JUL 
JIIL 
ND 
JUL_ 
JUL 
JUL 
JUL 
JUL 
Nl) 
JUL 
JIIL 
1,2-DICIILOROPROPANE 
c-1,3-DICHLOROFROPENE 
t-l,3-DICHL0R0PR0PENE 
TCE (TRICHLOROETHYLENE)---
1,1 ,2-TRICHLOROETHANE 
Dl BROMOCHLOROMETHANE 
BENZENE 
--
Dl ISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER • 
BROMOFORM 
-
1,1,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE) 
TOLUENE ---
CHLOROBENZENE 
ETHYLBENZENE 
--
ND 
ND 
NO 
ND 
JiD_ 
JUL 
NO 
JUL 
JUL 
NO 
NIL 
JUL 
J&\L 
Nl) 
JUL 
LT=Less Than, GT=Greater Than, ND-Not Detected 
dwb=Dry Weight Basis 
SURROGATE RECOVERIES; dj methylene chloride - 97Z 
d„ toluene - 67Z 
o 
BFB - 66Z 
j( 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg(ppm) dwb. 
Other compounds detected: 
• 
t 
MANAGEMENT, INC. 
I I I I I 
I ' l l l 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
NJDEP C e r t i f i e d Drinking Water/Wastewater 
Laboratory 10 iCltjIie 
Its; ROUIE to. RANDOini. NEW JERSEY 0/gS9 ?0I 5t« 0330 
M 
O 
O 
to 
Ul 
tn 
CLIENT; ENVIRO SCIENCES. INC. - Island Chemical Company Project 
SAMPLE DATE: February 19. 1986 SAMPLED BY; 
Alan Kyles 
REPORT 
LAB H 
SAMPLE 
DATE: March 10. 
52468 
ID: G-6 
1986 ' 
VOLATILE ORGANICS BY PURGE AND TRAP 
By GC/MS - HEADSPACE 
AT LAB DATE: February 21. 1986 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis. 
CHLOROMETHANE 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE ---
1,1-DICHLOROETHYLENE -• 
1,1-DICHLOROETHANE 
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
• 
1,2-OICHLOROETHANE 
t-BUTYL METHYL ETHER --
1 ,1,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE 
--
BROMODICHLOROMETHANE 
- -
ND 
NO 
ND 
JIIL 
JUL 
JUL 
JIJ) 
J I l i _ 
J U L -
JID 
J ^ I I _ 
JID 
.NIL 
JID 
ND 
1,2-DICIILOROPROPANE 
c-l,3-DICHL0R0PR0PENE 
t-l,3-DICIIL0R0PR0PENE 
TCE 
(TRICHLOROETHYLENE)---
1 ,1,2-TRICIILOROETHANE 
DIBROMOCHLOROMETHANE 
BENZENE 
DlISOPROPYL ETHER 
--• 
2-CHLOROETHYLVINYL ETHER • 
BROMOFORM 
• 
1,1,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE) 
TOLUENE 
-
CHLOROBENZENE 
--
ETHYLBENZENE 
JUL 
M -
JUL 
Nl) 
JUL 
JUL 
JUL 
JUL 
JID 
ND 
JUL 
JUL 
JUL 
LT=Less Than, GT=Greater Than, ND=Not Detected 
dwb=Dry Weight Basis 
SURROGATE RECOVERIES; dj methylene chloride - 84Z 
d„ toluene 
BFB - 59Z 
d„ toluene - 66Z 
o 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg(ppm) dwb. 
Other compounds detected: 
_ _ _ _ ^ 
1 
U, COIiVjKJON MANAGEMENT, INC. 
'-y./iff/zPz^z^ 
r 1 
13 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
lis? ROUIE to. RAND0iril.NEWJlllSEY0/eb9 
?0I )g« 0330 
H 
O 
O 
lO 
Ul 
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NJDEP Certified Drinking Water/Wastewater 
Laboratory ID ll\k\\(> 
REPORT DATE; March 10, 1986 
LAB 
ff 52469 
CLIENT: ENVIRO SCIENCES. INC. - Island Chemical Company Project 
SAMPLE ID: G-7 
SAMPLE DATE: Fphmnrv 19. 1986 SAMPLED BY: 
Alan Kvles 
^AT LAB DATE: February 21. 1986 
VOLATILE ORGANICS BY PURGE AND TRAP 
By GC/MS - HEADSPACE 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis. 
CHLOROMETHANE 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
1,1-DICHLOROETHYLENE -• 
1,1-DICHLOROETHANE 
t-l ,2-DICHLOROETHYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER --
1,1 ,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE -• 
BROMODICHLOROMETHANE --
NIL 
NIL 
JUL 
JID-
JUL 
JUL 
JJIL 
JUL 
ND_ 
ND_ 
ND 
NO 
ND 
Nl) 
ND 
1 ,2-DICIILOROPROPANE 
-
c-l,3-DICHL0R0PR0PENE 
t-I,3-DICHL0R0PR0PENE 
TCE (TRICHLOROETHYLENE)---
I,1,2-TRICHLOROETHANE 
DIBROMOCHLOROMETHANE 
BENZENE 
-
DIISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER • 
BROMOFORM -- 
--
1 ,1 ,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE) 
TOLUENE --
CHLOROBENZENE ---
ETHYLBENZENE 
ND 
ND 
ND 
Nl) 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
NI) 
ND 
ND 
ND 
LT=Less Than, GT=Greater Than, ND=Not Detected 
dwb=Dry Weight Basis 
SURROGATE RECOVERIES: 
62 methylene chloride - IllZ 
dg tol 
BFB -
do toluene - 126Z 
o 
j( 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg(ppm) dwb. 
_X 
Other compounds detected: hydrocarbon RT 44 min. approx. 0.5 me/kR(possIbly octane) 
I 
CQRK^^IPI^ MANAGEMENT, INC. 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCOnPORATED 
11)2 ROUIE 10. RANDOLPH. NEW JERSEY 07)69 ?0I )«< 0330 
NJDEP Cert if led Drinking Water/Wastewater 
Laboratory ID iflMl6 
o 
o 
to 
Ul 
-J 
CLIENT; ENVIRO SCIENCES. INC. - Island Chemical Company Project 
SAMPLE DATE: February 19. 1986 SAMPLED BY: 
Alan Kyles 
REPORT DATE; March 10, 
LAB # 
52470 
1986 
- : 
SAMPLE ID: G-8 
'' 
VOLATILE ORGANICS BY PURGE AND TRAP 
By GC/MS - HEADSPACE 
AT LAB DATE; February 21, 1986 
CHLOROMETHANE 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE ---
ACETONE 
1,1-DICHLOROETHYLENE -
1,1-DICHLOROETHANE ---
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE ---
t-BUTYL METHYL ETHER -
1,1 ,1-TRICHLOROETHANE 
CARBON TETRACHLORIDE -
BROMODICHLOROMETHANE -
Compounds detected in parts per million (milligrams/kilograms) dry weight basis. 
^p 
NI) 
ND 
.NIL 
Nl) 
JUL 
ND 
MIL 
NEL 
NIL 
ND 
ND 
JO. 
Nl) 
JUL 
1,2-DICHLOROPROPANE 
-
c-1 ,3-DICHLOROPROPENE 
l-l,3-DICHL0R0PR0PENE 
TCE (TRICHLOROETHYLENE)---
I .1,2-TRICHLOROETHANE 
DIBROMOCHLOROMETHANE 
BENZFNE 
DIISOPROPYL ETHER 
• 
2-CHLOROETHYLVINYL ETHER • 
BROMOFORM 
- 
• 
1 ,1 ,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE) 
TOLUENE --
CHLOROBENZENE 
ETHYLBENZENE 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
SURROGATE RECOVERIES; 
LT=Less Than, GT=Greater Than, ND=Not Detected 
dwb=Dry Weight Basis 
d2 methylene chloride - 104Z 
d_ toluene 
BFB - 55Z 
d_ toluene - 72Z 
_X 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg(ppm) dwb. 
Other compounds detected: 
• 
I 
INDIia^fUAK CORWKJCN MANAGEMENT, INC, 
'//y\ / ( y / i yA/,iy)y.^ *y 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPOnATED 
W i l ROUIE to, RANDOLPH. NEW JERSEY 07J69 JOI 584^330 
H 
O 
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to 
Ul 
CO 
NJDEP Certified Drinking Water/Wastewater 
Laboratory ID #1'|116 
REPORT DATE: March 10. 1986 
LAB If 
52471 
CLIENT: ENVIRO SCIENCES INC. - Island Chemical Company Project 
SAMPLE DATE: February 19. 1986 SAMPLED'BY: 
Alan Kyles 
SAMPLE ID: G-9 
VOLATILE ORGANICS BY PURGE AND TRAP 
By GC/MS - HEADSPACE 
AT LAB DATE: February 21. 1986 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis, 
CHLOROMETHANE 
BROMOMETHANE 
• 
VINYL CHLORIDE 
CHLOROETHANE 
METHYLENE CHLORIDE 
ACETONE 
1,1-DICHLOROETHYLENE -• 
1,1-DICHLOROETHANE ---• 
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
1 ,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER -• 
1,1 ,1-TRICHLOROETHANE -
CARBON TETRACHLORIDE --
BROMODICHLOROMETHANE -• 
ND 
ND 
ND 
ND 
JUL 
JUL 
JUL 
Nl) • 
JID_ 
NI) 
ND 
JO.-
.NU_ 
.Nl)_ 
JU1_ 
1,2-DICHLOROPROPANE 
c-1 ,3-DICHLOROPROPENE 
t-l,3-DICHL0R0PR0PENE 
TCE (TRICHLOROETHYLENE)---
1,1,2-TRICHLOROETHANE 
DIBROMOCHLOROMETHANE 
BENZENE 
• 
DIISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER • 
BROMOFORM -- 
-
1,1,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE) 
TOLUENE 
-
CHIORODENZENE 
ETHYLBENZENE 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
ND 
-NIL 
NI) 
LT=Less Than, GT=Greater Than, ND=Not Detected 
dwb=Dry Weight Basis 
SURROGATE RECOVERIES; dj methylene chloride 
d- toluene - 76Z 
o 
BFB - 68Z 
102Z 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 0.02 mg/kg(ppm) dwb. 
Other compounds detected: 
INDUSTRIAL 
CORROSION 
MANAGEMENT 
INCORPORATED 
IIS? ROUIE 10. RANOOlPH. NEW JERSEY 07869 201 $640330 
CLIENT: ENVIRO SCIENCES. TNC. - Island Chemical Company Project 
SAMPLE DATE: February 19. 1986 SAMPLED BY: 
Alan Kyles 
NJDEP Cert ified Drinking Water/Wastewater 
Laboratory ID ll\k\\f> 
REPORT DATE: March 10. 1986 
LAB H 
52473 
SAMPLE ID: G-11 
VOLATILE ORGANICS BY PURGE AND TRAP 
• By GC/MS - HEADSPACE 
AT LAB DATE: February 21. 1986 
Compounds detected in parts per million (milligrams/kilograms) dry weight basis. 
o 
o 
to 
Ul 
vo 
CHLOROMETHANE 
BROMOMETHANE 
VINYL CHLORIDE 
CHLOROETHANE 
• 
METHYLENE CHLORIDE 
ACETONE 
1,1-DICHLOROETHYLENE -• 
1,1-DICHLOROETHANE 
t-l,2-DICHLOROETHYLENE 
CHLOROFORM 
1,2-DICHLOROETHANE 
t-BUTYL METHYL ETHER -• 
1 ,1 ,1-TRICIILOROETIIANE -
CARBON TETRACHLORIDE --
BROMODICHLOROMETHANE --
JUL 
.mi 
J U 1 _ 
J U L — 
J I U _ 
JUL 
JUL 
JUL 
JIO_ 
JI 
ND 
JUL 
ND 
NI) 
LT=Less Than, GT=Greater Than, NI)=Not Detected 
dwb=Dry Weight Basis 
1,2-DICHLOROPROPANE 
c-1 ,3-OICHLOROPROPENE 
t-I,3-DICHL0R0PR0PENE 
TCE (TRICHLOROETHYLENE)---
1,1,2-TRICHLOROETHANE 
DIBROMOCHLOROMETHANE 
BENZENE 
- 
• 
DlISOPROPYL ETHER 
2-CHLOROETHYLVINYL ETHER • 
BROMOFORM - 
-
1,1,2,2-TETRACHLOROETHANE 
PCE (TETRACHLOROETHYLENE) 
TOLUENE --
CHLOROBENZENE 
ETHYLBENZENE ---
ND 
JUL 
JUL 
JUL 
JUL 
JUL 
JUL 
JUL 
JUL 
JUL 
JUL 
ND 
ND 
ND 
ND 
SURROGATE RECOVERIES; 
-WATER 
dj methylene chloride - lOIZ 
d toluene 
I 7 3 Z 
HKB 
163Z 
For the above listed Volatile Pollutants, nothing detected at a sensitivity level of 5 ug/l(ppb)-water 
0.1 mg/kg(ppm) - soil 
Other compounds detected: 
657. 
INDUSMd/y. COURCf^UJN MANAGEMENT, INC. 
MACi/<y,yi ynAZb^zz-^ 
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100260 
EnvffKS t£a 5a&K£i inc. 
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Received by; (Sign. ) Da te /: 
Received by: (Sign.) Date/' 
Relinquished by: (Sign.) 
Rec'd by Laboratory 
for field analysis 
(Sign.) 
Date/ 
dispatched by: (Sign.) 
Dace/Time Rec'd for Laboratory 
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Method of 
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100261 
• 
EnvmO E£4 JC&KZi IOC. 
19 CXJPtLAND RO.. DEWVILLE. NEW JERSEY 07834 
CHAIN OF CUSTODY RECORD 
I n s t a l l a t i o n : _ ^ ^ ^ ^ ^ ^ ^ ^ 
Survey No . : 
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Date/Time 
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Date/Time Rec'd for Laboratory 
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Method of Shipment: 
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100262 
METALS 
Pit Slud' 
Cadmium 
Chromium 
Copper 
Lead 
Zinc 
ge 
22.8 
592 
327 
688 
3594 
Samole Points 
(Avg.) 
1. 7 
58. 9 
45. 7 
39.7 
605 
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% Of 
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• " ^ " ^ ^ ^ ^ ^ 19 COPELAND RD.. DENVILLE, fEW JERSEY 07834 
* ^ ^ ^ ^ i ^ 
(201) 366^256 
February 1, 1986 
Mr. Conrad Simon 
USEPA Region II 
26 Federal Plaza 
New York, N.Y. 10007 
Dear Mr. Simon: 
Enviro-Sciences, Inc. (ESI) has completed the proposed 
scope of work for on site cleanup of the Island Chemical 
Company (Berlex) facility in St. Croix, U.S. Virgin Islands. 
The cleanup program and methodology were presented to Mr. 
Robert Harris of your office in December, 1984 and ammended 
in a subsequent report dated April 4,1985. 
Briefly, the cleanup involved decontamination at several 
locations. These are: 
1) soil around above ground storage tanks - Toluene; 
2) soil around a concrete pad - Toluene; 
3) soil along a collapsed drain line - Toluene, Heavy 
Metals; 
4) water and sludge in a process pit - Toluene, Heavy 
Metals, Benzyl Acetate; and 
5) soil in a laboratory waste pit - Pyridine. 
All materials from the first four (4) locations listed above 
were containerized in proper 55-gallon steel drums, manifested 
and shipped as hazardous wastes to Chemical Waste Management, 
Inc. (CWM) Emelle, Alabama. CWM acknowledged receipt of 
these materials for disposal. 
The laboratory waste pit soil was treated on sire to decrease 
pyridine contamination level from above 1000 ppm to less than 
2 ppm. ESI considers this level of contamination to be below 
levels which would require any additional cleanup efforts. 
100265 
February 7, 1986 
Paoe -2-
Tho collapse of the drain line and subsequent an.nlysis 
of soil has initiated the need to conduct additional 
sampling off-site in the "gut" or dry creekbed. ESI 
will undertake this sampling program immediately to 
ascertain the presence of contamination and, if present, 
concentration levels. 
We would appreciate any comments relating to our cleanup 
program at the Island Chemical Company site. 
You may contact me or Mr. Irving Cohen at (201) 366-6256. 
Very truly yours, 
ENVIRO-SCIENCES, INC. 
Alan L. Kyles, Ph.D. 
Vice President 
ALK/ak 
cc: Robert Milos 
Frank Curtis 
100266 
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LOUIS DIGUARDIA 
G*o<ogiit 
(809) 773-6257 
EXPERT H O M E REPAIRS 
No job i» too small 
WooODr.O^ A»»no« 
Eaiton. N«.» Je'i«v 06i37 
12011321.6712 
Rayniond Hay* 
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100267 
ATTACHMENT N 
100268 
ATTACHMENT N 
' 610 W. MAIN ST., ROCKAWAY, NEW JERSEY 07866 
MnviRO ^ sczncti inc. 
^ y . - y y - y ^9 COPELAND RD.. DENVILLE. NEW JERSEY 07834 
i i i i i i 
(201)365-6256 
April 21, 1986 
Mr. Conrad Simon 
USEPA Region II 
26 Federal Plaza 
New York, N.Y. 10007 
Dear Mr. Simon: 
This letter is to follow up on certain matters raised 
in our letter of February 7, 1986, a copy of which is 
enclosed. As we advised, Enviro-Sciences has sampled 
the "gut" area adjacent to the site. Analyses of these 
soil samples disclose the presence of the metal described 
on Exhibit A, at the levels set forth on the Exhibit. 
Subsequent EP Toxicity tests conducted on a composite 
of sample numbers 6, 7 and 11 indicate concentration 
levels do not exceed the maximum permissible concentration 
levels ser forth in 40 CFR, Part 261.24 (Exhibit A, page 
2). 
Operations personnel at Berlex Laboratories, Inc. (the 
corporate parent of Island Chemical) have reviewed the 
processes in use by Island Chemical at the site. The 
metals listed on Exhibit A were not involved in the 
processes run by Island Chemical. While we do not know 
for sure, it is likely that these elements are present 
in the anti-rust paint used on the buildings on site 
(and many other buildings on the island). 
In addition, volatile organic analyses for soil samples 
at these same locations indicate that none are present. 
100269 
m 
April 21, 1986 
Page -2-
In view of the relatively low leachability of metals 
found and the likely source of the material involved, 
no further action is planned. 
Very truly yours, 
ENVIRO-SCIENCES, INC. 
Alan L. Kyfes, Ph.D. 
Vice President 
ALK/ak (86-13) 
CC: Charles Dolan, USEPA 
B. Kilos, Berlex 
R. Willis, Berlex 
F. Curtis, Berlex 
I. Arshen, Berlex 
100270 
G - 1 
H 
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i 
GUT SOIL SAMPLING PROGRAM 
ISLAND CHEMICAL PLOT PLAN